CN207816686U - Particle analyte detection pretreating device - Google Patents

Particle analyte detection pretreating device Download PDF

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Publication number
CN207816686U
CN207816686U CN201721853465.7U CN201721853465U CN207816686U CN 207816686 U CN207816686 U CN 207816686U CN 201721853465 U CN201721853465 U CN 201721853465U CN 207816686 U CN207816686 U CN 207816686U
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China
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rinse bath
sub
analyte detection
elevating mechanism
particle
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CN201721853465.7U
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甘佳俊
陈砚
董宁
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SUZHOU CENTRE TESTING INTERNATIONAL Corp
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SUZHOU CENTRE TESTING INTERNATIONAL Corp
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Abstract

The utility model discloses a kind of particle analyte detection pretreating devices, including:Reservoir, rinse bath and fog water content, several mutually independent sub- rinse baths are equipped in the rinse bath, it is installed with cleaning solution in the reservoir, and the reservoir is connected to each sub- rinse bath, the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, particle sampling filter membrane is fixed on the ultrasonic cleaning apparatus, particle sampling filter membrane each sub- rinse bath as the ultrasonic cleaning apparatus enters, each sub- rinse bath is connected to the fog water content, and the fog water content connects large-scale experiment instrument.Thoroughly cleaning, particle analyte detection pretreating device simple in structure, high degree of automation can be carried out to the particulate matter on filter membrane the utility model discloses a kind of.

Description

Particle analyte detection pretreating device
Technical field
The utility model is related to particle sampling technical field more particularly to a kind of particulate matter on filter membrane can be carried out Thoroughly cleaning, particle analyte detection pretreating device simple in structure, high degree of automation.
Background technology
Atmospheric sampling is the process of pollutant sample or contaminated air sample in acquisition air.Spot sampling method has two Class:One kind is that large quantity of air is made to pass through liquid-absorbant or solid absorbent, and the lower enriching pollutants of concentration in air are risen Come, such as degassing method, filter membrane method.Another kind of is to acquire the air containing pollutant with container (vial, polybag etc.).The former surveys What is obtained is the mean concentration of pollutant in air in the sampling time;What the latter measured is instantaneous concentration or average dense in the short time Degree.The mode of sampling should be depending on the purpose of sampling and field condition.Institute's sample thief is answered representative.Sampling efficiency wants high, Operation must be easy, and is convenient for subsequent analysis and measures, to obtain the master data of reliable atmosphere pollution.Acquire air The sample of middle pollutant or the sample of contaminated air, to obtain the master data of atmosphere pollution.
Atmospheric sampling is the important step of atmosphere environment supervision, very big for the reliable sexual intercourse of monitoring data.Acquisition is big The method of gas sample product, there are two main classes:One kind is that large quantity of air is made to pass through liquid-absorbant or solid absorbent, to absorb or hinder Pollutant is stayed, the lower enriching pollutants of concentration in original air are got up, such as degassing method, filter membrane method.It is measured with such methods The result is that in the sampling time in air pollutant mean concentration.Another kind of is to use container (vial, polybag, rubber ball Courage, syringe etc.) air of the acquisition containing pollutant.Such methods are suitable for following situations:In air the concentration of pollutant compared with It is high;Or the sensitivity of assay method is higher;It is not easy by the polluted gas and steaming of liquid-absorbant absorption or solid absorbent absorption Vapour.The result measured with this method is the instantaneous concentration of pollutant or the mean concentration in the short time in air.In addition, also low temperature Freezing can be used for acquiring escaping gas and steam, such as alkyl lead.Liquid-absorbant in sampler is mainly used for absorbing gas State and steam-like substance.Common absorbent has:Water, compound water solution, organic solvent etc..Absorbent must be able to and pollutant Quickly chemical reaction occurs or pollutant can be promptly dissolved, and is convenient for analysis operation.Such as the fluorination in air Hydrogen, hydrogen chloride are with water as absorbent;Sulfur dioxide can use tetrachloro mercury sodium as absorbent;Thimet (3911), demeton (1059) etc. organophosphorus pesticides can use 5% methanol as absorbent etc..Solid absorbent has granular adsorbent and threadiness to inhale Attached dose two kinds.Common granular adsorbent has silica gel, unglazed pottery etc., is used for the sampling of gaseous state, steam-like and particulate matter.Fiber Shape adsorbent has filter paper, filter membrane, absorbent cotton, mineral wool etc., and suction-operated is mainly physical detention, for acquiring particle Object.Sometimes adsorbent makes pollutant that chemical action occur with it and adsorbed first with certain chemical reagent impregnation, main to use In acquisition gaseous state or steam-like pollutant.
Common outside atmosphere sample devices, it is small, it is easy to carry, but the performance ratio of its detection is relatively limited, it is difficult to do Accurate detection and analysis is carried out to particulate matter, and large-scale experimental facilities is then general bulky, is not easy to move, often put It is disposed within.So if selection filter membrane method, then need to clean out the particulate matter being accumulated on filter membrane from filter membrane, then will Particulate matter reenters large-scale experiment instrument and is tested and analyzed.
Therefore, there is an urgent need for it is a kind of can to the particulate matter on filter membrane carry out thoroughly cleaning, it is simple in structure, high degree of automation Particle analyte detection pretreating device.
Utility model content
The purpose of this utility model be to provide it is a kind of can to the particulate matter on filter membrane carry out thoroughly cleaning, it is simple in structure, The particle analyte detection pretreating device of high degree of automation.
To achieve the goals above, technical solution provided by the utility model is:A kind of particle analyte detection pre-treatment is provided Device, including:Reservoir, rinse bath and fog water content, the rinse bath is interior to be equipped with several mutually independent sub- rinse baths, the storage It is installed with cleaning solution in liquid bath, and the reservoir is connected to each sub- rinse bath, the rinse bath is additionally provided with can be into Entering the ultrasonic cleaning apparatus of each sub- rinse bath, particle sampling filter membrane is fixed on the ultrasonic cleaning apparatus, Particle sampling filter membrane enters each sub- rinse bath with the ultrasonic cleaning apparatus, each sub- rinse bath with The fog water content connection, the fog water content connect large-scale experiment instrument.
Further include sliding equipment, the sliding equipment is set to above the rinse bath, and can be above every sub- rinse bath Mobile, the ultrasonic cleaning apparatus is set on the sliding equipment and can enter in every sub- rinse bath.
The top both sides of the rinse bath are respectively equipped with two guide rails laid along the sub- rinse bath orientation, the cunning Motivation structure includes stepper motor, leading screw, portal frame, sliding block, and the ultrasonic cleaning apparatus is set on the portal frame, the dragon Door frame is slidably set on the guide rail by the sliding block, and the stepper motor drives the portal frame to exist by the leading screw It is moved back and forth on the guide rail.
Further include elevating mechanism, the elevating mechanism is set on the portal frame, and the elevating mechanism is described for executing The promotion of ultrasonic cleaning apparatus or dropping action.
The portal frame includes crossbeam and pillar, and the pillar is equipped with the elongated slot of vertical direction, the elevating mechanism edge The elongated slot does promotion or dropping action.
The elevating mechanism includes two mounting plates being oppositely arranged, and it is clear that each mounting plate is respectively equipped with the ultrasonic wave Equipment is washed, and particle sampling filter membrane is set between two ultrasonic cleaning apparatus.
Before each sub- rinse bath is connected to the fog water content, it is introduced into a dashpot, the dashpot is set to institute State bottom of rinse bath.
The atomization trench bottom is equipped with atomizing piece and heating device.
Solenoid valve I, the dashpot and the atomization are respectively equipped between the reservoir and each sub- rinse bath Solenoid valve II is equipped between slot.
Further include control device, the ultrasonic cleaning apparatus, sliding equipment, elevating mechanism, atomizing piece, heating device, Solenoid valve I and solenoid valve II are connect with the control device, and the control device controls the distance of the sliding equipment sliding, It controls the elevating mechanism and carries the ultrasonic cleaning apparatus promotion or landing, control the work of the ultrasonic cleaning apparatus Working frequency and run time control starting or stoping for the atomizing piece, control the heating power of the heating device, and control is every A solenoid valve I and solenoid valve II are turned on and off.
The entrance for allowing the elevating mechanism to enter, and every sub- rinse bath are equipped with above each sub- rinse bath Interior to be additionally provided with sealing plate at entrance underface, described sealing plate one end is installed in the shaft with resetting spring, When the elevating mechanism enters the sub- rinse bath by the entrance, the sealing plate can be opened by one angle of rotation, And when the elevating mechanism leaves the sub- rinse bath by the entrance, the sealing plate by the resetting spring again The entrance is sealed.
The elevating mechanism further includes having a level board, and two mounting plates are lifted below the level board, and described Level board surrounding is equipped with silica gel boss, and when the elevating mechanism enters the sub- rinse bath, the silica gel boss is to described Entrance is in interference fit and is sealed to the entrance.
Compared with prior art, due in the utility model particle analyte detection pretreating device, being set in the rinse bath There are several mutually independent sub- rinse baths, cleaning solution is installed in the reservoir, and the reservoir and each son are clear Washing trough is connected to, and the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, each son Rinse bath is connected to the fog water content, and the fog water content connects large-scale experiment instrument.Therefore, particle sampling filter membrane can be not It is cleaned in same sub- rinse bath, achievees the purpose that completely to clean up particulate matter.
By description below and in conjunction with attached drawing, the utility model will become more fully apparent, these attached drawings are for explaining this The embodiment of utility model.
Description of the drawings
Fig. 1 is the module diagram of the utility model particle analyte detection pretreating device.
Fig. 2 is the schematic diagram of the rinse bath of particle analyte detection pretreating device as shown in Figure 1.
Specific implementation mode
The embodiments of the present invention are described referring now to the drawings, similar element numbers represent similar member in attached drawing Part.As described above, as shown in Figure 1, 2, the particle analyte detection pretreating device 100 that the utility model embodiment provides, including:Storage Liquid bath 1, rinse bath 2 and fog water content 3, set that there are four mutually independent sub- rinse bath 21,22,23,24, institutes in the rinse bath 2 It states and is installed with cleaning solution in reservoir 1, illustratively, the cleaning solution can be liquid nitrogen or liquid carbon dioxide, and described Reservoir 1 is connected to each sub- rinse bath 21,22,23,24, and the rinse bath 2, which is additionally provided with, can enter each son The ultrasonic cleaning apparatus 4 of rinse bath 21,22,23,24, particle sampling filter membrane are fixed on the ultrasonic cleaning apparatus 4, Particle sampling filter membrane each sub- rinse bath 21,22,23,24 as the ultrasonic cleaning apparatus enters, it is each described Sub- rinse bath 21,22,23,24 is connected to the fog water content 3, and the fog water content 3 passes through 31 connection large-scale experiment instrument of outlet. Large-scale experiment instrument generally requires to enter by the form that air-flow is carried secretly to the test of particulate matter, and in other words particulate matter is described It is atomized into mist in fog water content 3, by the test probe of large-scale experiment equipment to particulate matter contained in air-flow entrainment It is tested.And large-scale laboratory apparatus is located in and is not easy to move in laboratory, and the sampling of particulate matter only need to be by small The specific filter membrane of atmospheric sampling coordinative composition of equipments of type, the utility model are to be carried out thoroughly to the filter membrane that accumulation has particulate matter Cleaning, allows particulate matter to flake off into cleaning solution, then the cleaning solution containing particulate matter carried out to be atomized into mist, enters back into large size Test apparatus is tested particulate matter and is analyzed.
In one embodiment, as shown in Fig. 2, further including sliding equipment 5, the sliding equipment 5 is set on the rinse bath 2 Side, and can be mobile above every sub- rinse bath 21,22,23,24, the ultrasonic cleaning apparatus 4 is set to the sliding equipment 5 Above and it can enter in every sub- rinse bath 21,22,23,24.
In above-described embodiment, as shown in Fig. 2, the top both sides of the rinse bath 2 are respectively equipped with two along the sub- cleaning 21,22,23,24 orientation of slot lay guide rail 6, the sliding equipment 5 include stepper motor 51, leading screw 52, portal frame 53, Sliding block 54, the ultrasonic cleaning apparatus 4 be set to the portal frame 53 on, the portal frame 53 by the sliding block 54 slidably On the guide rail 6, the stepper motor 51 drives the portal frame 53 reciprocal on the guide rail 6 by the leading screw 52 Movement.It only need to be by controlling the action of the stepper motor 51, you can control the ultrasonic cleaning apparatus 4 and enter different institutes State sub- rinse bath 21,22,23,24, and be that can be to particle sampling filter membrane for the purpose that multiple sub- rinse baths are arranged Thoroughly cleaned.
In one embodiment, as shown in Fig. 2, further including elevating mechanism 7, the elevating mechanism 7 is set to the portal frame 53 On, the elevating mechanism 7 is used to execute promotion or the dropping action of the ultrasonic cleaning apparatus 4.
In one embodiment, as shown in Fig. 2, the portal frame 53 includes crossbeam 531 and pillar 532, on the pillar 532 Elongated slot 533 equipped with vertical direction, the elevating mechanism 7 do promotion or dropping action along the elongated slot 533.
In one embodiment, as shown in Fig. 2, the elevating mechanism 7 includes two mounting plates 71 being oppositely arranged, it is each described Mounting plate 71 is respectively equipped with the ultrasonic cleaning apparatus 4, and particle sampling filter membrane is set to two ultrasonic cleaning apparatus 4 Between.
In one embodiment, as shown in Figure 1, 2, each sub- rinse bath 21,22,23,24 is connected to the fog water content 3 Before, it is introduced into a dashpot 8, the dashpot 8 is set to 21,22,23,24 bottom of the rinse bath.
In one embodiment, as shown in Figure 1,3 bottom of the fog water content is equipped with atomizing piece 9 and heating device 10.It is described to add Thermal 10 is in order to improve cleaning solution temperature, and the atomizing piece 9 is then in order to be atomized cleaning solution.
In one embodiment, as shown in Figure 1, dividing between the reservoir 1 and each sub- rinse bath 21,22,23,24 Not She You solenoid valve I 11, between the dashpot 8 and the fog water content 3 be equipped with solenoid valve II 12.
In one embodiment, as shown in Figure 1, further include control device (not showing on figure), the ultrasonic cleaning apparatus 4, Sliding equipment 5, elevating mechanism 7, atomizing piece 9, heating device 10, solenoid valve I 11 and solenoid valve II 12 with the control device Connection.By the solenoid valve I 11, the cleaning solution that can be controlled in the reservoir 1 enters any one described sub- rinse bath 21,22,23,24, and by the solenoid valve II 12, it can will be clear in any one described sub- rinse bath 21,22,23,24 Washing lotion is discharged into the dashpot 8, then enters the fog water content 3 by the dashpot 8, described in control device control The distance that sliding equipment 5 slides controls the elevating mechanism 7 and carries the promotion of the ultrasonic cleaning apparatus 4 or landing, control The working frequency and run time of the ultrasonic cleaning apparatus 4, control starting or stoping for the atomizing piece 9, described in control The heating power of heating device 10, each solenoid valve I 11 of control and solenoid valve II 12 are turned on and off.
In one embodiment, as shown in Fig. 2, 21,22,23,24 top of each sub- rinse bath is equipped with for allowing The entrance 13 of the entrance of elevating mechanism 7 is stated, and is located at immediately below the entrance 13 in every sub- rinse bath 21,22,23,24 and also sets There are sealing plate (not showing on figure), described sealing plate one end to be installed in the shaft with resetting spring, when the elevating mechanism 7 is logical When crossing the entrance 13 into sub- rinse bath 21,22,23,24, the sealing plate can be opened by one angle of rotation, and be worked as When the elevating mechanism 7 leaves the sub- rinse bath 21,22,23,24 by the entrance 13, the sealing plate passes through described multiple Position spring is again sealed the entrance 13.And it should be noted that the shaft with resetting spring is then mounted on often At the lower surface of a 21,22,23,24 upper head plate of the sub- rinse bath.
It is applied in example Ru above-mentioned, as shown in Fig. 2, the elevating mechanism 7 further includes having a level board 72, two mounting plates 71 It is lifted on 72 lower section of the level board, and 72 surrounding of the level board is equipped with the silica gel for being sealed to the entrance 13 Boss 73, when the elevating mechanism 7 enters sub- rinse bath 21,22,23,24, the silica gel boss 73 is to the entrance 13 are sealed the entrance in interference fit.
Compared with prior art, in conjunction with Fig. 1 and 2, due in the utility model particle analyte detection pretreating device 100, It is set in the rinse bath 2 there are four mutually independent sub- rinse bath 21,22,23,24, cleaning solution is installed in the reservoir 1, Illustratively, the cleaning solution can be liquid nitrogen or liquid carbon dioxide, and the reservoir 1 and each sub- rinse bath 21, it 22,23,24 is connected to, the rinse bath 2 is additionally provided with the ultrasonic wave that can enter each sub- rinse bath 21,22,23,24 Cleaning equipment 4, each sub- rinse bath 21,22,23,24 are connected to the fog water content 3, and the fog water content 3 connects large size Laboratory apparatus.Therefore, particle sampling filter membrane can be cleaned in different sub- rinse baths, reached and cleaned particulate matter completely Clean purpose.
It above disclosure is merely preferred embodiments of the utility model, certainly cannot be new to limit this practicality with this The interest field of type, therefore equivalent variations made according to the patent scope of the utility model still belong to the utility model and are covered Range.

Claims (12)

1. a kind of particle analyte detection pretreating device, including:Reservoir, rinse bath and fog water content, which is characterized in that the cleaning It is equipped with several mutually independent sub- rinse baths in slot, cleaning solution, and the reservoir and each institute are installed in the reservoir It states sub- rinse bath to be connected to, the rinse bath is additionally provided with the ultrasonic cleaning apparatus that can enter each sub- rinse bath, particle Object sampling membrane is fixed on the ultrasonic cleaning apparatus, and particle sampling filter membrane enters with the ultrasonic cleaning apparatus Each sub- rinse bath, each sub- rinse bath are connected to the fog water content, and the fog water content connects large-scale experiment instrument Device.
2. particle analyte detection pretreating device as described in claim 1, which is characterized in that further include sliding equipment, the cunning Motivation structure is set to above the rinse bath, and can be moved above every sub- rinse bath, and the ultrasonic cleaning apparatus is set to institute It states on sliding equipment and can enter in every sub- rinse bath.
3. particle analyte detection pretreating device as claimed in claim 2, which is characterized in that the top both sides of the rinse bath point Not She You two guide rails laid along the sub- rinse bath orientation, the sliding equipment includes stepper motor, leading screw, gantry Frame, sliding block, the ultrasonic cleaning apparatus are set on the portal frame, and the portal frame is slidably set to institute by the sliding block It states on guide rail, the stepper motor drives the portal frame to be moved back and forth on the guide rail by the leading screw.
4. particle analyte detection pretreating device as claimed in claim 3, which is characterized in that further include elevating mechanism, the liter Descending mechanism is set on the portal frame, and the elevating mechanism is used to execute the promotion of the ultrasonic cleaning apparatus or landing is moved Make.
5. particle analyte detection pretreating device as claimed in claim 4, which is characterized in that the portal frame includes crossbeam and branch Column, the pillar are equipped with the elongated slot of vertical direction, and the elevating mechanism does promotion or dropping action along the elongated slot.
6. particle analyte detection pretreating device as claimed in claim 4, which is characterized in that the elevating mechanism includes two opposite The mounting plate of setting, each mounting plate is respectively equipped with the ultrasonic cleaning apparatus, and particle sampling filter membrane is set to two Between the ultrasonic cleaning apparatus.
7. particle analyte detection pretreating device as claimed in any one of claims 1 to 6, each sub- rinse bath and the mist Before changing slot connection, it is introduced into a dashpot, the dashpot is set to the bottom of rinse bath.
8. particle analyte detection pretreating device as claimed in claim 7, which is characterized in that the atomization trench bottom is equipped with atomization Piece and heating device.
9. particle analyte detection pretreating device as claimed in claim 7, which is characterized in that the reservoir and each son It is respectively equipped with solenoid valve I between rinse bath, solenoid valve II is equipped between the dashpot and the fog water content.
10. particle analyte detection pretreating device as claimed in claim 9, which is characterized in that further include control device, it is described super Sound wave cleaning equipment, sliding equipment, elevating mechanism, atomizing piece, heating device, solenoid valve I and solenoid valve II with the control Device connects, and the control device controls the distance of the sliding equipment sliding, controls the elevating mechanism and carries the ultrasound Wave cleaning equipment is promoted or landing, controls the working frequency and run time of the ultrasonic cleaning apparatus, controls the mist Change piece to start or stop, control the heating power of the heating device, controls opening for each solenoid valve I and solenoid valve II It opens or closes.
11. particle analyte detection pretreating device as claimed in claim 6, which is characterized in that above each sub- rinse bath It is equipped with the entrance for allowing the elevating mechanism to enter, and is located at immediately below the entrance in every sub- rinse bath and is additionally provided with Sealing plate, described sealing plate one end are installed in the shaft with resetting spring, when the elevating mechanism by the entrance into When entering the sub- rinse bath, the sealing plate can be opened by one angle of rotation, and when the elevating mechanism passes through the entrance When leaving the sub- rinse bath, the sealing plate is again sealed the entrance by the resetting spring.
12. particle analyte detection pretreating device as claimed in claim 11, which is characterized in that the elevating mechanism further includes having One level board, two mounting plates are lifted below the level board, and the level board surrounding is equipped with silica gel boss, works as institute State elevating mechanism into the sub- rinse bath when, the silica gel boss to the entrance be in interference fit and to the entrance into Row sealing.
CN201721853465.7U 2017-12-26 2017-12-26 Particle analyte detection pretreating device Active CN207816686U (en)

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CN201721853465.7U CN207816686U (en) 2017-12-26 2017-12-26 Particle analyte detection pretreating device

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107991162A (en) * 2017-12-26 2018-05-04 苏州市华测检测技术有限公司 Particle analyte detection pre-processing device
CN108007729A (en) * 2017-12-26 2018-05-08 华测检测认证集团股份有限公司 The equipment for making atmospheric sampling filter membrane attaching particles thing float again
CN109632438A (en) * 2018-12-19 2019-04-16 华测检测认证集团股份有限公司 The fog water content of Atmospheric particulates sampling membrane cleaning equipment with heat insulation function

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107991162A (en) * 2017-12-26 2018-05-04 苏州市华测检测技术有限公司 Particle analyte detection pre-processing device
CN108007729A (en) * 2017-12-26 2018-05-08 华测检测认证集团股份有限公司 The equipment for making atmospheric sampling filter membrane attaching particles thing float again
CN109632438A (en) * 2018-12-19 2019-04-16 华测检测认证集团股份有限公司 The fog water content of Atmospheric particulates sampling membrane cleaning equipment with heat insulation function

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