CN107991162A - Particle analyte detection pre-processing device - Google Patents
Particle analyte detection pre-processing device Download PDFInfo
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- CN107991162A CN107991162A CN201711437343.4A CN201711437343A CN107991162A CN 107991162 A CN107991162 A CN 107991162A CN 201711437343 A CN201711437343 A CN 201711437343A CN 107991162 A CN107991162 A CN 107991162A
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- Prior art keywords
- rinse bath
- sub
- analyte detection
- processing device
- particle
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- 239000002245 particle Substances 0.000 title claims abstract description 40
- 238000001514 detection method Methods 0.000 title claims abstract description 26
- 239000012491 analyte Substances 0.000 title claims abstract description 25
- 238000007781 pre-processing Methods 0.000 title claims abstract description 25
- 238000004506 ultrasonic cleaning Methods 0.000 claims abstract description 36
- 239000012528 membrane Substances 0.000 claims abstract description 26
- 238000005070 sampling Methods 0.000 claims abstract description 24
- 239000003665 fog water Substances 0.000 claims abstract description 23
- 238000004140 cleaning Methods 0.000 claims abstract description 22
- 238000011173 large scale experimental method Methods 0.000 claims abstract description 10
- 230000003028 elevating effect Effects 0.000 claims description 34
- 238000010438 heat treatment Methods 0.000 claims description 12
- 238000007789 sealing Methods 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000741 silica gel Substances 0.000 claims description 7
- 229910002027 silica gel Inorganic materials 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000000889 atomisation Methods 0.000 claims description 3
- 239000003595 mist Substances 0.000 claims description 3
- 230000008450 motivation Effects 0.000 claims description 2
- 239000013618 particulate matter Substances 0.000 abstract description 18
- 239000003344 environmental pollutant Substances 0.000 description 14
- 231100000719 pollutant Toxicity 0.000 description 14
- 239000000523 sample Substances 0.000 description 10
- 239000002250 absorbent Substances 0.000 description 9
- 230000002745 absorbent Effects 0.000 description 9
- 238000000034 method Methods 0.000 description 9
- 239000007789 gas Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 239000003463 adsorbent Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- FAXIJTUDSBIMHY-UHFFFAOYSA-N diethoxy-(2-ethylsulfanylethoxy)-sulfanylidene-$l^{5}-phosphane;1-diethoxyphosphorylsulfanyl-2-ethylsulfanylethane Chemical compound CCOP(=O)(OCC)SCCSCC.CCOP(=S)(OCC)OCCSCC FAXIJTUDSBIMHY-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- DPQMPFBUHULHSC-UHFFFAOYSA-J [Na].[Hg](Cl)(Cl)(Cl)Cl Chemical compound [Na].[Hg](Cl)(Cl)(Cl)Cl DPQMPFBUHULHSC-UHFFFAOYSA-J 0.000 description 1
- 239000000809 air pollutant Substances 0.000 description 1
- 231100001243 air pollutant Toxicity 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 238000003682 fluorination reaction Methods 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011490 mineral wool Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003987 organophosphate pesticide Substances 0.000 description 1
- BULVZWIRKLYCBC-UHFFFAOYSA-N phorate Chemical compound CCOP(=S)(OCC)SCSCC BULVZWIRKLYCBC-UHFFFAOYSA-N 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2202—Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling
- G01N1/2205—Devices for withdrawing samples in the gaseous state involving separation of sample components during sampling with filters
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2273—Atmospheric sampling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The invention discloses a kind of particle analyte detection pre-processing device, including:Reservoir, rinse bath and fog water content, some mutually independent sub- rinse baths are equipped with the rinse bath, cleaning solution is equiped with the reservoir, and the reservoir is connected with each sub- rinse bath, the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, particle sampling filter membrane is fixed on the ultrasonic cleaning apparatus, particle sampling filter membrane each sub- rinse bath as the ultrasonic cleaning apparatus enters, each sub- rinse bath is connected with the fog water content, and the fog water content connects large-scale experiment instrument.Thoroughly cleaning, the particle analyte detection pre-processing device that simple in structure, the degree of automation is high can be carried out to the particulate matter on filter membrane the invention discloses a kind of.
Description
Technical field
The present invention relates to particle sampling technical field, more particularly to it is a kind of particulate matter on filter membrane can be carried out it is thorough
Cleaning, the particle analyte detection pre-processing device that simple in structure, the degree of automation is high.
Background technology
Atmospheric sampling is the process of pollutant sample or contaminated air sample in collection air.Spot sampling method has two
Class:One kind is large quantity of air is played the relatively low enriching pollutants of concentration in air by liquid-absorbant or solid absorbent
Come, such as degassing method, filter membrane method.Another kind of is with air of container (the vial, polybag etc.) collection containing pollutant.The former surveys
What is obtained is the mean concentration of pollutant in air in the sampling time;What the latter measured is instantaneous concentration or average dense in the short time
Degree.The mode of sampling should be depending on the purpose of sampling and field condition.Institute's sample thief should be representative.Sampling efficiency is high,
Operation must be easy, and is convenient for subsequent analysis measure, to obtain the master data of reliable atmosphere pollution.Gather air
The sample of middle pollutant or the sample of contaminated air, to obtain the master data of atmosphere pollution.
Atmospheric sampling is the important step of atmosphere environment supervision, and the reliable sexual intercourse for monitoring data is very big.Collection is big
The method of gas sample product, mainly there is two classes:One kind is to make large quantity of air by liquid-absorbant or solid absorbent, to absorb or hinder
Pollutant is stayed, the relatively low enriching pollutants of concentration in original air are got up, such as degassing method, filter membrane method.Measured with this kind of method
The result is that in the sampling time in air pollutant mean concentration.Another kind of is to use container (vial, polybag, rubber ball
Courage, syringe etc.) air of the collection containing pollutant.This kind of method is suitable for following situations:In air the concentration of pollutant compared with
It is high;Or the sensitivity of assay method is higher;It is not easy by the polluted gas and steaming of liquid-absorbant absorption or solid absorbent absorption
Vapour.The result measured with this method is the instantaneous concentration of pollutant or the mean concentration in the short time in air.In addition, also low temperature
Freezing, available for collection escaping gas and steam, such as alkyl lead.Liquid-absorbant in sampler is mainly used for absorbing gas
State and steam-like material.Common absorbent has:Water, compound water solution, organic solvent etc..Absorbent must be able to and pollutant
Quickly chemical reaction occurs or pollutant can be promptly dissolved, and is convenient for analysis operation.Such as the fluorination in air
Hydrogen, hydrogen chloride are with water as absorbent;Sulfur dioxide can be used as absorbent by the use of tetrachloro mercury sodium;Thimet (3911), demeton
(1059) etc. organophosphorus pesticide can be used as absorbent etc. by the use of 5% methanol.Solid absorbent has granular adsorbent and threadiness to inhale
Attached dose two kinds.Common granular adsorbent has silica gel, unglazed pottery etc., the sampling for gaseous state, steam-like and particulate matter.Fiber
Shape adsorbent has filter paper, filter membrane, absorbent cotton, mineral wool etc., and suction-operated is mainly physical detention, for gathering particle
Thing.Sometimes adsorbent makes pollutant that chemical action occur with it and adsorbed first with certain chemical reagent impregnation, main to use
In collection gaseous state or steam-like pollutant.
Common outside atmosphere sample devices, it is small, easily carry, but the performance ratio of its detection is relatively limited, it is difficult to do
Accurately detect and analyze to particulate matter progress, and large-scale experimental facilities is then general bulky, is not easy to move, often puts
It is disposed within.So if selection filter membrane method, then need to clean out the particulate matter being accumulated on filter membrane from filter membrane, then will
Particulate matter reenters large-scale experiment instrument and is tested and analyzed.
Therefore, there is an urgent need for it is a kind of can on filter membrane particulate matter carry out thoroughly cleaning, simple in structure, the degree of automation is high
Particle analyte detection pre-processing device.
The content of the invention
The object of the present invention is to provide it is a kind of can on filter membrane particulate matter carry out thoroughly cleaning, it is simple in structure, automatic
The high particle analyte detection pre-processing device of change degree.
To achieve these goals, technical solution provided by the invention is:A kind of particle analyte detection pre-processing device is provided,
Including:Reservoir, rinse bath and fog water content, the rinse bath is interior to be equipped with some mutually independent sub- rinse baths, the reservoir
Cleaning solution is inside equiped with, and the reservoir is connected with each sub- rinse bath, the rinse bath, which is additionally provided with, can enter often
The ultrasonic cleaning apparatus of a sub- rinse bath, particle sampling filter membrane are fixed on the ultrasonic cleaning apparatus, particle
Thing sampling membrane enters each sub- rinse bath with the ultrasonic cleaning apparatus, each sub- rinse bath with it is described
Fog water content connects, and the fog water content connects large-scale experiment instrument.
Sliding equipment is further included, the sliding equipment is arranged on above the rinse bath, and can be above every sub- rinse bath
Mobile, the ultrasonic cleaning apparatus is arranged on the sliding equipment and can enter in every sub- rinse bath.
The top both sides of the rinse bath are respectively equipped with two guide rails laid along the sub- rinse bath orientation, the cunning
Motivation structure includes stepper motor, leading screw, portal frame, sliding block, and the ultrasonic cleaning apparatus is arranged on the portal frame, the dragon
Door frame is slidably arranged on the guide rail by the sliding block, and the stepper motor drives the portal frame to exist by the leading screw
Moved back and forth on the guide rail.
Elevating mechanism is further included, the elevating mechanism is arranged on the portal frame, and the elevating mechanism is used to perform described
The lifting of ultrasonic cleaning apparatus or dropping action.
The portal frame includes crossbeam and pillar, and the pillar is equipped with the elongated slot of vertical direction, the elevating mechanism edge
The elongated slot is lifted or dropping action.
The elevating mechanism includes two installing plates being oppositely arranged, and it is clear that each installing plate is respectively equipped with the ultrasonic wave
Equipment is washed, and particle sampling filter membrane is arranged between two ultrasonic cleaning apparatus.
Before each sub- rinse bath is connected with the fog water content, a dashpot is introduced into, the dashpot is arranged on institute
State bottom of rinse bath.
The atomization trench bottom is equipped with atomizing piece and heating unit.
Solenoid valve I, the dashpot and the atomization are respectively equipped between the reservoir and each sub- rinse bath
Solenoid valve II is equipped between groove.
Further include control device, the ultrasonic cleaning apparatus, sliding equipment, elevating mechanism, atomizing piece, heating unit,
Solenoid valve I and solenoid valve II are connected with the control device, and the control device controls the distance that the sliding equipment slides,
Control the elevating mechanism to carry the ultrasonic cleaning apparatus lifting or landing, control the work of the ultrasonic cleaning apparatus
Working frequency and run time, control starting or stoping for the atomizing piece, control the heating power of the heating unit, and control is every
A solenoid valve I and solenoid valve II are turned on and off.
The entrance for allowing the elevating mechanism to enter, and every sub- rinse bath are equipped with above each sub- rinse bath
Interior to be additionally provided with sealing plate at entrance underface, described sealing plate one end is installed in the shaft with resetting spring,
When the elevating mechanism enters the sub- rinse bath by the entrance, the sealing plate can be opened by one angle of rotation,
And when the elevating mechanism leaves the sub- rinse bath by the entrance, the sealing plate by the resetting spring again
The entrance is sealed.
The elevating mechanism has further included a level board, and two installing plates are lifted on below the level board, and described
Level board surrounding is equipped with silica gel boss, and when the elevating mechanism enters the sub- rinse bath, the silica gel boss is to described
Entrance is in interference fit and the entrance is sealed.
Compared with prior art, due in particle analyte detection pre-processing device of the present invention, being equipped with if the rinse bath is interior
Mutually independent sub- rinse bath is done, cleaning solution, and the reservoir and each sub- rinse bath are equiped with the reservoir
Connect, the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, each sub- cleaning
Groove is connected with the fog water content, and the fog water content connects large-scale experiment instrument.Therefore, particle sampling filter membrane can be different
Cleaned in sub- rinse bath, achieve the purpose that completely to clean up particulate matter.
It will be become more fully apparent by following description and with reference to attached drawing, the present invention, these attached drawings are used to explain the present invention
Embodiment.
Brief description of the drawings
Fig. 1 is the module diagram of particle analyte detection pre-processing device of the present invention.
Fig. 2 is the schematic diagram of the rinse bath of particle analyte detection pre-processing device as shown in Figure 1.
Embodiment
The embodiment of the present invention described referring now to attached drawing, similar element numbers represent similar element in attached drawing.Such as
It is upper described, as shown in Figure 1, 2, particle analyte detection pre-processing device 100 provided in an embodiment of the present invention, including:It is reservoir 1, clear
Washing trough 2 and fog water content 3, the rinse bath 2 is interior to be equipped with four mutually independent sub- rinse baths 21,22,23,24, the reservoir 1
Inside be equiped with cleaning solution, exemplarily, the cleaning solution can be liquid nitrogen or liquid carbon dioxide, and the reservoir 1 with
Each sub- rinse bath 21,22,23,24 connects, the rinse bath 2 be additionally provided with can enter each sub- rinse bath 21,
22nd, 23,24 ultrasonic cleaning apparatus 4, particle sampling filter membrane are fixed on the ultrasonic cleaning apparatus 4, and particulate matter is adopted
Sample filter membrane each sub- rinse bath 21,22,23,24 as the ultrasonic cleaning apparatus enters, each sub- rinse bath
21st, 22,23,24 connected with the fog water content 3, the fog water content 3 passes through the connection of outlet 31 large-scale experiment instrument.Large-scale experiment
The form that test of the instrument to particulate matter generally requires to carry secretly by air-flow enters, and in other words particulate matter is in the fog water content 3
Mist is inside atomized into, particulate matter contained in air-flow entrainment is surveyed by the test probe of large-scale experiment equipment
Examination.And large-scale laboratory apparatus is located in laboratory and is not easy what is moved, and the sampling of particulate matter only need to be by small-sized big
The supporting specific filter membrane of gas sample devices, the present invention are thoroughly to be cleaned to accumulating the filter membrane for having particulate matter, are allowed
Grain thing is flaked off into cleaning solution, then the cleaning solution containing particulate matter carried out to be atomized into mist, enters back into large-scale experiment instrument,
Particulate matter is tested and is analyzed.
In one embodiment, as shown in Fig. 2, further including sliding equipment 5, the sliding equipment 5 is arranged on the rinse bath 2
Side, and can be mobile above every sub- rinse bath 21,22,23,24, the ultrasonic cleaning apparatus 4 is arranged on the sliding equipment 5
Above and it can enter in every sub- rinse bath 21,22,23,24.
In above-described embodiment, as shown in Fig. 2, the top both sides of the rinse bath 2 are respectively equipped with two along the sub- cleaning
21,22,23,24 orientation of groove lay guide rail 6, the sliding equipment 5 include stepper motor 51, leading screw 52, portal frame 53,
Sliding block 54, the ultrasonic cleaning apparatus 4 be arranged on the portal frame 53 on, the portal frame 53 by the sliding block 54 slidably
On the guide rail 6, the stepper motor 51 by the leading screw 52 drive the portal frame 53 on the guide rail 6 it is reciprocal
Movement.Only need to be by controlling the action of the stepper motor 51, you can control the ultrasonic cleaning apparatus 4 to enter different institutes
Sub- rinse bath 21,22,23,24 is stated, and the purposes of multiple sub- rinse baths is set be that can be to particle sampling filter membrane
Thoroughly cleaned.
In one embodiment, as shown in Fig. 2, further including elevating mechanism 7, the elevating mechanism 7 is arranged on the portal frame 53
On, the elevating mechanism 7 is used for lifting or the dropping action for performing the ultrasonic cleaning apparatus 4.
In one embodiment, as shown in Fig. 2, the portal frame 53 includes crossbeam 531 and pillar 532, on the pillar 532
Elongated slot 533 equipped with vertical direction, the elevating mechanism 7 is lifted along the elongated slot 533 or dropping action.
In one embodiment, as shown in Fig. 2, the elevating mechanism 7 includes two installing plates 71 being oppositely arranged, it is each described
Installing plate 71 is respectively equipped with the ultrasonic cleaning apparatus 4, and particle sampling filter membrane is arranged on two ultrasonic cleaning apparatus 4
Between.
In one embodiment, as shown in Figure 1, 2, each sub- rinse bath 21,22,23,24 is connected with the fog water content 3
Before, a dashpot 8 is introduced into, the dashpot 8 is arranged on 21,22,23,24 bottom of rinse bath.
In one embodiment, as shown in Figure 1,3 bottom of the fog water content is equipped with atomizing piece 9 and heating unit 10.It is described to add
Thermal 10 is in order to improve cleaning solution temperature, and the atomizing piece 9 is then in order to be atomized cleaning solution.
In one embodiment, as shown in Figure 1, dividing between the reservoir 1 and each sub- rinse bath 21,22,23,24
Not She You solenoid valve I 11, solenoid valve II 12 is equipped between the dashpot 8 and the fog water content 3.
In one embodiment, as shown in Figure 1, control device (not showing on figure) is further included, the ultrasonic cleaning apparatus 4,
Sliding equipment 5, elevating mechanism 7, atomizing piece 9, heating unit 10, solenoid valve I 11 and solenoid valve II 12 with the control device
Connection.By the solenoid valve I 11, the cleaning solution in the reservoir 1 can be controlled to enter any one described sub- rinse bath
21st, 22,23,24, and by the solenoid valve II 12, can will be clear in any one described sub- rinse bath 21,22,23,24
Washing lotion is discharged into the dashpot 8, then enters the fog water content 3 by the dashpot 8, described in control device control
The distance that sliding equipment 5 slides, controls the elevating mechanism 7 to carry the ultrasonic cleaning apparatus 4 and is lifted or landed, and controls
The working frequency and run time of the ultrasonic cleaning apparatus 4, control starting or stoping for the atomizing piece 9, described in control
The heating power of heating unit 10, controls being turned on and off for each solenoid valve I 11 and solenoid valve II 12.
In one embodiment, as shown in Fig. 2, each sub- top of rinse bath 21,22,23,24 is equipped with for allowing institute
The entrance 13 of the entrance of elevating mechanism 7 is stated, and is also set at the underface of entrance 13 in every sub- rinse bath 21,22,23,24
There is sealing plate (not showing on figure), described sealing plate one end is installed in the shaft with resetting spring, when the elevating mechanism 7 is logical
When crossing the entrance 13 into sub- rinse bath 21,22,23,24, the sealing plate can be opened by one angle of rotation, and be worked as
When the elevating mechanism 7 leaves sub- rinse bath 21,22,23,24 by the entrance 13, the sealing plate passes through described multiple
Position spring again seals the entrance 13.And it should be noted that the shaft with resetting spring is then installed on often
At the lower surface of a sub- 21,22,23,24 upper head plate of rinse bath.
Applied Ru above-mentioned in example, as shown in Fig. 2, the elevating mechanism 7 has further included a level board 72, two installing plates 71
The lower section of level board 72 is lifted on, and 72 surrounding of the level board is equipped with the silica gel for being sealed to the entrance 13
Boss 73, when the elevating mechanism 7 enters sub- rinse bath 21,22,23,24, the silica gel boss 73 is to the entrance
13 seal the entrance in interference fit.
Compared with prior art, it is described due in particle analyte detection pre-processing device 100 of the present invention with reference to Fig. 1 and 2
Four mutually independent sub- rinse baths 21,22,23,24 are equipped with rinse bath 2, cleaning solution, example are equiped with the reservoir 1
Property, the cleaning solution can be liquid nitrogen or liquid carbon dioxide, and the reservoir 1 and each sub- rinse bath 21,
22nd, 23,24 connect, the rinse bath 2 is additionally provided with the ultrasonic cleaning that can enter each sub- rinse bath 21,22,23,24
Equipment 4, each sub- rinse bath 21,22,23,24 are connected with the fog water content 3, and the fog water content 3 connects large-scale experiment
Instrument.Therefore, particle sampling filter membrane can be cleaned in different sub- rinse baths, reached and cleaned up particulate matter completely
Purpose.
It is above disclosed to be merely a preferred embodiment of the present invention, the right of the present invention cannot be limited with this certainly
Scope, therefore the equivalent variations made according to scope of the present invention patent, are still within the scope of the present invention.
Claims (12)
1. a kind of particle analyte detection pre-processing device, including:Reservoir, rinse bath and fog water content, it is characterised in that the cleaning
Some mutually independent sub- rinse baths are equipped with groove, cleaning solution, and the reservoir and each institute are equiped with the reservoir
State sub- rinse bath to connect, the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, particle
Thing sampling membrane is fixed on the ultrasonic cleaning apparatus, and particle sampling filter membrane enters with the ultrasonic cleaning apparatus
Each sub- rinse bath, each sub- rinse bath are connected with the fog water content, and the fog water content connects large-scale experiment instrument
Device.
2. particle analyte detection pre-processing device as claimed in claim 1, it is characterised in that further include sliding equipment, the cunning
Motivation structure is arranged on above the rinse bath, and can be moved above every sub- rinse bath, and the ultrasonic cleaning apparatus is arranged on institute
State on sliding equipment and can enter in every sub- rinse bath.
3. particle analyte detection pre-processing device as claimed in claim 2, it is characterised in that the top both sides of the rinse bath point
Not She You two guide rails laid along the sub- rinse bath orientation, the sliding equipment includes stepper motor, leading screw, gantry
Frame, sliding block, the ultrasonic cleaning apparatus are arranged on the portal frame, and the portal frame is slidably arranged on institute by the sliding block
State on guide rail, the stepper motor drives the portal frame to be moved back and forth on the guide rail by the leading screw.
4. particle analyte detection pre-processing device as claimed in claim 3, it is characterised in that further include elevating mechanism, the liter
Descending mechanism is arranged on the portal frame, and the elevating mechanism is used for the lifting for performing the ultrasonic cleaning apparatus or landing is dynamic
Make.
5. particle analyte detection pre-processing device as claimed in claim 4, it is characterised in that the portal frame includes crossbeam and branch
Column, the pillar are equipped with the elongated slot of vertical direction, and the elevating mechanism is lifted along the elongated slot or dropping action.
6. particle analyte detection pre-processing device as claimed in claim 4, it is characterised in that it is opposite that the elevating mechanism includes two
The installing plate of setting, each installing plate is respectively equipped with the ultrasonic cleaning apparatus, and particle sampling filter membrane is arranged on two
Between the ultrasonic cleaning apparatus.
7. such as claim 1-6 any one of them particle analyte detection pre-processing devices, each sub- rinse bath and the mist
Before changing groove connection, a dashpot is introduced into, the dashpot is arranged on the bottom of rinse bath.
8. particle analyte detection pre-processing device as claimed in claim 7, it is characterised in that it is described atomization trench bottom be equipped with atomizing piece and
Heating unit.
9. particle analyte detection pre-processing device as claimed in claim 7, it is characterised in that the reservoir and each sub- cleaning
Solenoid valve I is respectively equipped between groove, solenoid valve II is equipped between the dashpot and the fog water content.
10. particle analyte detection pre-processing device as claimed in claim 9, it is characterised in that further include control device, the ultrasonic wave
Cleaning equipment, sliding equipment, elevating mechanism, atomizing piece, heating unit, solenoid valve I and solenoid valve II with the control device
Connection, the control device control the distance that the sliding equipment slides, and control the elevating mechanism to carry the ultrasonic wave clear
Equipment lifting or landing are washed, the working frequency and run time of the ultrasonic cleaning apparatus is controlled, controls the atomizing piece
Start or stop, control the heating power of the heating unit, control each solenoid valve I and solenoid valve II unlatching or
Close.
11. particle analyte detection pre-processing device as claimed in claim 6, it is characterised in that be all provided with above each sub- rinse bath
The entrance for allowing the elevating mechanism to enter is useful for, and sealing is additionally provided with entrance underface in every sub- rinse bath
Plate, described sealing plate one end are installed in the shaft with resetting spring, when the elevating mechanism enters institute by the entrance
When stating sub- rinse bath, the sealing plate can be opened by one angle of rotation, and when the elevating mechanism is left by the entrance
During the sub- rinse bath, the sealing plate again seals the entrance by the resetting spring.
12. such as the particle analyte detection pre-processing device of claim 11, it is characterised in that the elevating mechanism has further included a water
Tablet, two installing plates are lifted on below the level board, and the level board surrounding is equipped with silica gel boss, when the liter
When descending mechanism enters the sub- rinse bath, the silica gel boss is in interference fit to the entrance and the entrance is carried out close
Envelope.
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