CN107970286A - It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray and preparation method thereof - Google Patents
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray and preparation method thereof Download PDFInfo
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- 230000007812 deficiency Effects 0.000 title claims abstract description 43
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- 241000018646 Pinus brutia Species 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
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- 239000000843 powder Substances 0.000 claims description 30
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- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 2
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- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 2
- 229960002675 xylitol Drugs 0.000 description 2
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 description 1
- 241000227129 Aconitum Species 0.000 description 1
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- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
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- 229940041616 menthol Drugs 0.000 description 1
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 1
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Classifications
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
- A61K36/714—Aconitum (monkshood)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/06—Aluminium, calcium or magnesium; Compounds thereof, e.g. clay
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/14—Alkali metal chlorides; Alkaline earth metal chlorides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/487—Psoralea
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/53—Lamiaceae or Labiatae (Mint family), e.g. thyme, rosemary or lavender
- A61K36/534—Mentha (mint)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/46—Ingredients of undetermined constitution or reaction products thereof, e.g. skin, bone, milk, cotton fibre, eggshell, oxgall or plant extracts
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K9/10—Dispersions; Emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation or decoction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/37—Extraction at elevated pressure or temperature, e.g. pressurized solvent extraction [PSE], supercritical carbon dioxide extraction or subcritical water extraction
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Abstract
The present invention relates to Chinese medical spray field, more particularly to it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray and preparation method thereof, formula includes the component of following parts by weight, 20 ~ 60 parts of gun additioner, 20 ~ 50 parts of psoralea corylifolia, 10 ~ 50 parts of gypsum, 10 ~ 100 parts of dried peppermint leaf, 20 ~ 60 parts of halite.Present invention supplement is used for the blank for treating or preventing renal deficiency type gomphiasis type Chinese medical spray in the prior art, improve the security of spraying, accomplish without any side effects to human body, the circulation of human body fluid environment is participated in a certain extent, strengthen renal function, the effect of improving gingival cell repair ability, reaching permanent tooth anticreep.
Description
Technical field
The present invention relates to Chinese medical spray field, and in particular to it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray and
Its preparation method.
Background technology
Tooth mobility is a kind of disease extremely common in the elderly, is also gradually developed in recent years to rejuvenation direction.Tooth
Loose compact not only influences the masticatory function of human normal, also results in profound odontopathy, enterogastric diseases, or even can induce
A variety of organ diseases.Tooth mobility seriously affects the physical and mental health and quality of the life of human body.
The traditional Chinese medical science thinks, Shen controls bone, tooth being the surplus of the bone, and kidney qi both declined, and essence is lost, tooth become homeless it is foster, by being that tooth must not pacify and shake.
Such as Southern Song Dynasty's Yang Shiying《Renzhai Zhi Zhi Fang, Effective Recipes from Renzhai House》In mention：" dentary, eventually, the institute of marrow is supported for the institute of bone, the real master's of kidney.Therefore renal failure then tooth
Slit, it is hard that essence contains then tooth." be thus renal failure then tooth and gap, the solid then tooth of essence is hard, and all teeth are not crisp hard, or easily shake, or dredge it is open-minded, must kidney qi it
Deficiency, is when based on special kidney tonifying gas.Bright Yu Tuan《Medicine main story》It is proposed：" or meaning pain and tooth shakes, or meaning pain and worm is invaded
Erosion, and there is slot to dredge open-minded diet inconvenience person, it is frequently.On the whole gingival atrophy and the person of shaking, nephrons void, control suitable enriching yin and nourishing kidney
To want.
Patent of invention " the oral spray " (applying date of Application No. 201010173269.1：2010.05.11) describe
A kind of oral spray.The product is by water-soluble menthol, fresh breath material, sweetener, xylitol, ethanol, deionization
Water is prepared.There is provisional elimination ozostomia, refresh the mind.But contain sweetener in its component, for a long time
Using may be adversely affected to body, and it is invalid for the symptom to be come off of tooth mobility caused by renal deficiency type.
Patent of invention " propolis oral spray and its preparation method and application " (Shen of Application No. 201310683694.9
Please day：2013.12.13) describe a kind of oral spray.The product is prepared by propolis, Tween 80, ethanol.The production
Product can effectively prevent the generation of canker sore, there is the effect of preferable anti-inflammatory anti-inflammatory.But Tween 80 has been used in component, this
It is a kind of nonionic surface active agent for having mild toxicity, does not have to generally in food, can as oral spray long-time service
It can influence health.Moreover, it is invalid for the symptom to be come off of tooth mobility caused by renal deficiency type.
Patent of invention " a kind of IgY antibody oral sprays of anti-caries " (application of Application No. 201010561959.4
Day：2010.11.26) describe a kind of oral spray.The product is by IgY, bacteriostatic agent, preservative, glycerine, ethanol, edible
Essence, distilled water are prepared.Carious tooth, treatment gingivitis, periodontitis and canker sore can effectively be prevented.But make in the product
With bacteriostatic agent, easily occur the resistance to the action of a drug in use, and fungistatic effect is declined rapidly, while also contain preservative, sweet in component
Oil etc., long-time service also be easy to cause harmful effect to human body；It is invalid for the symptom to be come off of tooth mobility caused by renal deficiency type.
The professional mouth fresh and cool spray of easypro visitor on the market, is by deionized water, ethanol, sorbierite, PEG-40 hydrogenated castors
Oil, xylitol, essence, menthol, methyl hydroxybenzoate, saccharin sodium are prepared.There is fresh breath.It is in component to use more
Sweetener, long-time service are unhealthful.It is and invalid for the symptom to be come off of tooth mobility caused by renal deficiency type.
The content of the invention
It is proposed in the above background technology to solve the problems, such as,
An object of the present invention be to provide it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, supplement existing skill
Be used to treating or preventing the blank of renal deficiency type gomphiasis type Chinese medical spray in art, improve the security of spraying, accomplish to human body without
Any toxic side effect, participates in the circulation of human body fluid environment, strengthens renal function, improve gingival cell reparation energy to a certain extent
Power, the effect of reaching permanent tooth anticreep.
The two of the object of the invention be to provide it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray preparation method, will
Chinese medicine preparation is combined with scientific and technological means preparation method, to greatest extent effective component extracting, herbal medicine efficacy is improved, easy to push away
It is wide to use.
To achieve the above object, the present invention provides following technical solution：
Scheme one：
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, including following components, gun additioner, psoralea corylifolia, gypsum,
Dried peppermint leaf and halite.
Preferably, it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, include the components of following parts by weight, big gun is attached
20~60 parts of 20~60 parts of son, 20~50 parts of psoralea corylifolia, 10~50 parts of gypsum, 10~100 parts of dried peppermint leaf and halite.
Preferably, treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, 35~45 parts of gun additioner, psoralea corylifolia 30~40
Part, 20~35 parts of gypsum, 30~70 parts of dried peppermint leaf and 30~50 parts of halite.
Scheme two：
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray preparation method, comprise the following steps,
(1) take gun additioner to crush, add purified water, homogeneous, after sterilizing, connects strain, ferments, and freezes, obtains
Fermentation product, crush, and sieving, obtains yeast powder, spare；
(2) take dried peppermint leaf to crush, add purified water, use CO2Supercritical extract 1~3 time, extracts volatile oil,
It is spare；
(3) psoralea corylifolia, gypsum are taken, adds purified water, concentration, extraction, obtain concentrate, and drying is dry cream,
Crush, sieving, get dry extract powder, spare；
(4) dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
Preferably, the gun additioner powder and the mass ratio of purified water are 1:5~20, homogenization pressure for 0.15~
0.35Mpa, homogenizing time are 5~15min, and sterilising temp is 100~120 DEG C, and sterilization time is 30~55min, accesses strain
For Trametes cinnabarina (Jacg) Franeh, fermentation temperature is 20~40 DEG C, and fermentation humidity is 45~75%, and fermentation time is 20~45d, crosses grit number and is
60~200 mesh；Dried peppermint leaf CO2The flow of supercritical extract is 20~60L/h, 32~37 DEG C of temperature, 20~70MPa of pressure, when
Between 30~80min；Gypsum, psoralea corylifolia concentration vacuum are -0.05Mpa~-0.10Mpa, and thickening temperature is 50~100 DEG C, will
Liquid is condensed into proportion to 1.00~1.25.
Preferably, gun additioner powder and the mass ratio of purified water are 1:13, homogenization pressure 0.25Mpa, homogenizing time are
10min, sterilising temp are 110 DEG C, sterilization time 43min, and access strain is Trametes cinnabarina (Jacg) Franeh, and fermentation temperature is 30 DEG C, fermentation
Humidity is 60%, fermentation time 33d, and it is 130 mesh to cross grit number；Dried peppermint leaf CO2The flow of supercritical extract is 40L/h, temperature
35 DEG C of degree, pressure 45MPa, time 55min；Gypsum, psoralea corylifolia concentration vacuum are -0.08Mpa, and thickening temperature is 75 DEG C, will
Liquid is condensed into proportion to 1.13.
Preferably, the auxiliary material includes lemonade, alcohol, purified water.
Preferably, preparation type is spray.
Preferably, tooth pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
Compared with prior art, the beneficial effects of the invention are as follows：
1. treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, supplement is used to treat or prevent kidney deficiency in the prior art
The blank of type gomphiasis type Chinese medical spray, improves the security of spraying, accomplishes without any side effects to human body, joins to a certain extent
With human body fluid enviromental cycle, strengthen renal function, improve gingival cell repair ability, reach the effect of permanent tooth.
2. by components such as the alkaloids in gun additioner, by fermentation method, retentive activity active ingredient, removes toxicant,
Gun additioner effective rate of utilization is improved, excites gingival cell self-repairing capability, will not be secondary caused by treating to gum, body etc.
Damage, so as to repair gum, permanent tooth anticreep.
3. using pure plant raw material, all active ingredients of product of the present invention are controlled in the tolerable scope of human body
It is interior, there is tight security evaluation.
4. Chinese medicine preparation is combined with scientific and technological means, to greatest extent effective component extracting, herbal medicine efficacy is improved, just
In promoting the use of.
5. we, using traditional Chinese medicine theory as guidance, carefully prescription forms.Gun additioner Xin Ganre in side, is longer than benefit fire and helps
Sun, recuperating depleted yang, are monarch.Psoralea corylifolia is worked hard temperature, warming kidney and enhancing yang, gas antidiarrheal of receiving, and is strengthened the work(that gun additioner is tonified the kidney and support yang, is minister.
The product of gun additioner, Psoralea warm, are quenched the thirst with gypsum sweet pungent Great Cold, clearing heat-fire, relieving restlessness；Peppermint is pungent cool, dispelling wind-heat, clearly
The work(of the head relaxes gun additioner, the property of psoralea corylifolia warm, and two taste of the above is adjutant.Halite is salty-cold, enters the heart, kidney channel, cool blood, bright
Mesh, and with tying-in be to make.All medicines share, plays warm kidney and receives gas, the effect of permanent tooth anticreep altogether.
6. clinical practice and pharmacological evaluation confirm, medicine of the present invention it is lift-off to tooth pine fall therapeutic effect it is obvious, curative effect
Definitely, particularly to caused by kidney deficiency tooth pine it is lift-off fall symptom have significant curative effect.
What 7.. product compared with the prior art of the invention possessed has the beneficial effect that table：
Embodiment
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, including following components, gun additioner, psoralea corylifolia, gypsum,
Dried peppermint leaf, halite.
Wherein, the sub- root of drying that gun additioner is cohosh rhizome of Chinese monkshood Aconitum carmichaeli Debx. processes
Product；Acrid flavour, sweet, property heat；Enter the heart, spleen, kidney channel；Recuperating depleted yang, mends fire supporing yang；
Psoralea corylifolia, is the dry mature fruit of legumes psoraleae Psoralea corylifolia L.；Acrid flavour, hardship,
It is warm-natured；Enter kidney, the spleen channel；Warming kidney and enhancing yang, receives gas antidiarrheal；
Gypsum, is Sulfates mineral anhydrite race gypsum；It is sweet in flavor, pungent, property Great Cold；Enter lung, stomach；Clearing heat-fire, is removed
It is tired to quench the thirst；
Dried peppermint leaf, is the dried leaf of labiate peppermint Mentha haplocalyx Briq.；Acrid flavour, it is cool in nature；Enter
Lung, Liver Channel；Dispelling wind-heat, refresh oneself, promoting eruption；
Halite, is halogenation species halite race lake salt crystalline solid；Taste is salty, cold in nature；Enter the heart, kidney channel；Cool blood, improving eyesight.
Further, it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, include the components of following parts by weight, big gun
20~60 parts of 20~60 parts of monkshood, 20~50 parts of psoralea corylifolia, 10~50 parts of gypsum, 10~100 parts of dried peppermint leaf and halite.
Further, treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, 35~45 parts of gun additioner, psoralea corylifolia 30~40
Part, 20~35 parts of gypsum, 30~70 parts of dried peppermint leaf and 30~50 parts of halite.
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray preparation method, comprise the following steps,
(1) take gun additioner to crush, add purified water, homogeneous, after sterilizing, connects strain, ferments, and freezes, obtains
Fermentation product, crush, and sieving, obtains yeast powder, spare；
(2) take dried peppermint leaf to crush, add purified water, use CO2Supercritical extract 1~3 time, extracts volatile oil,
It is spare；
(3) psoralea corylifolia, gypsum are taken, adds purified water, concentration, extraction, obtain concentrate, and drying is dry cream,
Crush, sieving, get dry extract powder, spare；
(4) dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
Further, the gun additioner powder and the mass ratio of purified water are 1:5~20, homogenization pressure for 0.15~
0.35Mpa, homogenizing time are 5~15min, and sterilising temp is 100~120 DEG C, and sterilization time is 30~55min, accesses strain
For Trametes cinnabarina (Jacg) Franeh, fermentation temperature is 20~40 DEG C, and fermentation humidity is 45~75%, and fermentation time is 20~45d, crosses grit number and is
60~200 mesh；Dried peppermint leaf CO2The flow of supercritical extract is 20~60L/h, 32~37 DEG C of temperature, 20~70MPa of pressure, when
Between 30~80min；Gypsum, psoralea corylifolia concentration vacuum are -0.05Mpa~-0.10Mpa, and thickening temperature is 50~100 DEG C, will
Liquid is condensed into proportion to 1.00~1.25.
Further, gun additioner powder and the mass ratio of purified water are 1:13, homogenization pressure 0.25Mpa, during homogeneous
Between be 10min, sterilising temp is 110 DEG C, sterilization time 43min, and access strain is Trametes cinnabarina (Jacg) Franeh, and fermentation temperature is 30 DEG C,
Fermentation humidity is 60%, fermentation time 33d, and it is 130 mesh to cross grit number；Dried peppermint leaf CO2The flow of supercritical extract is 40L/
H, 35 DEG C of temperature, pressure 45MPa, time 55min；Gypsum, psoralea corylifolia concentration vacuum are -0.08Mpa, thickening temperature 75
DEG C, liquid is condensed into proportion to 1.13.
Further, auxiliary material includes lemonade, alcohol, purified water.
Further, preparation type is spray.
Further, tooth pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
Embodiment 1：
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, include the components of following parts by weight, 40 parts of gun additioner,
20 parts of 20 parts of psoralea corylifolia, 50 parts of gypsum, 30 parts of dried peppermint leaf and halite.
(1) gun additioner of the above-mentioned formula parts by weight is taken, is crushed, crosses 80 mesh sieves, adds the purified water of 20 times of amounts, is carried out equal
Matter, homogenization pressure 0.25Mpa, homogenizing time 5min, sterilize after homogeneous, and sterilising temp is 120 DEG C, and sterilization time is
43min.After sterilizing, strain inoculation is carried out, access strain is Trametes cinnabarina (Jacg) Franeh, is put into incubator and ferments, and fermentation temperature is 20 DEG C,
Humidity of fermenting is 75%, fermentation time 33d.Mycelia uniformly, be plumply covered with homogenizing fluid after, -4 DEG C of freeze overnights, taking-up is put
Enter freeze dryer to freeze, crush, cross 80 mesh sieves, obtain yeast powder, it is spare；
(2) dried peppermint leaf of the above-mentioned formula parts by weight is taken, is crushed, adds the purified water of 5 times of amounts, dried peppermint leaf CO2It is overcritical
Extraction 3 times, wherein, setting flow is 60L/h, and 35 DEG C of temperature, pressure 20MPa, extract 80min, obtain volatile oil every time, spare；
(3) psoralea corylifolia, the gypsum of the above-mentioned formula parts by weight are taken, add 7 times amount purified waters, refluxing extraction 3 times, every time
30min, is filtered, and is concentrated in vacuo, and concentration vacuum is -0.08Mpa, and thickening temperature is 50 DEG C, and liquid is condensed into proportion extremely
1.25, concentrate is obtained, drying is dry cream, is crushed, and crosses 80 mesh sieves, get dry extract powder, spare；
(4) dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
Further, auxiliary material includes lemonade, alcohol, purified water.
Further, preparation type is spray.
Further, tooth pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
Embodiment 2：
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, include the components of following parts by weight, 60 parts of gun additioner,
45 parts of 30 parts of psoralea corylifolia, 10 parts of gypsum, 100 parts of dried peppermint leaf and halite.
(1) gun additioner of the above-mentioned formula parts by weight is taken, is crushed, crosses 100 mesh sieves, adds the purified water of 5 times of amounts, is carried out equal
Matter, homogenization pressure 0.35Mpa, homogenizing time 10min, sterilize after homogeneous, and sterilising temp is 100 DEG C, sterilization time
For 55min.After sterilizing, strain inoculation is carried out, access strain is Trametes cinnabarina (Jacg) Franeh, is put into incubator and ferments, fermentation temperature 30
DEG C, fermentation humidity is 45%, fermentation time 45d.Mycelia uniformly, be plumply covered with homogenizing fluid after, -4 DEG C of freeze overnights, take out
It is put into freeze dryer to freeze, crushes, crosses 100 mesh sieves, obtain yeast powder, it is spare；
(2) dried peppermint leaf of the above-mentioned formula parts by weight is taken, is crushed, adds the purified water of 5 times of amounts, dried peppermint leaf CO2It is overcritical
Extraction 3 times, wherein, setting flow is 20L/h, and 37 DEG C of temperature, pressure 70MPa, extract 30min, obtain volatile oil every time, spare；
(3) psoralea corylifolia, the gypsum of the above-mentioned formula parts by weight are taken, add 8 times amount purified waters, refluxing extraction 3 times, every time
30min, is filtered, and is concentrated in vacuo, and concentration vacuum is -0.1Mpa, and thickening temperature is 75 DEG C, and liquid is condensed into proportion to 1, is obtained
Concentrate, drying is dry cream, is crushed, and crosses 100 mesh sieves, get dry extract powder, spare；
(4) dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
Further, auxiliary material includes lemonade, alcohol, purified water.
Further, preparation type is spray.
Further, tooth pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
Embodiment 3：
It is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, include the components of following parts by weight, 20 parts of gun additioner,
60 parts of 50 parts of psoralea corylifolia, 35 parts of gypsum, 10 parts of dried peppermint leaf and halite.
(1) gun additioner of the above-mentioned formula parts by weight is taken, is crushed, crosses 100 mesh sieves, adds the purified water of 13 times of amounts, is carried out
Homogeneous, homogenization pressure 0.15Mpa, homogenizing time 15min, sterilize after homogeneous, and sterilising temp is 110 DEG C, during sterilizing
Between be 30min.After sterilizing, strain inoculation is carried out, access strain is Trametes cinnabarina (Jacg) Franeh, is put into incubator and ferments, fermentation temperature is
40 DEG C, fermentation humidity is 60%, fermentation time 20d.Mycelia uniformly, be plumply covered with homogenizing fluid after, -4 DEG C of freeze overnights, take
Go out to be put into freeze dryer and freeze, crush, cross 200 mesh sieves, obtain yeast powder, it is spare；
(2) dried peppermint leaf of the above-mentioned formula parts by weight is taken, is crushed, adds the purified water of 7 times of amounts, dried peppermint leaf CO2It is overcritical
Extraction 3 times, wherein, setting flow is 40L/h, and 32 DEG C of temperature, pressure 70MPa, extract 55min, obtain volatile oil every time, spare；
(3) psoralea corylifolia, the gypsum of the above-mentioned formula parts by weight are taken, add 10 times amount purified waters, refluxing extraction 3 times, often
Secondary 40min, is filtered, and is concentrated in vacuo, and concentration vacuum is -0.05Mpa, and thickening temperature is 100 DEG C, and liquid is condensed into proportion extremely
1.13, concentrate is obtained, drying is dry cream, is crushed, and crosses 130 mesh sieves, get dry extract powder, spare；
(4) dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
Further, auxiliary material includes lemonade, alcohol, purified water.
Further, preparation type is spray.
Further, tooth pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
Treatment renal deficiency type tooth pine that 1~embodiment of the embodiment of the present invention 3 produces it is lift-off fall Chinese medical spray, after testing its
Reliability and security comply fully with relative national standards requirement, clinical treatment for example under：
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of changes, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (9)
1. it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, it is characterised in that：Including following components, gun additioner, benefit
Bone fat, gypsum, dried peppermint leaf and halite.
2. it is a kind of treat renal deficiency type tooth pine it is lift-off fall Chinese medical spray, it is characterised in that：Include the component of following parts by weight, big gun
20 ~ 60 parts of 20 ~ 60 parts of monkshood, 20 ~ 50 parts of psoralea corylifolia, 10 ~ 50 parts of gypsum, 10 ~ 100 parts of dried peppermint leaf and halite.
3. treatment renal deficiency type tooth pine according to claim 1 it is lift-off fall Chinese medical spray, it is characterised in that：Gun additioner 35
30 ~ 50 parts of ~ 45 parts, 30 ~ 40 parts of psoralea corylifolia, 20 ~ 35 parts of gypsum, 30 ~ 70 parts of dried peppermint leaf and halite.
4. treatment renal deficiency type tooth pine according to claim 3 it is lift-off fall Chinese medical spray preparation method, its feature exists
In：Comprise the following steps,
（1）Taking gun additioner to crush, add purified water, homogeneous, after sterilizing, connects strain, ferments, and freezes, obtains fermentation product, crushes, sieving,
Yeast powder is obtained, it is spare；
（2）Take dried peppermint leaf to crush, add purified water, use CO2Supercritical extract 1~3 time, extracts volatile oil, spare；
（3）Psoralea corylifolia, gypsum are taken, adds purified water, concentration, extraction, obtain concentrate, and drying is dry cream, crush, and sieving, gets dry extract
Powder, it is spare；
（4）Dried cream powder, volatile oil, yeast powder, halite and auxiliary materials and mixing are taken, Chinese medical spray is made.
5. treatment renal deficiency type tooth pine according to claim 4 it is lift-off fall Chinese medical spray preparation method, its feature exists
In：The gun additioner powder and the mass ratio of purified water are 1:5~20, homogenization pressure is 0.15~0.35Mpa, and homogenizing time is
5~15min, sterilising temp are 100~120 DEG C, and sterilization time is 30~55min, and access strain is Trametes cinnabarina (Jacg) Franeh, fermentation temperature
For 20~40 DEG C, fermentation humidity is 45~75%, and fermentation time is 20~45d, and it is 60~200 mesh to cross grit number；Dried peppermint leaf CO2
The flow of supercritical extract is 20~60 L/h, 32~37 DEG C of temperature, 20~70MPa of pressure, 30~80 min of time；Stone
Cream, psoralea corylifolia concentration vacuum are -0.05Mpa~-0.10Mpa, and thickening temperature is 50~100 DEG C, and liquid is condensed into proportion
To 1.00~1.25.
6. treatment renal deficiency type tooth pine according to claim 4 it is lift-off fall Chinese medical spray preparation method, its feature exists
In：Gun additioner powder and the mass ratio of purified water are 1:13, homogenization pressure 0.25Mpa, homogenizing time 10min, sterilizing temperature
Spend for 110 DEG C, sterilization time 43min, access strain is Trametes cinnabarina (Jacg) Franeh, and fermentation temperature is 30 DEG C, and fermentation humidity is 60%, hair
The ferment time is 33d, and it is 130 mesh to cross grit number；Dried peppermint leaf CO2The flow of supercritical extract is 40L/h, 35 DEG C of temperature, pressure
45MPa, 55 min of time；Gypsum, psoralea corylifolia concentration vacuum are -0.08Mpa, and thickening temperature is 75 DEG C, and liquid is condensed into
Proportion is to 1.13.
7. treatment renal deficiency type tooth pine according to claim 4 it is lift-off fall Chinese medical spray preparation method, its feature exists
In：Auxiliary material includes lemonade, alcohol, purified water.
8. treatment renal deficiency type tooth pine according to claim 4 it is lift-off fall Chinese medical spray preparation method, its feature exists
In：Preparation type is spray.
9. treatment renal deficiency type tooth pine according to claim 4 it is lift-off fall Chinese medical spray, it is characterised in that：The tooth
Pine it is lift-off fall for renal deficiency type tooth pine it is lift-off fall.
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| CN114191484A (en) * | 2022-01-07 | 2022-03-18 | 大连医科大学 | Miao medicine tooth strengthening prescription for treating periodontitis and preparation method thereof |
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