CN107996635A - Sponge antibacterial filler and preparation method thereof - Google Patents

Sponge antibacterial filler and preparation method thereof Download PDF

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Publication number
CN107996635A
CN107996635A CN201710982207.7A CN201710982207A CN107996635A CN 107996635 A CN107996635 A CN 107996635A CN 201710982207 A CN201710982207 A CN 201710982207A CN 107996635 A CN107996635 A CN 107996635A
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boiling
preparation
sponge
antibacterial filler
leaf
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章发林
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Wuhu Pipilu Technology Co Ltd
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Wuhu Pipilu Technology Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N41/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
    • A01N41/02Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/06Aluminium; Calcium; Magnesium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/36Rutaceae [Rue family], e.g. lime, orange, lemon, corktree or pricklyash
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Environmental Sciences (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fodder In General (AREA)

Abstract

The invention discloses a kind of sponge antibacterial filler and preparation method thereof, this method includes:Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash mixed, boiling be made slurry M1;The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2;Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial filler.Sponge antibacterial filler has an excellent anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.

Description

Sponge antibacterial filler and preparation method thereof
Technical field
The present invention relates to sponge manufacturing field, and in particular, to a kind of sponge antibacterial filler and preparation method thereof.
Background technology
Sponge products it is widely used, such as face cleaning is flutterred, cleaning sponge and sanitary microphone cover etc..Wherein, microphone is either The speech ciphering equipments such as microphone, all can frequently use in daily life and work, rise and the prevalence of especially current network direct broadcasting Under trend, the routine work of main broadcasters is exactly against microphone or microphone.
It is well known that when using microphone or microphone, mouth is closer apart from the distance of microphone, so whether makes With public place microphone in place such as KTV, bar or it is live when main broadcaster dedicated microphone, microphone, using one section It all can cause microphone surface moisture after time and easily grow bacterium, so may result in microphone user and be easily subject to bacterium sense Even germ cross-infection is contaminated, so as to seriously affect the health of user.
At present, microphone cover is as a kind of a kind of one of effective measures that can reduce the growth of microphone surface bacteria, but very More businessmans are unwilling to replace microphone cover in time for cost-effective or workload, and most microphone cover is only merely general at present Logical sponges cover either nonwoven cloth case, its antibacterial, bacteriostasis property are much insufficient.Therefore, the anti-microbial property of sponge product is particularly It is important.And it is current, although having many documents (CN101423613, CN102512355A) it has been reported that some environmentally friendly konjaku seas Continuous product and preparation method thereof, but not publicly how to further improve the anti-microbial property of sponge product.
The content of the invention
The object of the present invention is to provide a kind of sponge antibacterial filler and preparation method thereof, which has with antibacterial filler Excellent anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.
To achieve these goals, the present invention provides a kind of preparation method of sponge antibacterial filler, this method to include:
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added Enter mixed into limewash, boiling be made slurry M1;
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2;
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial Filler.
Through the above technical solutions, the present invention selection first by tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, The plants such as bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, which are added in limewash, to carry out pre-processing obtained coarse fodder M2, then again will Chitosan, allicin and green alga hydrochlorate, which are added in the coarse fodder M2, to carry out being mixed to get the sponge antibacterial filler;Into one Step improves the anti-microbial property of obtained filler.The preparation method of the antibacterial filler is simple, and raw material are simple and easy to get and cost is low It is honest and clean to widely use.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The endpoint of disclosed scope and any value are not limited to the accurate scope or value herein, these scopes or Value should be understood to comprising the value close to these scopes or value.For number range, between the endpoint value of each scope, respectively It can be combined with each other between the endpoint value of a scope and single point value, and individually between point value and obtain one or more New number range, these number ranges should be considered as specific open herein.
The present invention provides a kind of preparation method of sponge antibacterial filler, this method includes:
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added Enter mixed into limewash, boiling be made slurry M1;
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2;
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial Filler.
In above-mentioned technical proposal, the dosage selection of each raw material can select in wide scope, but obtained in order to improve Antibacterial filler anti-microbial property, it is preferable that the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, Bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100: 120-150: 10- 15∶5-15∶1-5∶1-5∶5-10∶1-5∶1-5∶1-5∶1-5∶1-5∶5-9∶5-10∶1-5∶1-3。
In above-mentioned technical proposal, the condition of the boiling can select in wide scope, but obtained in order to improve The anti-microbial property and preparation efficiency of antibacterial filler, it is preferable that the boiling includes the first boiling and the second boiling, and described second The temperature of boiling is higher than 30 DEG C -50 DEG C of first boiling.
In above-mentioned technical proposal, the condition of first boiling can select in wide scope, but in order to improve system Antibacterial filler anti-microbial property and boiling efficiency, it is preferable that the condition of first boiling is:Temperature is 100-110 DEG C, And/or the time is 4-7d.
In above-mentioned technical proposal, the time of second boiling can select in wide scope, but in order to improve system The anti-microbial property and boiling efficiency of the antibacterial filler obtained, it is preferable that the time of second boiling is 1-2d.
In above-mentioned technical proposal, the condition of the drying can select in wide scope, but prepare effect to improve Rate, it is preferable that the condition of the drying is:Temperature is 50-60 DEG C, and/or the time is 12-24h.
In above-mentioned technical proposal, the particle diameter of the coarse fodder M2 can select in wide scope, but described in order to improve Mutual synergistic effect between coarse fodder M2 and other raw materials, it is preferable that the mean particle size of the coarse fodder M2 is 50-100 μm.
In order to further improve the anti-microbial property of obtained antibacterial filler in above-mentioned technical proposal, preferably by the tea Leaf, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash It is preceding further comprising the steps of:
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and five Batch mixing is made after the broken sieving of taste;
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
In above-mentioned preparation method, the particle diameter of the batch mixing can select in wide scope, but in order to further improve The anti-microbial property of obtained antibacterial filler, it is preferable that the mean particle size of the batch mixing is 50-100 μm.
Sponge antibacterial filler made from a kind of above-mentioned preparation method is additionally provided in the present invention.
The present invention will be described in detail by way of examples below.
Embodiment 1
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added Enter after being mixed into limewash, first in 100 DEG C of boiling 7d, then in 130 DEG C of boiling 2d slurry M1 is made;
The slurry M1 is rinsed, shines white, dnockout, 24h is dried at 50 DEG C, (particle is put down so that coarse fodder M2 is made for grinding Equal particle diameter is 50 μm);
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial Filler;It is denoted as A1;
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100: 120: 10: 5: 1: 1: 5: 1: 1: 2: 1: 1: 5: 5: 1 ∶1。
Embodiment 2
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added Enter after being mixed into limewash, first in 105 DEG C of boiling 6d, then in 145 DEG C of boiling 2d slurry M1 is made;
The slurry M1 is rinsed, shines white, dnockout, 20h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding Equal particle diameter is 80 μm);
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial Filler;It is denoted as A2;
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100: 130: 13: 10: 3: 3: 8: 3: 3: 3: 3: 3: 8: 8: 3∶2。
Embodiment 3
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added Enter after being mixed into limewash, first in 110 DEG C of boiling 4d, then in 160 DEG C of boiling 1d slurry M1 is made;
The slurry M1 is rinsed, shines white, dnockout, 12h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding Equal particle diameter is 100 μm);
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial Filler;It is denoted as A3;
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100: 150: 15: 15: 5: 5: 10: 5: 5: 5: 5: 5: 9: 10∶5∶3。
Embodiment 4
The sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A4;Unlike by the tealeaves, Before the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash It is further comprising the steps of:
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and five Batch mixing is made after the broken sieving of taste (mean particle size is 100 μm);
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
Embodiment 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A5, unlike directly in 100 DEG C of boilings 9 days Slurry M1 is made afterwards.
Embodiment 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A6, unlike directly in 130 DEG C of boilings 9 days Slurry M1 is made afterwards.
Comparative example 1
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D1, the difference is that not adding tealeaves in raw material.
Comparative example 2
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D2, the difference is that not adding the leaf of bamboo in raw material.
Comparative example 3
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D3, the difference is that not adding eucalyptus in raw material Leaf.
Comparative example 4
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D4, gathers the difference is that not adding shell in raw material Sugar.
Comparative example 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D5, the difference is that not adding garlic in raw material Element.
Comparative example 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D6, the difference is that not adding green alga acid in raw material Salt.
Detect example 1
Obtained antibacterial sponge microphone cover A1-A6 and D1-D6 are placed in 25-30 DEG C of open environment, and air Humidity is 8 grams of water/m3, total plate count (n/cfug is detected by the method for national standard GB 4789.2-2010 after 7 days-1), specifically It the results are shown in Table 1.
Table 1
n/cfu·g-1
A1 7
A2 8
A3 8
A4 5
A5 15
A6 14
D1 25
D2 18
D3 20
D4 21
D5 22
D6 23
On the preferred embodiment of the present invention is described in detail, still, during present invention is not limited to the embodiments described above Detail, in the range of the technology design of the present invention, can carry out a variety of simple variants to technical scheme, these Simple variant belongs to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally The thought of invention, it should equally be considered as content disclosed in this invention.

Claims (10)

1. a kind of preparation method of sponge antibacterial filler, its spy are, including:
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added to Mixed in limewash, boiling be made slurry M1;
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2;
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 to carry out being mixed to get the sponge and filled out with antibacterial Material.
2. preparation method according to claim 1, wherein, the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100: 120-150:10-15:5-15:1-5:1-5:5-10:1-5:1-5:1-5:1-5:1-5:5-9:5-10:1-5:1-3.
3. preparation method according to claim 2, wherein, the boiling includes the first boiling and the second boiling, and described The temperature of second boiling is higher than 30 DEG C -50 DEG C of first boiling.
4. preparation method according to claim 3, wherein, the condition of first boiling is:Temperature is 100-110 DEG C, And/or the time is 4-7d.
5. preparation method according to claim 4, wherein, the time of second boiling is 1-2d.
6. preparation method according to claim 2, wherein, the condition of the drying is:Temperature is 50-60 DEG C, and/or when Between be 12-24h.
7. according to the preparation method described in any one in claim 1-6, wherein, the mean particle size of the coarse fodder M2 is 50-100μm。
8. according to the preparation method described in any one in claim 1-6, wherein, by the tealeaves, leaf of bamboo, eucalyptus leaves, white The root of Dahurian angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added to preceding further comprising the steps of in limewash:
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and Schisandra chinensis Batch mixing is made after broken sieving;
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
9. preparation method according to claim 8, wherein, the mean particle size of the batch mixing is 50-100 μm.
10. sponge antibacterial filler made from the preparation method in a kind of 1-9 as claim described in any one.
CN201710982207.7A 2017-10-20 2017-10-20 Sponge antibacterial filler and preparation method thereof Withdrawn CN107996635A (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103686520A (en) * 2012-09-22 2014-03-26 青岛道合生物科技有限公司 Biological antibacterial microphone sleeve
CN105944135A (en) * 2016-04-29 2016-09-21 武汉理工大学 Composite sponge and preparation method thereof
CN106620824A (en) * 2016-12-30 2017-05-10 广东海洋大学 Preparation method for efficient anti-bacterial composite hemostatic sponge

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Application publication date: 20180508