CN108048879B - Electrolytic preparation device capable of collecting metal powder - Google Patents
Electrolytic preparation device capable of collecting metal powder Download PDFInfo
- Publication number
- CN108048879B CN108048879B CN201711335103.3A CN201711335103A CN108048879B CN 108048879 B CN108048879 B CN 108048879B CN 201711335103 A CN201711335103 A CN 201711335103A CN 108048879 B CN108048879 B CN 108048879B
- Authority
- CN
- China
- Prior art keywords
- collecting
- scraping
- electrolytic
- matched
- electrolytic tank
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000002184 metal Substances 0.000 title claims abstract description 47
- 239000000843 powder Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000463 material Substances 0.000 claims abstract description 133
- 238000007789 sealing Methods 0.000 claims abstract description 14
- 238000007790 scraping Methods 0.000 claims description 71
- 238000007664 blowing Methods 0.000 claims description 16
- 230000000903 blocking effect Effects 0.000 claims description 4
- 230000001154 acute effect Effects 0.000 claims description 3
- 230000003028 elevating effect Effects 0.000 claims description 2
- 238000009434 installation Methods 0.000 claims description 2
- 238000005868 electrolysis reaction Methods 0.000 abstract description 9
- 239000007788 liquid Substances 0.000 abstract description 9
- 238000000926 separation method Methods 0.000 abstract description 8
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000001704 evaporation Methods 0.000 description 16
- 230000001681 protective effect Effects 0.000 description 14
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 12
- 235000017491 Bambusa tulda Nutrition 0.000 description 12
- 241001330002 Bambuseae Species 0.000 description 12
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 12
- 239000011425 bamboo Substances 0.000 description 12
- 230000008020 evaporation Effects 0.000 description 12
- 238000009833 condensation Methods 0.000 description 9
- 230000005494 condensation Effects 0.000 description 9
- 239000003792 electrolyte Substances 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- 230000000694 effects Effects 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 238000005485 electric heating Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 210000001503 joint Anatomy 0.000 description 2
- 238000003475 lamination Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 230000014509 gene expression Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 238000004663 powder metallurgy Methods 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C5/00—Electrolytic production, recovery or refining of metal powders or porous metal masses
- C25C5/02—Electrolytic production, recovery or refining of metal powders or porous metal masses from solutions
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C7/00—Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells
- C25C7/06—Operating or servicing
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrolytic Production Of Metals (AREA)
Abstract
The invention relates to an electrolytic preparation device capable of collecting metal powder; the electrolytic tank comprises an electrolytic tank and an electrolytic frame, wherein a positive rod and a negative rod which are connected to a power supply and vertically penetrate into the electrolytic tank are arranged on the electrolytic frame, an evaporator is arranged at the lower part of the electrolytic tank, a material leakage opening is formed in the center of the bottom of the electrolytic tank, a material leakage lifting block which is in sealing fit with the material leakage lifting block is arranged in the material leakage opening, a material leakage lifting column is connected to the lower part of the material leakage lifting block, a material leakage lifting seat is connected to the lower part of the material leakage lifting column, and the material leakage lifting seat is connected with a material leakage lifting cylinder arranged at the lower part of the; according to the invention, the evaporator is arranged at the lower part of the electrolytic tank, the material leaking port is formed at the lower part of the electrolytic tank, the liftable material leaking lifting block is matched in the material leaking hole, and the solid-liquid mixture in the electrolytic tank is controlled to flow into the evaporator by the lifting of the material leaking lifting block, so that the continuous normal work of the electrolytic tank is ensured, the separation efficiency is improved, and the electrolysis efficiency of the electrolytic tank is also improved.
Description
Technical Field
The invention relates to the field of metal powder preparation equipment, in particular to an electrolytic preparation device capable of collecting metal powder.
Background
The metal powder refers to a group of metal particles having a size of less than 1 mm. Including single metal powders, alloy powders, and powders of certain refractory compounds having metallic properties, are the primary raw materials for powder metallurgy.
The preparation method of metal powder is various, wherein the electrolysis method is a commonly used metal powder processing method, put into the metal salt solution through circular telegram negative pole stick and positive pole stick, metal positive ion can be toward the negative pole removal and produce with the negative pole stick and get the electron reaction, and then obtain metal powder and adhere to on the negative pole stick, and there is a large amount of metal powder to fall into electrolyte, consequently need carry out solid-liquid separation to it, the separation of current metal powder and electrolyte mostly needs to pour out mixed liquid wholly, then separate through separator, the separation is complicated, low efficiency, and need stop the electrolysis in the electrolysis box.
Disclosure of Invention
The invention aims to provide an electrolytic preparation device capable of collecting metal powder, wherein an evaporator is arranged at the lower part of an electrolytic tank, a material leakage port is formed at the lower part of the electrolytic tank, a liftable material leakage lifting block is matched in the material leakage port, and a solid-liquid mixture in the electrolytic tank is controlled to flow into the evaporator by the lifting of the material leakage lifting block, so that the electrolytic preparation device is convenient to operate, can simplify the replacement operation of electrolyte in the electrolytic tank, ensures the continuous normal work of the electrolytic tank, improves the separation efficiency, and simultaneously improves the electrolysis efficiency of the electrolytic tank.
In order to achieve the above purpose, the invention adopts the technical scheme that: the electrolytic preparation device capable of collecting metal powder comprises an electrolytic tank (1) and an electrolytic frame (2), wherein the electrolytic frame (2) is provided with a positive electrode rod (3) and a negative electrode rod (4) which are connected to a power supply and vertically penetrate into the electrolytic tank (1), the lower part of the electrolytic tank (1) is provided with an evaporator, the center of the bottom of the electrolytic tank (1) is provided with a leakage opening, the leakage opening is internally provided with a leakage lifting block (40) which is in sealing fit with the leakage opening, the lower part of the leakage lifting block (40) is connected with a leakage lifting column (41), the lower part of the leakage lifting column (41) is connected with a leakage lifting seat (42), the leakage lifting seat (42) is connected with a leakage lifting cylinder (43) arranged at the lower part of the electrolytic tank (1), and the inner bottom surface of the electrolytic tank (1) is gradually reduced from two sides to the center height, the middle part of the material leaking lifting seat is provided with material leaking holes (44) which are distributed in an annular shape, and the two sides of the material leaking lifting seat are inclined planes which incline downwards.
Further, the evaporimeter including setting up evaporating pot (31) in electrolysis box (1) lower part, the lower part of evaporating pot (31) do not have the bottom plate and install in evaporation tank seat (32), evaporation tank seat (32) in link firmly protective sheath (33), protective sheath (33) in be provided with electric heat piece (34), and the upper portion of protective sheath (33) be heat conduction piece insulating block, lower part for thermal-insulated insulating block, evaporation tank seat (32) be located the position embedding of evaporating pot (31) and protective sheath (33) butt joint have sealed piece (35), the lateral wall of evaporating pot (31) seted up steam outlet (36), steam outlet (36) be connected with condensation collecting box (37), condensation collecting box (37) intercommunication have exhaust tube (38), exhaust tube (38) cooperate and have sealed lid (39).
Further, the both sides of negative pole stick (4) be provided with the material collection of scraping of mutually supporting and half a section of thick bamboo (14), and scrape material collection half a section of thick bamboo (14) and negative pole stick (4) complex position and seted up semi-circular mouth, the outside of scraping material collection half a section of thick bamboo (14) be connected with the head that can control the activity and go up and down, the upper portion of scraping material collection half a section of thick bamboo (14) links firmly rather than inhaling material pipe (18) of intercommunication, inhale material pipe (18) and be connected with and inhale material air pump (19), the material collection of scraping half a section of thick bamboo (14) be the insulating cylinder.
Furthermore, sealing strips (15) are arranged at the matching parts of the upper plate and the side plates of the two scraping and collecting half cylinders (14).
Furthermore, inhale material pipe (18) and be the L venturi tube, discharge gate (22) have been seted up to its horizontal part's middle part below, and inhale and be located discharge gate (22) in material pipe (18) and be close to one side of inhaling material air pump (19) and be provided with the fender material net (23) of slope, the below cooperation of discharge gate (22) have collection box (20), scrape and be provided with on material collection half section of thick bamboo (14) and collect box body stopper (21) of box (20) left and right sides complex.
Furthermore, the height of the collecting box (20) is lower than the lower surface of the horizontal part of the material sucking pipe (18), the front outer side and the rear outer side of the collecting box (20) are provided with collecting lifting blocks (24), the collecting lifting blocks (24) are locked on the outer side of the collecting box (20) through collecting locking bolts (25), the outer side of the collecting box (20) is provided with at least 2 collecting lifting adjusting holes (26) matched with the collecting locking bolts (25) along the vertical direction, and the upper part of the collecting lifting blocks (24) is provided with collecting stop blocks (27) matched with the lower surface of the horizontal part of the material sucking pipe (18).
Furthermore, the collecting block (27) is composed of two plates forming an acute angle, one plate is vertically arranged, the other plate is obliquely arranged and is connected with the collecting lifting block (24), and the outer side of the plate vertically arranged on the collecting block (27) is flush with the inner side of the collecting box (20).
Furthermore, the upper part of the other scraping and collecting half cylinder (14) is fixedly connected with an air blowing pipe (16) communicated with the other scraping and collecting half cylinder, the matched parts of the air blowing pipe (16) and the material suction pipe (18) and the scraping and collecting half cylinder (14) are symmetrical about the center of the negative pole rod (4), and the air blowing pipe (16) is connected with an air blowing pump (17).
Further, the movable device comprises a left movable block (13) and a right movable block (10) which are arranged at the upper parts of the left and right scraping and collecting half cylinders, the left movable block (13) is matched with a linkage rod (12) at the right side of the right movable block (10) through a linkage block (11), the middle part of the opposite side of the right movable block (10) and the linkage block (11) is provided with a scraping limit groove (8), a scraping reset spring (9) is arranged between the upper part and the lower part, a scraping opening and closing rotating block (7) is matched between the two scraping limit grooves (8), the scraping opening and closing rotating block (7) is oval, the center of the lower surface of the material scraping lifting cylinder is connected with a material scraping lifting cylinder (62), the lower part of the material scraping lifting cylinder (62) is connected with a material scraping rotating motor (61) coaxial with the material scraping lifting cylinder, the scraping rotary motor (61) is arranged on a collecting rack (5) arranged on the electrolytic tank (1).
Furthermore, the left movable block (13) is higher than the right movable block (10), and the upper part of the right movable block (10) is provided with a linkage limiting groove (28) matched with the linkage rod (12).
The invention has the beneficial effects that:
1. the evaporator is arranged at the lower part of the electrolytic tank, the material leakage port is formed in the lower part of the electrolytic tank, the material leakage lifting block which can lift is matched in the material leakage hole, the solid-liquid mixture in the electrolytic tank is controlled to flow into the evaporator through the lifting of the material leakage lifting block, the operation is convenient, the electrolyte replacement operation of the electrolytic tank can be simplified, the continuous normal work of the electrolytic tank is ensured, the separation efficiency is improved, and the electrolysis efficiency of the electrolytic tank is also improved.
2. The structural design of evaporimeter is ingenious, can be convenient for take out of zone of heating and pour out the remaining metal powder on the protective layer, also easy to assemble simultaneously, and condensation collecting box intercommunication has the exhaust tube, can make it become vacuum state before work, can make better entering into the condensation collecting box of steam collect in the case.
3. Be provided with two scrapes that can open and shut of negative pole stick complex and collect half a section of thick bamboo, cooperation elevating gear can realize that the metal powder on the negative pole stick scrapes the material to set up on the upper portion of scraping and collecting half a section of thick bamboo and inhale the material device, can realize the metal powder automatic collection on the negative pole stick, can not influence the normal electrolysis of negative pole stick simultaneously, can avoid too much metal powder and electrolyte to mix, avoid appearing the condition that the mouth that leaks blockked up.
4. The design of scraping and collecting the lateral part of half a section of thick bamboo and upper portion sealing strip can avoid gathering the in-process metal powder of material and scattering from scraping the upper portion and the lateral part of collecting half a section of thick bamboo at the material of inhaling, and the lower part is unsealed can make things convenient for the outflow of electrolyte, and then improves the dryness fraction of inhaling material in-process metal powder.
5. Discharge gate, keep off the material net and collect the cooperation design of box, can make things convenient for the collection of metal powder, avoid inhaling the in-process of material the condition that the effluvium appears, can also prevent simultaneously that metal powder from entering into to inhale the jam that the material air pump caused the pump.
6. The design of the collecting lifting block and the collecting stop block on the collecting box can ensure that the metal powder can completely fall into the collecting box.
7. The structural design of collecting the dog, for the dog of vertical shape, can avoid the box upper wall to appear metal powder, for L shape or the dog of type of falling the concave, can reduce and collect the dog and inhale the area of contact of material pipe lower part, and then avoid the clearance that the surface unevenness caused, also can ensure to collect simultaneously that the locking bolt can be accurate insert collect lift adjustment downthehole.
8. The design of gas blow pipe and gas blowing pump can be weathered the metal powder in the scraping collecting cylinder, can also blow up metal powder simultaneously, and the suction of material pipe and suction air pump is inhaled in the cooperation.
9. The movable device is ingenious in design, the movable blocks move in the opposite direction by adopting the oval material scraping, opening and closing rotating blocks which can rotate, meanwhile, the movable blocks can also be used as linkage parts for driving the left movable blocks and the right movable blocks to lift, the left movable blocks and the right movable blocks can lift synchronously, and the material scraping effect is greatly ensured.
10. The design of interlock spacing groove can avoid controlling the movable block and appear the condition of front and back dislocation when the activity, and then further ensure to scrape the material effect of scraping of material collection half a section of thick bamboo.
Drawings
FIG. 1 is a schematic view showing the construction of an electrolytic manufacturing apparatus capable of collecting metal powder.
Fig. 2 is a partially enlarged view of a in fig. 1.
Fig. 3 is a partially enlarged view of B in fig. 1.
Fig. 4 is a partially enlarged view of C in fig. 3.
Fig. 5 is a plan view of the scraper collection portion. .
Fig. 6 is a cross-sectional view of D-D in fig. 5.
Fig. 7 is a partial enlarged view of F in fig. 6.
The text labels shown in the figures are represented as: 1. an electrolytic tank; 2. an electrolytic rack; 3. a positive electrode bar; 4. a negative electrode bar; 5. a collection rack; 7. scraping, opening and closing the rotary block; 8. scraping a limiting groove; 9. a scraping return spring; 10. a right movable block; 11. a linkage block; 12. a linkage rod; 13. a left movable block; 14. a scraping and collecting half cylinder; 15. a sealing strip; 16. an air blowing pipe; 17. an air blower; 18. a material suction pipe; 19. a material suction air pump; 20. a collection box; 21. a box body limiting block; 22. a discharge port; 23. a material blocking net; 24. collecting the lifting block; 25. collecting the locking bolts; 26. collecting lifting adjusting holes; 27. collecting a stop block; 28. a linkage limiting groove; 31. an evaporation cylinder; 32. an evaporation groove seat; 33. a protective sleeve; 34. an electric heating block; 35. a sealing block; 36. a steam outlet; 37. a condensation collection box; 38. an air exhaust pipe; 39. a sealing cover; 40. a material leakage lifting block; 41. a leaking lifting column; 42. a material leaking lifting seat; 43. a material leakage lifting cylinder; 44. a material leaking hole; 61. a scraping rotary motor; 62. scrape material lift cylinder.
Detailed Description
The following detailed description of the present invention is given for the purpose of better understanding technical solutions of the present invention by those skilled in the art, and the present description is only exemplary and explanatory and should not be construed as limiting the scope of the present invention in any way.
As shown in fig. 1 to 7, the specific structure of the present invention is: an electrolytic preparation device capable of collecting metal powder comprises an electrolytic tank 1 and an electrolytic frame 2, the electrolytic frame 2 is provided with a positive pole rod 3 and a negative pole rod 4 which are connected with a power supply and vertically penetrate into the electrolytic tank 1, the lower part of the electrolytic tank 1 is provided with an evaporator, and the center of the bottom of the electrolytic tank 1 is provided with a material leakage opening, a material leakage lifting block 40 which is in sealing fit with the material leakage opening is arranged in the material leakage opening, the lower part of the material leakage lifting block 40 is connected with a material leakage lifting column 41, a material leakage lifting seat 42 is connected below the material leakage lifting column 41, the material leaking lifting seat 42 is connected with a material leaking lifting cylinder 43 arranged at the lower part of the electrolytic tank 1, the height of the inner bottom surface of the electrolytic tank 1 is gradually reduced from two sides to the center, the middle part of the material leaking lifting seat is provided with material leaking holes 44 which are distributed in an annular shape, and the two sides are inclined planes which incline downwards.
Preferably, the evaporator comprises an evaporation cylinder 31 arranged at the lower part of the electrolytic tank 1, the lower part of the evaporation cylinder 31 has no bottom plate and is arranged in an evaporation groove seat 32, a protective sleeve 33 is fixedly connected in the evaporation groove seat 32, an electric heating block 34 is arranged in the protective sleeve 33, the upper part of the protective sleeve 33 is a heat conducting block insulating block, the lower part of the protective sleeve 33 is a heat insulating block, a sealing block 35 is embedded at the butt joint part of the evaporation cylinder 31 and the protective sleeve 33 of the evaporation groove seat 32, a steam outlet 36 is arranged on the side wall of the evaporation cylinder 31, the steam outlet 36 is connected with a condensation collection box 37, the condensation collection box 37 is communicated with an extraction pipe 38, and the extraction pipe 38 is matched with a sealing cover 39.
Preferably, the two sides of the negative electrode rod 4 are provided with the material scraping and collecting half cylinders 14 which are matched with each other, the matched positions of the material scraping and collecting half cylinders 14 and the negative electrode rod 4 are provided with semicircular openings, the outer side of each material scraping and collecting half cylinder 14 is connected with a movable device which can move left and right and lift, the upper part of each material scraping and collecting half cylinder 14 is fixedly connected with a material suction pipe 18 communicated with the upper part of each material scraping and collecting half cylinder, each material suction pipe 18 is connected with a material suction air pump 19, and each material scraping and collecting half cylinder 14 is an insulating cylinder.
Preferably, the matching parts of the upper plate and the side plate of the two scraper collecting half cylinders 14 are provided with sealing strips 15.
Preferably, the material suction pipe 18 is an L-shaped pipe, a material discharge port 22 is formed in the lower middle portion of the horizontal portion of the material suction pipe 18, an inclined material blocking net 23 is arranged on one side, close to the material suction air pump 19, of the material discharge port 22 in the material suction pipe 18, a collection box 20 is matched with the lower portion of the material discharge port 22, and box body limiting blocks 21 matched with the left side and the right side of the collection box 20 are arranged on the scraping and collecting half cylinder 14.
Preferably, the height of the collecting box 20 is lower than the lower surface of the horizontal part of the material suction pipe 18, the front and rear outer sides of the collecting box 20 are provided with collecting lifting blocks 24, the collecting lifting blocks 24 are locked on the outer side of the collecting box 20 through collecting locking bolts 25, the outer side of the collecting box 20 is provided with at least 2 collecting lifting adjusting holes 26 matched with the collecting locking bolts 25 along the vertical direction, and the upper part of the collecting lifting blocks 24 is provided with collecting stops 27 matched with the lower surface of the horizontal part of the material suction pipe 18.
Preferably, the collecting block 27 is formed of two plates having an acute angle, one of the plates is vertically disposed, the other plate is obliquely disposed and connected to the collecting lifter 24, and the outer side of the plate where the collecting block 27 is vertically disposed is flush with the inner side of the collecting box 20.
Preferably, the upper part of the other scraping and collecting half cylinder 14 is fixedly connected with an air blowing pipe 16 communicated with the other scraping and collecting half cylinder, the matched parts of the air blowing pipe 16 and the material suction pipe 18 with the scraping and collecting half cylinder 14 are symmetrical about the center of the negative pole rod 4, and the air blowing pipe 16 is connected with an air blowing pump 17.
Preferably, the head includes left movable block 13 and right movable block 10 on the left and right scraping material collection half section of thick bamboo upper portion, left movable block 13 pass through the trace 12 cooperation on trace 11 and right movable block 10 right side, right movable block 10 and trace 11 middle part of inclining in opposite directions be provided with scrape and be provided with between material spacing groove 8, upper portion and the lower part and scrape material reset spring 9, two scrape the cooperation of material spacing groove 8 between have and scrape the material commentaries on classics piece 7 that opens and shuts, scrape the material and open and shut commentaries on classics piece 7 and be oval-shaped, its lower surface center is connected with scrapes material lift cylinder 62, the sub-unit connection of scraping material lift cylinder 62 have rather than the coaxial line scrape material rotation motor 61, scrape material rotation motor 61 set up on collection frame 5 of installation on electrolytic tank 1.
Preferably, the left movable block 13 is higher than the right movable block 10, and the upper portion of the right movable block 10 is provided with a linkage limiting groove 28 which is matched with the linkage rod 12.
When the device is used, the device is assembled firstly, then the air exhaust sealing cover 39 is taken down, the air exhaust pipe is connected to the air exhaust device, the air exhaust sealing cover 39 is covered after the air exhaust device is vacuumized, then the power supply is controlled to be opposite to the anode rod 3 and the cathode rod 4, the electrolytic reaction is carried out in the electrolytic box 1, metal positive ions can be concentrated at the cathode rod, further the metal positive ions can obtain electrons to form a metal lamination, anions such as chloride ions and the like can lose the electrons to form chlorine, then the scraping opening and closing rotating block 7 is driven to rotate by the scraping rotating motor 61, the elliptic long shaft end of the scraping opening and closing rotating block props against the right movable block 10 and the linkage block 11, further the left movable block and the right movable block can move in opposite directions, further the left and right collecting scraping semi-cylinders can move in opposite directions to form an integral scraping collecting cylinder, then the scraping opening and closing rotating block 7 is driven to lift by the scraping lifting, the lower part of the scraping collecting cylinder scrapes off the metal lamination attached to the cathode rod 4 to form powder, liquid flows out from the lower part of the scraping collecting cylinder along with the separation of the scraping collecting cylinder from an electrolyte level, then the liquid is started by a blowing pump 17, gas is blown into the scraping collecting cylinder from a blowing pipe 16, the metal powder is blown up while being dried, then the liquid is started by a sucking air pump 19, the metal powder in the scraping collecting cylinder is sucked into a sucking pipe 18, then the metal powder is intercepted by a material blocking net 23 and falls into a collecting box 20 from a discharge port 22 to finish the collection, then the movable device is returned to the original position, subsequent electrolytic reaction and the collection of the metal powder are continued, when the metal powder in the collecting box is fully collected, the collecting lifting block 24 is descended by loosening the collecting locking bolt 25, and then the collecting locking bolt 25 is used for locking the collecting lifting adjusting hole 26, then take the collection box away, go on to a certain extent when the electrolysis, metal ion in the electrolyte can all be electrolyzed into metal powder basically, later drive hourglass material lift seat 42 through leaking material lift cylinder 43 and rise, and then drive hourglass material elevator block 40 and rise and make its and hourglass material mouth separation, electrolyte and metal powder wherein can fall from the hourglass material mouth and enter into the upper portion of protective sheath 33, heat and the heat conduction on protective sheath 33 upper portion through heating block 34 in the protective sheath 33, make it become steam and inhale in the condensation collection box 37, the steam that enters into in the condensation collection box 37 touches the collection tank wall and can become the liquid form again, and metal powder can remain on protective sheath 33.
It should be noted that, in this document, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
The principles and embodiments of the present invention are explained herein using specific examples, which are presented only to assist in understanding the method and its core concepts of the present invention. The foregoing is only a preferred embodiment of the present invention, and it should be noted that there are objectively infinite specific structures due to the limited character expressions, and it will be apparent to those skilled in the art that a plurality of modifications, decorations or changes may be made without departing from the principle of the present invention, and the technical features described above may be combined in a suitable manner; such modifications, variations, combinations, or adaptations of the invention using its spirit and scope, as defined by the claims, may be directed to other uses and embodiments.
Claims (5)
1. An electrolytic preparation device capable of collecting metal powder comprises an electrolytic tank (1) and an electrolytic frame (2), wherein the electrolytic frame (2) is provided with a positive electrode rod (3) and a negative electrode rod (4) which are connected to a power supply and vertically penetrate into the electrolytic tank (1), and is characterized in that two sides of the negative electrode rod (4) are provided with scraping and collecting half cylinders (14) which are matched with each other, the matched part of each scraping and collecting half cylinder (14) and the negative electrode rod (4) is provided with a semicircular opening, the outer side of each scraping and collecting half cylinder (14) is connected with a movable device which can move left and right and lift, the upper part of one scraping and collecting half cylinder (14) is fixedly connected with a suction pipe (18) communicated with the suction pipe (18) which is connected with a suction air pump (19), the scraping and collecting half cylinders (14) are insulating cylinders, and sealing strips (15) are arranged at the matched parts of the upper plate and the side plates of the two scraping and collecting half cylinders (14), the material suction pipe (18) is an L-shaped pipe, a discharge port (22) is formed in the lower portion of the middle of the horizontal portion of the material suction pipe, an inclined material blocking net (23) is arranged on one side, close to a material suction air pump (19), of the discharge port (22) in the material suction pipe (18), a collection box (20) is matched with the lower portion of the discharge port (22), box body limiting blocks (21) matched with the left side and the right side of the collection box (20) are arranged on the material scraping collection half cylinder (14), the movable device comprises a left movable block (13) and a right movable block (10) which are arranged on the upper portion of the left material scraping collection half cylinder and are matched with a linkage rod (12) on the right side of the right movable block (10) through a linkage block (11), a material scraping limiting groove (8) is formed in the middle of the opposite side of the right movable block (10) and the linkage block (11), and a material scraping reset spring (9) is arranged between the upper, two scrape and to have the material to scrape between material spacing groove (8) and open and shut commentaries on classics piece (7), scrape the material and open and shut commentaries on classics piece (7) and be oval, its lower surface center is connected with scrapes material lift cylinder (62), the sub-unit connection of scraping material lift cylinder (62) have rather than the scraping of coaxial line material rotation motor (61), scrape material rotation motor (61) set up on collection frame (5) of installation on electrolytic tank (1).
2. The electrolytic preparation device capable of collecting metal powder according to claim 1, wherein the collecting box (20) is lower than the lower surface of the horizontal part of the suction pipe (18), the collecting lifting blocks (24) are arranged on the front and rear outer sides of the collecting box (20), the collecting lifting blocks (24) are locked on the outer sides of the collecting box (20) through collecting locking bolts (25), the outer sides of the collecting box (20) are provided with not less than 2 collecting lifting adjusting holes (26) matched with the collecting locking bolts (25) in the vertical direction, and the upper part of the collecting lifting blocks (24) is provided with collecting stoppers (27) matched with the lower surface of the horizontal part of the suction pipe (18).
3. An electrolytic preparation device capable of collecting metal powder according to claim 2, characterized in that said collecting stopper (27) is composed of two plates at an acute angle, one of which is vertically disposed and the other is obliquely disposed and connected to the collecting elevating block (24), and the outer side of the plate where the collecting stopper (27) is vertically disposed is flush with the inner side of the collecting box (20).
4. The electrolytic preparation device capable of collecting metal powder according to claim 1, wherein the upper part of the other scraping and collecting half cylinder (14) is fixedly connected with an air blowing pipe (16) communicated with the other scraping and collecting half cylinder, the matching parts of the air blowing pipe (16) and the material suction pipe (18) with the scraping and collecting half cylinder (14) are symmetrical about the center of the cathode bar (4), and the air blowing pipe (16) is connected with an air blowing pump (17).
5. The electrolytic preparation device capable of collecting metal powder as claimed in claim 1, wherein the left movable block (13) is higher than the right movable block (10), and the upper part of the right movable block (10) is provided with a linkage limiting groove (28) matched with the linkage rod (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711335103.3A CN108048879B (en) | 2017-12-14 | 2017-12-14 | Electrolytic preparation device capable of collecting metal powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711335103.3A CN108048879B (en) | 2017-12-14 | 2017-12-14 | Electrolytic preparation device capable of collecting metal powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN108048879A CN108048879A (en) | 2018-05-18 |
| CN108048879B true CN108048879B (en) | 2019-12-06 |
Family
ID=62132165
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711335103.3A Active CN108048879B (en) | 2017-12-14 | 2017-12-14 | Electrolytic preparation device capable of collecting metal powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108048879B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110773304A (en) * | 2019-11-14 | 2020-02-11 | 迟人源 | Grinder of polymer chemical material granule |
| CN111841352B (en) * | 2020-07-15 | 2022-03-15 | 武汉裕大华纺织有限公司 | Automatic size mixing system |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101363126A (en) * | 2008-09-05 | 2009-02-11 | 江苏技术师范学院 | Apparatus for preparing nanometer metal powder |
| CN203442189U (en) * | 2013-07-04 | 2014-02-19 | 青岛日辰食品有限公司 | Piston type kettle-bottom discharge valve |
| CN204999987U (en) * | 2015-10-09 | 2016-01-27 | 贵溪凌云铜业有限公司 | Equipment of preparing of single nickel salt crystalline solid |
| CN205774828U (en) * | 2016-05-17 | 2016-12-07 | 广东金业贵金属有限公司 | A kind of silver refining electrolyzing cell |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU1219678A1 (en) * | 1984-10-18 | 1986-03-23 | Научно-производственное объединение "Тулачермет" | Electrolyzer for producing metal powders |
| CN105177635B (en) * | 2015-09-12 | 2017-08-25 | 北京工业大学 | A kind of continuous system and method for preparing tungsten powder |
-
2017
- 2017-12-14 CN CN201711335103.3A patent/CN108048879B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101363126A (en) * | 2008-09-05 | 2009-02-11 | 江苏技术师范学院 | Apparatus for preparing nanometer metal powder |
| CN203442189U (en) * | 2013-07-04 | 2014-02-19 | 青岛日辰食品有限公司 | Piston type kettle-bottom discharge valve |
| CN204999987U (en) * | 2015-10-09 | 2016-01-27 | 贵溪凌云铜业有限公司 | Equipment of preparing of single nickel salt crystalline solid |
| CN205774828U (en) * | 2016-05-17 | 2016-12-07 | 广东金业贵金属有限公司 | A kind of silver refining electrolyzing cell |
Also Published As
| Publication number | Publication date |
|---|---|
| CN108048879A (en) | 2018-05-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108048879B (en) | Electrolytic preparation device capable of collecting metal powder | |
| CN110000394B (en) | Metal nano powder production system | |
| CN108048881B (en) | A kind of collecting mechanism for electrolysis production metal powder | |
| CN205443473U (en) | Electrolysis tombarthite smoke and dust gas clean system | |
| CN106679442A (en) | Smelting furnace flue gas treatment device with raw material preheating function | |
| CN106267945A (en) | The circulation filter of feed liquid is produced for filtering kwan-yin bean curd | |
| CN211739087U (en) | Multi-edge composite fixed fire grate segment | |
| CN209630824U (en) | A kind of high efficiency Entecavir Jet Mill | |
| CN110630314B (en) | Adsorption dust suppression and separation device for mine engineering construction | |
| CN210173907U (en) | Dust removal device for concrete bin | |
| CN206013896U (en) | A kind of cigarette machine wind-power cut tobacco feeding device with multi-group filter net | |
| CN107858709A (en) | A kind of fused salt electrolysis apparatus for preparing metal mixed powder | |
| CN110030796A (en) | A kind of environmental protection granular food drying agitating device | |
| CN210030946U (en) | Electroplating production line material collecting device | |
| CN209555322U (en) | A kind of novel molybdenum extraction equipment | |
| CN216500081U (en) | Scraper device in centrifugal machine | |
| CN214287056U (en) | Traditional chinese medicine draws concentrated machine | |
| CN210157816U (en) | Excrement and urine collection device for livestock-raising | |
| CN110528030A (en) | A kind of Rare Earth Electrolysis device | |
| CN113481543B (en) | Integral forming smoke exhausting device and method for cathode of electrolytic tank | |
| CN212857752U (en) | Long-life tapping runner skimmer | |
| CN104174589B (en) | A kind of refuse classification Packing Machine | |
| CN219355408U (en) | Efficient extraction and separation equipment for water-containing engineering sludge | |
| CN218395026U (en) | Cleaning equipment for ore mining | |
| CN212147260U (en) | Automatic feeding device of foam pre-foaming machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200603 Address after: 211223 mingjue Industrial Park, Shiqiu street, Lishui District, Nanjing City, Jiangsu Province Patentee after: Nanjing Wansheng Machine Tool Co.,Ltd. Address before: 523000 Guangdong province Dongguan City Songshan Lake Science and Technology Industrial Park University Road No. 1 Patentee before: DONGGUAN University OF TECHNOLOGY |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210408 Address after: 210000 Airport Road, Lishui Economic Development Zone, Nanjing City, Jiangsu Province Patentee after: NANJING LIYUAN JINXIN MAGNETIC MATERIAL TECHNOLOGY Co.,Ltd. Address before: 211223 mingjue Industrial Park, Shiqiu street, Lishui District, Nanjing City, Jiangsu Province Patentee before: Nanjing Wansheng Machine Tool Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220424 Address after: 211219 Honglan Town Industrial Concentration Zone, Lishui District, Nanjing City, Jiangsu Province Patentee after: Nanjing Meisen Intelligent Equipment Co.,Ltd. Address before: 210000 Airport Road, Lishui Economic Development Zone, Nanjing City, Jiangsu Province Patentee before: NANJING LIYUAN JINXIN MAGNETIC MATERIAL TECHNOLOGY CO.,LTD. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230116 Address after: 211225 Mingjue Industrial Park, Shiqiu Street, Lishui District, Nanjing, Jiangsu Province Patentee after: Jiangsu Dafeng Machinery Technology Co.,Ltd. Address before: 211219 Honglan Town Industrial Concentration Zone, Lishui District, Nanjing City, Jiangsu Province Patentee before: Nanjing Meisen Intelligent Equipment Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230831 Address after: Honglan Xiaomao Mountain Natural Village, Lishui District, Nanjing City, Jiangsu Province, 210000 Patentee after: Nanjing Guantai Roller Industry Co.,Ltd. Address before: 211225 Mingjue Industrial Park, Shiqiu Street, Lishui District, Nanjing, Jiangsu Province Patentee before: Jiangsu Dafeng Machinery Technology Co.,Ltd. |