CN108095061A - A kind of preparation method of sugar-free artificial aweto lozenge - Google Patents
A kind of preparation method of sugar-free artificial aweto lozenge Download PDFInfo
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- CN108095061A CN108095061A CN201611045695.0A CN201611045695A CN108095061A CN 108095061 A CN108095061 A CN 108095061A CN 201611045695 A CN201611045695 A CN 201611045695A CN 108095061 A CN108095061 A CN 108095061A
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- preparation
- sugar
- artificial aweto
- lozenge
- aweto
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- 239000007937 lozenge Substances 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 241001248610 Ophiocordyceps sinensis Species 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 19
- 239000011122 softwood Substances 0.000 claims abstract description 11
- 239000007788 liquid Substances 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 6
- 238000007654 immersion Methods 0.000 claims abstract description 6
- 238000012545 processing Methods 0.000 claims abstract description 6
- 239000000845 maltitol Substances 0.000 claims abstract description 5
- 235000010449 maltitol Nutrition 0.000 claims abstract description 5
- 238000005469 granulation Methods 0.000 claims abstract description 3
- 230000003179 granulation Effects 0.000 claims abstract description 3
- 230000001954 sterilising effect Effects 0.000 claims abstract description 3
- 239000000047 product Substances 0.000 claims description 11
- 239000000843 powder Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000003826 tablet Substances 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical class C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 5
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical class [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 239000002994 raw material Substances 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 235000015165 citric acid Nutrition 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000000314 lubricant Substances 0.000 claims description 3
- 235000019359 magnesium stearate Nutrition 0.000 claims description 3
- 229920001542 oligosaccharide Polymers 0.000 claims description 3
- 239000008188 pellet Substances 0.000 claims description 3
- 238000005453 pelletization Methods 0.000 claims description 3
- 238000002791 soaking Methods 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 230000008719 thickening Effects 0.000 claims description 3
- 239000000080 wetting agent Substances 0.000 claims description 3
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 abstract description 3
- 241000233866 Fungi Species 0.000 abstract description 3
- 235000003599 food sweetener Nutrition 0.000 abstract description 3
- 230000036541 health Effects 0.000 abstract description 3
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 abstract description 3
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 abstract description 3
- 229940035436 maltitol Drugs 0.000 abstract description 3
- 239000003765 sweetening agent Substances 0.000 abstract description 3
- 240000001307 Myosotis scorpioides Species 0.000 abstract description 2
- 240000006698 Spigelia anthelmia Species 0.000 abstract description 2
- 230000000675 anti-caries Effects 0.000 abstract description 2
- 210000000936 intestine Anatomy 0.000 abstract description 2
- 235000016709 nutrition Nutrition 0.000 abstract description 2
- 230000035764 nutrition Effects 0.000 abstract description 2
- 210000002784 stomach Anatomy 0.000 abstract description 2
- 238000011156 evaluation Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 235000013305 food Nutrition 0.000 description 3
- KQLDDLUWUFBQHP-UHFFFAOYSA-N Cordycepin Natural products C1=NC=2C(N)=NC=NC=2N1C1OCC(CO)C1O KQLDDLUWUFBQHP-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- OFEZSBMBBKLLBJ-BAJZRUMYSA-N cordycepin Chemical compound C1=NC=2C(N)=NC=NC=2N1[C@@H]1O[C@H](CO)C[C@H]1O OFEZSBMBBKLLBJ-BAJZRUMYSA-N 0.000 description 2
- OFEZSBMBBKLLBJ-UHFFFAOYSA-N cordycepine Natural products C1=NC=2C(N)=NC=NC=2N1C1OC(CO)CC1O OFEZSBMBBKLLBJ-UHFFFAOYSA-N 0.000 description 2
- 150000004676 glycans Chemical class 0.000 description 2
- 235000013402 health food Nutrition 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000000144 pharmacologic effect Effects 0.000 description 2
- 229920001282 polysaccharide Polymers 0.000 description 2
- 239000005017 polysaccharide Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000002929 anti-fatigue Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 230000002218 hypoglycaemic effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 150000005846 sugar alcohols Chemical class 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicinal Preparation (AREA)
Abstract
The invention belongs to Chinese caterpillar fungus health product technical fields, are related to a kind of preparation method of sugar-free artificial aweto lozenge.Sugar-free artificial aweto lozenge made from the preparation method of sugar-free artificial aweto lozenge of the present invention is through the following steps that be made：Manually extraction cordyceps sinensis liquid, the processing of dispensing, solid-liquid mix, prepare softwood, granulation and drying, sterilizing and tabletting for immersion, the preparation of artificial aweto.Preparation method of the present invention, which is used, to be had low energy, anti-caries tooth using D-sorbite, maltitol, isomalto-oligosaccharide etc., improves the sweetener of functions of intestines and stomach as carrier, add in artificial aweto extracting solution, make it is a kind of there is the new lozenge of nutrition health-care functions, it is serial worm grass product can be enriched.
Description
Technical field
The invention belongs to Chinese caterpillar fungus health product technical fields, are related to a kind of preparation method of sugar-free artificial aweto lozenge.
Background technology
Cordyceps sinensis, also known as cordyceps sinensis, are rare strong tonic Chinese herbal medicines, are a kind of to integrate edible, medicinal, health care
High-quality fungi.In recent years, the chemical composition and pharmacological activity of artificial aweto are conducted extensive research, the results showed that, manually
The chemical composition of cordyceps sinensis, pharmacological effect and natural cs are essentially identical and natural cs are the same, artificial aweto is except being rich in albumen
Matter, amino acid, vitamin and calcium, iron, manganese, zinc, outside selenium and other trace elements, it is also raw containing Cordyceps sinensis polysaccharide, cordycepin, cordycepic acid etc.
Active substances, wherein Cordyceps sinensis polysaccharide, the content of cordycepin have also been more than natural cs, have enhancing immunity of organisms, resist and swell
The different physiological roles such as knurl, radioresistance, hypoglycemic, reducing blood lipid, antifatigue, anti-aging.
The country is mainly oral liquid class product by the health food that raw material is developed of cordyceps sinensis at present, and the cordyceps sinensis of other forms eats
Product are more rare.With being continuously increased for artificial aweto yield, deep processing resource conversion approach seems very limited.
Therefore the deep processing of the present invention and artificial aweto provides a kind of new method.
The content of the invention
In view of the problems of the existing technology, it is an object of the invention to provide a kind of preparations of sugar-free artificial aweto lozenge
Method.Preparation method of the present invention, which is used, to be had low energy, anti-caries tooth with D-sorbite, maltitol, isomalto-oligosaccharide etc., changes
The sweetener of kind functions of intestines and stomach is carrier, adds in artificial aweto extracting solution, making is a kind of, and there is the new of nutrition health-care functions to contain
Piece can enrich the advantages that worm grass product is serial.
In order to solve the above technical problems, the technical solution adopted by the present invention is.
1. a kind of preparation method of sugar-free artificial aweto lozenge, step are as follows：Following raw materials by weight portion calculates.
（1）The immersion of artificial aweto
50 parts of artificial aweto coarse powder first are put into pulverizer to crush, particle is by 60 mesh sieves after crushing, by the particle of crushing
It is put into 300 parts of water, impregnates spare, obtained cordyceps sinensis mixed liquor.
（2）Prepare manually extraction cordyceps sinensis liquid
Cordyceps sinensis mixed liquor after immersion is filtered, filtrate is taken to be concentrated, treats that soluble solid content reaches 35- in feed liquid
40%, artificial aweto extracting solution is made, it is spare.
（3）The processing of dispensing
10 parts of D-sorbites, 10 parts of maltitols, 10 parts of isomalto-oligosaccharides by pulverizer are crushed, cross 100 mesh sieves；It is made
Powder blend mixture, it is spare.
（4）Solid-liquid mixes
5 parts of citric acids are dissolved in cordyceps sinensis extracting solution.By step（3）In obtained powder blend mixture input mixer
It is mixed, solidliquid mixture is made.
（5）Prepare softwood
To solidliquid mixture, 50% ethyl alcohol is slowly added to as wetting agent, humidity of materials is adjusted, softwood is made, terminal is done for softwood
Humidity is with agglomerating but tack-free with hand-tight energy of holding, until being split with the light pressure energy of finger.
（6）Granulation and drying
The softwood made is put into oscillating granulator and is granulated, with 20 mesh screen crushing and pelletizings.Wet granular is placed in 60
It is dry in DEG C air dry oven, it is stirred once every 30min, to accelerate rate of drying, dry terminal is down to 1- with pellet moisture
Until 3%.
（7）Sterilizing and tabletting, finished product
Its 5 parts of magnesium stearates are added in dry particle as lubricant, is uniformly mixed, is sent into tabletting in tablet press machine, will press
Tablet put irradiation under ultraviolet light and sterilize, packed after the completion of irradiation to get to finished product.
The step（2）Filtering times be 4-6 times.
The step（2）Thickening temperature for 50-60 DEG C, concentration pressure is 12-15KPa.
The step（2）Extracting temperature for 70-75 DEG C, extraction time is 3-5 times, soaking time 2-3h.
The step（7）Ultraviolet irradiation time be 30-40min.
Beneficial effects of the present invention：
Sugar-free artificial aweto lozenge remains worm using the sugar alcohol with healthcare function and oligosaccharide as sweetener and carrier
The active ingredient of grass, meeting food in the world, to low sugar, trend low in calories, health food development, there is good market to open
Hair prospect.
Specific embodiment
For a further understanding of the present invention, the preferred embodiment of the invention is described with reference to embodiment, still
It should be appreciated that these descriptions are simply for the feature and advantage that further illustrate the present invention rather than to the claims in the present invention
Limitation.
Embodiment 1
Artificial aweto coarse powder first is put into pulverizer to crush, the particle of crushing is put by particle by 60 mesh sieves after crushing
In water, spare, obtained cordyceps sinensis mixed liquor is impregnated；Cordyceps sinensis mixed liquor after immersion is filtered, filtering times are 4-6 times, take filtrate
It is concentrated, thickening temperature is 50-60 DEG C, and concentration pressure is 12-15KPa, treats that soluble solid content reaches 35- in feed liquid
40%, artificial aweto extracting solution is made, Extracting temperature is 70-75 DEG C, and extraction time is 3-5 times, soaking time 2-3h,
It is spare；D-sorbite, maltitol, isomalto-oligosaccharide by pulverizer are crushed, cross 100 mesh sieves；It is mixed that powder mixing is made
Object is closed, it is spare；Citric acid is dissolved in cordyceps sinensis extracting solution.It will be carried out in obtained powder blend mixture input mixer
Solidliquid mixture is made in mixing；To solidliquid mixture, 50% ethyl alcohol is slowly added to as wetting agent, humidity of materials is adjusted, is made
Softwood, terminal for softwood humidity with it is hand-tight hold can it is agglomerating but tack-free, until being split with the light pressure energy of finger；It is soft by what is made
It is granulated in material input oscillating granulator, with 20 mesh screen crushing and pelletizings.Wet granular is placed in 60 DEG C of air dry ovens
It is dry, it is stirred once every 30min, to accelerate rate of drying, dry terminal is until pellet moisture is down to 1-3%；At dry
Magnesium stearate is added in grain as lubricant, is uniformly mixed, is sent into tabletting in tablet press machine, the tablet pressed is put under ultraviolet light
Irradiation sterilizes, ultraviolet irradiation time 30-40min, is packed after the completion of irradiation to get to finished product.
Appraisal result is listed in table 3.
Embodiment 2
The method that embodiment 1 is repeated by each component content specified in following table 1, appraisal result is listed in table 3.
Embodiment 3
The method that embodiment 1 is repeated by each component content specified in following table 1, appraisal result is listed in table 3.
The raw material proportioning table of 1 embodiment 1-3 of table
Performance test
It judges personnel and evaluation group is formed by 15 people of professional for being engaged in food processing, it is desirable that do not inhaled before evaluating member evaluation
The irritable foods such as pungent are not eaten in cigarette, no drinking, mainly for the flavor of lozenge, mouthfeel and structural state these three aspect into
Row evaluation, after having evaluated a product, is gargled with clear water, and interval 5min is evaluating next product, finally fills in grade form simultaneously
Signature, the evaluation result of each evaluating member is collected, carries out analysis scoring, standard refers to table 2.
2 standards of grading of table
3 embodiment 1-3 of table feels tasting testing evaluation result
No matter sugar-free artificial aweto lozenge of the present invention as shown in Table 3 can expire in feature taste, mouthfeel, structural state or color and luster
The requirement of sufficient jury is a kind of lozenge to look good, smell good and taste good.
It is understood that above with respect to the specific descriptions of the present invention, it is merely to illustrate the present invention and is not limited to this
The described technical solution of inventive embodiments, it will be understood by those of ordinary skill in the art that, still the present invention can be carried out
Modification or equivalent substitution, to reach identical technique effect；As long as meeting using needs, all protection scope of the present invention it
It is interior.
Claims (5)
1. a kind of preparation method of sugar-free artificial aweto lozenge, it is characterised in that：Step is as follows：Following raw materials by weight portion meter
It calculates,
（1）The immersion of artificial aweto
50 parts of artificial aweto coarse powder first are put into pulverizer to crush, particle is by 60 mesh sieves after crushing, by the particle of crushing
It is put into 300 parts of water, impregnates spare, obtained cordyceps sinensis mixed liquor；
（2）Prepare manually extraction cordyceps sinensis liquid
Cordyceps sinensis mixed liquor after immersion is filtered, filtrate is taken to be concentrated, treats that soluble solid content reaches 35- in feed liquid
40%, artificial aweto extracting solution is made, it is spare；
（3）The processing of dispensing
10 parts of D-sorbites, 10 parts of maltitols, 10 parts of isomalto-oligosaccharides by pulverizer are crushed, cross 100 mesh sieves；It is made
Powder blend mixture, it is spare；
（4）Solid-liquid mixes
5 parts of citric acids are dissolved in cordyceps sinensis extracting solution；
By step（3）It is mixed in obtained powder blend mixture input mixer, solidliquid mixture is made；
（5）Prepare softwood
To solidliquid mixture, 50% ethyl alcohol is slowly added to as wetting agent, humidity of materials is adjusted, softwood is made, terminal is done for softwood
Humidity is with agglomerating but tack-free with hand-tight energy of holding, until being split with the light pressure energy of finger；
（6）Granulation and drying
The softwood made is put into oscillating granulator and is granulated, with 20 mesh screen crushing and pelletizings；
Wet granular is placed in drying in 60 DEG C of air dry ovens, is stirred once every 30min, it is dry whole to accelerate rate of drying
Point is until pellet moisture is down to 1-3%；
（7）Sterilizing and tabletting, finished product
5 parts of magnesium stearates are added in dry particle as lubricant, is uniformly mixed, tabletting in tablet press machine is sent into, by what is pressed
Tablet puts irradiation under ultraviolet light and sterilizes, and is packed after the completion of irradiation to get to finished product.
2. a kind of preparation method of sugar-free artificial aweto lozenge according to claim 1, it is characterised in that：The step
（2）Filtering times be 4-6 times.
3. a kind of preparation method of sugar-free artificial aweto lozenge according to claim 1, it is characterised in that：The step
（2）Thickening temperature for 50-60 DEG C, concentration pressure is 12-15KPa.
4. a kind of preparation method of sugar-free artificial aweto lozenge according to claim 1, it is characterised in that：The step
（2）Extracting temperature for 70-75 DEG C, extraction time is 3-5 times, soaking time 2-3h.
5. a kind of preparation method of sugar-free artificial aweto lozenge according to claim 1, it is characterised in that：The step
（7）Ultraviolet irradiation time be 30-40min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611045695.0A CN108095061A (en) | 2016-11-24 | 2016-11-24 | A kind of preparation method of sugar-free artificial aweto lozenge |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611045695.0A CN108095061A (en) | 2016-11-24 | 2016-11-24 | A kind of preparation method of sugar-free artificial aweto lozenge |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108095061A true CN108095061A (en) | 2018-06-01 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611045695.0A Pending CN108095061A (en) | 2016-11-24 | 2016-11-24 | A kind of preparation method of sugar-free artificial aweto lozenge |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109601676A (en) * | 2018-11-01 | 2019-04-12 | 防城港圣保堂制药有限公司 | A kind of ion Victoria C Chinese caterpillar fungus hypha pressed candy and preparation method thereof |
-
2016
- 2016-11-24 CN CN201611045695.0A patent/CN108095061A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109601676A (en) * | 2018-11-01 | 2019-04-12 | 防城港圣保堂制药有限公司 | A kind of ion Victoria C Chinese caterpillar fungus hypha pressed candy and preparation method thereof |
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Application publication date: 20180601 |
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| WD01 | Invention patent application deemed withdrawn after publication |