CN108164329A - A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer - Google Patents

A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer Download PDF

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Publication number
CN108164329A
CN108164329A CN201711483349.5A CN201711483349A CN108164329A CN 108164329 A CN108164329 A CN 108164329A CN 201711483349 A CN201711483349 A CN 201711483349A CN 108164329 A CN108164329 A CN 108164329A
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China
Prior art keywords
parts
attapulgite
organic fertilizer
preparation
bacterium
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Pending
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CN201711483349.5A
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Chinese (zh)
Inventor
傅剑锋
熊伟
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Anhui Lenong Environmental Protection Technology Co Ltd
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Anhui Lenong Environmental Protection Technology Co Ltd
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Priority to CN201711483349.5A priority Critical patent/CN108164329A/en
Publication of CN108164329A publication Critical patent/CN108164329A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05DINORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00Other inorganic fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F17/00Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/20Mixtures of one or more fertilisers with additives not having a specially fertilising activity for preventing the fertilisers being reduced to powder; Anti-dusting additives
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/10Solid or semi-solid fertilisers, e.g. powders
    • C05G5/12Granules or flakes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/40Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse

Abstract

The invention discloses a kind of preparation methods based on attapulgite material compound probiotic functional organic fertilizer, belong to microbial organic fertilizer technical field, EM bacterium and raw material are mixed even granulation by the preparation method using existing, the adhesive of addition promotes particle to obtain surface and forms mesh skeleton, surface spraying EM bacterium are obtained in particle, form inside and outside bio-organic fertilizer of the bilayer EM bacterium particle preparations containing following parts by weight again:Activate 15 20 parts of attapulgite, 15 25 parts of Chinese medicine slag, 25 30 parts of activated sludge, 5 10 parts of adhesive, 6 15 parts of EM bacterium, the Chinese medicine slag that the present invention uses contains a large amount of crude protein, crude fat, crude fibre, vitamin, iron, manganese, zinc, calcium, magnesium trace element and bioactive substance, the organic fertilizer of production has many advantages, such as to promote crop yield, improves crop quality, enhancing crop resistance and resistance, whole preparation process is short with the production time, environmental pollution is small, good product quality, fertilizer efficiency is high, effectively solves the defects of traditional processing technology.

Description

A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer
Technical field
The invention belongs to microbial organic fertilizer technical fields, and in particular to one kind is based on attapulgite material compound probiotic work( The preparation method of energy organic fertilizer.
Background technology
Soil Probiotics have activating soil nutrient, improve soil enzyme as a kind of soil bacteria for promoting plant strain growth The effect of activity, by the bio-feritlizer that it is mixed with organic compost, has both the advantage of organic compost and probiotics, organic While compost gives probiotics good growing environment, for probiotics also by itself, activity and its secretion promote compost The conversion of nutrient so as to adjust Ecological Distribution of Soil Microorganisms structure, improves utilization rate of fertilizer, meanwhile, the extensive use of bio-feritlizer The pollution that feces of livestock and poultry is brought to environment is efficiently solved, meets the requirement of China's agricultural sustainable development.At present, there is research It reports that organic compost is matched with probiotics to apply to plant growth, yield and quality with facilitation, while to various crop disease Evil has prevention and control effect.Such as Chinese patent publication No. CN107473797, disclose a kind of using excrement, dead leaf, vinasse and prebiotic Bacterium is prepared for a kind of chrysanthemum dedicated fertilizer as raw material, and the chrysanthemum of plantation is not only virus-free, pollution-free, and enhances chrysanthemum itself Nutritive value.Biological organic fertilizer the problem of be exactly to be influenced by weather and ambient humidity more apparent, utilization rate is relatively low, protects Water, water imbibition are poor.
Attapulgite is commonly called as palygorskite, is a kind of nonmetallic mineral resource with soil and stone characteristic.It is that one kind includes Layer, chain structure fibrous crystal, have larger specific surface area, include nanochannel, have stronger ion-exchange capacity and Good adsorptivity, slow release, suspension.As a kind of mineral clay substance, attapulgite has good water suction and guarantor It is aqueous, and it should not be reduced after absorbent drying, there is preferable stabilization under brine and hot environment.Attapulgite is also rich in Trace element needed for plant growth, such as Si, A1, Mg, Fe, K, Ca and Mn.Attapulgite has many good characteristics, closely It is widely applied to the fields such as environmental protection, medicine, agricultural, petrochemical industry, daily-use chemical industry within several years.
Invention content
According to more than the deficiencies in the prior art, the technical problems to be solved by the invention are to propose one kind based on concave-convex bar Expect the preparation method of compound probiotic functional organic fertilizer, in order to solve the above-mentioned technical problem, the technical solution adopted by the present invention is:
A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer, preparation are as follows: Attapulgite, activated sludge, Chinese medicine slag, the adhesive that high temperature alkaline process is activated carry out high speed dispersion and are uniformly mixed, and then add in The 1/3 of total EM bacterium amounts after being uniformly mixed, carries out extruder grain, then sprays remaining EM bacterium solutions to the particle surface made, Finally particle is put into fermentation tank, aerobic fermentation 30-35d is carried out at 35-55 DEG C of temperature.
Preferably, the grain size of the attapulgite is 50-100 mesh, and the grain size of the granulation is 5-15mm.
Preferably, the high temperature subtraction activation step is as follows:Attapulgite is put into NaOH solution and impregnates 10-12h, so Afterwards by attapulgite at 280-300 DEG C of temperature high-temperature activation 1.5-2h, then cooled down rapidly at 5-10 DEG C of temperature.
Preferably, a concentration of 1.5-2mol/L of the NaOH solution, volume are 5-8 times of attapulgite.
Preferably, the Chinese medicine slag is discards after production Chinese medicine antiviral oral liquor, the solid after spontaneous fermentation 10-20 days Residue.
Preferably, described adhesive is starch, cellulose, methylcellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxyl At least one of propyl cellulose and carboxymethyl cellulose.
Preferably, the parts by weight of each material are:It is dirty to activate 15-20 parts of attapulgite, 15-25 parts of Chinese medicine slag, activity 25-30 parts of mud, 5-10 parts of adhesive, 6-15 parts of EM bacterium.
Preferably, the parts by weight of each material are:20 parts of attapulgite, 20 parts of Chinese medicine slag, 25 parts of activated sludge are activated, 8 parts of adhesive, 10 parts of EM bacterium.
Compared with prior art, beneficial effects of the present invention:
1. EM bacterium and raw material are mixed even granulation by the present invention using existing, the adhesive of addition promotes particle to obtain surface and forms net Shape skeleton, then surface spraying EM bacterium are obtained in particle, inside and outside bilayer EM bacterium particles are formed, fermentation is inside and outside carried out at the same time in fermentation process Be conducive to the abundant fermentation of raw material, improve the efficiency of fermentation.
2. the adhesive that the present invention adds belongs to dialdehyde polysaccharide, adhesive is acted not only as, is also beneficial to the decomposition of EM bacterium, is made Standby fertilizer will not generate secondary pollution, have the advantages that environmentally protective.
Specific embodiment
It below by the description to embodiment, is described in further detail, to help those skilled in the art to this hair Bright inventive concept, technical solution have more complete, accurate and deep understanding.
Embodiment 1
A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer, preparation are as follows: The attapulgite of 100 mesh of grain size is immersed into concentration 1.5mol/L, volume is impregnated in the NaOH solution of 6 times of attapulgite volume 12h, after centrifugal filtration, then by the attapulgite after immersion at 290 DEG C of temperature high-temperature activation 1.5h, after high-temperature alkali is activated Attapulgite be placed at 5 DEG C of temperature and cool down rapidly, be conducive to getting through and being formed for attapulgite interior bore, finally by high temperature It is discarded after the attapulgite of alkaline process activation, activated sludge, production Chinese medicine antiviral oral liquor and the solid after spontaneous fermentation 15 days Chinese medicine slag, Chinese medicine slag main component include sweet wormwood, Radix Glycyrrhizae, rhizoma anemarrhenae, Fructus Forsythiae, Radix Isatidis and semen armeniacae amarae, by mass ratio be 1: 1:1 starch, cellulose and the adhesive of methylcellulose mixing, carries out high speed dispersion in rotating speed 1200r/min and is uniformly mixed Then 30min adds in the 1/3 of total EM bacterium amounts, after being uniformly mixed under rotating speed 600r/min, carry out extruder grain, squeezes Into particle obtain grain size as 10mm, then spray remaining EM bacterium solutions, side sprinkling to particle surface, side stirring ensures that sprinkling is mixed Particle after sprinkling is finally put into fermentation tank by the uniformity of conjunction, aerobic fermentation is carried out at 55 DEG C of temperature 30 days, finally will Organic fertilizer after fermentation, which is used directly in, to till the land, and can be administered when irrigating.
Wherein, the parts by weight of each ingredient are in organic fertilizer:Activate 20 parts of attapulgite, 20 parts of Chinese medicine slag, activated sludge 25 Part, 8 parts of adhesive, 10 parts of EM bacterium.
Embodiment 2
The present embodiment is with embodiment 1, the difference is that the parts by weight of each material are in the present embodiment:Activate attapulgite 15 Part, 15 parts of Chinese medicine slag, 30 parts of activated sludge, 5 parts of adhesive, 15 parts of EM bacterium.
Embodiment 3
The present embodiment is with embodiment 1, the difference is that the parts by weight of each material are in the present embodiment:Activate attapulgite 15 Part, 15 parts of Chinese medicine slag, 30 parts of activated sludge, 10 parts of adhesive, 6 parts of EM bacterium.
Embodiment 4
Comparative example, the present embodiment is with embodiment 1, the difference is that EM bacterium are not added in the present embodiment, other raw materials, item Part and preparation process and embodiment 1 are not different.
Measure total nutrient, total organic matter, full nitrogen, full phosphorus, full potassium in the organic fertilizer that embodiment 1-4 techniques obtain, all fingers Mark is calculated and is represented and with mass fraction to dry in terms of base, as a result as follows:
Raw material Organic matter/% Total nutrient/% Full nitrogen (N)/% Full phosphorus (P2O5)/% Full potassium (K2O)
Embodiment 4 (comparison) 30.28 6.42 1.43 0.19 3.19
Embodiment 1 53.2 12.45 4.05 3.91 3.94
Embodiment 2 48.5 10.59 3.45 3.51 3.48
Embodiment 3 49.5 11.35 3.8 3.85 3.82
The present invention is exemplarily described above in conjunction with specific embodiment, it is clear that present invention specific implementation is not by upper State the limitation of mode, if employ the inventive concept and technical scheme of the present invention progress various unsubstantialities improvement or It is not improved by the present invention design and technical solution directly apply to other occasions, protection scope of the present invention it It is interior.Protection scope of the present invention should be determined by the scope of protection defined in the claims.

Claims (8)

1. a kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer, which is characterized in that preparation it is specific Step is as follows:Attapulgite, activated sludge, Chinese medicine slag, the adhesive that high temperature alkaline process is activated carry out high speed dispersion and are uniformly mixed, Then the 1/3 of total EM bacterium amounts is added in, after being uniformly mixed, carries out extruder grain, is then sprayed to the particle surface made remaining EM bacterium solutions, finally particle is put into fermentation tank, aerobic fermentation 30-35d is carried out at 35-55 DEG C of temperature.
2. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, the grain size of the attapulgite is 50-100 mesh, and the grain size of the granulation is 5-15mm.
3. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, the high temperature subtraction activation step is as follows:Attapulgite is put into NaOH solution and impregnates 10-12h, then by concave convex rod Then soil high-temperature activation 1.5-2h at 280-300 DEG C of temperature is cooled down rapidly at 5-10 DEG C of temperature.
4. the preparation method according to claim 3 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, a concentration of 1.5-2mol/L of the NaOH solution, volume is 5-8 times of attapulgite.
5. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, the Chinese medicine slag is discards after production Chinese medicine antiviral oral liquor, the solid residue after spontaneous fermentation 10-20 days.
6. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, described adhesive is starch, cellulose, methylcellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose And at least one of carboxymethyl cellulose.
7. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, the parts by weight of each material are:15-20 parts of attapulgite, 15-25 parts of Chinese medicine slag, 25-30 parts of activated sludge are activated, 5-10 parts of adhesive, 6-15 parts of EM bacterium.
8. the preparation method according to claim 1 based on attapulgite material compound probiotic functional organic fertilizer, feature It is, the parts by weight of each material are:20 parts of attapulgite of activation, 20 parts of Chinese medicine slag, 25 parts of activated sludge, 8 parts of adhesive, 10 parts of EM bacterium.
CN201711483349.5A 2017-12-29 2017-12-29 A kind of preparation method based on attapulgite material compound probiotic functional organic fertilizer Pending CN108164329A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108794159A (en) * 2018-06-22 2018-11-13 安徽瑞然生物药肥科技有限公司 A method of preparing bio-feritlizer using lobster shell
CN113087447A (en) * 2021-04-08 2021-07-09 安徽新力电业科技咨询有限责任公司 Restoration type ecological brick in power transmission and transformation line construction and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108794159A (en) * 2018-06-22 2018-11-13 安徽瑞然生物药肥科技有限公司 A method of preparing bio-feritlizer using lobster shell
CN113087447A (en) * 2021-04-08 2021-07-09 安徽新力电业科技咨询有限责任公司 Restoration type ecological brick in power transmission and transformation line construction and preparation method thereof

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Application publication date: 20180615