CN108048879A - A kind of electrolytic preparation device for the metal powder for being capable of separation of solid and liquid - Google Patents
A kind of electrolytic preparation device for the metal powder for being capable of separation of solid and liquid Download PDFInfo
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- CN108048879A CN108048879A CN201711335103.3A CN201711335103A CN108048879A CN 108048879 A CN108048879 A CN 108048879A CN 201711335103 A CN201711335103 A CN 201711335103A CN 108048879 A CN108048879 A CN 108048879A
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- scraper
- block
- electrolyte tank
- material leakage
- metal powder
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- 239000002184 metal Substances 0.000 title claims abstract description 48
- 239000000843 powder Substances 0.000 title claims abstract description 47
- 239000007788 liquid Substances 0.000 title claims abstract description 25
- 238000000926 separation method Methods 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000007787 solid Substances 0.000 title claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 58
- 239000003792 electrolyte Substances 0.000 claims abstract description 56
- 238000005868 electrolysis reaction Methods 0.000 claims abstract description 14
- 230000001681 protective effect Effects 0.000 claims description 16
- 238000007789 sealing Methods 0.000 claims description 11
- 230000000694 effects Effects 0.000 claims description 9
- 238000001704 evaporation Methods 0.000 claims description 8
- 230000008020 evaporation Effects 0.000 claims description 8
- 238000009833 condensation Methods 0.000 claims description 7
- 230000005494 condensation Effects 0.000 claims description 7
- 230000000670 limiting effect Effects 0.000 claims description 7
- 238000005485 electric heating Methods 0.000 claims description 4
- 230000001154 acute effect Effects 0.000 claims description 3
- 238000007664 blowing Methods 0.000 claims description 3
- 238000009826 distribution Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- 230000003247 decreasing effect Effects 0.000 claims description 2
- 238000010025 steaming Methods 0.000 claims 1
- 230000003028 elevating effect Effects 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 7
- 229910021645 metal ion Inorganic materials 0.000 description 4
- 230000036961 partial effect Effects 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000000903 blocking effect Effects 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000036647 reaction Effects 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 241000370738 Chlorion Species 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000001174 ascending effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- -1 chlorion etc. Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 239000013528 metallic particle Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 238000005086 pumping Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C5/00—Electrolytic production, recovery or refining of metal powders or porous metal masses
- C25C5/02—Electrolytic production, recovery or refining of metal powders or porous metal masses from solutions
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/06—Operating or servicing
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
The present invention relates to a kind of electrolytic preparation devices for the metal powder for being capable of separation of solid and liquid；Including electrolyte tank and electrolysis frame, it is provided on electrolysis frame and is connected to power supply and penetrates into the anode bar in electrolyte tank and cathode rod vertically, the lower part of electrolyte tank is provided with evaporator, and the bottom centre of electrolyte tank offers drain spout, the material leakage elevator sealed engagement therewith is provided in drain spout, the lower part of material leakage elevator is connected with material leakage lifting column, and material leakage lifting seat is connected with below material leakage lifting column, and material leakage lifting seat is connected with the material leakage lifting cylinder that electrolysis lower box part is set；The present invention sets evaporator in the lower part of electrolyte tank, and open up drain spout in the lower part of electrolyte tank, coordinate the material leakage elevator that can be lifted in material spilling hole, it is flowed by the solid-liquid mixture in the elevating control electrolyte tank of material leakage elevator in evaporator, ensure the continuous normal work of electrolyte tank, separated efficiency is improved, while also improves the electrolytic efficiency of electrolyte tank.
Description
Technical field
Preparation equipment field more particularly to a kind of metal powder for being capable of separation of solid and liquid the present invention relates to metal powder
Electrolytic preparation device.
Background technology
Metal powder refers to that size is less than the metallic particles group of 1mm.Including single metal powder, alloy powder and have
Some infusible compound powder of metalline are the main raw material(s)s of powder metallurgy.
The preparation method of metal powder is various, and wherein electrolysis is a kind of common metal powder processing method, is by logical
The cathode rod and anode bar of electricity are put into metal salt solution, and positive metal ions can be mobile toward cathode and generate to obtain electronics with cathode rod
Reaction, and then obtain metal powder and be attached on cathode rod, and have substantial amounts of metal powder that can drop into electrolyte, therefore
It needs to carry out it separation of solid and liquid, the separation of existing metal powder and electrolyte needs integrally to pour out mixed liquor mostly, so
It is separated afterwards by separator, separation is complicated, inefficiency, and needs to stop the electrolysis in electrolyte tank.
The content of the invention
The object of the present invention is to provide a kind of electrolytic preparation device for the metal powder for being capable of separation of solid and liquid, in electrolyte tank
Lower part sets evaporator, and opens up drain spout in the lower part of electrolyte tank, and the material leakage elevator that can be lifted is coordinated in material spilling hole,
It is flowed by the solid-liquid mixture in the elevating control electrolyte tank of material leakage elevator in evaporator, it is easy to operate, moreover it is possible to simplify
The electrolyte replacement operation of electrolyte tank, it is ensured that the continuous normal work of electrolyte tank improves separated efficiency, while also improves
The electrolytic efficiency of electrolyte tank.
In order to achieve the goal above, the technical solution adopted by the present invention is：A kind of metal powder for being capable of separation of solid and liquid
Electrolytic preparation device, it includes electrolyte tank (1) and electrolysis frame (2), is provided on the electrolysis frame (2) and is connected to power supply and erects
The straight anode bar (3) and cathode rod (4) penetrated into electrolyte tank (1), the lower part of the electrolyte tank (1) are provided with evaporator,
And the bottom centre of electrolyte tank (1) offers drain spout, and the material leakage lifting sealed engagement therewith is provided in the drain spout
Block (40), the lower part of the material leakage elevator (40) are connected with material leakage lifting column (41), under the material leakage lifting column (41)
Side is connected with material leakage lifting seat (42), the material leakage lifting cylinder that the material leakage lifting seat (42) is set with electrolyte tank (1) lower part
(43) connect, the inner bottom surface of the electrolyte tank (1) is continuously decreased from both sides to centre-height, in the middle part of the material leakage lifting seat
The material spilling hole (44) for circularizing distribution is offered, both sides are the inclined-plane tilted down.
Further, the evaporator includes the evaporative cylinder (31) for being arranged on electrolyte tank (1) lower part, the evaporation
The lower part of cylinder (31) is fixed with protective case without bottom plate and in evaporation groove seat (32) in the evaporation groove seat (32)
(33), be provided with electric heating block (34) in the protective case (33), and the top of protective case (33) be heat-conducting block collets, under
Portion is partiting thermal insulation block, and the evaporation groove seat (32) is located at evaporative cylinder (31) and is embedded with the position that protective case (33) docks
Sealing block (35), the side wall of the evaporative cylinder (31) offer steam (vapor) outlet (36), and the steam (vapor) outlet (36) is connected with
Collecting box (37) is condensed, the condensation collecting box (37) is communicated with exhaust tube (38), and the exhaust tube (38) is combined with close
It covers (39).
Further, the both sides of the cathode rod (4) are provided with the scraper collection half (14) of mutual cooperation, and scraper
The position for collecting half (14) and cathode rod (4) cooperation offers semicircle mouth, and the scraper collects the outside of half (14)
The head of the activity of can controlling and lifting is connected with, the top that a scraper collects half (14) is fixed with the suction communicated therewith
Expects pipe (18), the suction tube (18) are connected with suction air pump (19), and it is insulating cylinder that the scraper, which collects half (14),.
Further, two scrapers collect half (14) upper plate and the matching part of side plate is provided with sealing strip (15).
Further, the suction tube (18) is L-shaped pipe, and discharge port is offered below the middle part of horizontal component
(22), the one side of suction air pump (19) and in suction tube (18) is provided with inclined material retaining net positioned at discharge port (22)
(23), be combined with collection box (20) below the discharge port (22), the scraper collect be provided on half (14) with
The box body limited block (21) of collection box (20) left and right sides cooperation.
Further, the height of the collection box (20) is less than the lower surface of suction tube (18) horizontal component, described
The front and rear outside of collection box (20), which is provided with, collects elevator (24), and collects elevator (24) by collecting clamping screw
(25) outside of the collection box (20) of locking, and the outside of collection box (20) is vertically provided with no less than 2 with collecting
The collection rising-falling tone knothole (26) of clamping screw (25) cooperation, the top of the collection elevator (24) is provided with and suction tube
(18) the collection block (27) of horizontal component lower surface cooperation.
Further, the collection block (27) is made of two blocks of plates at an acute angle, and one of plate is vertically arranged, separately
One block of plate is obliquely installed and is connected with collecting elevator (24), collects outside and the collection box of the plate that block (27) is vertically arranged
(20) inside is concordant.
Further, the top of another scraper collection half (14) is fixed with the gas blow pipe (16) with connecting, and blows
(18 collect the positions of half (14) cooperation on cathode rod (4) central symmetry, the air blowing with scraper for pipe (16) and suction tube
Pipe (16) is connected with blower pump (17).
Further, the head includes the left movable block (13) on half top of left and right scraper collection and right activity
Block (10), the left movable block (13) are coordinated by the interlocking lever (12) on the right side of linked block (11) and right movable block (10), institute
It is provided between scraper limiting slot (8), upper and lower part and sets in the middle part of the right movable block (10) and linked block (11) opposite sides stated
Scraper resetting spring (9) is equipped with, scraper folding switch block (7), the scraper folding are combined between two scraper limiting slots (8)
Switch block (7) is ellipse, and lower surface center is connected with scraper lifting cylinder (62), under the scraper lifting cylinder (62)
Portion is connected with the scraper rotation motor (61) for being coaxial therewith line, and the scraper rotation motor (61) is arranged in electrolyte tank (1)
On the collecting frame (5) of installation.
Further, the left movable block (13) is higher than right movable block (10), and the top of right movable block (10) is set
There is the interlocked limited slot (28) with interlocking lever (12) cooperation.
Beneficial effects of the present invention are：
1st, evaporator is set in the lower part of electrolyte tank, and drain spout is opened up in the lower part of electrolyte tank, coordinate in material spilling hole
The material leakage elevator that can be lifted is flowed into evaporator by the solid-liquid mixture in the elevating control electrolyte tank of material leakage elevator
It is interior, it is easy to operate, moreover it is possible to simplify the electrolyte replacement operation of electrolyte tank, it is ensured that the continuous normal work of electrolyte tank improves
Separated efficiency, while also improve the electrolytic efficiency of electrolyte tank.
2nd, the smart structural design of evaporator, the remaining metal powder that can be convenient in the taking-up and protective layer of heating layer
It pours out, while is also convenient for installing, and condense collecting box and be communicated with exhaust tube, vacuum state can be become before operation,
Steam can be made preferably to enter in condensation collecting box to be collected.
3rd, it is provided with and collects half with two openable and closable scrapers of cathode rod cooperation, coordinates lifting gear, can realize
Metal powder scraper on cathode rod, and the top setting suction device of half is collected in scraper, it can realize on cathode rod
Metal powder is collected automatically, while does not interfere with the normal electrolysis of cathode rod, can avoid excessive metal powder and electrolyte
Mixing avoids the occurrence of the situation of drain spout blocking.
4th, scraper collects the design of half side and top seal item, can to avoid during suction metal powder from
Scraper collects the top of half and side side sheds, and lower part blow-by can facilitate the outflow of electrolyte, and then improve suction
The aridity of metal powder in journey.
5th, the matching design of discharge port, material retaining net and collection box can facilitate the collection of metal powder, avoid in suction
Occur situation about shedding in the process, while can also prevent metal powder from entering the blocking that suction air pump causes pump.
6th, the design collected elevator and collect block in collection box, it can be ensured that metal powder can be fully contemplated to
In collection box.
7th, the structure design of block is collected, compared with the block of vertical shape, metal powder, phase can occur to avoid box upper wall
For the block of L-shaped or undercut type, the contact area for collecting block and suction tube lower part can be reduced, and then avoid uneven surface
Gap caused by whole, while can also ensure that collecting clamping screw can accurately be inserted into collection rising-falling tone knothole.
8th, the design of gas blow pipe and blower pump can dry up the metal powder in scraper surge drum, while can also
It is enough to blow afloat metal powder, coordinate the sucking-off of suction tube and suction air pump.
9th, head is ingenious in design, and left and right movable block is realized using rotary oval scraper folding switch block
It moves toward one another, while can also can realize left and right movable block synchronous as the linkage part for driving the lifting of left and right movable block
Lifting greatly ensures the effect of scraper.
10th, the design of interlocked limited slot the situation of front-back staggered can occur to avoid left and right movable block when activity,
And then one step ensure that scraper collects the scraper effect of half.
Description of the drawings
Fig. 1 is a kind of structure diagram of the electrolytic preparation device for the metal powder for being capable of separation of solid and liquid.
Fig. 2 is the partial enlarged view of A in Fig. 1.
Fig. 3 is the partial enlarged view of B in Fig. 1.
Fig. 4 is the partial enlarged view of C in Fig. 3.
Fig. 5 is the top view that scraper collects part.
Fig. 6 is the sectional view of D-D in Fig. 5.
Fig. 7 is the partial enlarged view of F in Fig. 6.
Label character is expressed as shown in figure：1st, electrolyte tank；2nd, it is electrolysed frame；3rd, anode bar；4th, cathode rod；5th, collecting frame；
7th, scraper folding switch block；8th, scraper limiting slot；9th, scraper resetting spring；10th, right movable block；11st, linked block；12nd, interlocking lever；
13rd, left movable block；14th, scraper collects half；15th, sealing strip；16th, gas blow pipe；17th, blower pump；18th, suction tube；19th, suction gas
Pump；20th, collection box；21st, box body limited block；22nd, discharge port；23rd, material retaining net；24th, elevator is collected；25th, locking screw is collected
Bolt；26th, rising-falling tone knothole is collected；27th, block is collected；28th, interlocked limited slot；31st, evaporative cylinder；32nd, groove seat is evaporated；33rd, protect
Set；34th, electric heating block；35th, sealing block；36th, steam (vapor) outlet；37th, collecting box is condensed；38th, exhaust tube；39th, sealing cover；40th, material leakage
Elevator；41st, material leakage lifting column；42nd, material leakage lifting seat；43rd, material leakage lifting cylinder；44th, material spilling hole；61st, scraper rotates horse
It reaches；62nd, scraper lifting cylinder.
Specific embodiment
In order to which those skilled in the art is made to more fully understand technical scheme, below in conjunction with the accompanying drawings to the present invention into
Row is described in detail, and the description of this part is only exemplary and explanatory, should not there is any limitation to protection scope of the present invention
Effect.
As shown in Fig. 1-Fig. 7, concrete structure of the invention is：A kind of electrolytic preparation for the metal powder for being capable of separation of solid and liquid
Device, it includes electrolyte tank 1 and electrolysis frame 2, is provided on the electrolysis frame 2 and is connected to power supply and penetrates into electrolyte tank vertically
Anode bar 3 and cathode rod 4 in 1, the lower part of the electrolyte tank 1 is provided with evaporator, and the bottom centre of electrolyte tank 1 opens up
There is drain spout, the material leakage elevator 40 sealed engagement therewith is provided in the drain spout, the material leakage elevator 40
Lower part is connected with material leakage lifting column 41, and 41 lower section of material leakage lifting column is connected with material leakage lifting seat 42, the material leakage liter
Drop seat 42 is connected with the material leakage lifting cylinder 43 that 1 lower part of electrolyte tank is set, and the inner bottom surface of the electrolyte tank 1 is from both sides to center
It highly continuously decreases, offers the material spilling hole 44 for circularizing distribution in the middle part of the material leakage lifting seat, both sides tilt down
Inclined-plane.
Preferably, the evaporator includes being arranged on the evaporative cylinder 31 of 1 lower part of electrolyte tank, under the evaporative cylinder 31
Portion is fixed with protective case 33, the protective case 33 without bottom plate and in evaporation groove seat 32 in the evaporation groove seat 32
Electric heating block 34 is inside provided with, and the top of protective case 33 is heat-conducting block collets, lower part is partiting thermal insulation block, the evaporator tank
Seat 32 is embedded with sealing block 35 positioned at evaporative cylinder 31 with the position that protective case 33 docks, and the side wall of the evaporative cylinder 31 offers
Steam (vapor) outlet 36, the steam (vapor) outlet 36 are connected with condensation collecting box 37, and the condensation collecting box 37 is communicated with exhaust tube
38, the exhaust tube 38 is combined with sealing cover 39.
Preferably, the both sides of the cathode rod 4 are provided with the scraper collection half 14 of mutual cooperation, and scraper is collected
Half 14 position coordinated with cathode rod 4 offers semicircle mouth, and the outside that the scraper is collected half 14 is connected with can be left
Right activity and the head of lifting, the top that a scraper is collected half 14 is fixed with the suction tube 18 communicated therewith, described
Suction tube 18 be connected with suction air pump 19, it is insulating cylinder that the scraper, which collects half 14,.
Preferably, two scrapers collect half 14 upper plate and the matching part of side plate is provided with sealing strip 15.
Preferably, the suction tube 18 is L-shaped pipe, and discharge port 22 is offered below the middle part of horizontal component, and is inhaled
The one side of suction air pump 19 is provided with inclined material retaining net 23 positioned at discharge port 22 in expects pipe 18, the discharge port 22
Lower section is combined with collection box 20, and the scraper collects the box body /V being provided on half 14 with the cooperation of 20 left and right sides of collection box
Block 21.
Preferably, the height of the collection box 20 is less than the lower surface of 18 horizontal component of suction tube, the collection box
20 front and rear outside, which is provided with, collects elevator 24, and collects the collection box that elevator 24 is locked by collecting clamping screw 25
20 outside, and the outside of collection box 20 is vertically provided with no less than 2 collections coordinated with collecting clamping screw 25
Rising-falling tone knothole 26, the top of the collection elevator 24 are provided with the collection with the cooperation of 18 horizontal component lower surface of suction tube
Block 27.
Preferably, the collection block 27 is made of two blocks of plates at an acute angle, and one of plate is vertically arranged, another piece
Plate is obliquely installed and is connected with collecting elevator 24, collects the outside for the plate that block 27 is vertically arranged and the inside of collection box 20
Concordantly.
Preferably, the top that another scraper is collected half 14 is fixed with the gas blow pipe 16 with connecting, and 16 He of gas blow pipe
Suction tube 18 collects half 14 position coordinated on 4 central symmetry of cathode rod with scraper, and the gas blow pipe 16, which is connected with, to be blown
Air pump 17.
Preferably, the head includes the left movable block 13 on half top of left and right scraper collection and right movable block
10, the left movable block 13 is coordinated by linked block 11 and the interlocking lever 12 on right 10 right side of movable block, the right movable block
10 and 11 opposite sides of linked block in the middle part of be provided between scraper limiting slot 8, upper and lower part and be provided with scraper resetting spring 9,
Scraper folding switch block 7 is combined between two scraper limiting slots 8, the scraper folding switch block 7 is oval, lower surface
Center is connected with scraper lifting cylinder 62, and the lower part of the scraper lifting cylinder 62 is connected with the scraper rotation for being coaxial therewith line
Motor 61, the scraper rotation motor 61 are arranged on the collecting frame 5 installed in electrolyte tank 1.
Preferably, the left movable block 13 is higher than right movable block 10, and the top of right movable block 10 is provided with and interlocks
The interlocked limited slot 28 that bar 12 coordinates.
When specifically used, first device is assembled, afterwards removes air extracting seal lid 39, exhaust tube is made to be connected to pumping dress
It puts, covers air extracting seal lid 39 after being vacuumized by air extractor, control power supply afterwards to anode bar 3 and cathode rod
4, make cell reaction occurs in electrolyte tank 1, positive metal ions can be focused at cathode rod, and then positive metal ions can be made to obtain electricity
Son formation metal laminate, anion such as chlorion etc., which can lose, electronically forms chlorine, is driven afterwards by scraper rotation motor 61
Scraper folding switch block 7 rotates, and the longitudinal end for making its oval withstands right movable block 10 and linked block 11, and then can make left and right activity
Block moves toward one another, and then left and right is driven to collect scraper half and moves toward one another to form whole scraper surge drum, passes through scraper liter afterwards
Sending down abnormally ascending cylinder 62 drives scraper folding switch block 7 to lift, and then scraper surge drum is driven to rise, and scraper surge drum lower part can be by cathode rod
The metal laminate adhered on 4 scrapes, and forms it into powder, while as scraper surge drum departs from electrolysis liquid surface, and liquid can be from scraping
Expect surge drum lower part outflow, started afterwards by blower pump 17, from gas blow pipe 16 in scraper surge drum blowing, by metal
Powder is blown afloat while drying, is started afterwards by suction air pump 19, and then can be by the metal powder in scraper surge drum
It is drawn into suction tube 18, can be intercepted from discharge port 22 dropped into collection box 20 by material retaining net 23 afterwards, complete to collect, it
After make head homing, continue subsequent cell reaction and the collection of metal powder, when the metal powder in collection box
When collection is full, declined by unclamping collection clamping screw 25 by elevator 24 is collected, locked afterwards with collection clamping screw 25
It is tightened to another to collect in rising-falling tone knothole 26, then takes collection box away, when electrolysis is carried out to a certain extent, in electrolyte
Metal ion can all be electrolyzed to produce metal powder substantially, by material leakage lifting cylinder 43 material leakage lifting seat 42 be driven to rise afterwards,
And then material leakage elevator 40 is driven, which to rise, makes it be separated with drain spout, electrolyte and metal powder therein can be fallen from drain spout
The top of protective case 33 is entered, by the heating of heat block 34 in protective case 33 and the heat conduction on 33 top of protective case, makes its change
It into steam and is drawn into condensation collecting box 37, the steam entered in condensation collecting box 37, which encounters collection tank wall, to be become again
It is liquid, and metal powder can be stayed on protective case 33.
It should be noted that herein, term " comprising ", "comprising" or its any other variant are intended to non-row
His property includes, so that process, method, article or equipment including a series of elements not only include those elements, and
And it further includes other elements that are not explicitly listed or further includes as this process, method, article or equipment institute inherently
Element.
Specific case used herein is set forth the principle of the present invention and embodiment, the explanation of above example
It is only intended to help the method and its core concept for understanding the present invention.The above is only the preferred embodiment of the present invention, should
When pointing out, due to the finiteness of literal expression, and objectively there are unlimited concrete structure, for the common skill of the art
For art personnel, without departing from the principle of the present invention, several improvement, retouching or variation can also be made, can also incited somebody to action
Above-mentioned technical characteristic is combined in the right way；These improve retouching, variation or combination or the not improved structure by invention
Think and technical solution directly applies to other occasions, be regarded as protection scope of the present invention.
Claims (10)
1. a kind of electrolytic preparation device for the metal powder for being capable of separation of solid and liquid, it includes electrolyte tank (1) and electrolysis frame (2), institute
It is provided on the electrolysis frame (2) stated and is connected to power supply and penetrates into the anode bar (3) in electrolyte tank (1) and cathode rod (4) vertically,
It is characterized in that, the lower part of the electrolyte tank (1) is provided with evaporator, and the bottom centre of electrolyte tank (1) offers material leakage
Mouthful, the material leakage elevator (40) sealed engagement therewith is provided in the drain spout, under the material leakage elevator (40)
Portion is connected with material leakage lifting column (41), and material leakage lifting seat (42), the leakage are connected with below the material leakage lifting column (41)
Material lifting seat (42) is connected with the material leakage lifting cylinder (43) that electrolyte tank (1) lower part is set, the inner bottom surface of the electrolyte tank (1)
It is continuously decreased from both sides to centre-height, offers the material spilling hole (44) for circularizing distribution in the middle part of the material leakage lifting seat, two
Side is the inclined-plane tilted down.
2. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 1, which is characterized in that
The evaporator includes the evaporative cylinder (31) for being arranged on electrolyte tank (1) lower part, and the lower part of the evaporative cylinder (31) is without bottom plate
And in evaporation groove seat (32), protective case (33), the protective case (33) are fixed in the evaporation groove seat (32)
Electric heating block (34) is inside provided with, and the top of protective case (33) is heat-conducting block collets, lower part is partiting thermal insulation block, the steaming
Hair groove seat (32) is located at evaporative cylinder (31) and is embedded with sealing block (35), the evaporative cylinder with the position that protective case (33) docks
(31) side wall offers steam (vapor) outlet (36), and the steam (vapor) outlet (36) is connected with condensation collecting box (37), and described is cold
Solidifying collecting box (37) is communicated with exhaust tube (38), and the exhaust tube (38) is combined with sealing cover (39).
3. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 1, which is characterized in that
The scraper that the both sides of the cathode rod (4) are provided with mutual cooperation collects half (14), and scraper collects half (14) with bearing
The position of pole stick (4) cooperation offers semicircle mouth, and the scraper, which collects to be connected on the outside of half (14), can control activity
With the head of lifting, the top that a scraper collects half (14) is fixed with the suction tube (18) communicated therewith, described
Suction tube (18) is connected with suction air pump (19), and it is insulating cylinder that the scraper, which collects half (14),.
4. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 3, which is characterized in that
Two scrapers collect half (14) upper plate and the matching part of side plate is provided with sealing strip (15).
5. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 3, which is characterized in that
The suction tube (18) is L-shaped pipe, and discharge port (22), and suction tube (18) interior position are offered below the middle part of horizontal component
The one side of suction air pump (19) is provided with inclined material retaining net (23) in discharge port (22), under the discharge port (22)
Side is combined with collection box (20), and the scraper collects the box body being provided on half (14) with the cooperation of collection box (20) left and right sides
Limited block (21).
6. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 5, which is characterized in that
The height of the collection box (20) be less than suction tube (18) horizontal component lower surface, the collection box (20) it is front and rear
Outside, which is provided with, collects elevator (24), and collects the collection box (20) that elevator (24) is locked by collecting clamping screw (25)
Outside, and the outside of collection box (20) be vertically provided with no less than 2 with collect clamping screw (25) coordinate receipts
Collect rising-falling tone knothole (26), the top of the collection elevator (24) is provided with matches somebody with somebody with suction tube (18) horizontal component lower surface
The collection block (27) of conjunction.
7. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 6, which is characterized in that
The collection block (27) is made of two blocks of plates at an acute angle, and one of plate is vertically arranged, and another block of plate is obliquely installed simultaneously
It is connected with collecting elevator (24), the outside for collecting the plate that block (27) is vertically arranged is concordant with the inside of collection box (20).
8. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 3, which is characterized in that
The top of another scraper collection half (14) is fixed with the gas blow pipe (16) with connecting, and gas blow pipe (16) and suction tube (18
On cathode rod (4) central symmetry, the gas blow pipe (16) is connected with air blowing at position with scraper collection half (14) cooperation
It pumps (17).
9. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 3, which is characterized in that
The head includes the left movable block (13) and right movable block (10) that left and right scraper collects half top, the left work
Motion block (13) is coordinated by the interlocking lever (12) on the right side of linked block (11) and right movable block (10), the right movable block (10) and
It is provided in the middle part of linked block (11) opposite sides between scraper limiting slot (8), upper and lower part and is provided with scraper resetting spring
(9), scraper folding switch block (7) is combined between two scraper limiting slots (8), the scraper folding switch block (7) is ellipse,
Its lower surface center is connected with scraper lifting cylinder (62), and the lower part of the scraper lifting cylinder (62), which is connected with, to be coaxial therewith
The scraper rotation motor (61) of line, the scraper rotation motor (61) are arranged on the collecting frame (5) installed in electrolyte tank (1)
On.
10. a kind of electrolytic preparation device of metal powder for being capable of separation of solid and liquid according to claim 9, feature exist
In the left movable block (13) is higher than right movable block (10), and the top of right movable block (10) is provided with and interlocking lever (12)
The interlocked limited slot (28) of cooperation.
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| CN201711335103.3A CN108048879B (en) | 2017-12-14 | 2017-12-14 | Electrolytic preparation device capable of collecting metal powder |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711335103.3A CN108048879B (en) | 2017-12-14 | 2017-12-14 | Electrolytic preparation device capable of collecting metal powder |
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| CN108048879B CN108048879B (en) | 2019-12-06 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110773304A (en) * | 2019-11-14 | 2020-02-11 | 迟人源 | Grinder of polymer chemical material granule |
| CN111841352A (en) * | 2020-07-15 | 2020-10-30 | 武汉裕大华纺织有限公司 | Automatic size mixing system |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1219678A1 (en) * | 1984-10-18 | 1986-03-23 | Научно-производственное объединение "Тулачермет" | Electrolyzer for producing metal powders |
| CN101363126A (en) * | 2008-09-05 | 2009-02-11 | 江苏技术师范学院 | Apparatus for preparing nanometer metal powder |
| CN203442189U (en) * | 2013-07-04 | 2014-02-19 | 青岛日辰食品有限公司 | Piston type kettle-bottom discharge valve |
| CN105177635A (en) * | 2015-09-12 | 2015-12-23 | 北京工业大学 | System and method for continuously preparing tungsten powder |
| CN204999987U (en) * | 2015-10-09 | 2016-01-27 | 贵溪凌云铜业有限公司 | Equipment of preparing of single nickel salt crystalline solid |
| CN205774828U (en) * | 2016-05-17 | 2016-12-07 | 广东金业贵金属有限公司 | A kind of silver refining electrolyzing cell |
-
2017
- 2017-12-14 CN CN201711335103.3A patent/CN108048879B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1219678A1 (en) * | 1984-10-18 | 1986-03-23 | Научно-производственное объединение "Тулачермет" | Electrolyzer for producing metal powders |
| CN101363126A (en) * | 2008-09-05 | 2009-02-11 | 江苏技术师范学院 | Apparatus for preparing nanometer metal powder |
| CN203442189U (en) * | 2013-07-04 | 2014-02-19 | 青岛日辰食品有限公司 | Piston type kettle-bottom discharge valve |
| CN105177635A (en) * | 2015-09-12 | 2015-12-23 | 北京工业大学 | System and method for continuously preparing tungsten powder |
| CN204999987U (en) * | 2015-10-09 | 2016-01-27 | 贵溪凌云铜业有限公司 | Equipment of preparing of single nickel salt crystalline solid |
| CN205774828U (en) * | 2016-05-17 | 2016-12-07 | 广东金业贵金属有限公司 | A kind of silver refining electrolyzing cell |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110773304A (en) * | 2019-11-14 | 2020-02-11 | 迟人源 | Grinder of polymer chemical material granule |
| CN111841352A (en) * | 2020-07-15 | 2020-10-30 | 武汉裕大华纺织有限公司 | Automatic size mixing system |
| CN111841352B (en) * | 2020-07-15 | 2022-03-15 | 武汉裕大华纺织有限公司 | Automatic size mixing system |
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| Publication number | Publication date |
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| CN108048879B (en) | 2019-12-06 |
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