CN107955214A - Sponge antibacterial filler and preparation method thereof - Google Patents
Sponge antibacterial filler and preparation method thereof Download PDFInfo
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- CN107955214A CN107955214A CN201710982218.5A CN201710982218A CN107955214A CN 107955214 A CN107955214 A CN 107955214A CN 201710982218 A CN201710982218 A CN 201710982218A CN 107955214 A CN107955214 A CN 107955214A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L5/00—Compositions of polysaccharides or of their derivatives not provided for in groups C08L1/00 or C08L3/00
- C08L5/08—Chitin; Chondroitin sulfate; Hyaluronic acid; Derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fodder In General (AREA)
Abstract
The invention discloses a kind of sponge antibacterial filler and preparation method thereof, this method includes：Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell are added in limewash mixed, boiling be made slurry M1；The slurry is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；Chitosan, allicin and curcumol are added in the coarse fodder M2 to be mixed the sponge antibacterial filler is made.Sponge antibacterial has an excellent anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.
Description
Technical field
The present invention relates to sponge manufacturing field, and in particular, to a kind of sponge antibacterial filler and preparation method thereof.
Background technology
Sponge products it is widely used, such as face cleaning is flutterred, cleaning sponge and sanitary microphone cover etc..Wherein, microphone is either
The speech ciphering equipments such as microphone, all can frequently use in daily life and work, rise and the prevalence of especially current network direct broadcasting
Under trend, the routine work of main broadcasters is exactly against microphone or microphone.
It is well known that when using microphone or microphone, mouth is closer apart from the distance of microphone, so whether makes
With public place microphone in place such as KTV, bar or it is live when main broadcaster dedicated microphone, microphone, using one section
It all can cause microphone surface moisture after time and easily grow bacterium, so may result in microphone user and be easily subject to bacterium sense
Even germ cross-infection is contaminated, so as to seriously affect the health of user.
At present, microphone cover is as a kind of a kind of one of effective measures that can reduce the growth of microphone surface bacteria, but very
More businessmans are unwilling to replace microphone cover in time for cost-effective or workload, and most microphone cover is only merely general at present
Logical sponges cover either nonwoven cloth case, its antibacterial, bacteriostasis property are much insufficient.Therefore, the anti-microbial property of sponge product is particularly
It is important.And it is current, although having many documents (CN101423613, CN102512355A) it has been reported that some environmentally friendly konjaku seas
Continuous product and preparation method thereof, but not publicly how to further improve the anti-microbial property of sponge product.
The content of the invention
The object of the present invention is to provide a kind of sponge antibacterial filler and preparation method thereof, sponge antibacterial has excellent
Anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.
To achieve these goals, the present invention provides a kind of preparation method of sponge antibacterial filler, this method to include：
By tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust
Worm shell be added in limewash mixed, boiling be made slurry M1；
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Chitosan, allicin and curcumol are added in the coarse fodder M2 to be mixed the sponge antibacterial is made
Filler.
Through the above technical solutions, present invention selection is first by tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, smalt
The plants such as leaf, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell and insect shell class are added in limewash the pretreatment system that carries out
Coarse fodder M2 is obtained, then chitosan, allicin and curcumol are added in the coarse fodder M2 again and carry out being mixed to get the sponge
Use antibacterial filler；Further increase the anti-microbial property of obtained filler.The preparation method of the antibacterial filler is simple, raw material letter
Singly it is easy to get and of low cost can widely uses.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The endpoint of disclosed scope and any value are not limited to the accurate scope or value herein, these scopes or
Value should be understood to comprising the value close to these scopes or value.For number range, between the endpoint value of each scope, respectively
It can be combined with each other between the endpoint value of a scope and single point value, and individually between point value and obtain one or more
New number range, these number ranges should be considered as specific open herein.
The present invention provides a kind of preparation method of sponge antibacterial filler, this method includes：
By tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust
Worm shell be added in limewash mixed, boiling be made slurry M1；
The slurry is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Chitosan, allicin and curcumol are added in the coarse fodder M2 to be mixed the sponge antibacterial is made
Filler.
In above-mentioned technical proposal, the dosage selection of each raw material can select in wide scope, but obtained in order to improve
Antibacterial filler anti-microbial property, it is preferable that the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, smalt
Leaf, peppermint, Schisandra chinensis, crab shell, hodmadod, locust shell, chitosan, the weight ratio of allicin and curcumol are 100：120-150：
10-15：5-15：1-5：1-5：5-10：1-5：1-5：1-5：5-10：3-5：5-9：5-10：1-5：1-3.
In above-mentioned technical proposal, the condition of the boiling can select in wide scope, but obtained in order to improve
The anti-microbial property and preparation efficiency of antibacterial filler, it is preferable that the boiling includes the first boiling and the second boiling, and described second
The temperature of boiling is higher than 30 DEG C -50 DEG C of first boiling.
In above-mentioned technical proposal, the condition of first boiling can select in wide scope, but in order to improve system
Antibacterial filler anti-microbial property and boiling efficiency, it is preferable that the condition of first boiling is：Temperature is 100-110 DEG C,
And/or the time is 4-7d.
In above-mentioned technical proposal, the time of second boiling can select in wide scope, but in order to improve system
The anti-microbial property and boiling efficiency of the antibacterial filler obtained, it is preferable that the time of second boiling is 1-2d.
In above-mentioned technical proposal, the condition of the drying can select in wide scope, but prepare effect to improve
Rate, it is preferable that the condition of the drying is：Temperature is 50-60 DEG C, and/or the time is 12-24h.
In above-mentioned technical proposal, the particle diameter of the coarse fodder M2 can select in wide scope, but described in order to improve
Mutual synergistic effect between coarse fodder M2 and other raw materials, it is preferable that the mean particle size of the coarse fodder M2 is 50-100 μm.
In order to further improve the anti-microbial property of obtained antibacterial filler in above-mentioned technical proposal, it is preferable that by the tea
Leaf, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell are added to stone
It is preceding further comprising the steps of in buck：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, crab shell, Cortex Magnoliae Officinalis, Cortex Phellodendri, hodmadod, locust shell, folium isatidis, peppermint
Batch mixing is made after crushing sieving with Schisandra chinensis,
Batch mixing is added in the limewash again mixed, boiling be made the slurry M1.
In above-mentioned preparation method, the particle diameter of the batch mixing can select in wide scope, but in order to further improve
The anti-microbial property of obtained antibacterial filler, it is preferable that the mean particle size of the batch mixing is 100-150 μm.
Sponge antibacterial filler made from a kind of above-mentioned preparation method is additionally provided in the present invention.
The present invention will be described in detail by way of examples below.
Embodiment 1
By the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell,
Hodmadod and locust shell are added to after being mixed in limewash, first in 100 DEG C of boiling 7d, then in 130 DEG C of boiling 2d to make
Obtain slurry M1；
The slurry M1 is rinsed, shines white, dnockout, 24h is dried at 50 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 50 μm)；
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial
Filler；It is denoted as A1；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100：120：10：5：1：1：5：1：1：1：5：3：5：5：
1：1.
Embodiment 2
By the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell,
Hodmadod and locust shell are added to after being mixed in limewash, first in 105 DEG C of boiling 6d, then in 145 DEG C of boiling 2d to make
Obtain slurry M1；
The slurry M1 is rinsed, shines white, dnockout, 20h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 80 μm)；
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial
Filler；It is denoted as A2；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100：130：13：10：3：3：8：3：3：3：7：4：6：8：
3：2.
Embodiment 3
By the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell,
Hodmadod and locust shell are added to after being mixed in limewash, first in 110 DEG C of boiling 4d, then in 160 DEG C of boiling 1d to make
Obtain slurry M1；
The slurry M1 is rinsed, shines white, dnockout, 12h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 100 μm)；
Chitosan, allicin and green alga hydrochlorate are added in the coarse fodder M2 and carry out being mixed to get the sponge antibacterial
Filler；It is denoted as A3；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, chitosan, the weight ratio of allicin and green alga hydrochlorate are 100：150：15：15：5：5：10：5：5：5：10：5：9：
10：5：3.
Embodiment 4
The sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A4；Unlike by the tealeaves,
The leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell are added to limewash
In it is preceding further comprising the steps of：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod
Batch mixing is made after crushing sieving with locust shell (mean particle size is 130 μm)；
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
Embodiment 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A5, unlike directly in 100 DEG C of boilings 9 days
Slurry M1 is made afterwards.
Embodiment 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A6, unlike directly in 130 DEG C of boilings 9 days
Slurry M1 is made afterwards.
Comparative example 1
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D1, the difference is that not adding crab shell in raw material.
Comparative example 2
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D2, the difference is that not adding snail in raw material
Shell.
Comparative example 3
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D3, the difference is that not adding locust in raw material
Shell.
Comparative example 4
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D4, gathers the difference is that not adding shell in raw material
Sugar.
Comparative example 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D5, the difference is that not adding garlic in raw material
Element.
Comparative example 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D6, the difference is that not adding turmeric in raw material
Alcohol.
Detect example 1
Obtained antibacterial sponge microphone cover A1-A6 and D1-D6 are placed in 25-30 DEG C of open environment, and air
Humidity is 8 grams of water/m3, total plate count (n/cfug is detected by the method for national standard GB 4789.2-2010 after 7 days-1), specifically
It the results are shown in Table 1.
Table 1
| n/cfu·g-1 | |
| A1 | 6 |
| A2 | 8 |
| A3 | 9 |
| A4 | 6 |
| A5 | 15 |
| A6 | 14 |
| D1 | 25 |
| D2 | 21 |
| D3 | 20 |
| D4 | 21 |
| D5 | 22 |
| D6 | 23 |
The preferred embodiment of the present invention described in detail above, still, during present invention is not limited to the embodiments described above
Detail, in the range of the technology design of the present invention, a variety of simple variants can be carried out to technical scheme, this
A little simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (10)
1. a kind of preparation method of sponge antibacterial filler, its spy are, including：
By tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell
Be added in limewash mixed, boiling be made slurry M1；
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Chitosan, allicin and curcumol are added in the coarse fodder M2 mixed i.e. be made the sponge filled out with antibacterial
Material.
2. preparation method according to claim 1, wherein, the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, Cortex Magnoliae Officinalis,
Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod, locust shell, chitosan, the weight ratio of allicin and curcumol are
100：120-150：10-15：5-15：1-5：1-5：5-10：1-5：1-5：1-5：5-10：3-5：5-9：5-10：1-5：1-3.
3. preparation method according to claim 2, wherein, the boiling includes the first boiling and the second boiling, and described
The temperature of second boiling is higher than 30 DEG C -50 DEG C of first boiling.
4. preparation method according to claim 3, wherein, the condition of first boiling is：Temperature is 100-110 DEG C,
And/or the time is 4-7d.
5. preparation method according to claim 4, wherein, the time of second boiling is 1-2d.
6. preparation method according to claim 2, wherein, the condition of the drying is：Temperature is 50-60 DEG C, and/or when
Between be 12-24h.
7. according to the preparation method described in any one in claim 1-6, wherein, the mean particle size of the coarse fodder M2 is
50-100μm。
8. according to the preparation method described in any one in claim 1-6, wherein, by the tealeaves, leaf of bamboo, eucalyptus leaves, white
The root of Dahurian angelica, Cortex Magnoliae Officinalis, Cortex Phellodendri, folium isatidis, peppermint, Schisandra chinensis, crab shell, hodmadod and locust shell further include following before being added in limewash
Step：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, crab shell, Cortex Magnoliae Officinalis, Cortex Phellodendri, hodmadod, locust shell, folium isatidis, peppermint and five
Batch mixing is made after the broken sieving of taste,
Batch mixing is added in the limewash again mixed, boiling be made the slurry M1.
9. preparation method according to claim 8, wherein, the mean particle size of the batch mixing is 100-150 μm.
10. sponge antibacterial filler made from the preparation method in a kind of 1-9 as claim described in any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710982218.5A CN107955214A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710982218.5A CN107955214A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107955214A true CN107955214A (en) | 2018-04-24 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710982218.5A Withdrawn CN107955214A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102585300A (en) * | 2012-01-06 | 2012-07-18 | 周允 | Plant fiber sponge with effects of diminishing inflammation and detoxifying and preparation method for plant fiber sponge |
| CN103686520A (en) * | 2012-09-22 | 2014-03-26 | 青岛道合生物科技有限公司 | Biological antibacterial microphone sleeve |
-
2017
- 2017-10-20 CN CN201710982218.5A patent/CN107955214A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102585300A (en) * | 2012-01-06 | 2012-07-18 | 周允 | Plant fiber sponge with effects of diminishing inflammation and detoxifying and preparation method for plant fiber sponge |
| CN103686520A (en) * | 2012-09-22 | 2014-03-26 | 青岛道合生物科技有限公司 | Biological antibacterial microphone sleeve |
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Application publication date: 20180424 |