CN107987305A - Sponge antibacterial filler and preparation method thereof - Google Patents
Sponge antibacterial filler and preparation method thereof Download PDFInfo
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- CN107987305A CN107987305A CN201710982202.4A CN201710982202A CN107987305A CN 107987305 A CN107987305 A CN 107987305A CN 201710982202 A CN201710982202 A CN 201710982202A CN 107987305 A CN107987305 A CN 107987305A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0095—Mixtures of at least two compounding ingredients belonging to different one-dot groups
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/0014—Use of organic additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0058—Biocides
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- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of sponge antibacterial filler and preparation method thereof, including：Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash mixed, boiling be made slurry M1；The slurry is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 to be mixed the sponge antibacterial filler is made.Sponge antibacterial filler has an excellent anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.
Description
Technical field
The present invention relates to sponge manufacturing field, and in particular, to a kind of sponge antibacterial filler and preparation method thereof.
Background technology
Sponge products it is widely used, such as face cleaning is flutterred, cleaning sponge and sanitary microphone cover etc..Wherein, microphone is either
The speech ciphering equipments such as microphone, all can frequently use in daily life and work, rise and the prevalence of especially current network direct broadcasting
Under trend, the routine work of main broadcasters is exactly against microphone or microphone.
It is well known that when using microphone or microphone, mouth is closer apart from the distance of microphone, so whether makes
With public place microphone in place such as KTV, bar or it is live when main broadcaster dedicated microphone, microphone, using one section
It all can cause microphone surface moisture after time and easily grow bacterium, so may result in microphone user and be easily subject to bacterium sense
Even germ cross-infection is contaminated, so as to seriously affect the health of user.
At present, microphone cover is as a kind of a kind of one of effective measures that can reduce the growth of microphone surface bacteria, but very
More businessmans are unwilling to replace microphone cover in time for cost-effective or workload, and most microphone cover is only merely general at present
Logical sponges cover either nonwoven cloth case, its antibacterial, bacteriostasis property are much insufficient.Therefore, the anti-microbial property of sponge product is particularly
It is important.And it is current, although having many documents (CN101423613, CN102512355A) it has been reported that some environmentally friendly konjaku seas
Continuous product and preparation method thereof, but not publicly how to further improve the anti-microbial property of sponge product.
The content of the invention
The object of the present invention is to provide a kind of sponge antibacterial filler and preparation method thereof, which has with antibacterial filler
Excellent anti-microbial property, and the antibacterial filler raw material sources are extensive and durable environmental protection, suitable for widely using.
To achieve these goals, the present invention provides a kind of preparation method of sponge antibacterial filler, this method to include：
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added
Enter mixed into limewash, boiling be made slurry M1；
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 and be mixed to get the sponge and use resisting
Bacterium filler.
Through the above technical solutions, the present invention selection first by tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri,
The plants such as bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, which are added in limewash, to carry out pre-processing obtained coarse fodder M2, then again will
Curcumol, citral and dihydro turmerone, which are added in the coarse fodder M2, to carry out being mixed to get the sponge antibacterial filler；Into
One step improves the anti-microbial property of obtained filler.The preparation method of the antibacterial filler is simple, and raw material are simple and easy to get and cost
It is cheap to widely use.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below.It is it should be appreciated that described herein specific
Embodiment is merely to illustrate and explain the present invention, and is not intended to limit the invention.
The endpoint of disclosed scope and any value are not limited to the accurate scope or value herein, these scopes or
Value should be understood to comprising the value close to these scopes or value.For number range, between the endpoint value of each scope, respectively
It can be combined with each other between the endpoint value of a scope and single point value, and individually between point value and obtain one or more
New number range, these number ranges should be considered as specific open herein.
The present invention provides a kind of preparation method of sponge antibacterial filler, this method includes：
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added
Enter mixed into limewash, boiling be made slurry M1；
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 and be mixed to get the sponge and use resisting
Bacterium filler.
In above-mentioned technical proposal, the dosage selection of each raw material can select in wide scope, but obtained in order to improve
Antibacterial filler anti-microbial property, it is preferable that the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri,
Bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, curcumol, the weight ratio of citral and dihydro turmerone are 100：120-150：
10-15：5-15：1-5：1-5：5-10：1-5：1-5：1-5：1-5：1-5：5-9：3-8：5-10：1-3.
In above-mentioned technical proposal, the condition of the boiling can select in wide scope, but obtained in order to improve
The anti-microbial property and preparation efficiency of antibacterial filler, it is preferable that the boiling includes the first boiling and the second boiling, and described second
The temperature of boiling is higher than 30 DEG C -50 DEG C of first boiling.
In above-mentioned technical proposal, the condition of first boiling can select in wide scope, but in order to improve system
Antibacterial filler anti-microbial property and boiling efficiency, it is preferable that the condition of first boiling is：Temperature is 100-115 DEG C,
And/or the time is 5-7d.
In above-mentioned technical proposal, the time of second boiling can select in wide scope, but in order to improve system
The anti-microbial property and boiling efficiency of the antibacterial filler obtained, it is preferable that the time of second boiling is 1-2d.
In above-mentioned technical proposal, the condition of the drying can select in wide scope, but prepare effect to improve
Rate, it is preferable that the condition of the drying is：Temperature is 50-60 DEG C, and/or the time is 12-24h.
In above-mentioned technical proposal, the particle diameter of the coarse fodder M2 can select in wide scope, but described in order to improve
Mutual synergistic effect between coarse fodder M2 and other raw materials, it is preferable that the mean particle size of the coarse fodder M2 is 100-150 μ
m。
In order to further improve the anti-microbial property of obtained antibacterial filler in above-mentioned technical proposal, preferably by the tea
Leaf, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash
It is preceding further comprising the steps of：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and five
Batch mixing is made after the broken sieving of taste；
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
In above-mentioned preparation method, the particle diameter of the batch mixing can select in wide scope, but in order to further improve
The anti-microbial property of obtained antibacterial filler, it is preferable that the mean particle size of the batch mixing is 100-200 μm.
Sponge antibacterial filler made from a kind of above-mentioned preparation method is additionally provided in the present invention.
The present invention will be described in detail by way of examples below.
Embodiment 1
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added
Enter after being mixed into limewash, first in 100 DEG C of boiling 7d, then in 130 DEG C of boiling 2d slurry M1 is made；
The slurry M1 is rinsed, shines white, dnockout, 24h is dried at 50 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 100 μm)；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 and be mixed to get the sponge and use resisting
Bacterium filler；It is denoted as A1；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, curcumol, the weight ratio of citral and dihydro turmerone are 100：120：10：5：1：1：5：1：1：2：1：1：5：
3：5：1.
Embodiment 2
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added
Enter after being mixed into limewash, first in 105 DEG C of boiling 6d, then in 145 DEG C of boiling 2d slurry M1 is made；
The slurry M1 is rinsed, shines white, dnockout, 20h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 130 μm)；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 and be mixed to get the sponge and use resisting
Bacterium filler；It is denoted as A2；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, curcumol, the weight ratio of citral and dihydro turmerone are 100：130：13：10：3：3：8：3：3：3：3：3：8：
6：8：2.
Embodiment 3
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added
Enter after being mixed into limewash, first in 115 DEG C of boiling 5d, then in 165 DEG C of boiling 1d slurry M1 is made；
The slurry M1 is rinsed, shines white, dnockout, 12h is dried at 60 DEG C, (particle is put down so that coarse fodder M2 is made for grinding
Equal particle diameter is 150 μm)；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 and be mixed to get the sponge and use resisting
Bacterium filler；It is denoted as A3；
Wherein, tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, thin
Lotus, Schisandra chinensis, curcumol, the weight ratio of citral and dihydro turmerone are 100：150：15：15：5：5：10：5：5：5：5：5：
9：8：10：3.
Embodiment 4
The sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A4；Unlike by the tealeaves,
Before the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added in limewash
It is further comprising the steps of：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and five
Batch mixing is made after the broken sieving of taste (mean particle size is 150 μm)；
The batch mixing is then added in the limewash mixed, boiling be made the slurry M1.
Embodiment 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A5, unlike directly in 100 DEG C of boilings 9 days
Slurry M1 is made afterwards.
Embodiment 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as A6, unlike directly in 130 DEG C of boilings 9 days
Slurry M1 is made afterwards.
Comparative example 1
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D1, the difference is that not adding tealeaves in raw material.
Comparative example 2
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D2, the difference is that not adding the leaf of bamboo in raw material.
Comparative example 3
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D3, the difference is that not adding eucalyptus in raw material
Leaf.
Comparative example 4
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D4, the difference is that not adding turmeric in raw material
Alcohol.
Comparative example 5
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D5, the difference is that not adding lemon in raw material
Aldehyde.
Comparative example 6
Sponge antibacterial filler is prepared Following the procedure of Example 1, is denoted as D6, the difference is that not adding dihydro ginger in raw material
Flavones.
Detect example 1
Obtained antibacterial sponge microphone cover A1-A6 and D1-D6 are placed in 25-30 DEG C of open environment, and air
Humidity is 8 grams of water/m3, total plate count (n/cfug is detected by the method for national standard GB 4789.2-2010 after 7 days-1), specifically
It the results are shown in Table 1.
Table 1
| n/cfu·g-1 | |
| A1 | 8 |
| A2 | 9 |
| A3 | 7 |
| A4 | 6 |
| A5 | 13 |
| A6 | 14 |
| D1 | 25 |
| D2 | 18 |
| D3 | 20 |
| D4 | 21 |
| D5 | 22 |
| D6 | 23 |
On the preferred embodiment of the present invention is described in detail, still, during present invention is not limited to the embodiments described above
Detail, in the range of the technology design of the present invention, can carry out a variety of simple variants to technical scheme, these
Simple variant belongs to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, can be combined by any suitable means, in order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.
Claims (10)
1. a kind of preparation method of sponge antibacterial filler, its spy are, including：
Tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added to
Mixed in limewash, boiling be made slurry M1；
The slurry M1 is rinsed, shines white, dnockout, drying, grinding with obtained coarse fodder M2；
Curcumol, citral and dihydro turmerone are added in the coarse fodder M2 to be mixed the sponge antibacterial is made
Filler.
2. preparation method according to claim 1, wherein, the tealeaves, limewash, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine,
Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis, curcumol, the weight ratio of citral and dihydro turmerone are
100：120-150：10-15：5-15：1-5：1-5：5-10：1-5：1-5：1-5：1-5：1-5：5-9：3-8：5-10：1-3.
3. preparation method according to claim 2, wherein, the boiling includes the first boiling and the second boiling, and described
The temperature of second boiling is higher than 30 DEG C -50 DEG C of first boiling.
4. preparation method according to claim 3, wherein, the condition of first boiling is：Temperature is 100-115 DEG C,
And/or the time is 5-7d.
5. preparation method according to claim 4, wherein, the time of second boiling is 1-2d.
6. preparation method according to claim 2, wherein, the condition of the drying is：Temperature is 50-60 DEG C, and/or when
Between be 12-24h.
7. according to the preparation method described in any one in claim 1-6, wherein, the mean particle size of the coarse fodder M2 is
100-150μm。
8. according to the preparation method described in any one in claim 1-6, wherein, by the tealeaves, leaf of bamboo, eucalyptus leaves, white
The root of Dahurian angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint, Schisandra chinensis are added to preceding further comprising the steps of in limewash：
By the tealeaves, the leaf of bamboo, eucalyptus leaves, the root of Dahurain angelica, cape jasmine, Cortex Magnoliae Officinalis, Cortex Phellodendri, bush, ophiopogon, folium isatidis, peppermint and Schisandra chinensis
Batch mixing is made after broken sieving,
The batch mixing is added in the limewash again mixed, boiling be made the slurry M1.
9. preparation method according to claim 8, wherein, the mean particle size of the batch mixing is 100-200 μm.
10. sponge antibacterial filler made from the preparation method in a kind of 1-9 as claim described in any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710982202.4A CN107987305A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710982202.4A CN107987305A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107987305A true CN107987305A (en) | 2018-05-04 |
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ID=62029872
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| CN201710982202.4A Withdrawn CN107987305A (en) | 2017-10-20 | 2017-10-20 | Sponge antibacterial filler and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102585300A (en) * | 2012-01-06 | 2012-07-18 | 周允 | Plant fiber sponge with effects of diminishing inflammation and detoxifying and preparation method for plant fiber sponge |
| CN103686520A (en) * | 2012-09-22 | 2014-03-26 | 青岛道合生物科技有限公司 | Biological antibacterial microphone sleeve |
-
2017
- 2017-10-20 CN CN201710982202.4A patent/CN107987305A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102585300A (en) * | 2012-01-06 | 2012-07-18 | 周允 | Plant fiber sponge with effects of diminishing inflammation and detoxifying and preparation method for plant fiber sponge |
| CN103686520A (en) * | 2012-09-22 | 2014-03-26 | 青岛道合生物科技有限公司 | Biological antibacterial microphone sleeve |
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Application publication date: 20180504 |