CN108130206A - A kind of military high detergence dry detergent - Google Patents

A kind of military high detergence dry detergent Download PDF

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Publication number
CN108130206A
CN108130206A CN201711420225.2A CN201711420225A CN108130206A CN 108130206 A CN108130206 A CN 108130206A CN 201711420225 A CN201711420225 A CN 201711420225A CN 108130206 A CN108130206 A CN 108130206A
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China
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parts
detergence
dry detergent
military high
mixture
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张成如
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Beijing Oumeizhong Science and Technology Research Institute
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Beijing Oumeizhong Science and Technology Research Institute
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Priority to CN201711420225.2A priority Critical patent/CN108130206A/en
Publication of CN108130206A publication Critical patent/CN108130206A/en
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/825—Mixtures of compounds all of which are non-ionic
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/06—Phosphates, including polyphosphates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2006—Monohydric alcohols
    • C11D3/2034—Monohydric alcohols aromatic
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2041—Dihydric alcohols
    • C11D3/2044—Dihydric alcohols linear
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2068—Ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2086—Hydroxy carboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2093—Esters; Carbonates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/28—Heterocyclic compounds containing nitrogen in the ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/30—Amines; Substituted amines ; Quaternized amines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40—Dyes ; Pigments
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/008—Polymeric surface-active agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/662—Carbohydrates or derivatives
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols

Abstract

The application belongs to chemical field, and in particular to a kind of military clear dry cleaning agent of strong dirt-removing.Raw material including following portions by weight, 20 25 parts of coco imidoazolinium dicarboxyl, 15 18 parts of 2 pyrrolidones of N methyl, 5 15 parts of potassium pyrophosphate, 30 35 parts of succinic acid monoalkyl esters, 25 27 parts of ethylene glycol list isopropoxy ether, 15 20 parts of monoethanolamine, 15 20 parts of butanediol, 15 parts of surfactant, 0.2 0.5 parts of essence, 0.1 0.3 parts of pigment, 12 parts of thickener, 0.5 3 parts of softening agent, 23 parts of fungicide, 12 parts of disinfectant, 23 parts of antioxidant.The advantageous effect of the application is：Manufacture craft is simple, easy to use, time saving, laborsaving, decontamination is superpower, use scope is wide, and suitable for various clothes and bottom surface, fabric color and feel are not damaged after use.

Description

A kind of military high detergence dry detergent
Technical field
The application belongs to chemical field, and in particular to a kind of military clear dry cleaning agent of strong dirt-removing.
Background technology
With the development of society, the increasingly raising of people's living standard, the requirement to quality of life is also higher and higher, simultaneously People’s lives rhythm is also original faster, and the time that people are used to arrange household is fewer and fewer, and by investigation, people are being clear Clean health is worried endlessly, e.g., the daily necessitiess such as sofa, down jackets, quilt, if with being articles for washing on the market, washing effect Do not think, and need to consume a large amount of water, down jackets and the quilt for being stained with water are very heavy, and washing is inconvenient, is not easy to dry.
Invention content
In order to solve the above-mentioned technical problem, this application provides a kind of military clear dry cleaning agent of strong dirt-removing, the application is logical Cross following proposal realization：
A kind of military high detergence dry detergent, the raw material including following portions by weight, 20-25 parts of coco imidoazolinium dicarboxyl, N- 15-18 parts of N-methyl-2-2-pyrrolidone N, 5-15 parts of potassium pyrophosphate, 30-35 parts of succinic acid monoalkyl esters, ethylene glycol list isopropoxy 25-27 parts of ether, 15-20 parts of monoethanolamine, 15-20 parts of butanediol, 1-5 parts of surfactant, 0.2-0.5 parts of essence, pigment 0.1-0.3 parts, 1-2 parts of thickener, 0.5-3 parts of softening agent, 2-3 parts of fungicide, 1-2 parts of disinfectant, 2-3 parts of antioxidant.
Preferably, the thickener is hydroxyethyl cellulose.
Preferably, the softening agent is alkyl polyglycoside, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin The mass ratio of mixture, the alkyl polyglycoside, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin is 7：1：1：2.
Preferably, the fungicide is o-phenyl phenol and salicylic mixture, the o-phenyl phenol and salicylic acid Mass ratio be 3:2.
Preferably, the disinfectant is calcium hypochlorite.
Preferably, the antioxidant is butyl anisole, and di-t-butyl mixes phenyl methylcarbamate and propylgallate Object, the butyl anisole are closed, di-t-butyl is 1 to the mass ratio of phenyl methylcarbamate and propylgallate：3：4.
A kind of preparation method of military high detergence dry detergent, includes the following steps：（1）By coco imidoazolinium dicarboxyl, N-methyl-2-pyrrolidone, potassium pyrophosphate, succinic acid monoalkyl esters, ethylene glycol list isopropoxy ether, monoethanolamine and fourth two Alcohol is placed in reaction kettle and is dehydrated at 100-150 DEG C；（2）To step（1）After dehydration surface-active is added in gained mixture Agent simultaneously stirs 0.5h at 100-120 DEG C；（3）To step（2）Essence and pigment are added in mixture and is stirred at 90-95 DEG C 1h；（4）To step（3）Thickener, softening agent, fungicide, disinfectant and antioxidant are added in gained mixture, after 80- 2h is stirred at 90 DEG C, most after be dehydrated at 120-130 DEG C both decontamination dry cleaning agent
Preferably, the step（1）Dewatering pressure be -0.1MPa；The step（2）Mixing speed be 5000r/min.
Preferably, the step（3）Mixing speed be 5500r/min.
Preferably, the step（4）Mixing speed for 6000r/min, the dewatering pressure is -0.3 MPa.
The advantageous effect of the application is：Manufacture craft is simple, easy to use, time saving, laborsaving, decontamination is superpower, use scope Extensively, suitable for various clothes and bottom surface, fabric color and feel are not damaged after use.
Specific embodiment
Embodiment 1
A kind of military high detergence dry detergent, the raw material including following portions by weight, 25 parts of coco imidoazolinium dicarboxyl, N- first 18 parts of base -2-Pyrrolidone, 15 parts of potassium pyrophosphate, 35 parts of succinic acid monoalkyl esters, 27 parts of ethylene glycol list isopropoxy ether are single 20 parts of ethanol amine, 20 parts of butanediol, 5 parts of surfactant, 0.5 part of essence, 0.3 part of pigment, 2 parts of thickener, 3 parts of softening agent, 3 parts of fungicide, 2 parts of disinfectant, 3 parts of antioxidant.
Preferably, the thickener is hydroxyethyl cellulose；
Preferably, the softening agent be alkyl polyglycoside, fatty alcohol polyoxyethylene ether, the mixing of fatty acid alkanol amides and Tea Saponin The mass ratio of object, the alkyl polyglycoside, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin is 7：1：1：2；
Preferably, the fungicide is o-phenyl phenol and salicylic mixture, the o-phenyl phenol and salicylic matter Amount is than being 3:2；
Preferably, the disinfectant is calcium hypochlorite；
Preferably, the antioxidant is butyl anisole, di-t-butyl to the mixture of phenyl methylcarbamate and propylgallate, The butyl anisole, di-t-butyl are 1 to the mass ratio of phenyl methylcarbamate and propylgallate：3：4；
A kind of preparation method of military high detergence dry detergent, includes the following steps：（1）By coco imidoazolinium dicarboxyl, N- first Base -2-Pyrrolidone, potassium pyrophosphate, succinic acid monoalkyl esters, ethylene glycol list isopropoxy ether, monoethanolamine and butanediol are put It is dehydrated in reaction kettle and at 100-150 DEG C；（2）To step（1）After dehydration surfactant is added in gained mixture simultaneously 0.5h is stirred at 100-120 DEG C；（3）To step（2）Essence and pigment are added in mixture and stirs 1h at 90-95 DEG C； （4）To step（3）Thickener, softening agent, fungicide, disinfectant and antioxidant are added in gained mixture, after 80-90 DEG C Lower stirring 2h, most after be dehydrated at 120-130 DEG C both decontamination dry cleaning agent；
Preferably, the step（1）Dewatering pressure be -0.1MPa；The step（2）Mixing speed be 5000r/min；
Preferably, the step（3）Mixing speed be 5500r/min；
Preferably, the step（4）Mixing speed for 6000r/min, the dewatering pressure is -0.3 MPa.
Embodiment 2
A kind of military high detergence dry detergent, the raw material including following portions by weight, 20- parts of coco imidoazolinium dicarboxyl, N- first 15 parts of base -2-Pyrrolidone, 5 parts of potassium pyrophosphate, 30 parts of succinic acid monoalkyl esters, 25 parts of ethylene glycol list isopropoxy ether are single 15 parts of ethanol amine, 15 parts of butanediol, 1 part of surfactant, 0.2 part of essence, 0.1 part of pigment, 1 part of thickener, softening agent 0.5 Part, 2 parts of fungicide, 1 part of disinfectant, 2 parts of antioxidant；
Preferably, the thickener is hydroxyethyl cellulose；
Preferably, the softening agent be alkyl polyglycoside, fatty alcohol polyoxyethylene ether, the mixing of fatty acid alkanol amides and Tea Saponin The mass ratio of object, the alkyl polyglycoside, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin is 7：1：1：2；
Preferably, the fungicide is o-phenyl phenol and salicylic mixture, the o-phenyl phenol and salicylic matter Amount is than being 3:2；
Preferably, the disinfectant is calcium hypochlorite；
Preferably, the antioxidant is butyl anisole, di-t-butyl to the mixture of phenyl methylcarbamate and propylgallate, The butyl anisole, di-t-butyl are 1 to the mass ratio of phenyl methylcarbamate and propylgallate：3：4；
A kind of preparation method of military high detergence dry detergent, includes the following steps：（1）By coco imidoazolinium dicarboxyl, N- first Base -2-Pyrrolidone, potassium pyrophosphate, succinic acid monoalkyl esters, ethylene glycol list isopropoxy ether, monoethanolamine and butanediol are put It is dehydrated in reaction kettle and at 100 DEG C；（2）To step（1）Surfactant is added in after dehydration in gained mixture and in 100 0.5h is stirred at DEG C；（3）To step（2）Essence and pigment are added in mixture and stirs 1h at 90 DEG C；（4）To step（3） Thickener, softening agent, fungicide, disinfectant and antioxidant are added in gained mixture, after stirring 2h at 80 DEG C, most after It is dehydrated at 120 DEG C and both obtains decontamination dry cleaning agent；
Preferably, the step（1）Dewatering pressure be -0.1MPa；The step（2）Mixing speed be 5000r/min；
Preferably, the step（3）Mixing speed be 5500r/min；
Preferably, the step（4）Mixing speed for 6000r/min, the dewatering pressure is -0.3 MPa.
Embodiment 3
A kind of military high detergence dry detergent, the raw material including following portions by weight, 22 parts of coco imidoazolinium dicarboxyl, N- first 16 parts of base -2-Pyrrolidone, 10 parts of potassium pyrophosphate, 32 parts of succinic acid monoalkyl esters, 26 parts of ethylene glycol list isopropoxy ether are single 18 parts of ethanol amine, 17 parts of butanediol, 3 parts of surfactant, 0.3 part of essence, 0.2 part of pigment, 1.5 parts of thickener, softening agent 2 Part, 2.5 parts of fungicide, 1.5 parts of disinfectant, 2.5 parts of antioxidant；
Preferably, the thickener is hydroxyethyl cellulose；
Preferably, the softening agent be alkyl polyglycoside, fatty alcohol polyoxyethylene ether, the mixing of fatty acid alkanol amides and Tea Saponin The mass ratio of object, the alkyl polyglycoside, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin is 7：1：1：2；
Preferably, the fungicide is o-phenyl phenol and salicylic mixture, the o-phenyl phenol and salicylic matter Amount is than being 3:2；
Preferably, the disinfectant is calcium hypochlorite；
Preferably, the antioxidant is butyl anisole, di-t-butyl to the mixture of phenyl methylcarbamate and propylgallate, The butyl anisole, di-t-butyl are 1 to the mass ratio of phenyl methylcarbamate and propylgallate：3：4；
A kind of preparation method of military high detergence dry detergent, includes the following steps：（1）By coco imidoazolinium dicarboxyl, N- first Base -2-Pyrrolidone, potassium pyrophosphate, succinic acid monoalkyl esters, ethylene glycol list isopropoxy ether, monoethanolamine and butanediol are put It is dehydrated in reaction kettle and at 125 DEG C；（2）To step（1）Surfactant is added in after dehydration in gained mixture and in 110 0.5h is stirred at DEG C；（3）To step（2）Essence and pigment are added in mixture and stirs 1h at 93 DEG C；（4）To step（3） Thickener, softening agent, fungicide, disinfectant and antioxidant are added in gained mixture, after stirring 2h at 85 DEG C, most after It is dehydrated at 125 DEG C and both obtains decontamination dry cleaning agent；
Preferably, the step（1）Dewatering pressure be -0.1MPa；The step（2）Mixing speed be 5000r/min；
Preferably, the step（3）Mixing speed be 5500r/min；
Preferably, the step（4）Mixing speed for 6000r/min, the dewatering pressure is -0.3 MPa.

Claims (10)

1. a kind of military high detergence dry detergent, which is characterized in that the raw material including following portions by weight, coco imidoazolinium two 20-25 parts of carboxylic, 15-18 parts of n-methyl-2-pyrrolidone, 5-15 parts of potassium pyrophosphate, 30-35 parts of succinic acid monoalkyl esters, second two 25-27 parts of alcohol list isopropoxy ether, 15-20 parts of monoethanolamine, 15-20 parts of butanediol, 1-5 parts of surfactant, essence 0.2-0.5 parts, 0.1-0.3 parts of pigment, 1-2 parts of thickener, 0.5-3 parts of softening agent, 2-3 parts of fungicide, 1-2 parts of disinfectant, resist 2-3 parts of oxidant.
2. a kind of military high detergence dry detergent as described in claim 1, which is characterized in that the thickener is fine for ethoxy Dimension element.
3. a kind of military high detergence dry detergent as described in claim 1, which is characterized in that the softening agent is more for alkyl The mixture of glycosides, fatty alcohol polyoxyethylene ether, fatty acid alkanol amides and Tea Saponin, the alkyl polyglycoside, fatty alcohol polyoxy second The mass ratio of alkene ether, fatty acid alkanol amides and Tea Saponin is 7：1：1：2.
4. a kind of military high detergence dry detergent as described in claim 1, which is characterized in that the fungicide is adjacent phenyl benzene Phenol and salicylic mixture, the o-phenyl phenol and salicylic mass ratio are 3:2.
5. a kind of military high detergence dry detergent as described in claim 1, which is characterized in that the disinfectant is hypochlorous acid Calcium.
6. a kind of military high detergence dry detergent as described in claim 1, which is characterized in that the antioxidant is fourth hydroxyl Anisole, di-t-butyl is to the mixture of phenyl methylcarbamate and propylgallate, and the butyl anisole, di-t-butyl is to benzene first The mass ratio of phenol and propylgallate is 1：3：4.
7. a kind of preparation method of military high detergence dry detergent as described in claim 1, which is characterized in that including following steps Suddenly：（1）By coco imidoazolinium dicarboxyl, n-methyl-2-pyrrolidone, potassium pyrophosphate, succinic acid monoalkyl esters, ethylene glycol Dan Yi Propoxyl group ether, monoethanolamine and butanediol are placed in reaction kettle and are dehydrated at 100-150 DEG C；（2）To step（1）After dehydration Surfactant is added in gained mixture and stirs 0.5h at 100-120 DEG C；（3）To step（2）It is added in mixture fragrant Essence and pigment simultaneously stir 1h at 90-95 DEG C；（4）To step（3）Add in thickener in gained mixture, softening agent, fungicide, Disinfectant and antioxidant, after stirring 2h at 80-90 DEG C, most after be dehydrated at 120-130 DEG C both decontamination dry cleaning agent.
A kind of 8. preparation method of military high detergence dry detergent as claimed in claim 7, which is characterized in that the step （1）Dewatering pressure be -0.1MPa；The step（2）Mixing speed be 5000r/min.
A kind of 9. preparation method of military high detergence dry detergent as claimed in claim 9, which is characterized in that the step （3）Mixing speed be 5500r/min.
A kind of 10. preparation method of military high detergence dry detergent as claimed in claim 10, which is characterized in that the step （4）Mixing speed for 6000r/min, the dewatering pressure is -0.3 MPa.
CN201711420225.2A 2017-12-25 2017-12-25 A kind of military high detergence dry detergent Pending CN108130206A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1095409A (en) * 1993-05-14 1994-11-23 沈阳化工学院科技开发公司 Dry-cleaning agent for skin
CN1200400A (en) * 1997-05-26 1998-12-02 戴恒 Dry cleaning agent and method for preparing same
CN107267299A (en) * 2017-06-28 2017-10-20 太仓红桥服饰有限公司 A kind of antistatic dry cleaning agent

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1095409A (en) * 1993-05-14 1994-11-23 沈阳化工学院科技开发公司 Dry-cleaning agent for skin
CN1200400A (en) * 1997-05-26 1998-12-02 戴恒 Dry cleaning agent and method for preparing same
CN107267299A (en) * 2017-06-28 2017-10-20 太仓红桥服饰有限公司 A kind of antistatic dry cleaning agent

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Application publication date: 20180608