CN107970172A - A kind of eye cream and preparation method thereof - Google Patents
A kind of eye cream and preparation method thereof Download PDFInfo
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- CN107970172A CN107970172A CN201810002891.2A CN201810002891A CN107970172A CN 107970172 A CN107970172 A CN 107970172A CN 201810002891 A CN201810002891 A CN 201810002891A CN 107970172 A CN107970172 A CN 107970172A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Abstract
A kind of eye cream of the present invention and preparation method thereof, is formulated by the raw material of following portions by weight：200 230 parts of the petal of base Pilea Basicordata W. T. Wang, 95 115 parts of the blade of heptangle leaf taro orchid, 140 180 parts of the pulp of net vein meat support fruit, 45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water, the eye cream is obtained by a series of preparation processes, subject's eye is smeared, daily morning and evening respectively once, takes the eye cream component of soybean grain size every time, it is massaged into absorption, continuous to smear 90 days, subject's eye livid ring around eye are significantly thin out, and livid ring around eye area is reduced significantly；The eye cream have the advantages that efficacy stability, do not rebound, short treating period, evident in efficacy, preparation process is simple.
Description
Technical field
The present invention relates to skin care industry, specifically a kind of eye cream and preparation method thereof.
Background technology
Black-eyed formation is related with following factor：Sleep insufficiency, excessive fatigue, makes eyelid to rest, in tight
Contraction state is opened, the blood flow at the position increases for a long time, causes eyelet subcutaneous tissue angioplerosis, so as to cause eyelet to become silted up
Blood, dim black shade under delay；Kidney qi loss, makes two to lack moistening for vital essence, makes on black floats on, therefore black eye；
Eipathia asthenia or the people to just recover from a dangerous illness, since eye surrounding subcutaneous tissue is weak, pigmentation easily occurs for skin, and is easily emerging in
On upper and lower eyelid, there is one layer of black circle；The women of irregular menstruation, as functional uterine bleeding, primary dysmenorrhea, menstruation in advance,
After mistake, menstrual period it is long, excessive etc. through measuring, livid ring around eye occur.This kind of black-eyed origin cause of formation and age growth are closely bound up, and one
As appear in the middle age after.Chronic sun exposure causes pigementation to be formed what be can't get rid of in the course of time in eyes surrounding
Livid ring around eye.Commonly using mascara, informer, eye shadow, do not unloaded when removing stage makeup and costume totally, the particulate of dark element slowly penetrates into eyelid
It is interior, livid ring around eye are formed in the course of time.In addition, melanin metabolism caused by blood is detained is slow, it also can all cause dark brown livid ring around eye
Formation.It has to be noted that pigment type livid ring around eye necessarily focus on prevention, once it is it is difficult to eliminate, although in the market to occur
Also there is a similar eye cream product, but effect and a unobvious, the defects of this is the prior art.
The content of the invention
It is an object of the invention to overcome the prior art existing weak curative effect, side effect in terms of eye part skin is nursed it is big,
High cost, and the deficiency of secondary injury is easily brought to patient, and offer one kind is using simplicity, safe and reliable, cost is low, treatment
Effect is obvious, especially for black-eyed eye cream of eye and preparation method thereof.
The object of the present invention is achieved like this：
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200-230 parts of the petal of base Pilea Basicordata W. T. Wang, 95-115 parts of the blade of heptangle leaf taro orchid, the pulp of net vein meat support fruit
140-180 parts, 45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) the petal 200-230 parts by weight of base Pilea Basicordata W. T. Wang, the blade 95-115 parts by weight of heptangle leaf taro orchid, net are taken
The pulp 140-180 parts by weight of arteries and veins meat support fruit, are dried in an oven after cleaning, and oven temperature is arranged to 60 DEG C, and the time is small for 24
When, mix, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
In the present invention, three kinds of plants are organized as major function additive：Base Pilea Basicordata W. T. Wang (Classification system：Pilea
Basicordata W.T.Wang) it is Urticaceae Pilea stunted brushwood, inflorescence list is born in stem top axil, poly- umbrella circular cone
Shape, the base Pilea Basicordata W. T. Wang used in of the invention pick up from Guangxi Liucheng；Heptangle leaf taro orchid (Classification system：Nervilia
Mackinnonii (Duthie) Schltr.) it is orchid family Nervilia plant, Ye Yimei, grows, green, heptangle after flower withers
Shape, 2.5-4.5 centimetres long, 3.7-5 centimetres wide, the heptangle leaf taro orchid used in the present invention picks up from the only mountain of South of Guizhou；Net vein meat
Hold in the palm fruit (Classification system：Semecarpus reticulate Lecte.) it is Anacardiaceae meat support fruit category arbor, drupe oval, footpath
About 1 centimetre, the net vein meat support fruit used in of the invention is picked up from the woods of 540-1350 meters of south of Yunnan height above sea level.
The lanolin brand used in the present invention is sun card, purchased from Tianjin Zhi Yuan chemical reagent Co., Ltd；This hair
The grape-kernel oil brand used in bright is Yu Xiangfang, purchased from love soap mill handmade soap raw material shop；The ultrasonic wave used in the present invention carries
It is depth Hua Tai, model ps-60AL to take instrument brand, purchased from safe ultrasonic washing/cleaning equipment Co., Ltd of deep China of Shenzhen；In the present invention
The Rotary Evaporators brand used is triumphant auspicious, model RE-5003, purchased from the triumphant auspicious experimental instruments and equipment limited in Zhengzhou.The present invention
In the extracting method used be the prior art, those skilled in the art should know.
Properties of product evaluation test of the present invention is as follows：
First, skin irritation test：
2.5~3kg healthy rabbits 60 are selected, every rabbit back is symmetrical to select shaving 2.5cm at 202, it is right with itself
Carried out according to test method(s), apply 0.5g products of the present invention every time, twice daily, left or right side is smeared at random, observe and record 24h,
The reacting phenomenon of skin after 72h.
The result shows that：Have no that the local excitations such as rubefaction, dermexanthesis, water lump are reacted after applying product 24h, 72h of the present invention, say
Bright eye cream of the present invention is to be perfectly safe, without any adverse reaction.
2nd, efficacy validation
120 eyes are selected to have obvious black-eyed 30-35 Sui volunteer, each 60 people of men and women, test site is Jiangxi Province south
Prosperous city, above volunteer meet standard by the hospital expert inspection of Nanchang City, Jiangxi Province ten and select, without disease and bad
Hobby, is divided into 12 groups, and 11 groups are test group, and one group is control group, every group of 10 people, each 5 people of men and women, the no plant group of control group
The product of part, test group product of the present invention, was compared simultaneously before on-test with colour atla with every volunteer's eye livid ring around eye
Color number is recorded, meanwhile, measure and record every volunteer's eye livid ring around eye width (this width refers to lower informer to normal skin tone
Distance).Product is applied to whole eye during on-test, once in the morning and once at night, each dosage is that every eye soybean grain is big
Product, is used continuously 90 days.With the eye color number of every volunteer of colour chart comparison after 90 days, while measure every volunteer's eye
Livid ring around eye width, contrasts with list before experiment.In addition, diet work and rest during experiment according to volunteer in itself usually
Custom, does not require deliberately, should if personnel's generation major disease or other accidents can not continue experiment during experiment
Stop the experiment of the people, other staff carry out as usual.The colour atla name of an article used in experiment is the color logical colours of skin of PANTONETMGuide, product
Board is PANTONE, model STG201, and manufacturer is located at the U.S..Logical colour of skin guide [the PANTONE SkinTone of coloured silk
Guide] it is to be worked out according to the thousands of kinds of actual colours of skin in the various human skin types of scientific measurement.Reproduction is aimed at closest to entity
The colour of skin and formulate, the color storehouse be human skin complete visual reference, be accurately to match suitable for the relevant any market of the colour of skin
Unique international color standard of the colour of skin.Each color logical colour of skin guide numbering is made of four alphanumerics, and front two refers to skin
Colour of skin degree or background color, latter two refer to skin color or brightness.
The present invention could also say that a kind of eye cream of galenical and preparation method thereof, a kind of using plant tissue as raw material
Eye cream and preparation method thereof, a kind of using plant extracts as eye cream of raw material and preparation method thereof, it is one that the present invention, which might also say that,
Kind is used to improve black-eyed eye cream and preparation method thereof, a kind of eye cream for having livid ring around eye significant curative effect and preparation method thereof.
Embodiment
Embodiment 1-11 is test group, and embodiment 12 is control group, and per embodiment, experiment 10 people of number, each 5 people of men and women are right
Product according to group with no plant composition, test group product of the present invention are black with colour atla and every volunteer's eye before on-test
Eyelet is compared and records color number, meanwhile, measure and record every volunteer's eye livid ring around eye width (this width refers to down
Distance of the informer to normal skin tone).Product is applied to whole eye during on-test, once in the morning and once at night, each dosage is every
The big product of eye soybean grain, is used continuously 90 days.With the eye color number of every volunteer of colour chart comparison after 90 days, measure at the same time
Every volunteer's eye livid ring around eye width, contrasts with list before experiment.In addition, the diet during experiment is worked and rested according to will
The custom of hope person usually itself, does not require deliberately, if during experiment personnel major disease or other accidents occur can not be after
Continue what is tested, the experiment of the people should be stopped, other staff carry out as usual.It is color for PANTONE that the colour atla name of an article is used in experiment
The logical colour of skinTMGuide, brand PANTONE, model STG201, manufacturer are located at the U.S..The logical colour of skin guide [PANTONE of coloured silk
SkinTone Guide] it is to be worked out according to the thousands of kinds of actual colours of skin in the various human skin types of scientific measurement.Aim at reproduction
Formulated closest to the entity colour of skin, which is the complete visual reference of human skin, suitable for the relevant any market of the colour of skin,
It is unique international color standard of the accurate matching colour of skin.Each color logical colour of skin guide numbering is made of four alphanumerics,
Front two refers to skin colourity or background color, and latter two refer to skin color or brightness.The present invention is made with reference to specific embodiment into
One step describes：
Embodiment 1
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200 parts of the petal of base Pilea Basicordata W. T. Wang, 110 parts of the blade of heptangle leaf taro orchid, 160 parts of the pulp of net vein meat support fruit,
45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang, 110 parts by weight of blade of heptangle leaf taro orchid, net vein meat support fruit are taken
160 parts by weight of pulp, dried in an oven after cleaning, oven temperature is arranged to 60 DEG C, the time for 24 it is small when, be blended in one
Rise, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 2
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
230 parts of the petal of base Pilea Basicordata W. T. Wang, 95 parts of the blade of heptangle leaf taro orchid, 170 parts of the pulp of net vein meat support fruit, sheep
45 parts of fat of hair, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 230 parts by weight of petal of base Pilea Basicordata W. T. Wang, 95 parts by weight of blade of heptangle leaf taro orchid, net vein meat support fruit are taken
170 parts by weight of pulp, dried in an oven after cleaning, oven temperature is arranged to 60 DEG C, the time for 24 it is small when, be blended in one
Rise, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 3
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
210 parts of the petal of base Pilea Basicordata W. T. Wang, 100 parts of the blade of heptangle leaf taro orchid, 180 parts of the pulp of net vein meat support fruit,
45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 210 parts by weight of petal of base Pilea Basicordata W. T. Wang, 100 parts by weight of blade of heptangle leaf taro orchid, net vein meat support fruit are taken
180 parts by weight of pulp, dried in an oven after cleaning, oven temperature is arranged to 60 DEG C, the time for 24 it is small when, be blended in one
Rise, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 4
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
220 parts of the petal of base Pilea Basicordata W. T. Wang, 105 parts of the blade of heptangle leaf taro orchid, 150 parts of the pulp of net vein meat support fruit,
45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 220 parts by weight of petal of base Pilea Basicordata W. T. Wang, 105 parts by weight of blade of heptangle leaf taro orchid, net vein meat support fruit are taken
150 parts by weight of pulp, dried in an oven after cleaning, oven temperature is arranged to 60 DEG C, the time for 24 it is small when, be blended in one
Rise, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 5
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
225 parts of the petal of base Pilea Basicordata W. T. Wang, 115 parts of the blade of heptangle leaf taro orchid, 140 parts of the pulp of net vein meat support fruit,
45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 225 parts by weight of petal of base Pilea Basicordata W. T. Wang, 115 parts by weight of blade of heptangle leaf taro orchid, net vein meat support fruit are taken
140 parts by weight of pulp, dried in an oven after cleaning, oven temperature is arranged to 60 DEG C, the time for 24 it is small when, be blended in one
Rise, it is spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 6
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200 parts of the petal of base Pilea Basicordata W. T. Wang, 45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang are taken, are dried in an oven after cleaning, oven temperature is arranged to 60
DEG C, it is spare when the time is 24 small；
(2) after the material that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition of 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains concentrated extracting solution, is -80 DEG C of conditions in temperature
Under be freeze-dried, obtain extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 7
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
110 parts of the blade of heptangle leaf taro orchid, 45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 110 parts by weight of blade of heptangle leaf taro orchid are taken, are dried in an oven after cleaning, oven temperature is arranged to 60 DEG C,
It is spare when time is 24 small；
(2) after the material that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition of 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains concentrated extracting solution, is -80 DEG C of conditions in temperature
Under be freeze-dried, obtain extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) (3) are obtained into mixed extract and is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 8
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
160 parts of the pulp of net vein meat support fruit, 45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 160 parts by weight of pulp of net vein meat support fruit are taken, are dried in an oven after cleaning, oven temperature is arranged to 60 DEG C,
It is spare when time is 24 small；
(2) after the material that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition of 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains concentrated extracting solution, is -80 DEG C of conditions in temperature
Under be freeze-dried, obtain extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 9
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200 parts of the petal of base Pilea Basicordata W. T. Wang, 110 parts of the blade of heptangle leaf taro orchid, 45 parts of lanolin, grape-kernel oil 75
Part, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang are taken, 110 parts by weight of blade of heptangle leaf taro orchid, are drying after cleaning
Dried in case, oven temperature is arranged to 60 DEG C, when the time is 24 small, mixes, spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 10
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200 parts of the petal of base Pilea Basicordata W. T. Wang, 160 parts of the pulp of net vein meat support fruit, 45 parts of lanolin, grape-kernel oil 75
Part, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang are taken, 160 parts by weight of pulp of net vein meat support fruit, are drying after cleaning
Dried in case, oven temperature is arranged to 60 DEG C, when the time is 24 small, mixes, spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 11
A kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
110 parts of the blade of heptangle leaf taro orchid, 160 parts of the pulp of net vein meat support fruit, 45 parts of lanolin, 75 parts of grape-kernel oil,
500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) 110 parts by weight of blade of heptangle leaf taro orchid, 160 parts by weight of pulp of net vein meat support fruit, in baking oven after cleaning are taken
Middle drying, oven temperature is arranged to 60 DEG C, when the time is 24 small, mixes, spare；
(2) after the mixture that (1) step obtains is mixed with 500 parts by weight water temperature be 35 DEG C, power 200W, frequency
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition that rate is 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 in temperature
It is freeze-dried under the conditions of DEG C, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C,
Up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Embodiment 12
The present embodiment is control group, includes the raw material of following parts by weight：
45 parts of lanolin, 75 parts of grape-kernel oil, 500 parts of water.
A kind of preparation method of eye cream, it is characterised in that comprise the following steps：
(1) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, standby
With；
(2) it is uniformly mixed, 25 DEG C is naturally cooling to, up to the eye cream.
Result of the test：Eye livid ring around eye color change and change width are as shown in the table after 10 people 90 days：
Claims (2)
1. a kind of eye cream, it is characterised in that the eye cream includes the raw material of following parts by weight：
200 parts of the petal of base Pilea Basicordata W. T. Wang, 110 parts of the blade of heptangle leaf taro orchid, 160 parts of the pulp of net vein meat support fruit, wool
45 parts of fat, 75 parts of grape-kernel oil, 500 parts of water；
And making step is as follows：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang, 110 parts by weight of blade of heptangle leaf taro orchid, the fruit of net vein meat support fruit are taken
160 parts by weight of meat, are dried in an oven after cleaning, and oven temperature is arranged to 60 DEG C, when the time is 24 small, mixes, standby
With；
(2) in temperature it is 35 DEG C, power 200W after the mixture that (1) step obtains is mixed with 500 parts by weight water, frequency is
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition of 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 DEG C of bars in temperature
It is freeze-dried under part, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, spare；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C, to obtain the final product
The eye cream.
2. a kind of eye cream and preparation method thereof, it is characterised in that including following preparation process：
(1) 200 parts by weight of petal of base Pilea Basicordata W. T. Wang, 110 parts by weight of blade of heptangle leaf taro orchid, the fruit of net vein meat support fruit are taken
160 parts by weight of meat, are dried in an oven after cleaning, and oven temperature is arranged to 60 DEG C, when the time is 24 small, mixes, standby
With；
(2) in temperature it is 35 DEG C, power 200W after the mixture that (1) step obtains is mixed with 500 parts by weight water, frequency is
It is spare with obtaining filtrate after 0.55um filtering with microporous membrane after carrying out ultrasonic extraction 40min under the ultrasound condition of 60KHz；
(3) filtrate for obtaining (2) step carries out rotary evaporation, obtains mixture concentrated extracting solution, is -80 DEG C of bars in temperature
It is freeze-dried under part, obtains mixed extract, it is spare；
(4) by 45 parts by weight of lanolin, 75 parts by weight of grape-kernel oil, are heated to 85-95 DEG C of stirring and dissolving after mixing, spare；
(5) mixed extract that (3) step obtains is heated to 85-95 DEG C, it is spare；
(6) mixture that (4) step obtains is uniformly mixed with the mixture that (5) step obtains, is naturally cooling to 25 DEG C, to obtain the final product
The eye cream.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810002891.2A CN107970172A (en) | 2018-01-02 | 2018-01-02 | A kind of eye cream and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810002891.2A CN107970172A (en) | 2018-01-02 | 2018-01-02 | A kind of eye cream and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107970172A true CN107970172A (en) | 2018-05-01 |
Family
ID=62005752
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810002891.2A Withdrawn CN107970172A (en) | 2018-01-02 | 2018-01-02 | A kind of eye cream and preparation method thereof |
Country Status (1)
| Country | Link |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705414A (en) * | 2013-12-12 | 2014-04-09 | 诺斯贝尔(中山)无纺日化有限公司 | Eye cream customized for Night Cats |
| CN106983700A (en) * | 2017-03-29 | 2017-07-28 | 北海市宝珠林海洋科技有限公司 | One kind effectively removes black-eyed eye cream |
-
2018
- 2018-01-02 CN CN201810002891.2A patent/CN107970172A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103705414A (en) * | 2013-12-12 | 2014-04-09 | 诺斯贝尔(中山)无纺日化有限公司 | Eye cream customized for Night Cats |
| CN106983700A (en) * | 2017-03-29 | 2017-07-28 | 北海市宝珠林海洋科技有限公司 | One kind effectively removes black-eyed eye cream |
Non-Patent Citations (3)
| Title |
|---|
| 佚名: "《Chantelle 香娜露儿 羊胎素眼霜》", 《COSDNA》 * |
| 张明明等: "《眼部皮肤常见问题及眼部护理化妆品的发展现状》", 《香料香精化妆品》 * |
| 谢宗万: "《全国中草药明鉴》", 31 December 1995 * |
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