CN108078840A - One kind is refreshed oneself wet tissue liquid - Google Patents
One kind is refreshed oneself wet tissue liquid Download PDFInfo
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- CN108078840A CN108078840A CN201711409202.1A CN201711409202A CN108078840A CN 108078840 A CN108078840 A CN 108078840A CN 201711409202 A CN201711409202 A CN 201711409202A CN 108078840 A CN108078840 A CN 108078840A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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Abstract
The present invention provides one kind and refreshes oneself wet tissue liquid.Distinguish 40 60 parts of following 7 10 parts of 10 20 parts of menthyl lactate, 13 parts of mint extract and rosemary hydrosol, 58 parts of borneol, 10 15 parts of thyme extract, 10 15 parts of wormwood extract, 25 parts of antioxidant, 5 10 parts of solubilizer and deionized water including mass fraction.In the present invention using menthyl lactate, mint extract, rosemary hydrosol, borneol, thyme extract, wormwood extract, apply play the role of in disposable sanitary articles field it is refrigerant, refresh the mind；Menthyl lactate persistence, have it is slight it is mint flavored, peppermint cooling effect is strong and very brief, the mild cooling effect of rosemary hydrosol, fragrance has accomplished the unification of strong cooling effect and lasting cooling effect in short-term.
Description
Technical field
Refresh oneself wet tissue liquid and preparation method the invention belongs to functional agent field more particularly to one kind.
Background technology
Freshener species is rare at present or cooling effect is poor or refrigerant continuation is poor so that using effect is poor, nothing
Method reaches the unification of cooling effect and lasting cooling effect, it is impossible to reach user demand.
The content of the invention
The wet tissue liquid in view of the above-mentioned problems, the present invention refreshes oneself.
In order to achieve the above objectives, one kind of the present invention is refreshed oneself wet tissue liquid, and following lactic acid peppermint is distinguished including mass fraction
7-10 parts of 10-20 parts of ester, 1-3 parts of mint extract and rosemary hydrosol, 5-8 parts of borneol, 10-15 parts of thyme extract, Chinese mugwort
40-60 parts of careless extract 10-15 parts, 2-5 parts of antioxidant, 5-10 parts of solubilizer and deionized water；
Mass fraction distinguish following 1-5 parts of polyalcohol, 1-5 parts of Phenoxyethanol, 1-5 parts of Sensiva SC50, to hydroxyl
1-5 parts of acetophenone and inorganic anti-interference agent.
Further, the preparation method of the wet tissue liquid of refreshing oneself is as follows：
(1) remove 40-60 parts of ionized water to add in HV XLPE power cables, take inorganic anti-interference agent 1-3 parts and solubilizer 5-10
Part add in, adjustment temperature to 40-60 DEG C, enclosed with 100-150/stirring of the speed low speed of minute under, with 1 part/minute
Speed adds 1-3 parts of mint extract, then adds 10-20 parts of menthyl lactate with the speed of 3 parts/minute, then with 2 parts/point
Speed 5-8 parts of the borneol of addition of clock, it is 0.5-2MPa finally to adjust operating pressure, is kept stirring 5-15 minutes, and it is mixed to be made first
Close object；
(2) into 1-5 parts of polyalcohol, 1-5 parts of Phenoxyethanol, Sensiva SC50 are sequentially added with the speed of 5 parts/minute
2-5 parts of 1-5 parts, 1-5 parts of parahydroxyacet-ophenone and antioxidant, and be kept stirring 10-15 minutes, the second mixture is made；
(3) extracted with 7-10 parts of the rosemary hydrosol of speed addition of 5 parts/minute, 10-15 parts of thyme extract, wormwood
10-15 parts of object；It is kept stirring 10-15 minutes, the 3rd mixture is made；
(4) the first mixture is added slowly to the speed of 1-2 parts/minute in the 3rd mixture, and is kept stirring 10-
15 minutes, the second mixture is finally added with the speed of 2-3 parts/minute, continues stirring 20-30 minutes, wet tissue medicine of refreshing oneself is made
Liquid.
Further, the preparation method of wherein rosemary hydrosol is as follows：
(1) it is 5-8% that fresh rosemary leave, flower, stem is taken, which to be freeze-dried to water content,；
(2) rosemary obtained in step (1) is crushed into powder；
(3) 7-10 parts of rosemary is taken, 40-50 parts of deionized water is added in and stirs evenly, be warming up to 90-100 DEG C, be kept stirring
110-220 minutes；Distillate is collected in distillation；
(4) distillate being collected into is subjected to grease layering, collects water layer, that is, rosemary primary hydrosol；
(5) by rosemary primary hydrosol ageing 48-72 it is small when after, with the strainer or filter-cloth filtering of >=200 mesh, gained filtrate
As rosemary hydrosol.
Further, the preparation method of Peppermint essential oil is as follows：
(1) distilled by the way of distillation using dried peppermint leaf, prepare crude essential oil respectively：
(2) crude essential oil is subjected to carbon dioxide supercritical extraction respectively, obtains two level essential oil, wherein carbon dioxide, which surpasses, faces
Boundary extraction operation be：Crude essential oil is fitted into extractor, is heated to 40-50 DEG C, extracting pressure 20-25MPa, extract stream
Speed is 35-50L/h, continuous extraction 2-3h, in the mixture input separator of carbon dioxide and the essential oil extracted, reduces to normal pressure
And room temperature is down to, carbon dioxide therein is separated with essential oil, obtains two level essential oil；
(3) two level essential oil being fractionated respectively again, peppermint two level essential oil collects 220~240 DEG C of fraction in fractionation,
Obtain Peppermint essential oil.
Further, the preparation method of wherein menthyl lactate is as follows：
One) menthol preparation method：
(1) geraniol and/or nerol hydrogenation for optically-active citronellol and are converted into optically-active citronellal, citronellal is cyclized
For optically-active isopulegol and to be hydrogenated be optically-active menthol；
(2) the optically-active menthol obtained in step (1) is dissolved in nitrile series solvent, cools down the solution and obtain crystallization peppermint
Alcohol；
Two) preparation method of menthyl lactate：
Excessive lactic acid and step 1 are added in into reactor) in crystallization menthol obtained, add toluene and sulfuric acid,
Be heated to reflux being reacted, be poured into acid salt saturated solution or buffer solution and hydrolyze after reaction, it is filtered, point
Liquid, drying, vacuum distillation obtain menthyl lactate.
Further, the preparation method of wherein thyme extract or wormwood extract is as follows：
(1) 20-25 parts of 20-25 parts of thyme or wormwood is taken to be crushed into powder addition mixer, the speed of 50-70 circles/minute
Under the stirring of low speed, do not had raw material powder as 75% medicinal alcohol using the speed addition mass concentration of 500 ml/mins,
After addition by mixing speed be adjusted to 10-25 circles/minute be kept stirring 12-24 it is small when；After stirring, filter to get filtrate and filter residue,
Waste；
(2) obtained filtered fluid is fermented, adds the medicinal alcohol that mass concentration is 90% and mend to 1000 milliliters,
After mixing up to mixed extract.
Further, the antioxidant is propylgallate, butylated hydroxy anisole, tocopherol, tertiary butyl are to benzene
One or more of diphenol and 2,6- di-tert-butyl-4-methy phenol；
The solubilizer includes one in rilanit special polyoxyethylene, cetearyl alcohol alcohol ether, aliphatic ester and propylene glycol
Kind is several.
Further, inorganic anti-interference agent 1-3 parts are further included, the inorganic anti-interference agent is EDETATE SODIUM, phosphoric acid hydrogen two
Potassium, potassium dihydrogen phosphate, citric acid or sodium citrate.
In order to achieve the above objectives, the present invention is a kind of refreshes oneself wet tissue liquid in the cloth for cleaning such as wet paper immersion or wet tissue finished product
Using.
Using menthyl lactate, mint extract, rosemary hydrosol in the present invention, apply and inhibiting disposable sanitary articles
Play the role of in field it is refrigerant, refresh the mind.
Menthyl lactate persistence, have it is slight it is mint flavored, peppermint cooling effect is strong and very brief, rosemary hydrosol temperature
And cooling effect, fragrance, accomplish the unification of strong cooling effect and lasting cooling effect in short-term, borneol, thyme extraction
Object or wormwood extract have the effect of reminding restoring consciouness, and are pure plant extracts, use without security risk.
Specific embodiment
The implementation of specific embodiments of the present invention is further described below.
Embodiment 1
One kind is refreshed oneself wet tissue liquid, distinguishes the following raw material including mass fraction：
19 parts of menthyl lactate, 1.5 parts of Peppermint essential oil, 9 parts of rosemary hydrosol, 7 parts of borneol, 13 parts of thyme extract,
55 parts of 12 parts of wormwood extract, 3 parts of antioxidant, 7 parts of solubilizer and deionized water.
Mass fraction distinguishes following raw material：3 parts of polyalcohol, 3 parts of Phenoxyethanol, 3 parts of Sensiva SC50, para hydroxybenzene
2 parts of 3 parts of ethyl ketone and inorganic anti-interference agent.
Using menthyl lactate, mint extract, rosemary hydrosol in the present embodiment, apply and led in disposable sanitary articles
Play the role of in domain it is refrigerant, refresh the mind.
Menthyl lactate persistence, have it is slight it is mint flavored, peppermint cooling effect is strong and very brief, rosemary hydrosol temperature
And cooling effect, fragrance, accomplish the unification of strong cooling effect and lasting cooling effect in short-term, borneol, thyme extraction
Object or wormwood extract have the effect of reminding restoring consciouness, and are pure plant extracts, use without security risk,
It also can relieving insomnia, palpitaition, headache.There is stronger astriction, nurse one's health greasy skin, promote blood circulation.
Preferably, the antioxidant is propylgallate, butylated hydroxy anisole, tocopherol, tertiary butyl are to benzene two
One or more of phenol and 2,6- di-tert-butyl-4-methy phenol；
Solubilizer include rilanit special polyoxyethylene, cetearyl alcohol alcohol ether, aliphatic ester and one kind in propylene glycol or
It is several.
Preferably, the inorganic anti-interference agent is EDETATE SODIUM, dipotassium hydrogen phosphate, potassium dihydrogen phosphate, citric acid or lemon
Sour sodium.
Peppermint, menthyl lactate, borneol, compared with indissoluble solution, add in solubilizer and reach excellent solute effect in aqueous systems.
Embodiment 1 is complete.
Embodiment 2
On the basis of embodiment 1,
The preparation method of the wet tissue liquid of refreshing oneself is as follows：
(1) remove 40-60 parts of ionized water to add in HV XLPE power cables, inorganic 2 parts of anti-interference agent is taken to add for 7 parts with solubilizer
Enter, adjustment temperature is to 50 DEG C, under the stirring of the speed low speed of 120 circles/minute, peppermint is added with the speed of 1 part/minute
Then 2 parts of extract adds 15 parts of menthyl lactate with the speed of 3 parts/minute, then adds borneol 6 with the speed of 2 parts/minute
Part, it is 0.8MPa finally to adjust operating pressure, is kept stirring 1215 minutes, and the first mixture is made；
(2) into 4 parts of polyalcohol, with the speed of 5 parts/minute sequentially add 4 parts of Phenoxyethanol, 4 parts of Sensiva SC50,
4 parts of 3 parts of parahydroxyacet-ophenone and antioxidant, and be kept stirring 12 minutes, the second mixture is made；
(3) with 9 parts of the speed addition rosemary hydrosol of 5 parts/minute, 12 parts of thyme extract, 12 parts of wormwood extract；
It is kept stirring 12 minutes, the 3rd mixture is made；
(4) the first mixture is added slowly to the speed of 1- parts/minute in the 3rd mixture, and is kept stirring 10 points
Clock finally adds the second mixture with the speed of 2- parts/minute, continues stirring 30 minutes, and wet tissue liquid of refreshing oneself is made.
Embodiment 2 is complete.
Conventional method preparation may be employed in above-mentioned rosemary hydrosol, and preferable preparation method is as follows：
(1) fresh rosemary leave, flower, stem is taken to be freeze-dried to water content to be broken into powder after 5-8%；
(3) 8 parts of rosemary is taken, 45 parts of deionized water is added in and stirs evenly, be warming up to 95 DEG C, be kept stirring 120 minutes；It steams
It evaporates, collects distillate；
(4) distillate being collected into is subjected to grease layering, collects water layer, that is, rosemary primary hydrosol；
(5) by rosemary primary hydrosol ageing 48 it is small when after, with the strainer or filter-cloth filtering of >=200 mesh, gained filtrate is
For rosemary hydrosol.
Conventional method preparation may be employed in above-mentioned Peppermint essential oil, and preferable preparation method is as follows：
(1) distilled by the way of distillation using dried peppermint leaf, prepare crude essential oil respectively：
(2) crude essential oil is subjected to carbon dioxide supercritical extraction respectively, obtains two level essential oil, wherein carbon dioxide, which surpasses, faces
Boundary extraction operation be：Crude essential oil is fitted into extractor, is heated to 40-50 DEG C, extracting pressure 20-25MPa, extract stream
Speed is 35-50L/h, continuous extraction 2-3h, in the mixture input separator of carbon dioxide and the essential oil extracted, reduces to normal pressure
And room temperature is down to, carbon dioxide therein is separated with essential oil, obtains two level essential oil；
(3) two level essential oil being fractionated respectively again, peppermint two level essential oil collects 220~240 DEG C of fraction in fractionation,
Obtain Peppermint essential oil.
Conventional method preparation may be employed in above-mentioned thyme extract or wormwood extract, and preferable preparation method is such as
Under：
(1) take that thyme carries 20-25 parts or 20-25 parts of wormwood is crushed into powder addition mixer, the speed of 50-70 circles/minute
It spends under the stirring of low speed, did not had raw material as 75% medicinal alcohol using the speed addition mass concentration of 500 ml/mins
Powder, after addition by mixing speed be adjusted to 10-25 circles/minute be kept stirring 12-24 it is small when；After stirring, filter to get filtrate and filter
Slag, waste；
(2) obtained filtered fluid is fermented, adds the medicinal alcohol that mass concentration is 90% and mend to 1000 milliliters,
After mixing up to mixed extract.
Embodiment 3
On the basis of embodiment 1 or embodiment 2, one kind refreshes oneself wet tissue liquid in the wipings such as wet paper immersion or wet tissue finished product
Application in towel.
It is a kind of hydro-entangled non-woven fabric that wherein wet tissue, which uses, including basal layer, water accepting layer and functional layer, the basis
Layer, water accepting layer and functional layer from top to bottom set gradually and are reinforced by spun lacing and connected；
The basal layer includes the first plant fiber 61-71 mass parts and fine-denier synthetic fibers 29-39 mass parts；The suction
Water layer is the second plant fiber layer；The functional layer includes the 3rd plant fiber 65-75 mass parts and fine-denier synthetic fibers 25-35
Mass parts；
The basal layer square grammes per square metre accounts for the 35% of total square of grammes per square metre；The water accepting layer square grammes per square metre accounts for total square of grammes per square metre
40%；Functional layer square grammes per square metre accounts for the 25% of total square of grammes per square metre；So that water absorption, intensity and functionality reach most desired effect.
First plant fiber include mass fraction be respectively 90 parts bamboo pulp and 16 parts of tea tree wood pulps；Basal layer uses
A large amount of bamboo fibres, length of bamboo fibre is longer, improves the strength of basal layer.
Second plant fiber include mass fraction be respectively 35 parts bamboo pulp and 50 parts of tea tree wood pulps；
3rd plant fiber include mass fraction be respectively 62 parts bamboo pulp, 27 parts of tea tree wood pulps, 12 parts of frutus cnidiis
Straw pulp and 11 parts of Cortex Phellodendri slurries；Frutus cnidii straw pulp and Cortex Phellodendri slurry have preferable bactericidal anti-inflammatory effect, make hydro-entangled non-woven fabric will not
Bacterium is grown, use is more comfortable.So that the good antimicrobial effect of the hydro-entangled non-woven fabric, and can be with long-effective corrosion, in wet tissue
Preservative need not be additionally added in liquid formula, can realize the diversity of wet tissue liquid formula.The hydro-entangled non-woven fabric should
Not only having good fungistatic effect for wet tissue and not having has injury to human body and skin, production after product use,
It can inhibit growth of the mushroom microorganism in wet tissue during storage and sale, ensure product quality.And it can play
Some are to human body beneficial effect.
Length of bamboo fibre in the bamboo pulp is more than 10mm.
The fine-denier synthetic fibers are high curling fine-denier Biodegradable fibers.Using high crispation number fiber, increase and tangle
Cohesive force between degree and fiber, to improve intensity.Make hydro-entangled non-woven fabric that can break up using Biodegradable fibers, and can
Biodegradation, the environment protecting being optimal.
The high curling fine-denier Biodegradable fibers are by the PBAT with degradation property and/or with degradation property
PBS is made by melt spinning method；
Monofilament linear density is 0.5~2dtex, and crispation number is 18~28/25mm, and crimp index is 0.55 ± 0.10.
The breaking up property of non-woven cloth can be improved by only adding a small amount of fine-denier synthetic fibers, but frequently can lead to its intensity
Not enough, and using height curling fine count fiber to improve interfibrous mutual entanglement, the intensity of non-woven cloth is improved, so as to reality
The unification of the intensity and breaking up property of existing non-woven cloth.It can be taken into account using the PBAT with biodegradability and/or PBS non-
Woven cloths break up and biodegradable.
The manufacturing method of the hydro-entangled non-woven fabric is as follows：
Basal layer, water accepting layer and functional layer are from top to bottom laid with successively, are mutually tangled by spun lacing, it is non-to obtain spun lacing
Woven cloths；
It is 50%-70% that hydro-entangled non-woven fabric is gone moisture removal to humidity with suction flat box；
Hydro-entangled non-woven fabric after dehydration carries out spraying a kind of modified carboxy methyl cellulose sodium, modified carboxy methyl fiber
The concentration of plain sodium is 1-5%；；
Hydro-entangled non-woven fabric after spray treatment is dried, obtains composite water-spurt non-woven cloth.
Hydro-entangled non-woven fabric after dehydration carries out spraying a kind of modified carboxy methyl cellulose sodium, modified carboxy methyl fiber
The concentration of plain sodium is 1-5%, and modified carboxy methyl cellulose sodium, as a kind of binding agent, improves hydro-entangled non-woven fabric in wet tissue
Intensity, but modified carboxy methyl cellulose sodium hydrolyzes under a large amount of water existence conditions, cementation, which disappears, to be beneficial to break up.
The manufacturing method of wherein basal layer is as follows：
(1) under the stirring for taking the speed low speed of 10-20 parts of tea tree wood pulp 50-70 circles/minutes, with 20 parts/minute
Speed adds 80-100 parts of bamboo pulp, is kept stirring 5-9 minutes and mixed slurry is made；
(2) mixed slurry and 42-66 parts of fine-denier synthetic fibers are added in into random web-laying equipment, is spread using air laid processes
Web is made in net.
Gene basis layer needs preferable strength, therefore selects relatively low mixing speed and shorter mixing time, prevents bamboo
Fibre length is destroyed.
The manufacturing method of wherein functional layer is as follows：
(1) under the stirring for taking the speed low speed of 20-30 parts of tea tree wood pulp 70-100 circles/minutes, with 30 parts/minute
Speed adds 8-15 parts of frutus cnidii straw pulps and 8-15 parts of Cortex Phellodendri slurries, is kept stirring 10-20 minutes；
(2) again under the stirring of the speed low speed of 70-100 circles/minute, 50-70 is added with the speed of 30 parts/minute
The bamboo pulp of part, is kept stirring 40-60 minutes；
(3) mixed slurry and 33-60 parts of fine-denier synthetic fibers are added in into random web-laying equipment, is spread using air laid processes
Web is made in net.
The manufacturing method of wherein water accepting layer is as follows：
(1) under the stirring for taking the speed low speed of 20-30 parts of tea tree wood pulp 70-100 circles/minutes, with 30 parts/minute
Speed adds 8-15 parts of frutus cnidii straw pulps and 8-15 parts of Cortex Phellodendri slurries, is kept stirring 10-20 minutes；
(2) again under the stirring of the speed low speed of 70-100 circles/minute, 50-70 is added with the speed of 30 parts/minute
The bamboo pulp of part, is kept stirring 40-60 minutes；
(3) mixed slurry is warming up to 90-105 DEG C with 10-15 DEG C/min of speed, is added with the speed of 3 parts/minute
Mass fraction is 3-5 parts of wet strength agent, is stirred；
(4) web is made using wet-laid method lapping in mixed slurry.
More than, it is only presently preferred embodiments of the present invention, but protection scope of the present invention is not limited thereto, and it is any to be familiar with sheet
In the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in should all be covered those skilled in the art
Within protection scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection domain that claim is defined.
Claims (8)
- The wet tissue liquid 1. one kind is refreshed oneself, which is characterized in that following raw material is distinguished including mass fraction：7-10 parts of 10-20 parts of menthyl lactate, 1-3 parts of mint extract and rosemary hydrosol, 5-8 parts of borneol, thyme extraction 40-60 parts of 10-15 parts of object, 10-15 parts of wormwood extract, 2-5 parts of antioxidant, 5-10 parts of solubilizer and deionized water；1-5 parts of polyalcohol, 1-5 parts of Phenoxyethanol, 1-5 parts of Sensiva SC50,1-5 parts of parahydroxyacet-ophenone and inorganic anti-dry Disturb 1-3 parts of agent.
- The wet tissue liquid 2. one kind according to claim 1 is refreshed oneself, which is characterized in that the preparation side of the wet tissue liquid of refreshing oneself Method is as follows：(1) remove 40-60 parts of ionized water to add in HV XLPE power cables, take inorganic anti-interference agent 1-3 part and 5-10 parts of solubilizer adds Enter, adjustment temperature to 40-60 DEG C, enclosed with 100-150/stirring of the speed low speed of minute under, with the speed of 1 part/minute 1-3 parts of mint extract is added, 10-20 parts of menthyl lactate is then added with the speed of 3 parts/minute, then with 2 parts/minute Speed adds 5-8 parts of borneol, and it is 0.5-2MPa finally to adjust operating pressure, is kept stirring 5-15 minutes, and the first mixture is made；(2) into 1-5 parts of polyalcohol, 1-5 parts of Phenoxyethanol, Sensiva SC50 1-5 are sequentially added with the speed of 5 parts/minute 2-5 parts of part, 1-5 parts of parahydroxyacet-ophenone and antioxidant, and be kept stirring 10-15 minutes, the second mixture is made；(3) with 7-10 parts of rosemary hydrosol of speed addition, 10-15 parts of thyme extract, the wormwood extract 10- of 5 parts/minute 15 parts；It is kept stirring 10-15 minutes, the 3rd mixture is made；(4) the first mixture is added slowly to the speed of 1-2 parts/minute in the 3rd mixture, and is kept stirring 10-15 points Clock finally adds the second mixture with the speed of 2-3 parts/minute, continues stirring 20-30 minutes, and wet tissue liquid of refreshing oneself is made.
- The wet tissue liquid 3. one kind according to claim 1 is refreshed oneself, which is characterized in that the wherein preparation method of rosemary hydrosol It is as follows：(1) fresh rosemary leave, flower, stem is taken to be freeze-dried to water content to be broken into powder after 5-8%；(3) 7-10 parts of above-mentioned rosemary powder is taken, 40-50 parts of deionized water is added in and stirs evenly；90-100 DEG C is warming up to again, is protected Hold stirring 110-220 minutes；Distillate is collected in distillation；(4) distillate being collected into is subjected to grease layering, collects water layer, that is, rosemary primary hydrosol；(5) by rosemary primary hydrosol ageing 48-72 it is small when after, with the strainer or filter-cloth filtering of >=200 mesh, gained filtrate is Rosemary hydrosol.
- The wet tissue liquid 4. one kind according to claim 1 is refreshed oneself, which is characterized in that the preparation method of Peppermint essential oil is as follows：(1) distilled by the way of distillation using dried peppermint leaf, prepare crude essential oil：(2) crude essential oil is subjected to carbon dioxide supercritical extraction respectively, obtains two level essential oil；Wherein CO 2 supercritical extracts The operation taken is：Crude essential oil is fitted into extractor, is heated to 40-50 DEG C, extracting pressure 20-25MPa, extraction flow velocity is In the mixture input separator of 35-50L/h, continuous extraction 2-3h, carbon dioxide and the essential oil extracted, reduce to normal pressure and drop To room temperature, carbon dioxide therein is separated with essential oil, obtains two level essential oil；(3) two level essential oil is fractionated respectively again, peppermint two level essential oil collects 220~240 DEG C of fraction in fractionation, obtains Peppermint essential oil.
- The wet tissue liquid 5. one kind according to claim 1 is refreshed oneself, which is characterized in that wherein thyme extract or wormwood carries The preparation method for taking object is as follows：(1) 20-25 parts of 20-25 parts of thyme or wormwood is taken to be crushed into powder addition mixer, the speed low speed of 50-70 circles/minute Stirring under, do not had raw material powder as 75% medicinal alcohol using the speed of 500 ml/mins addition mass concentration, addition Afterwards by mixing speed be adjusted to 10-25 circles/minute be kept stirring 12-24 it is small when；After stirring, filter to get filtrate and filter residue, waste；(2) obtained filtered fluid is fermented, adds the medicinal alcohol that mass concentration is 90% and mend to 1000 milliliters, mix Up to mixed extract after uniformly.
- The wet tissue liquid 6. one kind according to claim 1 is refreshed oneself, which is characterized in that the antioxidant is gallic acid third Ester, butylated hydroxy anisole, tocopherol, tert-butylhydroquinone and one kind or several in 2,6- di-tert-butyl-4-methy phenol Kind；The solubilizer include rilanit special polyoxyethylene, cetearyl alcohol alcohol ether, aliphatic ester and one kind in propylene glycol or It is several.
- The wet tissue liquid 7. one kind according to claim 1 is refreshed oneself, which is characterized in that inorganic anti-interference agent 1-3 parts are further included, The inorganic anti-interference agent is EDETATE SODIUM, dipotassium hydrogen phosphate, potassium dihydrogen phosphate, citric acid or sodium citrate.
- The wet tissue 8. one kind is refreshed oneself, using the wet tissue medicine of refreshing oneself having described in above-mentioned 1-7 any claims in the wet tissue Liquid.
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| CN201711409202.1A CN108078840B (en) | 2017-12-22 | 2017-12-22 | Wet tissue capable of dispersing and refreshing |
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| CN112641650A (en) * | 2020-12-29 | 2021-04-13 | 福建恒安集团有限公司 | Skin feeling regulator and wet tissue |
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| CN108078840B (en) | 2021-10-15 |
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