CN210079461U - Vacuum condensation reaction kettle - Google Patents
Vacuum condensation reaction kettle Download PDFInfo
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- CN210079461U CN210079461U CN201920502089.XU CN201920502089U CN210079461U CN 210079461 U CN210079461 U CN 210079461U CN 201920502089 U CN201920502089 U CN 201920502089U CN 210079461 U CN210079461 U CN 210079461U
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 29
- 238000002207 thermal evaporation Methods 0.000 title claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 238000007789 sealing Methods 0.000 claims description 3
- 239000004519 grease Substances 0.000 claims 3
- 238000000605 extraction Methods 0.000 claims 1
- 238000009434 installation Methods 0.000 claims 1
- 238000005086 pumping Methods 0.000 claims 1
- 230000007306 turnover Effects 0.000 claims 1
- 238000007599 discharging Methods 0.000 abstract description 7
- 238000009833 condensation Methods 0.000 description 4
- 230000005494 condensation Effects 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
本实用新型公开了一种真空冷凝反应釜,包含罐体和盖体,所述罐体的罐壁内部设有中空的油室,所述罐体的底部设有与罐体内部相连通的进出料管和与油室相连通的进油管,罐体的上部设有与油室相连通的排油管,盖体上安装有搅拌器,搅拌器的轴杆底部安装的桨叶位于盖体下方,盖体上设有抽真空管和冷凝器,所述冷凝器的热交换管与盖体相连通。本实用新型将冷凝器、抽真空管、温度计、压力计、搅拌器全部集成到盖体上,极大的增加了反应釜内的空间,采用常压负压进行进料和出料,结构简单紧凑。
The utility model discloses a vacuum condensation reaction kettle, which comprises a tank body and a cover body. A hollow oil chamber is arranged inside the tank wall of the tank body, and an inlet and outlet that communicate with the inside of the tank body are arranged at the bottom of the tank body. The material pipe and the oil inlet pipe communicated with the oil chamber, the upper part of the tank body is provided with an oil discharge pipe communicated with the oil chamber, the cover body is installed with an agitator, and the paddle installed at the bottom of the shaft of the agitator is located under the cover body, The cover body is provided with an evacuation tube and a condenser, and the heat exchange tube of the condenser communicates with the cover body. The utility model integrates the condenser, the evacuating tube, the thermometer, the pressure gauge and the stirrer on the cover body, which greatly increases the space in the reaction kettle, adopts normal pressure and negative pressure for feeding and discharging, and has a simple and compact structure .
Description
技术领域technical field
本实用新型涉及反应釜设备领域,特别涉及一种真空冷凝反应釜。The utility model relates to the field of reaction kettle equipment, in particular to a vacuum condensation reaction kettle.
背景技术Background technique
反应釜在食品、医药、化工等领域的应用十分广泛,传统的反应釜通常是一个容器,内部设有搅拌装置,在反应釜本体上设置进料口和出料口,常规设置是将进料口设置于反应釜的上部,出料口设置于反应釜的下部,另外冷凝设备都设置于反应釜内部,占用很大的空间。The reaction kettle is widely used in food, medicine, chemical industry and other fields. The traditional reaction kettle is usually a container with a stirring device inside. The outlet is arranged at the upper part of the reaction kettle, the discharge outlet is arranged at the lower part of the reaction kettle, and the condensing equipment is arranged inside the reaction kettle, which occupies a large space.
实用新型内容Utility model content
本实用新型所要解决的技术问题在于克服现有技术的缺陷,提出一种真空冷凝反应釜,结构简单,布局合理,极大的提升了反应釜的内部空间。The technical problem to be solved by the utility model is to overcome the defects of the prior art, and propose a vacuum condensation reaction kettle, which has a simple structure and a reasonable layout, and greatly improves the inner space of the reaction kettle.
本实用新型的技术方案:The technical scheme of the present utility model:
一种真空冷凝反应釜,包含罐体和盖体,所述罐体的罐壁内部设有中空的油室,所述罐体的底部设有与罐体内部相连通的进出料管和与油室相连通的进油管,罐体的上部设有与油室相连通的排油管,盖体上安装有搅拌器,搅拌器的轴杆底部安装的桨叶位于盖体下方,盖体上设有抽真空管和冷凝器,所述冷凝器的热交换管与盖体相连通。A vacuum condensation reaction kettle, comprising a tank body and a cover body, a hollow oil chamber is arranged inside the tank wall of the tank body, and an inlet and outlet pipe that communicates with the inside of the tank body and the oil chamber are arranged at the bottom of the tank body. The upper part of the tank body is provided with an oil discharge pipe that communicates with the oil chamber, the cover body is installed with an agitator, and the paddle installed at the bottom of the shaft of the agitator is located under the cover body. The evacuated pipe and the condenser, the heat exchange pipe of the condenser is communicated with the cover body.
进一步地,所述热交换管为一根直管,位于冷凝器内,热交换管的底部与反应釜内连通。Further, the heat exchange pipe is a straight pipe, located in the condenser, and the bottom of the heat exchange pipe is communicated with the reactor.
进一步地,所述冷凝器为水冷式冷凝器,所述冷凝器竖直安装在盖体上,进水管位于冷凝器的下部,出水管位于冷凝器的上部,所述进水管和出水管与冷水机组成水循环。Further, the condenser is a water-cooled condenser, the condenser is vertically installed on the cover body, the water inlet pipe is located at the lower part of the condenser, the water outlet pipe is located at the upper part of the condenser, and the water inlet pipe and the water outlet pipe are connected with the cold water. The unit forms a water cycle.
进一步地,所述抽真空管上设置三通管后连接气阀后再连接空气滤清器。Further, after the three-way pipe is set on the vacuum pipe, the air valve is connected, and then the air filter is connected.
进一步地,所述盖体上设有挂耳,盖体上设有吊机,吊机通过吊绳和挂耳与盖体相连接。Further, the cover body is provided with a hanging lug, the cover body is provided with a hoist, and the hoist is connected with the cover body through a hanging rope and the hanging lug.
进一步地,所述盖体上设有添料口,添料口设有密封盖。Further, the cover body is provided with a feeding port, and the feeding port is provided with a sealing cover.
进一步地,所述盖体上设有温度表。Further, a temperature gauge is provided on the cover body.
进一步地,所述盖体上设有压力表。Further, a pressure gauge is provided on the cover body.
与现有技术相比,本实用新型通过罐体底部设置的进出料管,配合抽真空管,依靠负压和常压进行进料和出料,冷凝管设置于盖体上方,水蒸气上升进入热交换管,凝结后向下滴落返回反应釜内,采用循环热油进行加热,能有效控制反应釜的温度和温度稳定性,抽真空管在某些特殊反应下,将反应釜内抽成真空条件;本实用新型将冷凝器、抽真空管、温度计、压力计、搅拌器全部集成到盖体上,极大的增加了反应釜内的空间,采用常压负压进行进料和出料,结构简单紧凑;热交换管为直管有利于水蒸气上升,低进高出的循环冷却水设计,有利于冷凝水的凝结,关键是冷凝器远离反应釜,不会和加热装置冲突,影响加热的效率;抽真空管上接三通后接空滤,再反应釜恢复常压时,关闭抽真空后,直接打开气阀,迅速恢复常压,过滤后的空气,也不会影响和污染反应釜内物质;挂耳和吊机可以快速将盖体吊起,方便检修和清洗;压力计和温度计可以实时观测到反应釜内的压力和温度情况。Compared with the prior art, the utility model uses the feeding and discharging pipes arranged at the bottom of the tank body, and cooperates with the vacuuming pipes, and relies on negative pressure and normal pressure for feeding and discharging. The exchange tube, after condensation, drips down and returns to the reaction kettle. It is heated by circulating hot oil, which can effectively control the temperature and temperature stability of the reaction kettle. The vacuum tube can evacuate the reaction kettle to a vacuum condition under some special reactions. The utility model integrates the condenser, the vacuum tube, the thermometer, the pressure gauge and the agitator into the cover body, which greatly increases the space in the reaction kettle, adopts the normal pressure negative pressure for feeding and discharging, and has a simple structure. Compact; the heat exchange tube is a straight tube, which is conducive to the rise of water vapor, and the design of circulating cooling water with low input and high output is conducive to the condensation of condensed water. The key is that the condenser is far away from the reaction kettle and will not conflict with the heating device, which will affect the heating efficiency. ; Connect the tee to the vacuum tube and then connect the air filter. When the reactor returns to normal pressure, close the vacuum and open the air valve directly to quickly restore the normal pressure. The filtered air will not affect and pollute the contents of the reactor. ; Hanging lugs and hoists can quickly lift the cover for easy maintenance and cleaning; pressure gauges and thermometers can observe the pressure and temperature in the reactor in real time.
附图说明Description of drawings
图1为本实用新型盖体结构示意图;Fig. 1 is the structural schematic diagram of the cover body of the present invention;
图2为本实用新型罐体结构示意图。Figure 2 is a schematic diagram of the structure of the tank body of the present invention.
具体实施方式Detailed ways
下面结合附图对本实用新型的具体实施方式进行详细说明。The specific embodiments of the present utility model will be described in detail below with reference to the accompanying drawings.
实施例1:Example 1:
一种真空冷凝反应釜,如图1和2所示,包含罐体1和盖体2,所述罐体1的罐壁内部设有中空的油室11,所述罐体1的底部设有与罐体内部相连通的进出料管3和与油室11相连通的进油管41,罐体1的上部设有与油室11相连通的排油管42,盖体2上安装有搅拌器5,搅拌器5的轴杆51底部安装的桨叶52位于盖体2下方,盖体2上设有抽真空管6和冷凝器7,所述冷凝器7的热交换管71与盖体2相连通。A vacuum condensation reaction kettle, as shown in Figures 1 and 2, comprises a tank body 1 and a
进一步地,所述热交换管71为一根直管,位于冷凝器7内,热交换管71的底部与反应釜内连通。Further, the
进一步地,所述冷凝器7为水冷式冷凝器,所述冷凝器7竖直安装在盖体上,进水管72位于冷凝器7的下部,出水管73位于冷凝器7的上部,所述进水管72和出水管73与冷水机组成水循环。Further, the
进一步地,所述抽真空管6上设置三通管61后连接气阀62后再连接空气滤清器63。Further, a three-
进一步地,所述盖体2上设有挂耳21,盖体2上设有吊机,吊机通过吊绳和挂耳与盖体2相连接。也可以采用盖体固定,而罐体上下移动的设计。本实施例采用固定罐体,移动盖体。Further, the
进一步地,所述盖体2上设有添料口22,添料口22设有密封盖23。Further, the
进一步地,所述盖体2上设有温度表24。Further, a
进一步地,所述盖体2上设有压力表25。Further, the
与现有技术相比,本实用新型通过罐体底部设置的进出料管,配合抽真空管,依靠负压和常压进行进料和出料,冷凝管设置于盖体上方,水蒸气上升进入热交换管,凝结后向下滴落返回反应釜内,采用循环热油进行加热,能有效控制反应釜的温度和温度稳定性,抽真空管在某些特殊反应下,将反应釜内抽成真空条件;本实用新型将冷凝器、抽真空管、温度计、压力计、搅拌器全部集成到盖体上,极大的增加了反应釜内的空间,采用常压负压进行进料和出料,结构简单紧凑;热交换管为直管有利于水蒸气上升,低进高出的循环冷却水设计,有利于冷凝水的凝结,关键是冷凝器远离反应釜,不会和加热装置冲突,影响加热的效率;抽真空管上接三通后接空滤,再反应釜恢复常压时,关闭抽真空后,直接打开气阀,迅速恢复常压,过滤后的空气,也不会影响和污染反应釜内物质;挂耳和吊机可以快速将盖体吊起,方便检修和清洗;压力计和温度计可以实时观测到反应釜内的压力和温度情况。Compared with the prior art, the utility model uses the feeding and discharging pipes arranged at the bottom of the tank body, and cooperates with the vacuuming pipes, and relies on negative pressure and normal pressure for feeding and discharging. The exchange tube, after condensation, drips down and returns to the reaction kettle. It is heated by circulating hot oil, which can effectively control the temperature and temperature stability of the reaction kettle. The vacuum tube can evacuate the reaction kettle to a vacuum condition under some special reactions. The utility model integrates the condenser, the vacuum tube, the thermometer, the pressure gauge and the agitator into the cover body, which greatly increases the space in the reaction kettle, adopts the normal pressure negative pressure for feeding and discharging, and has a simple structure. Compact; the heat exchange tube is a straight tube, which is conducive to the rise of water vapor, and the design of circulating cooling water with low input and high output is conducive to the condensation of condensed water. The key is that the condenser is far away from the reaction kettle and will not conflict with the heating device, which will affect the heating efficiency. ; Connect the tee to the vacuum tube and then connect the air filter. When the reactor returns to normal pressure, close the vacuum and open the air valve directly to quickly restore the normal pressure. The filtered air will not affect and pollute the contents of the reactor. ; Hanging lugs and hoists can quickly lift the cover for easy maintenance and cleaning; pressure gauges and thermometers can observe the pressure and temperature in the reactor in real time.
以上显示和描述了本实用新型的基本原理、主要特征和本实用新型的优点。本实用新型不受上述实施例的限制,上述实施例和说明书中描述的只是说明本实用新型的原理,在不脱离本实用新型精神和范围的前提下本实用新型还会有各种变化和改进,这些变化和改进都落入要求保护的本实用新型的范围内。本实用新型要求保护范围由所附的权利要求书及其等同物界定。The basic principles, main features and advantages of the present invention have been shown and described above. The present utility model is not limited by the above-mentioned embodiments. The above-mentioned embodiments and descriptions only illustrate the principles of the present utility model. The present utility model will have various changes and improvements without departing from the spirit and scope of the present utility model. , these changes and improvements all fall within the scope of the claimed invention. The claimed scope of the present invention is defined by the appended claims and their equivalents.
Claims (8)
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| CN201920502089.XU CN210079461U (en) | 2019-04-15 | 2019-04-15 | Vacuum condensation reaction kettle |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113181866A (en) * | 2021-05-12 | 2021-07-30 | 峰特(浙江)新材料有限公司 | Polylactic acid polycondensation synthesis equipment and method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113181866A (en) * | 2021-05-12 | 2021-07-30 | 峰特(浙江)新材料有限公司 | Polylactic acid polycondensation synthesis equipment and method |
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