CN108143766A - The preparation process of ultramicro kudzu root powder - Google Patents

The preparation process of ultramicro kudzu root powder Download PDF

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Publication number
CN108143766A
CN108143766A CN201711288189.9A CN201711288189A CN108143766A CN 108143766 A CN108143766 A CN 108143766A CN 201711288189 A CN201711288189 A CN 201711288189A CN 108143766 A CN108143766 A CN 108143766A
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Prior art keywords
pueraria lobata
powder
ultramicro
root powder
kudzu
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CN201711288189.9A
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Chinese (zh)
Inventor
张万林
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ANHUI JINLONGSHAN GE INDUSTRY Co Ltd
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ANHUI JINLONGSHAN GE INDUSTRY Co Ltd
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Priority to CN201711288189.9A priority Critical patent/CN108143766A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/48Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
    • A61K36/488Pueraria (kudzu)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/14Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/141Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
    • A61K9/148Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with compounds of unknown constitution, e.g. material from plants or animals
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/13Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/51Concentration or drying of the extract, e.g. Lyophilisation, freeze-drying or spray-drying
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/50Methods involving additional extraction steps
    • A61K2236/53Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization

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  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Chemical & Material Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Botany (AREA)
  • Veterinary Medicine (AREA)
  • Medicinal Chemistry (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Epidemiology (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Zoology (AREA)
  • Biotechnology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses the preparation process of ultramicro kudzu root powder, including following technological process:Step 1:It chooses high-quality pueraria lobata to clean, and the end of the root on pueraria lobata surface and both ends is cut;Step 2:By step 1, treated that pueraria lobata is placed in soaking sterilization 15 30 minutes in 500 mg/kg brine;Step 3:By step 2, treated that pueraria lobata is put into crushes in beater and crush slurries at the beginning of obtaining pueraria lobata particle and pueraria lobata;Pass through above-mentioned technical proposal, the preparation process of ultramicro kudzu root powder proposed by the present invention, it is crushed by the way that pueraria lobata will be given birth to, mashing, precipitation, filters, pueraria lobata block is made after drying, and pueraria lobata block is ground and carries out ultramicro grinding processing, and with honey powder co-grinding, final pasteurising pack, entire technique have passed through moisture, the acerbity inside pueraria lobata precipitation and is separated by filtration, the kudzu-vine root powder drawn is in good taste, while will be kept down by active ingredient in pueraria lobata.

Description

The preparation process of ultramicro kudzu root powder
Technical field
The present invention relates to a kind of preparation technique of traditional Chinese medicine, and in particular to the preparation process of ultramicro kudzu root powder.
Background technology
Kudzuvine root starch, also referred to as kudzu-vine root powder.It can be divided into pueraria starch and kudzuvine root total powder, and difference lies in processing skill is different for the two. Pueraria lobata includes 12% flavone compound, such as Puerarin, daizeol glycosides, peanut element nutritional ingredient, also protein, The minerals such as amino acid, sugar and iron needed by human, calcium, copper, selenium, are rare invigorants suitable for people of all ages, there is " people in thousand The good reputation of ginseng ".It has it is clearing heat and detoxicating, promote the production of body fluid to quench thirst, kidney and spleen invigorating, beneficial stomach tranquilizing the mind, the improving eyesight that clears away heart-fire, ease constipation road just and are sobered up Etc. functions.Existing medical value, and nutritious healthy function.Mainly originate in Hubei, Guizhou, Guangxi, Jiangsu, Jiangxi, Hunan Etc. ground.
Traditional kudzuvine root starch prepares processing, is by raw pueraria lobata granulated and dried, dry pueraria lobata grain can be with direct marketing, can also be by Pueraria lobota The crushing and processing of root grain, since high temperature dehydration is dried, stay in the ingredients such as the Puerarin contained by pueraria lobata and arachidic acid into kudzu-vine root powder The inside, the kudzu-vine root powder taste meta-acid of this method processing are puckery.
Invention content
In order to solve the above technical problems, we have proposed one kind, solve the problems, such as.
To solve the above problems, technical scheme is as follows:
The preparation process of ultramicro kudzu root powder, including following technological process:
Step 1:It chooses high-quality pueraria lobata to clean, and the end of the root on pueraria lobata surface and both ends is cut;
Step 2:By step 1, treated that pueraria lobata is placed in soaking sterilization 15-30 minutes in 500 mg/kg brine;
Step 3:By step 2, treated that pueraria lobata is put into crushes in beater and crush to obtain pueraria lobata particle and pueraria lobata First slurries;
Step 4:Pueraria lobata particle in step 3 is added in the water of 30% volume, and is carried out in input crushing beater together Mashing handles to obtain pueraria lobata waste material and the secondary slurries of pueraria lobata again;
Step 5:Slurries at the beginning of the pueraria lobata that the secondary slurries of pueraria lobata and step 3 are obtained mix, and carry out screen filtration, will starch In liquid remaining pueraria lobata particle or pueraria lobata waste material filtering removal, while by the filtering slurries being obtained by filtration carry out precipitation 2-5 it is small When, water and kudzuvine root starch active principle is made to generate layering, and the water on upper strata is sucked out, leaves the kudzuvine root starch sediment of bottom;
Step 6:Kudzuvine root starch sediment in step 5, is put into drying tray, and is put into dryer and is dried to obtain kudzuvine root starch Precipitate block;
Step 7:Kudzuvine root starch precipitation block is ground crushing and obtains kudzu-vine root powder, and kudzu-vine root powder is passed through into micronizer It crushes to 500-1500 mesh, obtains ultramicro kudzu root powder;
Step 8:By the ultramicro kudzu root powder in step 7 according to weight ratio 10:1 addition honey powder is mixed, must It adds in pulverizer and is crushed to 150 mesh together, the mixed powder after crushing is finally subjected to microwave sterilization, metering pack.
In the present invention, the drying temperature of the dryer in the step 6 is controlled at 115 DEG C ± 5 DEG C.
In the present invention, temperature is relatively wet no more than 80 DEG C in the crushing process of the micronizer in the step 7 Degree is no more than 7%.
Through the above technical solutions, the preparation process of ultramicro kudzu root powder proposed by the present invention, crushed by the way that pueraria lobata will be given birth to, Pueraria lobata block is made after mashing, precipitation, filtering, drying, and pueraria lobata block is ground and carries out ultramicro grinding processing, and and honey Dry powder blend crushes, and final pasteurising pack, entire technique have passed through moisture, the acerbity inside pueraria lobata precipitation and be separated by filtration , the kudzu-vine root powder drawn is in good taste, while will be kept down by active ingredient in pueraria lobata.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical solution in the embodiment of the present invention is clearly and completely retouched It states, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.Based on this hair Embodiment in bright, the every other reality that those of ordinary skill in the art are obtained without creative efforts Example is applied, shall fall within the protection scope of the present invention.
With reference to embodiment and specific embodiment, the present invention is described in further detail.
The preparation process of ultramicro kudzu root powder, including following technological process:
Step 1:It chooses high-quality pueraria lobata to clean, and the end of the root on pueraria lobata surface and both ends is cut;
Step 2:By step 1, treated that pueraria lobata is placed in soaking sterilization 15-30 minutes in 500 mg/kg brine;
Step 3:By step 2, treated that pueraria lobata is put into crushes in beater and crush to obtain pueraria lobata particle and pueraria lobata First slurries;
Step 4:Pueraria lobata particle in step 3 is added in the water of 30% volume, and is carried out in input crushing beater together Mashing handles to obtain pueraria lobata waste material and the secondary slurries of pueraria lobata again;
Step 5:Slurries at the beginning of the pueraria lobata that the secondary slurries of pueraria lobata and step 3 are obtained mix, and carry out screen filtration, will starch In liquid remaining pueraria lobata particle or pueraria lobata waste material filtering removal, while by the filtering slurries being obtained by filtration carry out precipitation 2-5 it is small When, water and kudzuvine root starch active principle is made to generate layering, and the water on upper strata is sucked out, leaves the kudzuvine root starch sediment of bottom;
Step 6:Kudzuvine root starch sediment in step 5, is put into drying tray, and is put into dryer and is dried to obtain kudzuvine root starch Precipitate block;
Step 7:Kudzuvine root starch precipitation block is ground crushing and obtains kudzu-vine root powder, and kudzu-vine root powder is passed through into micronizer It crushes to 500-1500 mesh, obtains ultramicro kudzu root powder;
Step 8:By the ultramicro kudzu root powder in step 7 according to weight ratio 10:1 addition honey powder is mixed, must It adds in pulverizer and is crushed to 150 mesh together, the mixed powder after crushing is finally subjected to microwave sterilization, metering pack.
In the present invention, the drying temperature of the dryer in the step 6 is controlled at 115 DEG C ± 5 DEG C.In the step 7 Temperature is no more than 80 DEG C in the crushing process of micronizer, and relative humidity is no more than 7%.
What has been described above is only a preferred embodiment of the present invention, it is noted that for those of ordinary skill in the art For, without departing from the concept of the premise of the invention, various modifications and improvements can be made, these belong to this hair Bright protection domain.

Claims (3)

1. the preparation process of ultramicro kudzu root powder, which is characterized in that including following technological process:
Step 1:It chooses high-quality pueraria lobata to clean, and the end of the root on pueraria lobata surface and both ends is cut;
Step 2:By step 1, treated that pueraria lobata is placed in soaking sterilization 15-30 minutes in 500 mg/kg brine;
Step 3:By step 2, treated that pueraria lobata is put into crushes in beater and crush to obtain pueraria lobata particle and pueraria lobata centrotheca Liquid;
Step 4:Pueraria lobata particle in step 3 is added in the water of 30% volume, and is carried out again in input crushing beater together Mashing handles to obtain pueraria lobata waste material and the secondary slurries of pueraria lobata;
Step 5:Slurries at the beginning of the pueraria lobata that the secondary slurries of pueraria lobata and step 3 are obtained mix, and carry out screen filtration, will be residual in slurries Stay pueraria lobata particle or pueraria lobata waste material filtering removal, while by the filtering slurries being obtained by filtration carry out precipitation 2-5 hour, make water with Kudzuvine root starch active principle generates layering, and the water on upper strata is sucked out, and leaves the kudzuvine root starch sediment of bottom;
Step 6:Kudzuvine root starch sediment in step 5, is put into drying tray, and is put into dryer and is dried to obtain kudzuvine root starch precipitation Block;
Step 7:Kudzuvine root starch precipitation block is ground crushing and obtains kudzu-vine root powder, and kudzu-vine root powder is subjected to powder by micronizer 500-1500 mesh is broken to, obtains ultramicro kudzu root powder;
Step 8:By the ultramicro kudzu root powder in step 7 according to weight ratio 10:1 addition honey powder is mixed, must be together It adds in pulverizer and crushes to 150 mesh, the mixed powder after crushing is finally subjected to microwave sterilization, metering pack.
2. the preparation process of ultramicro kudzu root powder according to claim 1, which is characterized in that the dryer in the step 6 Drying temperature control at 115 DEG C ± 5 DEG C.
3. the preparation process of ultramicro kudzu root powder according to claim 1, which is characterized in that the Ultramicro-powder in the step 7 Temperature is no more than 80 DEG C in the crushing process of pulverizer, and relative humidity is no more than 7%.
CN201711288189.9A 2017-12-07 2017-12-07 The preparation process of ultramicro kudzu root powder Pending CN108143766A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110240990A (en) * 2019-07-17 2019-09-17 安徽华粮液国粹生物药业科技有限公司 A kind of chu chrysanthemum pueraria lobata assembled alcoholic drinks and its preparation process
CN112335807A (en) * 2020-11-06 2021-02-09 贵州垦郎食品有限公司 Processing method of flavored radix Puerariae powder

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104522571A (en) * 2014-12-05 2015-04-22 安徽金龙山葛业有限公司 Technology for making wild radix puerariae into full powder of ultramicro radix puerariae powder
CN105831652A (en) * 2016-03-30 2016-08-10 慈利县宏达农林开发有限公司 Multi-flavored radix puerariae food and production method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104522571A (en) * 2014-12-05 2015-04-22 安徽金龙山葛业有限公司 Technology for making wild radix puerariae into full powder of ultramicro radix puerariae powder
CN105831652A (en) * 2016-03-30 2016-08-10 慈利县宏达农林开发有限公司 Multi-flavored radix puerariae food and production method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110240990A (en) * 2019-07-17 2019-09-17 安徽华粮液国粹生物药业科技有限公司 A kind of chu chrysanthemum pueraria lobata assembled alcoholic drinks and its preparation process
CN112335807A (en) * 2020-11-06 2021-02-09 贵州垦郎食品有限公司 Processing method of flavored radix Puerariae powder

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Application publication date: 20180612