CN104164123B - Multifunctional waterborne environment-friendly internal wall putty and production method thereof - Google Patents
Multifunctional waterborne environment-friendly internal wall putty and production method thereof Download PDFInfo
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- CN104164123B CN104164123B CN201410411819.7A CN201410411819A CN104164123B CN 104164123 B CN104164123 B CN 104164123B CN 201410411819 A CN201410411819 A CN 201410411819A CN 104164123 B CN104164123 B CN 104164123B
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses multifunctional waterborne environment-friendly internal wall putty and a production method thereof. The wall putty not only can purify air to be beneficial for human health by releasing air negative ions for long time, and but also can play a certain role of restraining and killing multiple bacteria and fungi such as staphylococcus, colon bacillus and gram-positive bacteria, and simultaneously has fragrant odor, is clean and refreshing, and can mitigate tension as well repel mosquitoes; the wall putty has the advantages of strong adhesion, good leveling property, no curling, resistance against washing and polishing, no falling, no cracks, non-toxicity, harmlessness and nonradioactive, can effectively protect wall bodies, can be combined with various paints, more importantly, has no adverse impact on the bodies of people of all age when used for long time, and therefore has a wide application prospect.
Description
Technical field
The present invention relates to a kind of building and ornament materials, particularly to multifunctional aqueous environment protection interior wall putty and manufacture method.
Background technology
Powder of lacquer putty for use on, it is widely used in construction and decoration as metope packing material, but the anti-corrosion material used in traditional putty, also multiple volatile harmful material such as formaldehyde, benzene, radon, ammonia is contained in it, pollution room air, and present building generally divulge information not good, for a long time in such room, health for people brings serious threat, destroys the living environment of people；On the other hand, traditional putty paste only serves filling effect, does not possess other functions, can not meet the daily demand of people.
Content of the invention
In view of the shortcomings of the prior art, one of the technical problem to be solved is to provide a kind of Environmental Safety, and nontoxic, smell is pure and fresh, there is the multifunctional aqueous environment protection interior wall putty of health-care effect, negative aeroion not only can be discharged for a long time, purify air, beneficial to health；Also to staphylococcus, Escherichia coli, gram-positive bacteria etc., multiple germs and fungi have certain suppression, killing action；Fragrant odour simultaneously, pure and fresh soothe the spirit, pressure of releiving, also can expelling mosquito, harmful effect will not be produced it is adaptable to each age groups to human body.
The two of the technical problem to be solved are the manufacture methods providing multifunctional aqueous environment protection interior wall putty.
The purpose of the present invention is achieved by the following technical solution：
Multifunctional aqueous environment protection interior wall putty, its raw material is by the material composition of following parts by weight：Water 200-280 part, heavy calcium carbonate 55-70 part, sierozem power 16-25 part, white cement 10-15 part, hydroxypropyl methyl cellulose 2.5-4 part, anion natural mineral powder 3-6 part, brightening agent 2-2.5 part, tarragon 2-3 part, selfheal 2-3 part, anemone vitifolia 1-2 part, camphorwood 1-2 part, agalloch eaglewood 1-1.5 part, desmodium triquetrum 2-3 part, ambergris 0.5-1 part, described anion natural mineral powder is tourmaline, lanthanide rare composite salt and titanium oxide by weight 4：2：4 mixture, wherein tourmaline are dravite and elbaite by weight 5：5 mixture.
Specifically, the fineness of described anion natural mineral powder is 1000-8000 mesh；The viscosity of described hydroxypropyl methyl cellulose is 80000-100000
mPa•s；The fineness particle diameter of described heavy calcium carbonate is 600-1200 mesh；The fineness particle diameter of described sierozem power is 600-1200 mesh；The fineness particle diameter of described white cement is 500-800 mesh；Described brightening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid is initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
The manufacture method of multifunctional aqueous environment protection interior wall putty, is made up of following step：
S1, take tarragon 2-3 part, selfheal 2-3 part, anemone vitifolia 1-2 part respectively by above-mentioned each component, camphorwood 1-2 part, agalloch eaglewood 1-1.5 part, desmodium triquetrum 2-3 part, ambergris 0.5-1 part, and put into the herb powder being crushed to 800-1200 mesh in micronizer respectively, standby；
S2, the herb powder in S1 and other raw material are put in large-scale mixing and blending machine, add appropriate water, be sufficiently stirred for mixing well 15-20 minute, get product.
The present invention with reference to modern Chinese medicine pharmacological research, verifies from the drug screening of existing Chinese medicine and repeatedly, gives full play to each component and act synergistically, the effect of the Chinese medicine material employed in it is described as follows.
Tarragon：All there is antibacterial action to 10 kinds of gram-positive Aeromonas bacterias such as bacillus anthracis, Alpha-hemolytic streptococcus, B- Streptococcus hemolyticus, corynebacterium diphtheriae, bacillus pseudodiphthericus, lung diplococcoid, staphylococcus aureus, Staphylococcus citreus, white Portugal Portugal coccus, hay bacilluses in vitro, also have bacteriostasis for multiple pathomycetes.
Selfheal：Cold in nature, sweet, pungent, slight bitter, there is to let out clearly irascibility, mass dissipating and swelling eliminating, clearing heat and detoxicating, expelling phlegm and arresting coughing, cooling blood and hemostasis, all have certain inhibitory action to shigella dysenteriae, typhoid bacillus, comma bacillus, Escherichia coli, proteus, Pseudomonas aeruginosa and staphylococcus, streptococcus and Bacillus tuberculosis.Selfheal can make the pulmonary lesion of experimental M disease mouse mitigate.Selfheal fresh goods is squeezed the juice all has inhibitory action to staphylococcus aureus, beta hemolytic streptococcus, Escherichia coli, typhoid bacillus, shigella dysenteriae, corynebacterium diphtheriae, bacillus anthracis, Pseudomonas aeruginosa.Flooding agent（1：4）In vitro also there is different degrees of inhibitory action to some common pathogenic dermatophytes such as trichophyton schoenleini, Du big belly microspore achorions difficult to understand.
Anemone vitifolia：①《Shaanxi Chinese herbal medicine》：" bitter, cool, slightly poisonous.”②《Chinese herbal medicine is commonly used in Sichuan》：" toil, temperature, slightly poisonous.” 【Chemical composition】Root and herb contain Anemonin (anemonin) and triterpene soap oleanolic acid -3-O- β-D- ribopyranoside base-(1 → 3)-α-L- rhamnopyranosyl-(1 → 3)-α-L- arabopyranose glucoside, oleanolic acid 3-O- β-D- ribopyranoside base-(1 → 3)-α-L- rhamnopyranosyl-(1 → 2)-β-D- xylopyranose glucoside, and oleanolic acid.【Function cures mainly】Kill maggot, wriggler, change long-pending, detumescence, the scattered stasis of blood, control stubborn dermatitis, the favus of the scalp, malaria, infantile malnutrition, dysentery, carbuncle furuncle sore swells, scrofula, traumatic injury.
Camphorwood：Aiphyllium, bark yellowish-brown, there is irregular longitudinal crack, on the south main product the Changjiang river and southwestern various places.Winter cuts down trees and splits broken or be sawn into bulk, dries or air-dries.Timber bulk is not of uniform size, surface rufous to burgundy, the visible annual ring in cross section.Matter is again hard.There is strong camphor fragrance, taste is refrigerant, have pungent sense, warm in nature, taste is pungent；Sensible can ward off dirty, warm in pain, dampness removing desinsection.
Agalloch eaglewood：《Compendium of Materia Medica》Record that wood has strong antibacterial efficacy, fragrance enters spleen, refreshing clearly qi-regulating, tonifying five zang organs, relieving cough and reducing sputum, warm stomach temperature spleen, ventilation analgesic therapy, can be used as medicine, be first-class medicinal material superfine product.
Ambergris：It is lasting spices the most lasting, any spices all can not compare favourably therewith in the world, have the saying of " perfume of imperial saliva and life coexist ".《Compendium of Materia Medica》Described in：Ambergris can invigorate blood circulation, beneficial marrow, supporing yang road, promoting blood circulation, resolving sputum and relieving asthma；A lump in the abdomen causing distension and pain；Trusted subordinate's pain；Coma；《Detailed outline is picked up any lost article from the road》：Promoting blood circulation, beneficial marrow, supporing yang road, promoting blood circulation.Liao Yongyan again：Promoting diuresis for stranguria, dissipating bind, knot of cooling down, by labor worm.
Beneficial effects of the present invention：
The present invention is nontoxic, and smell is pure and fresh, has health-care effect, is conducive to health, and it still is able to keep original intensity and quality after the other function ingredients of appropriate interpolation.
1st, tourmaline is a kind of silicate mineral, and its chemical formula is Na (Mg, Fe, Mn, Li, Al) 3Al6 (Si6O18) (Bo3) 3 (OH, F) 4, it is contacted with hydrone under electrostatic field, just hydrone can be ionized into hydrogen ion（H+）With hydroxide ion (OH-), hydroxide ion and water molecules formation basic hydroxide group anion（H2O•OH-）, as " negative aeroion ", current scientific research proves：Anion can not only facilitate human body synthesis and vitamin storage, the physiological activity of strengthening and human activin, have highly important impact to the vital movement of human body and other biological, be referred to as " air vitamin ".Anion effectively adsorbs indoor harmful substance, the such as construction and decoration harmful substance such as formaldehyde, toluene, not only itself does not increase pollution, and Cress room air, it is inherently eliminated construction and decoration syndrome, ensure that health is unaffected, be a kind of decorating and renovating material of environmental protection.
2nd, the traditional Chinese medicine ingredients containing in the present invention：Tarragon, selfheal, anemone vitifolia, camphorwood, agalloch eaglewood, desmodium triquetrum and ambergris, can not only expelling mosquito, also to staphylococcus, tubercle bacillus, Pseudomonas aeruginosa, gram-negative bacteria and gram-positive bacteria etc., multiple germs and fungi have certain suppression, killing action, breathing problem can be prevented, strengthen immune function of human body；Can fresh air, and can restraining and sterilizing bacteria, fragrant odour simultaneously, property is gentle, pure and fresh soothe the spirit, help hormone secretion, anxiety of releiving, the effects such as improve insomnia, can help for sleep it is adaptable to the decoration of bedroom interior wall.
In addition; adhesive force of the present invention is strong, good leveling property; do not roll up skin, scrubbing resistance, resistance to polishing, do not fall off, be not cracked, nontoxic, harmless, "dead"; body of wall can effectively be protected; and organically combine with various coating, more it is essential that the Long-Time Service present invention will not produce harmful effect to human body; it is applied to each age groups, there is application prospect widely.
Specific embodiment
Embodiment 1.
Multifunctional aqueous environment protection interior wall putty, its raw material is by the material composition of following parts by weight：Water 200kg, heavy calcium carbonate 70 kg, sierozem power 16 kg, white cement 15v, hydroxypropyl methyl cellulose 2.5 kg, anion natural mineral powder 6 kg, brightening agent 2 kg, tarragon 3 kg, selfheal 2 kg, anemone vitifolia 2 kg, camphorwood 1 kg, agalloch eaglewood 1.5 kg, desmodium triquetrum 2 kg, ambergris 1 kg, described anion natural mineral powder is tourmaline, lanthanide rare composite salt and titanium oxide by weight 4：2：4 mixture, wherein tourmaline are dravite and elbaite by weight 5：5 mixture.
Specifically, the fineness of described anion natural mineral powder is 8000 mesh；The viscosity of described hydroxypropyl methyl cellulose is 80000mPa s；The fineness particle diameter of described heavy calcium carbonate is 700；The fineness particle diameter of described sierozem power is 700 mesh；The fineness particle diameter of described white cement is 600 mesh；Described brightening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid is initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
The manufacture method of multifunctional aqueous environment protection interior wall putty, is made up of following step：
S1, take tarragon 3 kg, selfheal 2 kg, anemone vitifolia 2 kg, camphorwood 1 kg, agalloch eaglewood 1.5 kg, desmodium triquetrum 2 kg, ambergris 1 kg respectively by above-mentioned each component, and put into the herb powder being crushed to 1000 mesh in micronizer respectively, standby；
S2, the herb powder in S1 and other raw material are put into the water adding 200kg in large-scale mixing and blending machine, be sufficiently stirred for mixing well 16 minutes, get product.
Embodiment 2.
Multifunctional aqueous environment protection interior wall putty, its raw material is by the material composition of following parts by weight：Water 280kg heavy calcium carbonate 55 kg, sierozem power 25 kg, white cement 10 kg, hydroxypropyl methyl cellulose 4 kg, anion natural mineral powder 3 kg, brightening agent 2.5 kg, tarragon 2kg, selfheal 3kg, anemone vitifolia 1 kg, camphorwood 2 kg, agalloch eaglewood 1 kg, desmodium triquetrum 3 kg, ambergris 0.5 kg, described anion natural mineral powder is tourmaline, lanthanide rare composite salt and titanium oxide by weight 4：2：4 mixture, wherein tourmaline are dravite and elbaite by weight 5：5 mixture.
Specifically, the fineness of described anion natural mineral powder is 6000 mesh；The viscosity of described hydroxypropyl methyl cellulose is 100000mPa s；The fineness particle diameter of described heavy calcium carbonate is 1200 mesh；The fineness particle diameter of described sierozem power is 1200 mesh；The fineness particle diameter of described white cement is 800 mesh；Described brightening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent of the prior art, this brightening agent is mainly used in brightening of papermaking, coating, ink and yarn fabric, it utilizes ANSD acid is initial reactant, synthesize compounding mixed type fluorescent whitening agent, substantially solve pollution problem, expand the range of application of fluorescent whitening agent simultaneously.
Its further technical scheme is, the manufacture method of multifunctional aqueous environment protection interior wall putty, is made up of following step：
S1, take tarragon 2kg, selfheal 3kg, anemone vitifolia 1 kg, camphorwood 2 kg, agalloch eaglewood 1 kg, desmodium triquetrum 3 kg, ambergris 0.5 kg respectively by above-mentioned each component, and put into the herb powder being crushed to 1200 mesh in micronizer respectively, standby；
S2, the herb powder in S1 and other raw material are put into the water adding 280kg in large-scale mixing and blending machine, be sufficiently stirred for mixing well 15-20 minute, get product.
Common putty 1.
Heavy calcium carbonate 80kg, sierozem power 25kg, white cement 40kg, HPMC4kg, ultramarine 0.9kg, water 200kg.
Common putty 2.
Sierozem power 20kg, powdered whiting 50 kg, precipitated calcium carbonate 30
Kg, talcum powder 100 kg, lithopone 45
Kg, titanium dioxide 30 kg, polyvinyl alcohol 10
Kg, edible vegetable oil 3.5 kg, machine oil 1.5
Kg, 95% industrial alcohol 2
Kg, 10% amide solution 1.5
Kg, water 380 kg.
The method checking above-mentioned putty is as follows：
（1）The putty of embodiment 1 and 2, sampled through Zhongshan city's mass metrology supervisory detection and tested, product of the present invention is carried out with water-fast, the alkaline-resisting, performance test such as antibacterial, Durability of antimicrobial effect, soluble heavy metal content, wherein main performance test is with reference to national JG/T3049---1998《Architecture indoor putty》, antibacterial and mouldproof test is with reference to HG/T3950-2007《Paint film antibacterial and mouldproof method of testing》Standard requirement, test result asks for an interview table 1.
（2）Purifying formaldehyde is tested：
According to the putty in above-described embodiment 1 and embodiment 2 according to JC/T1074-2008《Function of purifying indoor air coating material purifying property》The standard of regulation is tested：
In 41 m3The customized chest fully sealing in, putty in embodiment 1 and embodiment 2 in common putty and the present invention is criticized respectively to be scraped on four faces of chest, after putty is dried, spray into the formalin that 5 ml concentration are 36%, when formalin is volatilized completely in airtight chest simultaneously（About 30 minutes）Then after 4 hours, carry out the content of formaldehyde is measured by sampling for the first time, after 12 hours, after 24 hours, take sample to measure the content of formaldehyde in air respectively.
Measure the content of formaldehyde using phenol reagent method, its principle is：The formaldehyde of in the air generates piperazine after reacting with phenol reagent, and piperazine is aoxidized by ferric ion in an acidic solution and forms glaucous compound, and then further according to the depth of color, colorimetric carries out quantitation, to obtain a result.
4 sub-samplings are respectively labeled as A1, A2, A3, A4, test data asks for an interview table 2.
| Common putty 1 | Common putty 2 | Embodiment 1 | Embodiment 2 | |
| A1( mg/ m3) | 1907 | 1938 | 1807 | 1796 |
| A2( mg/ m3) | 1879 | 1902 | 1603 | 1531 |
| A3( mg/ m3) | 1726 | 1807 | 1291 | 1200 |
| A4( mg/ m3) | 1620 | 1782 | 795 | 703 |
Conclusion：Putty in Example 1 and Example 2 of the present invention all can play the effect of good purifying formaldehyde, and compared with common putty on market, the present invention has certain advantage.
（3）Anion collecting test.
Common putty is tempered respectively with the putty in Example 1 and Example 2 of the present invention, brush is in 20 × 20cm2Plank on, dry, then brush emulsion paint on this plank, then dry, lie on grating type ion collectors, collector is put into 0.4 m3Closed bin in, carry out follow-on test with still air ion tester, test result shows：In putty in Example 1 and Example 2 of the present invention, anion average increase is 1617/scm3, the common putty anion average increase of contrast is 1180/scm3, and sustained release negative aeroion, it is more beneficial for purifying the air of a room for a long time；And common putty of the prior art（Common putty 1 and common putty 2）The anion quantity being discharged is 0/scm3, it does not possess the function of anion releasing.
Conclusion：Putty in Example 1 and Example 2 of the present invention all can be purified the air of a room with sustained release negative aeroion for a long time, with common putty of the prior art（Common putty 1 and common putty 2）Compare, the present invention has obviously advantage.
（4）Repelling effect is tested.
Repelling effect according to common putty and putty in above-described embodiment 1 and embodiment 2 carries out contrast test, and test data asks for an interview table 3.
| Common putty 1 | Common putty 2 | Embodiment 1 | Embodiment 2 | |
| Mosquito repellent rate after placing one day | 17% | 16.2% | 92.5% | 93% |
| Place the mosquito repellent rate after January | 16.7% | 16% | 92% | 93.7% |
| Mosquito repellent rate after placing 6 months | 15.6% | 15.2% | 91.1% | 92.6% |
| Mosquito repellent rate after placing 1 year | 14.8% | 14.3% | 90.7% | 91.6% |
Conclusion：Putty in Example 1 and Example 2 of the present invention all can play good mosquito-repelling function, and compared with common putty on market, the present invention has obviously repelling effect.
The foregoing is only presently preferred embodiments of the present invention; not in order to limit the present invention; for those of ordinary skill in the field; can also make other changes in different forms on the basis of the above description; there is no need to be exhaustive to all of embodiment; all any modification, equivalent substitution and improvement within the spirit and principles in the present invention, done etc., are still included within protection scope of the present invention.
Claims (2)
1. multifunctional aqueous environment protection interior wall putty it is characterised in that：Its raw material is by the material composition of following parts by weight：Water 200-280 part, heavy calcium carbonate 55-70 part, sierozem power 16-25 part, white cement 10-15 part, hydroxypropyl methyl cellulose 2.5-4 part, anion natural mineral powder 3-6 part, brightening agent 2-2.5 part, tarragon 2-3 part, selfheal 2-3 part, anemone vitifolia 1-2 part, camphorwood 1-2 part, agalloch eaglewood 1-1.5 part, desmodium triquetrum 2-3 part, ambergris 0.5-1 part, described anion natural mineral powder is tourmaline, lanthanide rare composite salt and titanium oxide by weight 4：2：4 mixture, wherein tourmaline are dravite and elbaite by weight 5：5 mixture, wherein, the fineness of described anion natural mineral powder is 1000-8000 mesh；The viscosity of described hydroxypropyl methyl cellulose is 80000-100000 mPa s；The fineness particle diameter of described heavy calcium carbonate is 600-1200 mesh；The fineness particle diameter of described sierozem power is 600-1200 mesh；The fineness particle diameter of described white cement is 500-800 mesh；Described brightening agent adopts environment friendly triazine amino stilbene fluorescent bleachng agent.
2. one kind as claimed in claim 1 multifunctional aqueous environment protection interior wall putty it is characterised in that：The manufacture method of this putty is made up of following step：
S1, take tarragon 2-3 part, selfheal 2-3 part, anemone vitifolia 1-2 part respectively by above-mentioned each component, camphorwood 1-2 part, agalloch eaglewood 1-1.5 part, desmodium triquetrum 2-3 part, ambergris 0.5-1 part, and put into the herb powder being crushed to 800-1200 mesh in micronizer respectively, standby；
S2, the herb powder in S1 and other raw material are put in large-scale mixing and blending machine, add appropriate water, be sufficiently stirred for mixing well 15-20 minute, get product.
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| CN105271969A (en) * | 2015-11-26 | 2016-01-27 | 白山市和一硅藻科技有限公司 | Indoor inner wall health environment-friendly coating material as well as preparation method and application thereof |
| CN115386262B (en) * | 2022-09-26 | 2023-05-12 | 杭州海维特化工科技有限公司 | Gravure ink applied to slow-release essence and anions of automotive interior decorative plastic film and preparation method thereof |
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| CN1179754C (en) * | 2002-07-08 | 2004-12-15 | 中国建筑材料科学研究院 | Composition tourmaline powder able to effectively generate negative ions in air and its preparing process |
| CN1204214C (en) * | 2002-07-08 | 2005-06-01 | 北京市建筑涂料厂 | Inner wall paint and putty capable of producing negative air ion |
| KR101030281B1 (en) * | 2008-10-28 | 2011-04-19 | 주식회사 자연담은 | Putty for construction |
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