CN104849167B - Grade for piece cigarette or pipe tobacco biomass water the detection means of warm adsorption/desorption - Google Patents

Grade for piece cigarette or pipe tobacco biomass water the detection means of warm adsorption/desorption Download PDF

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CN104849167B
CN104849167B CN201510307227.5A CN201510307227A CN104849167B CN 104849167 B CN104849167 B CN 104849167B CN 201510307227 A CN201510307227 A CN 201510307227A CN 104849167 B CN104849167 B CN 104849167B
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adsorption
desorption
air
temperature
gas
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CN104849167A (en
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李斌
李志刚
周苏旸
孙淼
鲁端峰
张龙
张彩云
刘勇
王兵
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Hefei Zwotech Instrument Technology Co ltd
Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
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Hefei Zwotech Instrument Technology Co ltd
Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
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Abstract

A kind of detection means for the warm adsorption/desorption that grades for piece cigarette or pipe tobacco biomass water, is made up of gas hybrid cell, adsorption/desorption unit, weighing unit, data acquisition and control unit, and gas hybrid cell, adsorption/desorption unit are independently set;The device can carry out the detection of piece cigarette or pipe tobacco reclaimed water point isothermal adsorption and desorption process at a certain temperature and humidity conditions.Changed with time situation by analyzing moisture in sample, the result of moisture content under water adsorption and the speed and poised state of desorption in different samples is obtained, so as to characterize water adsorption and desorption performance in the biological materials such as piece cigarette or pipe tobacco.The advantage of the invention is that:Operating temperature humidity is interval wide:The adjusting range of temperature humidity:Temperature is at 5 DEG C~90 DEG C, and relative humidity can ensure the stability of the weighing sensor under the conditions of high temperature test 5%~95%, realize the adsorption/desorption test of biological material under hot environment.

Description

Grade for piece cigarette or pipe tobacco biomass water the detection means of warm adsorption/desorption
Technical field
The present invention relates to a kind of device for the warm adsorption/desorption that grades for biomass water, specifically one kind is applied adds in tobacco Work field detection lug cigarette or pipe tobacco(Biomass)The device of reclaimed water point isothermal adsorption and desorption process.
Background technology
The porous media that piece cigarette or pipe tobacco are made up of complicated organic substance, can in the heat and wet treatment of tobacco processing course Some changes can be produced to tobacco leaf or pipe tobacco pore structure, at the same the addition of the outside feed liquid of some in process change tobacco leaf or Pipe tobacco Surface Physical Chemistry property, causes after processing that moisture absorbs moisture under certain temperature and humidity conditions in piece cigarette or tobacco sample Certain change is produced with the ability of removing moisture.Piece cigarette or tobacco sample are to the isothermal adsorption of moisture and de- after evaluation processing When attached ability and changing rule, it will usually including multiple continuous Mass and heat transfer processes, only by entering Mobile state to the process On-line checking, could carry out effective detection and evaluation to sample water adsorption and desorption ability.Piece is understood by this evaluation Cigarette or pipe tobacco dry to water adsorption and desorption performance, the physics humectation effect for adding humectant, optimal storage requirement and high temperature Roasting and moisture regain performance etc..
The migration such as to adsorb and be desorbed under certain temperature and humidity conditions existing for moisture in the biomass such as piece cigarette or pipe tobacco As.Majority detection method is that different temperature and humidity conditions are set in climatic chamber at present, carries out the detection of process, by offline Weigh and obtain the data of change in process, and existing commercial on-line checking product is below 30mg moisture to sample bearing capacity majority The detection of migration, temperature controlling range is more than normal temperature(Normal temperature can not be less than)Or can not complete wet using same complete equipment Spend continuously adjustable experiment detection work.In addition, the adjustment control response time of existing detection means humidity and temperature is long, surely It is qualitative to be difficult to meet requirement of experiment.Because moisture transition process is a continuous process in piece cigarette or pipe tobacco, so needing to combine Online with the advantage of offline two methods, the device for the warm adsorption/desorption that grades for piece cigarette or pipe tobacco reclaimed water is developed.
Inventor once applied for the patent of invention of a Patent No. 201210267723.9, and its is entitled《For Biomass water grades the device of warm adsorption/desorption》, its principle is by adjusting the flowrate proportioning of dry and wet air so as to reach regulation Humidity in adsorption/desorption room;At the same time, the temperature in adsorption/desorption room, example weight are controlled using the method for water bath with thermostatic control Change the weight of sample is gathered by high accuracy balance in real time, realize to adsorption/desorption process on-line checking, measure sample Weight can reach more than 40g, meanwhile, realize and experiment test carried out in large temperature range, detection means humidity with The adjustment control response time of temperature is shorter.But the device has the following disadvantages in test application:1)Because balance is in The reason in incubator, so calorstat temperature should be arranged on 5 DEG C -50 DEG C(This temperature range is the normal condition of balance, day Put down when near or above 50 DEG C, be also easy to produce temperature drift or damage), it is difficult to realize adsorption/desorption of the test higher than more than 50 DEG C Experiment(Need to be operated and tested in the range of 50 DEG C~90 DEG C to most in the baking of piece cigarette and the performance test that gets damp again, be higher than 50 DEG C have application value);2)Because saturated moist air is directly produced by water-bath, it is de- that saturated moist air temperature is slightly below absorption Temperature in alcove, relative humidity under room temperature condition higher than 90%RH is extremely difficult to, and the quick adjustment tested to high humility is made Into difficulty;3)The temperature of saturated moist air is due to above-mentioned 2)Middle reason, is easily condensed under conditions of high humidity, influence test effect Fruit and measuring accuracy, meanwhile, damage balance.
The content of the invention
In view of the above-mentioned problems, being used for the biological material moisture isothermals such as piece cigarette or pipe tobacco it is an object of the invention to provide one kind The device of adsorption/desorption, the device can carry out piece cigarette or pipe tobacco reclaimed water point isothermal adsorption at a certain temperature and humidity conditions With the detection of desorption process.Changed with time situation by analyzing moisture in sample, obtain in different samples water adsorption and The result of moisture content under the speed and poised state of desorption, thus characterize in the biological materials such as piece cigarette or pipe tobacco water adsorption with Desorption performance.
The purpose of the present invention is achieved through the following technical solutions:
A kind of detection means for the warm adsorption/desorption that grades for piece cigarette or pipe tobacco biomass water, by gas hybrid cell, inhales Attached desorption unit, weighing unit, data acquisition and control unit composition, and gas hybrid cell, adsorption/desorption unit difference are only Erect and put;
The gas hybrid cell includes gas cylinder, constant water bath box, the mixing air chamber being arranged in constant water bath box, A, b two-way admission line are passed through in constant water bath box, wherein a roads admission line is entered after entering constant water bath box by serpentine coil Water bath with thermostatic control lower box part, two-way are directly exposed to after entering mixed air vessel, the outlet side connection bubble generator of b roads admission line Admission line is connected by air mass flow detection control apparatus with gas cylinder respectively, and the wet sky of a saturation is provided with mixed air vessel Gas air inlet pipe, the inlet port of saturated moist air air inlet pipe is above the water surface of constant water bath box, in constant water bath box It is additionally provided with heater and temperature sensor;
The adsorption/desorption unit includes the thermostatic box with adiabatic closure, the absorption being arranged in thermostatic box and taken off Alcove and thermostatic box and the heating kind of refrigeration cycle device being connected by circulation line with thermostatic box are placed on, it is de- in absorption It is provided with Temperature Humidity Sensor in alcove, and is connected between the mixed air vessel in adsorption/desorption room and gas mixing units wet Air intake duct;
The weighing unit is arranged on including the weighing sensor in weighing sensor protection room, by pallet pole Weighing tray and protection gas air inlet pipeline and gas exhaust piping above weighing sensor and in adsorption/desorption room, biography of weighing Sensor protection room in be additionally provided with temperature sensor, pallet pole is made of heat-insulating material, and weighing sensor protection room with Be provided with the protection air flue for installing pallet pole between adsorption/desorption room, protection air flue bottom by protect gas air inlet pipe with Gas cylinder is connected and controlled by air mass flow detection control apparatus, and protection upper airways, which are provided with, can be passed through the exhaust of air Pipe;
The data acquisition and control unit includes temperature acquisition card, humidity collection card, heating controller, flow control Device, heating kind of refrigeration cycle controller, adsorption/desorption data record collector and industrial computer composition.
In the present invention, liquid level gauge, liquid injection pipe and tapping valve are additionally provided with constant water bath box;The saturated moist air air inlet The downward curved pipe of Guan Weiyi arc cores, the suction for saturated moist air of being more convenient for.
The case of constant water bath box outer case in the gas hybrid cell and the thermostatic box in adsorption/desorption unit Volume surrounding is provided with heat insulation layer.
The adsorption/desorption room being arranged in thermostatic box is a high-thermal conductive metal inner bag.
Heating kind of refrigeration cycle medium in adsorption/desorption unit is distilled water, heating refrigerant inlet ductwork and outlet Road is arranged on the diagonal position in thermostatic box.
The present invention is described further below in conjunction with control process to each composition cell operation principle:
Gas hybrid cell is mainly snakelike including gas cylinder, a roads air mass flow detection control apparatus, the air preheat of a roads Pipeline, b roads air mass flow detection control apparatus, b roads bubble generator, constant water bath box, heater, mixing air chamber, wet sky The part such as gas air inlet pipe, liquid level gauge, liquid injection pipe, discharging tube is constituted.The drying that gas cylinder is used to produce needed for testing is without aqueous vapor Body, a roads and b roads two-way gas are used to produce the dry and wet air needed for test.Unit main body structure is a constant water bath box Body, thermostatic box outer layer sets heat insulation layer.Liquid level gauge is used for the height for showing the liquid level of water bath, liquid injection pipe and discharging tube Liquid for filling and discharging water bath.The basic functional principle of whole unit:Two-way gas is mixed after certain processing With the gas for obtaining certain temperature and humidity, the gas after mixing enters in the environment of adsorption/desorption as processing medium.Gas Mixing process can be described as:Air is divided into two-way in the presence of flow detection control device after being exported through gas cylinder and enters thermostatted water In bath cabinet, wherein air enters after water bath with thermostatic control casing all the way, entered by serpentine coil and mix air chamber, serpentine coil is immersed in In constant water bath box, the road air reaches that certain temperature is laggard by occurring heat exchange with constant water bath box reclaimed water during coiled pipe Enter to mix air chamber.Another road air enters after constant water bath box, and the bubble generator set by pipe end enters constant temperature In water in water bath body, gas enter certain temperature water in separate out after, then as saturated moist air at a certain temperature, Entered by the pipeline of particular design and mix air chamber;Two-way gas after fully being mixed in mixed air vessel is entered by inlet tube to be adsorbed In the environment of desorption unit.By adjusting the flow of control two-way air, temperature can be formed in normal temperature~90 in mixed air vessel DEG C, humid air of the relative humidity in the range of 5%~95%.
Adsorption/desorption unit include thermostatic box, adsorption/desorption room, adiabatic closure, Temperature Humidity Sensor, it is external plus Refrigeration heat circulator, heating refrigerant inlet ductwork and export pipeline etc. part are constituted.Unit main body structure is a constant temperature Casing, thermostatic box outer layer sets by external heating kind of refrigeration cycle device to pass through inside heat insulation layer, thermostatic box and heated Refrigerant inlet ductwork enters box house, and returning to heating refrigeration by heating refrigerant export pipeline after case interior circulation follows In ring device, ensure the constant of constant temperature the temperature inside the box with this.Heat cycles medium is distilled water, heats refrigerant inlet ductwork Case inner opposite angle position is arranged on export pipeline, to ensure fully circulating for heat cycles medium.Absorption and desorption environment Realized by the high-thermal conductive metal inner bag being arranged in thermostatic box, the control method of temperature is to detect the temperature in inner bag in inner bag Afterwards, it is adjusted and controls by adjusting external heating kind of refrigeration cycle device temperature control, the control method of humidity is in inner bag The humidity in inner bag is detected, control is gas pre-mixed to be realized with two-way flow in system by adjusting.Top in adsorption/desorption room Adiabatic closure is provided with, it is ensured that the measuring accuracy under different temperature and humidity regulations, in order to prevent the temperature in the external world to adsorption/desorption The influence of room, it is necessary to assure the sealing and thermal insulation of adsorption/desorption.Temperature Humidity Sensor is located at the lower section of adsorption/desorption, for detecting The warm and humid angle value of adsorption/desorption, and the humiture situation of adsorption/desorption room is detected by control unit in real time.
Weighing unit includes weighing sensor, weighing tray, pallet pole, weighing sensor protection room, c roads air mass flow Meter, temperature sensor, the protection composition such as air inlet pipeline and outlet pipe.In order to protect weighing sensor, weighing sensor is located at In design protection room, it is connected by pole with pallet, pallet is used to place test sample.In order to protect weighing sensor, prevent The heat of adsorption/desorption room is delivered on weighing sensor by pole damages weighing sensor, and pallet pole uses heat-insulating material It is made.The gas gas exchanges that may be present of energy between adsorption/desorption room and sensor protection room are prevented, sensor is devised Protect gas circuit.Gas cylinder gas enters air inlet pipeline by c roads mass air flow sensor, distinguishes in the downside of tray support and upside The air inlet pipeline and outlet pipe of protection gas are devised, while outlet pipe or the humid air outlet of adsorption/desorption room, are protected Protect after gas enters from the bottom of pole, being protected the jacking of the gas of room flows up protection gas, the top of pole with The humid air of adsorption/desorption room is discharged from outlet pipe together, and so design can not only avoid the Hot wet air heating of adsorption/desorption room Support thermolysis is given in flowing possibly into sensor protection room, and protection gas, is played certain effect of cooling, is kept away Exempt from due to pallet pole in upper contact to Hot wet air heating the influence to weighing sensor to the heating of support.
Data acquisition and control unit include temperature acquisition card, humidity collection card, heating controller, flow controller, plus Refrigeration heat cycle controller, industrial computer and control software and adsorption/desorption data logging software(That is collector)Deng composition.Temperature Capture card gathers constant water bath box, adsorption/desorption room, the temperature of weighing sensor protection room respectively.Humidity collection card is used to gather The humidity of adsorption/desorption room.Heating controller is used for the temperature for controlling constant water bath box.Flow controller controls a, b, c road respectively The flow of gas, it is ensured that the humidity of adsorption/desorption room and the flow of protection gas.Heating kind of refrigeration cycle controller is used to control constant temperature The temperature of the heating refrigerant of case, so as to control the temperature of adsorption/desorption room.Industrial computer and control software control by with it is each Individual capture card and controller connection, controls the parameters of this device, it is ensured that the normal operation of device.Adsorption/desorption data are remembered Recording software records adsorption/desorption room temperature humidity value and sample quality in real time, and can reflect sample by the form of chart Adsorption/desorption performance.
The invention has the advantages that:
1) operating temperature humidity is interval wide:The adjusting range of temperature humidity:Temperature is at 5 DEG C~90 DEG C, and relative humidity is 5% ~95%.
2) special weighing unit is designed, weighing sensor is separated with weighing tray, adds weighing sensor protection gas Road, it is ensured that can not influence weighing sensor stability in high temperature test, protects weighing sensor.
3) new gas mixing units are devised, adsorption/desorption room is separated with mixing chamber, it is possible to achieve subregion temperature control, is made The temperature of mixing chamber is more than 3 DEG C~5 DEG C of adsorption/desorption room, it is ensured that the humidity at a higher temperature of mixing chamber, so Mixing chamber will not produce condensation, it is ensured that the precision of experiment.Realize the adsorption/desorption test of high temperature.
4) adsorption/desorption logging software is devised, the parameter of unit can be controlled in real time, test parameters setting is convenient, Experimental data is preserved, and can be realized and automatically adjusted and monitor in real time.
Brief description of the drawings
Fig. 1 is that biomass water grades warm adsorption/desorption structure drawing of device;
1- gas cylinders;2-c roads air-flow control device;3-b roads air flow rate detecting device;4- a roads air mass flow Control device;5- liquid level gauges;6- serpentine coils;7- foaming generating means;8- saturated moist air inlet tubes;9- mixed air vessel; 10- constant water bath box;11- liquid injection pipes;12- humid air inlet tubes;13- thermal insulation closures;14- adsorption/desorptions room;15- is warm and humid Spend sensor;16- sample trays;17- gas exhaust pipings;18- thermostatic box;19- pallet poles;19.1- protect air flue;20- claims Weight sensor protection room;21- weighing sensors;22- heats refrigerant outlet;23- heats kind of refrigeration cycle device;24- is heated Refrigerant inlet tube;25- protects room temperature sensor;26- protective gas air inlet pipe;27- tapping valves;28- thermostatted waters bathroom Temperature sensor;29- heaters;30- data acquisition and control units;31- industrial computers;
Fig. 2 is certain sample water adsorption characteristic curve under 50 DEG C and different humidity
Fig. 3 is certain sample water adsorption characteristic curve in the case where 50 DEG C and program rise wet control.
Embodiment
Structure of the present invention and annexation are described below in conjunction with Fig. 1:
As shown in Figure 1:A kind of detection means for the warm adsorption/desorption that grades for piece cigarette or pipe tobacco biomass water, is mixed by gas With unit, adsorption/desorption unit, weighing unit, data acquisition and control unit composition, and gas hybrid cell, adsorption/desorption list Member is independently set;
The gas hybrid cell includes gas cylinder 1, constant water bath box 10, the mixed air being arranged in constant water bath box A, b two-way admission line are passed through in room 9, constant water bath box 10, wherein a roads admission line enters after constant water bath box by snakelike Coil pipe 6 is directly exposed to constant water bath box after entering mixed air vessel 9, the outlet side connection bubble generator 7 of b roads admission line 10 bottoms, two-way admission line is connected by air mass flow detection control apparatus (3,4) with gas cylinder 1 respectively, in gaseous mixture A saturated moist air air inlet pipe 8 is provided with room 9, the saturated moist air air inlet pipe is the downward curved pipe of an arc core, and saturation is empty The inlet port of air humidity air inlet pipe is additionally provided with heater 29 above the water surface of constant water bath box in constant water bath box 10 With temperature sensor 28, liquid level gauge 5, liquid injection pipe 11 and tapping valve 27.
The adsorption/desorption unit includes the thermostatic box 18 with adiabatic closure 13, the suction being arranged in thermostatic box Attached desorption chamber 14 and thermostatic box and the heating kind of refrigeration cycle device 23 being connected by circulation line with thermostatic box are placed on, Temperature Humidity Sensor 15, and the gaseous mixture in adsorption/desorption room 14 and gas mixing units are provided with adsorption/desorption room 14 Humid air air inlet pipe 12 is connected between room 9;The adsorption/desorption room is a high-thermal conductive metal inner bag.Heat kind of refrigeration cycle medium For distilled water, heating refrigerant inlet ductwork 24 is arranged on the diagonal position in thermostatic box 18 with export pipeline 22.
The weighing unit include be located at weighing sensor protect room 20 in weighing sensor 21, pass through pallet pole 19 It is arranged on the top of weighing sensor 21 and the weighing tray 16 in adsorption/desorption room 14 and the He of protection gas air inlet pipeline 26 Gas exhaust piping 17, weighing sensor protection is additionally provided with temperature sensor 25 in room 20, and pallet pole 19 is made of heat-insulating material, And the protection air flue for being provided with and being installed for pallet pole 19 between room 20 and adsorption/desorption room 14 is protected in weighing sensor 19.1, protection air flue bottom is by protecting gas air inlet pipe 26 to be connected with gas cylinder 1 and by c roads air mass flow detection control dress 2 controls are put, protection upper airways, which are provided with, can be passed through the gas exhaust piping 17 of air;
The data acquisition and control unit 30 includes temperature acquisition card, humidity collection card, heating controller, flow control Device, heating kind of refrigeration cycle controller, adsorption/desorption data record collector and industrial computer 31 are constituted.
The present invention is described in more detail with reference to Fig. 1 and embodiment:
As shown in Figure 1:The present invention is grade for the biomass water detection means of warm adsorption/desorption, including constant water bath box 10th, thermostatic box 18, weighing sensor protection room 20 and data acquisition and control unit 30 etc..On the right side of constant water bath box 10 There is drying from gas cylinder 1 of a, b two-way respectively through a roads air-flow control device 4, b roads volume control device 3 side Air, a roads admission line enters after constant water bath box 10 by serpentine coil 6 into mixed air vessel 9, and b roads admission line enters Be connected after constant water bath box 10 with being immersed in the foaming generating means 7 of distilled water in constant water bath box 10, it is foamed after gas Enter mixed air vessel 9 from the saturation air inlet pipe 8 being connected with mixed air vessel 9;Constant water bath box 10 is provided with liquid injection pipe 11, tapping valve 27th, liquid level gauge 5;The steaming for controlling temperature in real time by heating kind of refrigeration cycle device 23 is full of in thermostatic box 18, adiabatic closure 13 Distilled water, is provided with adsorption/desorption room 14, the adsorption/desorption room 14 in the space that thermostatic box 18 and adiabatic closure 13 are surrounded Provided with Temperature Humidity Sensor 15, sample tray 16;Closed weighing sensor protection room 20 is provided with below thermostatic box 18, Weighing sensor protection passes through solid in room 20 provided with protection air chamber temperature sensor 25, weighing sensor 21, weighing sensor 21 Fixed pallet pole 19 mounted thereto is connected with sample tray 16;Set between adsorption/desorption room 14 and weighing sensor protection room The drying compressed air for controlling flow through c roads air-flow control device all the way, the other end and the height of c roads flow controller are put Air bottle is connected;Acquisition and control system includes industrial computer 31, data acquisition and control unit 30 and signal acquisition transmission Line, signal transfer line respectively with c roads air-flow control device 2, b roads air-flow control device 3, the air flow control of a roads Device 4, Temperature Humidity Sensor 15, weighing sensor 21, protection room temperature sensor 25, water bath with thermostatic control room temperature sensor 28, Heater 29, heating kind of refrigeration cycle device 23 etc. are connected.
Circulatory mediator in thermostatic box 18 is distilled water, and the inlet ductwork 24 and export pipeline 22 of circulatory mediator are set respectively The diagonal position in thermostatic box is put, to ensure fully circulating for heat cycles medium.
The course of work of apparatus of the present invention is described in detail with reference to two embodiments:
Case study on implementation one
Industrial computer 31 and heating kind of refrigeration cycle device 23 and adsorption/desorption device master switch are opened, adsorption/desorption test is opened Software, checks whether acquisition and control system communication is normal.Device can be with after the normal communication of industrial computer 31, setting each experiment The experiment parameters such as temperature, humidity, stabilization time, protection air-flow amount, mixed gas flow, the sampling period in stage, specific experiment ginseng Number is as shown in table 1.Start test program, program is by according to the experiment parameter set, the temperature of each part of apparatus for automatic control And air mass flow is with the experimental situation needed for obtaining.Meanwhile, the real time data of each experiment parameter also will be in industry control in experimentation Show and preserve on machine.Experiment can be transferred to next step from a step automatically under the control of a test program.Tobacco sample Product can adsorb or be desorbed moisture under the humiture environment of setting, and weight can be continually changing.Experimental result is as shown in Figure 2.
Case study on implementation two
Industrial computer 31 and heating kind of refrigeration cycle device 23 and adsorption/desorption device master switch are opened, adsorption/desorption test is opened Software, checks whether acquisition and control system communication is normal.Device can be with after the normal communication of industrial computer 31, setting each experiment The experiment parameters such as temperature, humidity, stabilization time, protection air-flow amount, mixed gas flow, the sampling period in stage.Specific experiment is joined Number is as shown in table 2.Humidity value is generally set to 0 in the first stage and final stage tested every time, stabilization time is arranged on 30 More than minute, for the residual moisture in emptying adsorption/desorption room 14 and pipeline.Adiabatic heat-insulation lid 13 is opened, by load weighted sample Product are put into the sample tray 16 in adsorption/desorption room 14, then by the good seal of adiabatic heat-insulation lid 13.Start test program, program will According to the experiment parameter set, the temperature and air mass flow of each part of apparatus for automatic control are with the experimental situation needed for obtaining. Meanwhile, the real time data of each experiment parameter also will show and preserve on industrial computer in experimentation.Experiment is in test program Next step can be transferred under control from a step automatically.Tobacco sample can be adsorbed or taken off under the humiture environment of setting Attached water point, weight can be continually changing.Experimental result is as shown in Figure 3.

Claims (6)

1. a kind of detection means for the warm adsorption/desorption that grades for piece cigarette or pipe tobacco biomass water, it is characterised in that:Mixed by gas With unit, adsorption/desorption unit, weighing unit, data acquisition and control unit composition, and gas hybrid cell, adsorption/desorption list Member, which is independently set, to be located in two casings arranged side by side;
The gas hybrid cell includes gas cylinder, constant water bath box, the mixing air chamber being arranged in constant water bath box, constant temperature A, b two-way admission line are passed through in water bath, wherein a roads admission line enters by serpentine coil to enter after constant water bath box and mixed Water bath with thermostatic control lower box part, two-way air inlet are directly exposed to after closing air chamber, the outlet side connection bubble generator of b roads admission line Pipeline is connected by air mass flow detection control apparatus with gas cylinder respectively, is entered in mixed air vessel provided with a saturated moist air Tracheae, the inlet port of saturated moist air air inlet pipe is also set above the water surface of constant water bath box in constant water bath box Having heaters and temperature sensor;
The adsorption/desorption unit includes the thermostatic box with adiabatic closure, the adsorption/desorption room being arranged in thermostatic box And thermostatic box and the heating kind of refrigeration cycle device being connected by circulation line with thermostatic box are placed on, in adsorption/desorption room In be provided with Temperature Humidity Sensor, and be connected with humid air between the mixed air vessel in adsorption/desorption room and gas mixing units Air inlet pipe;
The weighing unit include be located at weighing sensor protect room in weighing sensor, be arranged on and weighed by pallet pole Weighing tray and protection gas air inlet pipeline and gas exhaust piping above sensor and in adsorption/desorption room, weighing sensor Protection is additionally provided with temperature sensor in room, and pallet pole is made of heat-insulating material, and in weighing sensor protection room and absorption The protection air flue for installing pallet pole is provided between desorption chamber, protection air flue bottom is by protecting gas air inlet pipe and high pressure Gas cylinder is connected and controlled by air mass flow detection control apparatus, and protection upper airways, which are provided with, can be passed through the blast pipe of air;
The data acquisition and control unit include temperature acquisition card, humidity collection card, heating controller, flow controller, plus Refrigeration heat cycle controller, adsorption/desorption data record collector and industrial computer composition.
2. the detection means of the warm adsorption/desorption according to claim 1 that grades for piece cigarette or pipe tobacco biomass water, it is special Levy and be:Liquid level gauge, liquid injection pipe and tapping valve are additionally provided with constant water bath box.
3. the detection means of the warm adsorption/desorption according to claim 1 that grades for piece cigarette or pipe tobacco biomass water, it is special Levy and be:The casing of constant water bath box outer case in the gas hybrid cell and the thermostatic box in adsorption/desorption unit Outer layer is provided with heat insulation layer.
4. the detection means of the warm adsorption/desorption according to claim 1 that grades for piece cigarette or pipe tobacco biomass water, it is special Levy and be:The adsorption/desorption room being arranged in thermostatic box is a high-thermal conductive metal inner bag.
5. the detection means of the warm adsorption/desorption according to claim 1 that grades for piece cigarette or pipe tobacco biomass water, it is special Levy and be:Heating kind of refrigeration cycle medium in adsorption/desorption unit is distilled water, heating refrigerant inlet ductwork and outlet Road is arranged on the diagonal position in thermostatic box.
6. the detection means of the warm adsorption/desorption according to claim 1 that grades for piece cigarette or pipe tobacco biomass water, it is special Levy and be:The saturated moist air air inlet pipe is the downward curved pipe of an arc core.
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