CN108007729A - The equipment for making atmospheric sampling filter membrane attaching particles thing float again - Google Patents
The equipment for making atmospheric sampling filter membrane attaching particles thing float again Download PDFInfo
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- CN108007729A CN108007729A CN201711437341.5A CN201711437341A CN108007729A CN 108007729 A CN108007729 A CN 108007729A CN 201711437341 A CN201711437341 A CN 201711437341A CN 108007729 A CN108007729 A CN 108007729A
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- rinse bath
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- water content
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- 239000012528 membrane Substances 0.000 title claims abstract description 53
- 238000005070 sampling Methods 0.000 title claims abstract description 52
- 239000002245 particle Substances 0.000 title claims abstract description 30
- 239000003665 fog water Substances 0.000 claims abstract description 51
- 238000004140 cleaning Methods 0.000 claims abstract description 28
- 239000004065 semiconductor Substances 0.000 claims abstract description 17
- 230000003028 elevating effect Effects 0.000 claims description 33
- 238000004506 ultrasonic cleaning Methods 0.000 claims description 32
- 238000007789 sealing Methods 0.000 claims description 12
- 238000010438 heat treatment Methods 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000741 silica gel Substances 0.000 claims description 7
- 229910002027 silica gel Inorganic materials 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 239000004020 conductor Substances 0.000 claims description 5
- 238000000889 atomisation Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims 2
- 239000013618 particulate matter Substances 0.000 abstract description 18
- 238000011173 large scale experimental method Methods 0.000 abstract description 10
- 239000003344 environmental pollutant Substances 0.000 description 14
- 231100000719 pollutant Toxicity 0.000 description 14
- 238000000034 method Methods 0.000 description 10
- 239000002250 absorbent Substances 0.000 description 9
- 230000002745 absorbent Effects 0.000 description 9
- 239000000523 sample Substances 0.000 description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 239000003463 adsorbent Substances 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 239000003595 mist Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- FAXIJTUDSBIMHY-UHFFFAOYSA-N diethoxy-(2-ethylsulfanylethoxy)-sulfanylidene-$l^{5}-phosphane;1-diethoxyphosphorylsulfanyl-2-ethylsulfanylethane Chemical compound CCOP(=O)(OCC)SCCSCC.CCOP(=S)(OCC)OCCSCC FAXIJTUDSBIMHY-UHFFFAOYSA-N 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- GCNLQHANGFOQKY-UHFFFAOYSA-N [C+4].[O-2].[O-2].[Ti+4] Chemical compound [C+4].[O-2].[O-2].[Ti+4] GCNLQHANGFOQKY-UHFFFAOYSA-N 0.000 description 1
- DPQMPFBUHULHSC-UHFFFAOYSA-J [Na].[Hg](Cl)(Cl)(Cl)Cl Chemical compound [Na].[Hg](Cl)(Cl)(Cl)Cl DPQMPFBUHULHSC-UHFFFAOYSA-J 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000003682 fluorination reaction Methods 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011490 mineral wool Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 230000008450 motivation Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003987 organophosphate pesticide Substances 0.000 description 1
- BULVZWIRKLYCBC-UHFFFAOYSA-N phorate Chemical compound CCOP(=S)(OCC)SCSCC BULVZWIRKLYCBC-UHFFFAOYSA-N 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2273—Atmospheric sampling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a kind of equipment for making atmospheric sampling filter membrane attaching particles thing float again, including:Reservoir, rinse bath and fog water content, some mutually independent sub- rinse baths are equipped with rinse bath, cleaning solution is equiped with reservoir, and reservoir is connected with every sub- rinse bath, every sub- rinse bath is connected with fog water content, fog water content connects large-scale experiment instrument, semiconductor chilling plate and electromagnet group are equipped with outside fog water content, electromagnet group is made of a pair of of electromagnet, electromagnet group is coated on outside fog water content, and a holding tank is also equipped with electromagnet group, semiconductor chilling plate is contained in holding tank, electromagnet group holds fog water content tightly when energized, semiconductor chilling plate heats fog water content.Thoroughly cleaning, the equipment for making atmospheric sampling filter membrane attaching particles thing float again simple in structure, the degree of automation is high can be carried out to the particulate matter on filter membrane the invention discloses a kind of.
Description
Technical field
The present invention relates to Atmospheric particulates sampling technique field, more particularly to a kind of particulate matter on filter membrane can be carried out
What thoroughly cleaning, simple in structure, the degree of automation were high makes the equipment that atmospheric sampling filter membrane attaching particles thing floats again.
Background technology
Atmospheric sampling is the process of pollutant sample or contaminated air sample in collection air.Spot sampling method has two
Class:One kind is large quantity of air is played the relatively low enriching pollutants of concentration in air by liquid-absorbant or solid absorbent
Come, such as degassing method, filter membrane method.Another kind of is with air of container (the vial, polybag etc.) collection containing pollutant.The former surveys
What is obtained is the mean concentration of pollutant in air in the sampling time;What the latter measured is instantaneous concentration or average dense in the short time
Degree.The mode of sampling should be depending on the purpose of sampling and field condition.Institute's sample thief should be representative.Sampling efficiency is high,
Operation must be easy, and is convenient for subsequent analysis measure, to obtain the master data of reliable atmosphere pollution.Gather air
The sample of middle pollutant or the sample of contaminated air, to obtain the master data of atmosphere pollution.
Atmospheric sampling is the important step of atmosphere environment supervision, and the reliable sexual intercourse for monitoring data is very big.Collection is big
The method of gas sample product, mainly there is two classes:One kind is to make large quantity of air by liquid-absorbant or solid absorbent, to absorb or hinder
Pollutant is stayed, the relatively low enriching pollutants of concentration in original air are got up, such as degassing method, filter membrane method.Measured with this kind of method
The result is that in the sampling time in air pollutant mean concentration.Another kind of is to use container (vial, polybag, rubber ball
Courage, syringe etc.) air of the collection containing pollutant.This kind of method is suitable for following situations:In air the concentration of pollutant compared with
It is high;Or the sensitivity of assay method is higher;It is not easy by the polluted gas and steaming of liquid-absorbant absorption or solid absorbent absorption
Vapour.The result measured with this method is the instantaneous concentration of pollutant or the mean concentration in the short time in air.In addition, also low temperature
Freezing, available for collection escaping gas and steam, such as alkyl lead.Liquid-absorbant in sampler is mainly used for absorbing gas
State and steam-like material.Common absorbent has:Water, compound water solution, organic solvent etc..Absorbent must be able to and pollutant
Quickly chemical reaction occurs or pollutant can be promptly dissolved, and is convenient for analysis operation.Such as the fluorination in air
Hydrogen, hydrogen chloride are with water as absorbent;Sulfur dioxide can be used as absorbent by the use of tetrachloro mercury sodium;Thimet (3911), demeton
(1059) etc. organophosphorus pesticide can be used as absorbent etc. by the use of 5% methanol.Solid absorbent has granular adsorbent and threadiness to inhale
Attached dose two kinds.Common granular adsorbent has silica gel, unglazed pottery etc., the sampling for gaseous state, steam-like and particulate matter.Fiber
Shape adsorbent has filter paper, filter membrane, absorbent cotton, mineral wool etc., and suction-operated is mainly physical detention, for gathering particle
Thing.Sometimes adsorbent makes pollutant that chemical action occur with it and adsorbed first with certain chemical reagent impregnation, main to use
In collection gaseous state or steam-like pollutant.
Common outside atmosphere sample devices, it is small, easily carry, but the performance ratio of its detection is relatively limited, it is difficult to do
Accurately detect and analyze to particulate matter progress, and large-scale experimental facilities is then general bulky, is not easy to move, often puts
It is disposed within.So if selection filter membrane method, then need to clean out the particulate matter being accumulated on filter membrane from filter membrane, then will
Particulate matter reenters large-scale experiment instrument and is tested and analyzed.
Therefore, there is an urgent need for it is a kind of can on filter membrane particulate matter carry out thoroughly cleaning, simple in structure, the degree of automation is high
The equipment for making atmospheric sampling filter membrane attaching particles thing float again.
The content of the invention
The object of the present invention is to provide it is a kind of can on filter membrane particulate matter carry out thoroughly cleaning, it is simple in structure, automatic
Change degree it is high make the equipment that atmospheric sampling filter membrane attaching particles thing floats again.
To achieve these goals, technical solution provided by the invention is:There is provided one kind makes the attachment of atmospheric sampling filter membrane
The equipment that grain thing floats again, including:Reservoir, rinse bath and fog water content, the rinse bath is interior to be equipped with some mutually independent sons
Rinse bath, cleaning solution is equiped with the reservoir, and the reservoir is connected with each sub- rinse bath, the cleaning
Groove is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, and Atmospheric particulates sampling membrane is fixed on described super
On sound wave cleaning equipment, Atmospheric particulates sampling membrane each sub- rinse bath as the ultrasonic cleaning apparatus enters,
Each sub- rinse bath is connected with the fog water content, the fog water content connection large-scale experiment instrument, outside the fog water content
Equipped with semiconductor chilling plate and electromagnet group, the electromagnet that the electromagnet group attracts each other when being powered by a pair forms, described
Electromagnet group is coated on outside the fog water content, and a holding tank, the semiconductor refrigerating are also equipped with the electromagnet group
Piece is contained in the holding tank, and the electromagnet group holds the fog water content tightly when energized, and the semiconductor chilling plate is to institute
Fog water content is stated to be heated.
Sliding equipment is further included, the sliding equipment is arranged on above the rinse bath, and can be above every sub- rinse bath
Mobile, the ultrasonic cleaning apparatus is arranged on the sliding equipment and can enter in every sub- rinse bath.
The top both sides of the rinse bath are respectively equipped with two guide rails laid along the sub- rinse bath orientation, the cunning
Motivation structure includes stepper motor, leading screw, portal frame, sliding block, and the ultrasonic cleaning apparatus is arranged on the portal frame, the dragon
Door frame is slidably arranged on the guide rail by the sliding block, and the stepper motor drives the portal frame to exist by the leading screw
Moved back and forth on the guide rail.
Elevating mechanism is further included, the elevating mechanism is arranged on the portal frame, and the elevating mechanism is used to perform described
The lifting of ultrasonic cleaning apparatus or dropping action.
The portal frame includes crossbeam and pillar, and the pillar is equipped with the elongated slot of vertical direction, the elevating mechanism edge
The elongated slot is lifted or dropping action.
The elevating mechanism includes two installing plates being oppositely arranged, and it is clear that each installing plate is respectively equipped with the ultrasonic wave
Equipment is washed, and Atmospheric particulates sampling membrane is arranged between two ultrasonic cleaning apparatus.
Before each sub- rinse bath is connected with the fog water content, a dashpot is introduced into, the dashpot is arranged on institute
State bottom of rinse bath.
The atomization trench bottom sets atomizing piece.
Solenoid valve I, the dashpot and the atomization are respectively equipped between the reservoir and each sub- rinse bath
Solenoid valve II is equipped between groove.
Further include control device, the ultrasonic cleaning apparatus, sliding equipment, elevating mechanism, atomizing piece, conductor refrigeration
Piece, solenoid valve I and solenoid valve II are connected with the control device, the control device control that the sliding equipment slides away from
From controlling the elevating mechanism to carry the ultrasonic cleaning apparatus lifting or landing, control the ultrasonic cleaning apparatus
Working frequency and run time, control starting or stoping for the atomizing piece, control the heating power of the conductor cooling piece,
The control each solenoid valve I and solenoid valve II are turned on and off.
Temperature sensor is additionally provided with the fog water content, the temperature sensor is connected with the control device and will detection
To the fog water content in temperature information feed back to the control device, the control device is according to the temperature sensor institute
The temperature information of feedback controls the heating power of the semiconductor chilling plate.
The entrance for allowing the elevating mechanism to enter, and every sub- rinse bath are equipped with above each sub- rinse bath
Interior to be additionally provided with sealing plate at entrance underface, described sealing plate one end is installed in the shaft with resetting spring,
When the elevating mechanism enters the sub- rinse bath by the entrance, the sealing plate can be opened by one angle of rotation,
And when the elevating mechanism leaves the sub- rinse bath by the entrance, the sealing plate by the resetting spring again
The entrance is sealed.
The elevating mechanism has further included a level board, and two installing plates are lifted on below the level board, and described
Level board surrounding is equipped with silica gel boss, and when the elevating mechanism enters the sub- rinse bath, the silica gel boss is to described
Entrance is in interference fit and the entrance is sealed.
Compared with prior art, in due to making the equipment that atmospheric sampling filter membrane attaching particles thing floats again in the present invention, institute
State and be equipped with some mutually independent sub- rinse baths in rinse bath, be equiped with cleaning solution in the reservoir, and the reservoir and
Each sub- rinse bath connects, and the rinse bath, which is additionally provided with, to be set into the ultrasonic cleaning of each sub- rinse bath
Standby, each sub- rinse bath is connected with the fog water content, and the fog water content connects large-scale experiment instrument.Therefore, air
Grain thing sampling membrane can be cleaned in different sub- rinse baths, achieve the purpose that completely to clean up particulate matter.
It will be become more fully apparent by following description and with reference to attached drawing, the present invention, these attached drawings are used to explain the present invention
Embodiment.
Brief description of the drawings
Fig. 1 is the module diagram of the equipment of the invention for making atmospheric sampling filter membrane attaching particles thing float again.
Fig. 2 is the schematic diagram of the rinse bath of the equipment for making atmospheric sampling filter membrane attaching particles thing float again as shown in Figure 1.
Embodiment
The embodiment of the present invention described referring now to attached drawing, similar element numbers represent similar element in attached drawing.Such as
It is upper described, as shown in Figure 1, 2, the equipment 100 provided in an embodiment of the present invention for making atmospheric sampling filter membrane attaching particles thing float again,
Including:Reservoir 1, rinse bath 2 and fog water content 3, be equipped with the rinse bath 2 four mutually independent sub- rinse baths 21,22,
23rd, 24, cleaning solution is equiped with the reservoir 1, and exemplarily, the cleaning solution can be liquid nitrogen or liquid titanium dioxide
Carbon, and the reservoir 1 is connected with each sub- rinse bath 21,22,23,24, the rinse bath 2, which is additionally provided with, can enter often
The ultrasonic cleaning apparatus 4 of a sub- rinse bath 21,22,23,24, Atmospheric particulates sampling membrane are fixed on the ultrasonic wave
On cleaning equipment 4, Atmospheric particulates sampling membrane with the ultrasonic cleaning apparatus enter each sub- rinse bath 21,
22nd, 23,24, each sub- rinse bath 21,22,23,24 is connected with the fog water content 3, and the fog water content 3 passes through outlet 31
Large-scale experiment instrument is connected, the outside of fog water content 3 is equipped with semiconductor chilling plate 60 and electromagnet group 70, the electromagnet group 70
The electromagnet to attract each other when being powered by a pair forms, and the electromagnet group 70 is coated on outside the fog water content 3, and the electricity
A holding tank is also equipped with group of magnets 70, the semiconductor chilling plate 60 is contained in the holding tank, described when energized
Electromagnet group 70 holds the fog water content 3 tightly, and the semiconductor chilling plate 60 heats the fog water content 3.Need what is illustrated
It is when heating the fog water content 3 using conventional heating unit, temperature control not to be accomplished very accurately, to power off it
Still there is one section of temperature rise afterwards, and be that electromagnet moment can be allowed to hold the atomization tightly by setting the effect of electromagnet group 70
Groove 3 departs from the fog water content 3, disconnected to the electromagnet group 70 when the temperature in the fog water content 3 reaches design temperature
Electricity, then then moment rests on design temperature to the temperature in the fog water content 3, and when the temperature in the fog water content 3 is fallen after rise, then
Again allow the electromagnet group 70 to power on, allow the semiconductor chilling plate 60 to rework, therefore can more precisely control
Temperature in the fog water content 3.The form that test of the large-scale experiment instrument to particulate matter generally requires to carry secretly by air-flow enters,
In other words particulate matter is atomized into mist in the fog water content 3, by the test probe of large-scale experiment equipment to air-flow
Contained particulate matter is tested in entrainment.And large-scale laboratory apparatus is located in laboratory and is not easy what is moved, and it is big
The sampling of aerated particle thing only need to be by the small-sized specific filter membrane of atmospheric sampling coordinative composition of equipments, and the present invention is that have to accumulation
The filter membrane of grain thing is thoroughly cleaned, and allows particulate matter to flake off into cleaning solution, then the cleaning solution containing particulate matter is atomized
Into mist, allow atmospheric sampling filter membrane to lie prostrate particulate matter and float again into large-scale experiment instrument, particulate matter is tested and is divided
Analysis.
In one embodiment, as shown in Fig. 2, further including sliding equipment 5, the sliding equipment 5 is arranged on the rinse bath 2
Side, and can be mobile above every sub- rinse bath 21,22,23,24, the ultrasonic cleaning apparatus 4 is arranged on the sliding equipment 5
Above and it can enter in every sub- rinse bath 21,22,23,24.
In above-described embodiment, as shown in Fig. 2, the top both sides of the rinse bath 2 are respectively equipped with two along the sub- cleaning
21,22,23,24 orientation of groove lay guide rail 6, the sliding equipment 5 include stepper motor 51, leading screw 52, portal frame 53,
Sliding block 54, the ultrasonic cleaning apparatus 4 be arranged on the portal frame 53 on, the portal frame 53 by the sliding block 54 slidably
On the guide rail 6, the stepper motor 51 by the leading screw 52 drive the portal frame 53 on the guide rail 6 it is reciprocal
Movement.Only need to be by controlling the action of the stepper motor 51, you can control the ultrasonic cleaning apparatus 4 to enter different institutes
Sub- rinse bath 21,22,23,24 is stated, and sets the purpose of multiple sub- rinse baths to be that and can be sampled to Atmospheric particulates
Filter membrane is thoroughly cleaned.
In one embodiment, as shown in Fig. 2, further including elevating mechanism 7, the elevating mechanism 7 is arranged on the portal frame 53
On, the elevating mechanism 7 is used for lifting or the dropping action for performing the ultrasonic cleaning apparatus 4.
In one embodiment, as shown in Fig. 2, the portal frame 53 includes crossbeam 531 and pillar 532, on the pillar 532
Elongated slot 533 equipped with vertical direction, the elevating mechanism 7 is lifted along the elongated slot 533 or dropping action.
In one embodiment, as shown in Fig. 2, the elevating mechanism 7 includes two installing plates 71 being oppositely arranged, it is each described
Installing plate 71 is respectively equipped with the ultrasonic cleaning apparatus 4, and Atmospheric particulates sampling membrane is arranged on two ultrasonic cleanings
Between equipment 4.
In one embodiment, as shown in Figure 1, 2, each sub- rinse bath 21,22,23,24 is connected with the fog water content 3
Before, a dashpot 8 is introduced into, the dashpot 8 is arranged on 21,22,23,24 bottom of rinse bath.The dashpot 8 is set
It can make the particle concentration homogenization contained by the cleaning solution of each sub- rinse bath 21,22,23,24 out.
In one embodiment, as shown in Figure 1,3 bottom of the fog water content sets atomizing piece 9.The atomizing piece 9 is then in order to right
Cleaning solution is atomized.And after cleaning solution is atomized, the particulate matter on atmospheric sampling filter membrane is attached to originally then with cleaning
The spray pattern of liquid float again, forms large-scale experiment instrument to be entered without words air-flow.
In one embodiment, as shown in Figure 1, dividing between the reservoir 1 and each sub- rinse bath 21,22,23,24
Not She You solenoid valve I 11, solenoid valve II 12 is equipped between the dashpot 8 and the fog water content 3.
In one embodiment, as shown in Figure 1, control device (not showing on figure) is further included, the ultrasonic cleaning apparatus 4,
Sliding equipment 5, elevating mechanism 7, atomizing piece 9, conductor cooling piece 60, solenoid valve I 11 and solenoid valve II 12 are filled with the control
Put connection.By the solenoid valve I 11, the cleaning solution in the reservoir 1 can be controlled to enter any one described sub- cleaning
Groove 21,22,23,24, and by the solenoid valve II 12, can be by any one described sub- rinse bath 21,22,23,24
Cleaning solution is discharged into the dashpot 8, then enters the fog water content 3 by the dashpot 8, and the control device controls institute
The distance of the slip of sliding equipment 5 is stated, controls the elevating mechanism 7 to carry the ultrasonic cleaning apparatus 4 and is lifted or landed, is controlled
The working frequency and run time of the ultrasonic cleaning apparatus 4 are made, controls starting or stoping for the atomizing piece 9, controls institute
The heating power of conductor cooling piece 60 is stated, controls being turned on and off for each solenoid valve I 11 and solenoid valve II 12.
In one embodiment, temperature sensor 10, the temperature sensor 10 and the control are additionally provided with the fog water content 3
Device processed connects and the temperature information in the fog water content 3 detected is fed back to the control device, the control device
The temperature information fed back according to the temperature sensor 10 controls the heating power of the semiconductor chilling plate 60.
In one embodiment, as shown in Fig. 2, each sub- top of rinse bath 21,22,23,24 is equipped with for allowing institute
The entrance 13 of the entrance of elevating mechanism 7 is stated, and is also set at the underface of entrance 13 in every sub- rinse bath 21,22,23,24
There is sealing plate (not showing on figure), described sealing plate one end is installed in the shaft with resetting spring, when the elevating mechanism 7 is logical
When crossing the entrance 13 into sub- rinse bath 21,22,23,24, the sealing plate can be opened by one angle of rotation, and be worked as
When the elevating mechanism 7 leaves sub- rinse bath 21,22,23,24 by the entrance 13, the sealing plate passes through described multiple
Position spring again seals the entrance 13.And it should be noted that the shaft with resetting spring is then installed on often
At the lower surface of a sub- 21,22,23,24 upper head plate of rinse bath.
Applied Ru above-mentioned in example, as shown in Fig. 2, the elevating mechanism 7 has further included a level board 72, two installing plates 71
The lower section of level board 72 is lifted on, and 72 surrounding of the level board is equipped with the silica gel for being sealed to the entrance 13
Boss 73, when the elevating mechanism 7 enters sub- rinse bath 21,22,23,24, the silica gel boss 73 is to the entrance
13 seal the entrance in interference fit.
Compared with prior art, with reference to Fig. 1 and 2, due to making atmospheric sampling filter membrane attaching particles thing float again in the present invention
Equipment 100 in, four mutually independent sub- rinse baths 21,22,23,24 are equipped with the rinse bath 2, in the reservoir 1
Be equiped with cleaning solution, exemplarily, the cleaning solution can be liquid nitrogen or liquid carbon dioxide, and the reservoir 1 with it is every
A sub- rinse bath 21,22,23,24 connects, the rinse bath 2 be additionally provided with can enter each sub- rinse bath 21,22,
23rd, 24 ultrasonic cleaning apparatus 4, each sub- rinse bath 21,22,23,24 are connected with the fog water content 3, the mist
Change groove 3 and connect large-scale experiment instrument.Therefore, Atmospheric particulates sampling membrane can be cleaned in different sub- rinse baths, be reached
To the purpose for cleaning up particulate matter completely.
It is above disclosed to be merely a preferred embodiment of the present invention, the right of the present invention cannot be limited with this certainly
Scope, therefore the equivalent variations made according to scope of the present invention patent, are still within the scope of the present invention.
Claims (14)
1. a kind of equipment for making atmospheric sampling filter membrane attaching particles thing float again, including:Reservoir, rinse bath and fog water content, institute
State and be equipped with some mutually independent sub- rinse baths in rinse bath, be equiped with cleaning solution in the reservoir, and the reservoir and
Each sub- rinse bath connects, and each sub- rinse bath is connected with the fog water content, and the fog water content connection is large-scale
Laboratory apparatus, it is characterised in that be equipped with semiconductor chilling plate and electromagnet group outside the fog water content, the electromagnet group is by one
The electromagnet to attract each other during to being powered forms, and the electromagnet group is coated on outside the fog water content, and the electromagnet group
A holding tank is inside also equipped with, the semiconductor chilling plate is contained in the holding tank, and the electromagnet group is embraced when energized
The tight fog water content, the semiconductor chilling plate heat the fog water content.
2. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 1, it is characterised in that described clear
Washing trough is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, and Atmospheric particulates sampling membrane is fixed on described
On ultrasonic cleaning apparatus, each sub- cleaning as the ultrasonic cleaning apparatus enters of Atmospheric particulates sampling membrane
Groove.
3. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 1, it is characterised in that further include
Sliding equipment, the sliding equipment are arranged on above the rinse bath, and can be moved above every sub- rinse bath, the ultrasonic wave
Cleaning equipment is arranged on the sliding equipment and can enter in every sub- rinse bath.
4. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 3, it is characterised in that described clear
The top both sides of washing trough are respectively equipped with two guide rails laid along the sub- rinse bath orientation, and the sliding equipment includes stepping
Motor, leading screw, portal frame, sliding block, the ultrasonic cleaning apparatus are arranged on the portal frame, and the portal frame passes through the cunning
Block is slidably arranged on the guide rail, the stepper motor by the leading screw drive the portal frame on the guide rail it is reciprocal
Movement.
5. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 4, it is characterised in that further include
Elevating mechanism, the elevating mechanism are arranged on the portal frame, and the elevating mechanism is used to perform the ultrasonic cleaning apparatus
Lifting or dropping action.
6. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 5, it is characterised in that the dragon
Door frame includes crossbeam and pillar, and the pillar is equipped with the elongated slot of vertical direction, and the elevating mechanism is lifted along the elongated slot
Or dropping action.
7. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 5, it is characterised in that the liter
Descending mechanism includes two installing plates being oppositely arranged, and each installing plate is respectively equipped with the ultrasonic cleaning apparatus, and air
Particle sampling filter membrane is arranged between two ultrasonic cleaning apparatus.
8. such as claim 1-7 any one of them makes the equipment that atmospheric sampling filter membrane attaching particles thing floats again, each described
Before sub- rinse bath is connected with the fog water content, a dashpot is introduced into, the dashpot is arranged on the bottom of rinse bath.
9. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 8, it is characterised in that the fog water content
Bottom sets atomizing piece.
10. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 8, it is characterised in that the liquid storage
Solenoid valve I is respectively equipped between groove and each sub- rinse bath, solenoid valve is equipped between the dashpot and the fog water content
Ⅱ。
11. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again such as claim 10, it is characterised in that further include control
Device processed, the ultrasonic cleaning apparatus, sliding equipment, elevating mechanism, atomizing piece, semiconductor chilling plate, solenoid valve I and electromagnetism
Valve II is connected with the control device, and the control device controls the distance that the sliding equipment slides, and controls the lifting
Mechanism carries the ultrasonic cleaning apparatus lifting or landing, controls working frequency and the operation of the ultrasonic cleaning apparatus
Time, controls starting or stoping for the atomizing piece, controls the heating power of the conductor cooling piece, controls each electromagnetism
Valve I and solenoid valve II are turned on and off.
12. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again such as claim 10, it is characterised in that the atomization
Temperature sensor is additionally provided with groove, the temperature sensor is connected with the control device and by the fog water content detected
Temperature information feed back to the control device, the temperature information control that the control device is fed back according to the temperature sensor
Make the heating power of the semiconductor chilling plate.
13. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again as claimed in claim 7, it is characterised in that each described
The entrance for allowing the elevating mechanism to enter is equipped with above sub- rinse bath, and is being located at the entrance just in every sub- rinse bath
Sealing plate is additionally provided with lower section, described sealing plate one end is installed in the shaft with resetting spring, when the elevating mechanism leads to
When crossing the entrance and entering the sub- rinse bath, the sealing plate can be opened by one angle of rotation, and work as the elevating mechanism
When leaving the sub- rinse bath by the entrance, the sealing plate again carries out the entrance by the resetting spring close
Envelope.
14. make the equipment that atmospheric sampling filter membrane attaching particles thing floats again such as claim 12, it is characterised in that the lifting
Mechanism has further included a level board, and two installing plates are lifted on below the level board, and the level board surrounding is equipped with
Silica gel boss, when the elevating mechanism enters the sub- rinse bath, the silica gel boss is in interference fit to the entrance
And the entrance is sealed.
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