CN108101628A - The preparation process of three red sweet shaddock plantation soil amendment fertilizers - Google Patents
The preparation process of three red sweet shaddock plantation soil amendment fertilizers Download PDFInfo
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- CN108101628A CN108101628A CN201711350265.4A CN201711350265A CN108101628A CN 108101628 A CN108101628 A CN 108101628A CN 201711350265 A CN201711350265 A CN 201711350265A CN 108101628 A CN108101628 A CN 108101628A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/30—Layered or coated, e.g. dust-preventing coatings
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
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Abstract
The invention discloses the preparation processes of a kind of three red sweet shaddock plantation soil amendment fertilizers, belong to fertilizer preparing technical field.The three red sweet shaddock plantation soil amendment fertilizers, including following raw material：Ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea bubble powder, calcium magnesium phosphate, compound bacteria, diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, starch graft acrylic acid potassium, the three red sweet shaddock plantations are by preparing compound fertilizer granules, preparing coating feed liquid, fertiliser granulates coating, made of drying and other steps with soil amendment fertilizer.The soil amendment fertilizer of the present invention can improve the per mu yield of three red sweet shaddocks.
Description
【Technical field】
The invention belongs to fertilizer preparing technical fields, and in particular to the system of a kind of three red sweet shaddock plantation soil amendment fertilizers
Standby technique.
【Background technology】
Shaddock also known as pomelo, fragrant goldenrain tree, grapefruit, interior purple etc. are the ripening fruits of Citrus paradisi Macfadyen, originate in China Fujian,
The southern areas such as Jiangxi, Hunan, Guangdong, Guangxi, Zhejiang, Sichuan.Pomelo fragrant, sour-sweet, Liang Run, full of nutrition, medical value
It is very high, it is one of fruit of people's eating and the fruit of most food therapy effect that medical field is generally acknowledged.Citron tea and pomelo peel
It all has practical value, and can be used as medicine.
The policy of China's modern times fruits industry development is " lower beach of going up a hill ", this just determines that most grapefruits are planted in
On mountain area, hills, sandy beach and salt-soda soil.The general soil property in these places is more barren, and dysplasia, the content of organic matter is low, unfavorable
In the growth and development of grapefruit.Particularly South China Tropical or subtropical zone, high temperature and humidity, the soil organism in shaddock garden
Content is few, grogs is thin, dysplasia, and mostly in acidity, iron aluminium is opposite to be gathered, and available phosphorus is less.Soil is in the pasty state, arid after rain
When soil block become especially hard, be unfavorable for the growth and development of shaddock.
Soil is one of important ecological environmental condition of grapefruit and builds high standard shaddock garden, ensures that shaddock garden is excellent
The material base of matter.Loam is the important step for realizing production modernization shaddock Orchard Soil management, its growth with grapefruit
Development is closely related with the taste quality of shaddock.Fully to develop and utilize soil resource, high-quality shaddock garden is established, creates shaddock
The good ecological environment of growth is set, extends the grapefruit economic life, soil improvement must be carried out by increasing economic efficiency.
A kind of Chinese patent application document " shaddock Orchard Soil modifying agent and preparation method thereof (application publication number：
CN106116952A) " open a kind of shaddock Orchard Soil modifying agent and preparation method thereof of knowing clearly, including following component：Organic fertilizer 18-
39 parts by weight, peat soil 5-12 parts by weight, montmorillonite 1-5 parts by weight, zeolite 1-5 parts by weight, sepiolite 2-6 parts by weight, calcium and magnesium
Phosphate fertilizer 4-8 parts by weight, bacillus licheniformis 1-3 parts by weight, blown-ball Azotobacter 1-3 parts by weight, actinobacillus capsulatus 1-3 weight
Part.Compared with prior art, the present invention is with organic fertilizer, peat soil, montmorillonite, zeolite, sepiolite, calcium magnesium phosphate, lichens gemma
Bacillus, blown-ball Azotobacter, actinobacillus capsulatus are prepared for shaddock Orchard Soil modifying agent for raw material, improve the soil in shaddock garden,
Supplemented with trace element, soil physics structure is improved, enhances soil fertility, however there is using after the soil amendment fertilizer
The problem of yield of the three red sweet shaddocks obtained is relatively low.
【The content of the invention】
The present invention provides the preparation process of a kind of three red sweet shaddock plantation soil amendment fertilizers, to solve in Chinese patent Shen
It please a kind of document " shaddock Orchard Soil modifying agent and preparation method thereof (application publication number：CN106116952A soil changes disclosed in) "
On the basis of good agent prescription, how to optimize component, dosage etc., improve the per mu yield of three red sweet shaddocks.
For solution more than technical problem, the present invention uses following technical scheme：
The preparation process of a kind of three red sweet shaddock plantation soil amendment fertilizers, comprises the following steps：
S1：Powder, calcium magnesium phosphate are steeped into ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea, answered
It closes bacterium ratio by weight to mix, ferments, ferment 5-10 days in the case where temperature is 35-52 DEG C, fermentate is made；
The preparation process of the compound bacteria, comprises the following steps：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus
Ratio is activated in the case where temperature is 23-26 DEG C, expands culture by weight, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, brown ball fixed nitrogen will be expanded to step a
Bacterium, phosphobacteria, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 500-800 part water and be uniformly mixed, in temperature
After spending to cultivate 15-18h at 24-26 DEG C, water removal is centrifuged in the case where rotating speed is 2000-3000r/min, compound bacteria is made；Institute
Biological nutritive agent is stated, including following raw material：Yeast extract, sucrose, peptone, potassium acetate, sodium phosphate；The biological growth stimulant
In units of parts by weight, including following raw material：Cerium chloride, aluminum sulfate；
S2：Fermentate made from step S1 at 50-62 DEG C is concentrated, obtains concentrate, by the concentrate in 65-72
It dries to water content≤4% at DEG C, is then granulated, compound fertilizer granules are made；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to
72-80 DEG C, continue stirring l.2-2.5h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in the silicon of parts by weight
Diatomaceous earth, polyethylene glycol oxide, starch graft acrylic acid potassium are warming up to 80-90 DEG C, accelerate stirring 1.2-1.8h, stop heating, continue
Stirring, is cooled to room temperature, and coating feed liquid is made；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, by coating feed liquid liter made from step S3
Then temperature is equably sprayed on compound fertilizer granules surface, then air drying to 52-70 DEG C with high-pressure spray-painted rifle, it is red to be made three
Sweet shaddock plantation soil amendment fertilizer.
Further, diatomite described in step S1, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, shallow lake
The weight ratio of powder grafted propylene acid potassium is (6-18):(3-6):(5-9):(2-4):(2.6-3.5):(2-4.6).
Further, the diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, starch-grafted third
The weight ratio of olefin(e) acid potassium is 15:5:8:3:3.2:3.8.
Further, the compound bacteria described in step S1 is in units of parts by weight, including following raw material：Bacillus licheniformis
20-32 parts, 12-22 parts of nitrobacteria, 10-15 parts of saccharomycete, 3-6 parts of photosynthetic bacteria, 6-10 parts of blown-ball Azotobacter, phosphobacteria 4-9
Part, 3-5 parts of B. mucilaginocus.
Further, the compound bacteria is in units of parts by weight, including following raw material：26 parts of bacillus licheniformis, nitre
Change 20 parts of bacterium, 12 parts of saccharomycete, 5 parts of photosynthetic bacteria, 8 parts of blown-ball Azotobacter, 8 parts of phosphobacteria, 3 parts of B. mucilaginocus.
Further, biological nutritive agent described in step S1 is in units of parts by weight, including following raw material：Yeast extract 50-
60 parts, 30-50 parts of sucrose, 14-22 parts of peptone, 15-20 parts of potassium acetate, 12-16 parts of sodium phosphate.
Further, the biological nutritive agent is in units of parts by weight, including following raw material：54 parts of yeast extract, sucrose 42
Part, 18 parts of peptone, 16 parts of potassium acetate, 15 parts of sodium phosphate.
Further, biological growth stimulant described in step S1 is in units of parts by weight, including following raw material：Cerium chloride
42-56 parts, 25-30 parts of aluminum sulfate.
Further, the biological growth stimulant is in units of parts by weight, including following raw material：52 parts of cerium chloride, sulphur
Sour 28 parts of aluminium.
Further, in step S4 air drying to water content≤1%.
The invention has the advantages that：
(1) by the data of embodiment 1-3 and comparative example 8 as it can be seen that using the red sweet shaddock plantation soil improvements of embodiment 1-3 tri-
Three red sweet shaddock per mu yields of fertilizer significantly improve；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment 1 is optimal implementation
Example..
(2) by embodiment 1 and the data of comparative example 1-7 as it can be seen that diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium,
Polyethylene glycol oxide, starch graft acrylic acid potassium are preparing three red sweet shaddock plantations with playing synergistic effect in soil amendment fertilizer,
Collaboration improves the per mu yield of three red sweet shaddocks, this may be：Using diatomite as major ingredient, using itaconic acid as crosslinking agent, gather
Vinyl alcohol is a kind of water soluble polymer, has good film forming.Polyaminoacid potassium can increase soil porosity and water holding
Amount, helps to improve soil water-reataining fertilizer-keeping ability, creates good conditions for three red sweet shaddock root growth and developments.Polyethylene glycol oxide contains
There is water-wet side, can be combined with compound fertilizer granule, polyethylene glycol oxide has good water resistance, and its strand can be in water
In stretch well, be uniformly arranged in interface, increase steric hindrance, make the sub- rapid dispersion of compound fertilizer granule in water；It forms sediment
Powder grafted propylene acid potassium when being used cooperatively with polyaminoacid potassium, can increase fertilizer absorption as the slow releasing carrier material of fertilizer
Rate.Diatomite is porous material, while substantial amounts of hydroxyl is contained on its surface, the hydroxyl on diatomite surface can be utilized, in clothing health
Under sour modifying function, even closer, and the filming function in polyvinyl alcohol and starch-grafted propylene are combined with compound fertilizer granule
Under sour potassium slow releasing function, effective sustained release to compound fertilizer granule can be realized so that compound fertilizer granule is entered in soil
After can slowly enter in soil, slowly supply fertilizer particle is carried out to soil, soil depletion and hardened is avoided, ties simultaneously
The retain water and nutrients ability of polyaminoacid potassium is closed, the efficiency and yield of three red sweet shaddock growths can be effectively improved.
(3) diatomite in the present invention, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, starch-grafted third
Olefin(e) acid potassium is as reinforcement system, and embodiment 1-3 is by controlling diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyoxygenated
Ethylene, the weight ratio of starch graft acrylic acid potassium are (6-18):(3-6):(5-9):(2-4):(2.6-3.5):(2-4.6), it is real
It is used as the leading role raw material of reinforcement system in present reinforcement system using diatomite, polyethylene glycol oxide, while utilization itaconic acid
Crosslinking agent performance, the filming function of polyvinyl alcohol, polyaminoacid potassium can increase soil porosity and water-holding capacity, improve soil and protect
The ability of water fertilizer conservation and the slow releasing function of starch graft acrylic acid potassium so that entire reinforcement system applies to the soil of the present invention
The per mu yield of three red sweet shaddocks can be effectively improved in earth improvement fertilizer.
【Specific embodiment】
It for ease of more fully understanding the present invention, is illustrated by following instance, these examples belong to the protection of the present invention
Scope, but do not limit the scope of the invention.
In embodiment, the three red sweet shaddock plantation soil amendment fertilizers, in units of parts by weight, including following original
Material：42-60 parts of ammonium carbonate, 12-15 parts of monoammonium phosphate, 14-35 parts of potassium chloride, 8-15 parts of peat soil, 3-5 parts of montmorillonite powder, boiling
2-4 parts of mountain flour, sea bubble 4-8 parts of powder, 7-12 parts of calcium magnesium phosphate, 20-30 parts of compound bacteria, 6-18 parts of diatomite, 3-6 parts of itaconic acid,
5-9 parts of polyvinyl alcohol, 2-4 parts of polyaminoacid potassium, 2.6-3.5 parts of polyethylene glycol oxide, 2-4.6 parts of starch graft acrylic acid potassium；
The compound bacteria is in units of parts by weight, including following raw material：20-32 parts of bacillus licheniformis, nitrobacteria
12-22 parts, 10-15 parts of saccharomycete, 3-6 parts of photosynthetic bacteria, 6-10 parts of blown-ball Azotobacter, 4-9 parts of phosphobacteria, 3-5 parts of B. mucilaginocus；
The preparation process of the three red sweet shaddock plantation soil amendment fertilizers, comprises the following steps：
S1：Powder, calcium magnesium phosphate are steeped into ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea, answered
It closes bacterium ratio by weight to mix, ferments, ferment 5-10 days in the case where temperature is 35-52 DEG C, fermentate is made；
The preparation process of compound bacteria, comprises the following steps described in step S1：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus
Ratio is activated in the case where temperature is 23-26 DEG C, expands culture by weight, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, brown ball fixed nitrogen will be expanded to step a
Bacterium, phosphobacteria, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 500-800 part water and be uniformly mixed, in temperature
After spending to cultivate 15-18h at 24-26 DEG C, water removal is centrifuged in the case where rotating speed is 2000-3000r/min, compound bacteria is made；Institute
Biological nutritive agent is stated in units of parts by weight, including following raw material：50-60 parts of yeast extract, 30-50 parts of sucrose, peptone 14-22
Part, 15-20 parts of potassium acetate, 12-16 parts of sodium phosphate；The biological growth stimulant is in units of parts by weight, including following raw material：
42-56 parts of cerium chloride, 25-30 parts of aluminum sulfate；
S2：Fermentate made from step S1 at 50-62 DEG C is concentrated, obtains concentrate, by the concentrate in 65-72
It dries to water content≤4% at DEG C, is then granulated, compound fertilizer granules are made；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to
72-80 DEG C, continue stirring l.2-2.5h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in the silicon of parts by weight
Diatomaceous earth, polyethylene glycol oxide, starch graft acrylic acid potassium are warming up to 80-90 DEG C, accelerate stirring 1.2-1.8h, stop heating, continue
Stirring, is cooled to room temperature, and coating feed liquid is made；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, by coating feed liquid liter made from step S3
Then temperature is equably sprayed on compound fertilizer granules surface to 52-70 DEG C with high-pressure spray-painted rifle, then air drying to water content≤
1%, three red sweet shaddock plantation soil amendment fertilizers are made.
Below by more specific embodiment, the present invention will be described.
Embodiment 1
The red sweet shaddock plantation soil amendment fertilizer of one kind three, in units of parts by weight, including following raw material：Ammonium carbonate 52
Part, 13 parts of monoammonium phosphate, 24 parts of potassium chloride, 12 parts of peat soil, 4 parts of montmorillonite powder, 3 parts of zeolite powder, sea 7 parts of powder of bubble, calcium and magnesium phosphorus
10 parts of fertilizer, 26 parts of compound bacteria, 15 parts of diatomite, 5 parts of itaconic acid, 8 parts of polyvinyl alcohol, 3 parts of polyaminoacid potassium, polyethylene glycol oxide
3.2 parts, 3.8 parts of starch graft acrylic acid potassium；
The compound bacteria is in units of parts by weight, including following raw material：26 parts of bacillus licheniformis, nitrobacteria 20
Part, 12 parts of saccharomycete, 5 parts of photosynthetic bacteria, 8 parts of blown-ball Azotobacter, 8 parts of phosphobacteria, 3 parts of B. mucilaginocus；
The preparation process of the three red sweet shaddock plantation soil amendment fertilizers, comprises the following steps：
S1：Powder, calcium magnesium phosphate are steeped into ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea, answered
It closes bacterium ratio by weight to mix, ferments, ferment 8 days in the case where temperature is 46 DEG C, fermentate is made；
The preparation process of compound bacteria, comprises the following steps described in step S1：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus
Ratio is activated in the case where temperature is 23-26 DEG C, expands culture by weight, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, brown ball fixed nitrogen will be expanded to step a
Bacterium, phosphobacteria, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 700 parts of water are uniformly mixed, and are in temperature
After cultivating 17h at 25 DEG C, water removal is centrifuged in the case where rotating speed is 3000r/min, compound bacteria is made；The biological nutritive agent is with weight
Amount part is unit, including following raw material：54 parts of yeast extract, 42 parts of sucrose, 18 parts of peptone, 16 parts of potassium acetate, 15 parts of sodium phosphate；
The biological growth stimulant is in units of parts by weight, including following raw material：52 parts of cerium chloride, 28 parts of aluminum sulfate；
S2：Fermentate made from step S1 at 60 DEG C is concentrated, obtains concentrate, the concentrate is done at 38 DEG C
It is dry to water content be 4%, be then granulated, be made compound fertilizer granules；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to 75
DEG C, continue to stir 2h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in diatomite, the polyoxygenated of parts by weight
Ethylene, starch graft acrylic acid potassium are warming up to 86 DEG C, accelerate stirring 1.5h, stop heating, continue to stir, be cooled to room temperature, make
Obtain coating feed liquid；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, by coating feed liquid liter made from step S3
Then temperature is equably sprayed on compound fertilizer granules surface to 65 DEG C with high-pressure spray-painted rifle, then air drying to water content is
1%, three red sweet shaddock plantation soil amendment fertilizers are made.
Embodiment 2
The red sweet shaddock plantation soil amendment fertilizer of one kind three, in units of parts by weight, including following raw material：Ammonium carbonate 43
Part, 12 parts of monoammonium phosphate, 16 parts of potassium chloride, 8 parts of peat soil, 3 parts of montmorillonite powder, 2 parts of zeolite powder, sea 5 parts of powder of bubble, calcium magnesium phosphate
7 parts, 22 parts of compound bacteria, 6 parts of diatomite, 3 parts of itaconic acid, 5 parts of polyvinyl alcohol, 2 parts of polyaminoacid potassium, 3 parts of polyethylene glycol oxide, form sediment
2.2 parts of powder grafted propylene acid potassium；
The compound bacteria is in units of parts by weight, including following raw material：20 parts of bacillus licheniformis, nitrobacteria 12
Part, 10 parts of saccharomycete, 3 parts of photosynthetic bacteria, 6 parts of blown-ball Azotobacter, 4 parts of phosphobacteria, 3 parts of B. mucilaginocus；
The preparation process of the three red sweet shaddock plantation soil amendment fertilizers, comprises the following steps：
S1：Powder, calcium magnesium phosphate are steeped into ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea, answered
It closes bacterium ratio by weight to mix, ferments, ferment 10 days in the case where temperature is 35 DEG C, fermentate is made；
The preparation process of compound bacteria, comprises the following steps described in step S1：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus
Ratio is activated in the case where temperature is 23 DEG C, expands culture by weight, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, brown ball fixed nitrogen will be expanded to step a
Bacterium, phosphobacteria, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 500 parts of water are uniformly mixed, and are in temperature
After cultivating 18h at 24 DEG C, water removal is centrifuged in the case where rotating speed is 2000r/min, compound bacteria is made；The biological nutritive agent is with weight
Amount part is unit, including following raw material：50 parts of yeast extract, 30 parts of sucrose, 14 parts of peptone, 15 parts of potassium acetate, 12 parts of sodium phosphate；
The biological growth stimulant is in units of parts by weight, including following raw material：42 parts of cerium chloride, 26 parts of aluminum sulfate；
S2：Fermentate made from step S1 at 50 DEG C is concentrated, obtains concentrate, the concentrate is done at 65 DEG C
It is dry to water content be 3.6%, be then granulated, be made compound fertilizer granules；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to 72
DEG C, continue to stir 2.5h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in diatomite, the polyoxy of parts by weight
Change ethylene, starch graft acrylic acid potassium, be warming up to 80 DEG C, accelerate stirring 1.8h, stop heating, continue to stir, be cooled to room temperature,
Coating feed liquid is made；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, by coating feed liquid liter made from step S3
Then temperature is equably sprayed on compound fertilizer granules surface to 52 DEG C with high-pressure spray-painted rifle, then air drying to water content is
0.8%, three red sweet shaddock plantation soil amendment fertilizers are made.
Embodiment 3
The red sweet shaddock plantation soil amendment fertilizer of one kind three, in units of parts by weight, including following raw material：Ammonium carbonate 58
Part, 15 parts of monoammonium phosphate, 32 parts of potassium chloride, 15 parts of peat soil, 5 parts of montmorillonite powder, 4 parts of zeolite powder, sea 8 parts of powder of bubble, calcium and magnesium phosphorus
11 parts of fertilizer, 28 parts of compound bacteria, 17 parts of diatomite, 6 parts of itaconic acid, 9 parts of polyvinyl alcohol, 4 parts of polyaminoacid potassium, polyethylene glycol oxide
3.5 parts, 4.3 parts of starch graft acrylic acid potassium；
The compound bacteria is in units of parts by weight, including following raw material：32 parts of bacillus licheniformis, nitrobacteria 22
Part, 15 parts of saccharomycete, 6 parts of photosynthetic bacteria, 10 parts of blown-ball Azotobacter, 9 parts of phosphobacteria, 5 parts of B. mucilaginocus；
The preparation process of the three red sweet shaddock plantation soil amendment fertilizers, comprises the following steps：
S1：Powder, calcium magnesium phosphate are steeped into ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea, answered
It closes bacterium ratio by weight to mix, ferments, ferment 5 days in the case where temperature is 52 DEG C, fermentate is made；
The preparation process of compound bacteria, comprises the following steps described in step S1：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus
Ratio is activated in the case where temperature is 26 DEG C, expands culture by weight, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, brown ball fixed nitrogen will be expanded to step a
Bacterium, phosphobacteria, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 800 parts of water are uniformly mixed, and are in temperature
After cultivating 15h at 26 DEG C, water removal is centrifuged in the case where rotating speed is 3000r/min, compound bacteria is made；The biological nutritive agent is with weight
Amount part is unit, including following raw material：60 parts of yeast extract, 50 parts of sucrose, 22 parts of peptone, 20 parts of potassium acetate, 16 parts of sodium phosphate；
The biological growth stimulant is in units of parts by weight, including following raw material：56 parts of cerium chloride, 30 parts of aluminum sulfate；
S2：Fermentate made from step S1 at 62 DEG C is concentrated, obtains concentrate, the concentrate is done at 72 DEG C
It is dry to water content be 3%, be then granulated, be made compound fertilizer granules；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to 80
DEG C, continue stirring l.2h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in diatomite, the polyoxy of parts by weight
Change ethylene, starch graft acrylic acid potassium, be warming up to 90 DEG C, accelerate stirring 1.2h, stop heating, continue to stir, be cooled to room temperature,
Coating feed liquid is made；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, by coating feed liquid liter made from step S3
Then temperature is equably sprayed on compound fertilizer granules surface to 70 DEG C with high-pressure spray-painted rifle, then air drying to water content is
0.7%, three red sweet shaddock plantation soil amendment fertilizers are made.
Comparative example 2
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack diatomite in the raw material of material.
Comparative example 3
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack itaconic acid in the raw material of material.
Comparative example 4
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack polyvinyl alcohol in the raw material of material.
Comparative example 5
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack polyaminoacid potassium in the raw material of material.
Comparative example 6
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack polyethylene glycol oxide in the raw material of material.
Comparative example 7
It is essentially identical with the preparation process of embodiment 1, it has only the difference is that preparing three red sweet shaddock plantation soil improvements fertilizer
Lack starch graft acrylic acid potassium in the raw material of material.
Comparative example 8
Using a kind of Chinese patent application document " shaddock Orchard Soil modifying agent and preparation method thereof (application publication number：
CN106116952A) " technique of embodiment 1-3 prepares soil conditioner.
Enforcement place plants identical product in Nanning Qingxiu District cleverness town, 13 pieces of basically identical plot of planning condition
Kind and the basically identical three red sweet shaddocks of specification, respectively using the soil amendment fertilizer in embodiment 1-3 and comparative example 1-8, wherein
The soil conditioner of embodiment 1-3 in comparative example 8 is separately tested, during application, by three red sweet shaddock shaddock Orchard Soil improving fertilizers
Material is ploughed under in soil when earth's surface, site preparation according to uniformly being spread fertilizer over the fields before 50 kilograms of amount of application site preparations per acre, is sufficiently mixed with soil, three is red
After sweet shaddock maturation, per mu yield is detected, testing result is as shown in the table.
As seen from the above table：(1) by the data of embodiment 1-3 and comparative example 8 as it can be seen that using the red sweet shaddock kinds of embodiment 1-3 tri-
Plant is significantly improved with three red sweet shaddock per mu yields of soil amendment fertilizer；Simultaneously by the data of embodiment 1-3 as it can be seen that embodiment
1 is optimum embodiment..
(2) by embodiment 1 and the data of comparative example 1-7 as it can be seen that diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium,
Polyethylene glycol oxide, starch graft acrylic acid potassium are preparing three red sweet shaddock plantations with playing synergistic effect in soil amendment fertilizer,
Collaboration improves the per mu yield of three red sweet shaddocks, this may be：Using diatomite as major ingredient, using itaconic acid as crosslinking agent, gather
Vinyl alcohol is a kind of water soluble polymer, has good film forming.Polyaminoacid potassium can increase soil porosity and water holding
Amount, helps to improve soil water-reataining fertilizer-keeping ability, creates good conditions for three red sweet shaddock root growth and developments.Polyethylene glycol oxide contains
There is water-wet side, can be combined with compound fertilizer granule, polyethylene glycol oxide has good water resistance, and its strand can be in water
In stretch well, be uniformly arranged in interface, increase steric hindrance, make the sub- rapid dispersion of compound fertilizer granule in water；It forms sediment
Powder grafted propylene acid potassium when being used cooperatively with polyaminoacid potassium, can increase fertilizer absorption as the slow releasing carrier material of fertilizer
Rate.Diatomite is porous material, while substantial amounts of hydroxyl is contained on its surface, the hydroxyl on diatomite surface can be utilized, in clothing health
Under sour modifying function, even closer, and the filming function in polyvinyl alcohol and starch-grafted propylene are combined with compound fertilizer granule
Under sour potassium slow releasing function, effective sustained release to compound fertilizer granule can be realized so that compound fertilizer granule is entered in soil
After can slowly enter in soil, slowly supply fertilizer particle is carried out to soil, soil depletion and hardened is avoided, ties simultaneously
The retain water and nutrients ability of polyaminoacid potassium is closed, the efficiency and yield of three red sweet shaddock growths can be effectively improved.
Diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, starch graft acrylic acid in the present invention
Potassium as reinforcement system, embodiment 1-3 by control diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide,
The weight ratio of starch graft acrylic acid potassium is (6-18):(3-6):(5-9):(2-4):(2.6-3.5):(2-4.6) is realized and mended
The leading role raw material of reinforcement system, while the crosslinking agent of utilization itaconic acid are used as in strong system using diatomite, polyethylene glycol oxide
Performance, the filming function of polyvinyl alcohol, polyaminoacid potassium can increase soil porosity and water-holding capacity, improve soil water-reataining fertilizer-keeping
Ability and starch graft acrylic acid potassium slow releasing function so that entire reinforcement system applies to the soil improvement of the present invention
The per mu yield of three red sweet shaddocks can be effectively improved in fertilizer.
More than content is it cannot be assumed that present invention specific implementation is confined to these explanations, for the technical field of the invention
Those of ordinary skill for, under the premise of present inventive concept is not departed from, several simple deduction or replace can also be made, all should
When being considered as belonging to present invention scope of patent protection determined by the appended claims.
Claims (10)
1. the preparation process of a kind of three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that comprise the following steps：
S1：By ammonium carbonate, monoammonium phosphate, potassium chloride, peat soil, montmorillonite powder, zeolite powder, sea bubble powder, calcium magnesium phosphate, compound bacteria
Ratio mixes by weight, ferments, ferments 5-10 days in the case where temperature is 35-52 DEG C, fermentate is made；
The preparation process of the compound bacteria, comprises the following steps：
A, respectively by bacillus licheniformis, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphobacteria, B. mucilaginocus by weight
Amount part ratio is activated in the case where temperature is 23-26 DEG C, expands culture, with spare；
B, the bacillus licheniformis after culture, nitrobacteria, saccharomycete, photosynthetic bacteria, blown-ball Azotobacter, phosphorus will be expanded to step a
Bacterium, B. mucilaginocus mix and add biological growth stimulant, biological nutritive agent, 500-800 part water and be uniformly mixed, and are in temperature
After cultivating 15-18h at 24-26 DEG C, water removal is centrifuged in the case where rotating speed is 2000-3000r/min, compound bacteria is made；The life
Object nutritional agents, including following raw material：Yeast extract, sucrose, peptone, potassium acetate, sodium phosphate；The biological growth stimulant is with weight
Amount part is unit, including following raw material：Cerium chloride, aluminum sulfate；
S2：Fermentate made from step S1 at 50-62 DEG C is concentrated, obtains concentrate, by the concentrate at 65-72 DEG C
Drying is then granulated to water content≤4%, compound fertilizer granules is made；
S3：Itaconic acid, polyvinyl alcohol, polyaminoacid potassium are added in reaction kettle by weight, stirs evenly, is heated to 72-80
DEG C, continue stirring l.2-2.5h, treat that polyvinyl alcohol is completely dissolved, stop heating, continue to stir, add in parts by weight diatomite,
Polyethylene glycol oxide, starch graft acrylic acid potassium are warming up to 80-90 DEG C, accelerate stirring 1.2-1.8h, stop heating, continue to stir,
It is cooled to room temperature, coating feed liquid is made；
S4：Compound fertilizer granules made from step S2 are put into the rotary drum of rotation, coating feed liquid made from step S3 is warming up to
52-70 DEG C, compound fertilizer granules surface is equably then sprayed on high-pressure spray-painted rifle, then air drying, three red sweet shaddocks are made
Plantation soil amendment fertilizer.
2. the preparation process of according to claim 1 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that step
Diatomite described in S1, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, the weight ratio of starch graft acrylic acid potassium
For (6-18):(3-6):(5-9):(2-4):(2.6-3.5):(2-4.6).
3. the preparation process of according to claim 2 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that described
Diatomite, itaconic acid, polyvinyl alcohol, polyaminoacid potassium, polyethylene glycol oxide, the weight ratio of starch graft acrylic acid potassium are 15:5:
8:3:3.2:3.8。
4. the preparation process of according to claim 1 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that step
Compound bacteria described in S1 is in units of parts by weight, including following raw material：20-32 parts of bacillus licheniformis, nitrobacteria 12-22
Part, 10-15 parts of saccharomycete, 3-6 parts of photosynthetic bacteria, 6-10 parts of blown-ball Azotobacter, 4-9 parts of phosphobacteria, 3-5 parts of B. mucilaginocus.
5. the preparation process of according to claim 4 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that described
Compound bacteria in units of parts by weight, including following raw material：26 parts of bacillus licheniformis, 20 parts of nitrobacteria, 12 parts of saccharomycete,
5 parts of photosynthetic bacteria, 8 parts of blown-ball Azotobacter, 8 parts of phosphobacteria, 3 parts of B. mucilaginocus.
6. the preparation process of according to claim 1 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that step
Biological nutritive agent described in S1 is in units of parts by weight, including following raw material：50-60 parts of yeast extract, 30-50 parts of sucrose, albumen
14-22 parts of peptone, 15-20 parts of potassium acetate, 12-16 parts of sodium phosphate.
7. the preparation process of according to claim 6 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that described
Biological nutritive agent is in units of parts by weight, including following raw material：54 parts of yeast extract, 42 parts of sucrose, 18 parts of peptone, potassium acetate 16
Part, 15 parts of sodium phosphate.
8. the preparation process of according to claim 1 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that step
Biological growth stimulant described in S1 is in units of parts by weight, including following raw material：42-56 parts of cerium chloride, aluminum sulfate 25-30
Part.
9. the preparation process of according to claim 8 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that described
Biological growth stimulant is in units of parts by weight, including following raw material：52 parts of cerium chloride, 28 parts of aluminum sulfate.
10. the preparation process of according to claim 1 three red sweet shaddock plantation soil amendment fertilizers, which is characterized in that step
Air drying is to water content≤1% in rapid S4.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108658671A (en) * | 2018-06-28 | 2018-10-16 | 靖西市秀美边城农业科技有限公司 | A kind of preparation method being retained long-acting fructus crataegi pinnatifidae tree dedicated fertilizer |
| CN108911836A (en) * | 2018-06-28 | 2018-11-30 | 靖西市秀美边城农业科技有限公司 | A kind of preparation method of Ponkan dedicated fertilizer |
| CN108911835A (en) * | 2018-06-28 | 2018-11-30 | 靖西市秀美边城农业科技有限公司 | A method of compound fertilizer is prepared using monosodium glutamate waste liquid |
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| JPS60262886A (en) * | 1984-06-08 | 1985-12-26 | Seikaken:Kk | Soil conditioner |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108658671A (en) * | 2018-06-28 | 2018-10-16 | 靖西市秀美边城农业科技有限公司 | A kind of preparation method being retained long-acting fructus crataegi pinnatifidae tree dedicated fertilizer |
| CN108911836A (en) * | 2018-06-28 | 2018-11-30 | 靖西市秀美边城农业科技有限公司 | A kind of preparation method of Ponkan dedicated fertilizer |
| CN108911835A (en) * | 2018-06-28 | 2018-11-30 | 靖西市秀美边城农业科技有限公司 | A method of compound fertilizer is prepared using monosodium glutamate waste liquid |
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