A kind of whitening and moisturizing profit body frost containing plant extract and preparation method thereof
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of whitening and moisturizing profit body frost containing plant extract and preparation method thereof.
Background technology
Skin covers the surface texture of whole body, and it can make the interior tissue of human body and organ from infringement, can also prevent loss of moist in body simultaneously, stop harmful substance to invade the functions such as human body.Therefore, skin is the important component part of human body, directly expresses health and old and feeble mark especially.When skin metabolism is vigorous, blood circulation is unimpeded, and time nutritious, then skin is fine and smooth, smooth, tender, is rich in elasticity, and not easily occurs wrinkle and mottle.When skin metabolism weakens, poor blood circulation, when nutrient substance is bad, then skin can become gloomy, old and feeble, and easily produces wrinkle and mottle.Current cosmetics, usually cannot improve skin metabolism, promote cutaneous circulation, increase skin-nourishing, and wrinkle and the mottle that more cannot remove skin appearance make fine and smooth, smooth, the tender white and springiness of skin.Therefore can not meet the whitening of people to body skin, the skin protection requirement of moisturizing, bring inconvenience to the daily nursing of people to body skin.
Summary of the invention
The object of this invention is to provide a kind of whitening and moisturizing profit body frost containing plant extract and preparation method thereof, the moisture that it can make skin keep sufficient for a long time, can also make the tenderer white and springiness of skin.This profit body frost whitening and moisturizing successful, instant effect, natural safety.
The present invention to achieve these goals, by the following technical solutions:
A kind of whitening and moisturizing profit body frost containing plant extract, is characterized in that comprising following component by weight:
Caulis et Folium Brassicae campestris fruit 5-9 part, Semen Coicis stem 10-15 part, extra large silkweed blade 12-18 part, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts of D, triethanolamine 3 parts
The method of the whitening and moisturizing profit body frost containing plant extract as above, is characterized in that comprising the following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 5-9 weight portion, Semen Coicis stem 10-15 weight portion, extra large silkweed blade 12-18 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
In the present invention, three kind of plant are major function additive, Caulis et Folium Brassicae campestris (Classification system: BrassicacampestrisL.var.campestris) is the annual or biennial herb of Cruciferae Brassica genus, siliqua, long 2 ~ 4 centimetres, diameter about 5 millimeters, the long beak of tip tool one, the fruit phase 4-6 month; Semen Coicis (Classification system: Coixlacryma-jobiL.) is grass family Coix annual herb; Sea silkweed (Classification system: GlauxmaritimaL.) is that Primulaceae sea silkweed belongs to perennial herb, and leaf is intensive, meat, alternately to life, closely to raw or alternate, nearly stockless or have short handle; Linear, the oval shape lanceolar of blade is to ovum shape lanceolar, and long 5-15 millimeter, wide 1.8-3.5 millimeter, base portion wedge shape, tip is blunt, Quan Yuan.
This technology of homogenizing is had in the preparation process (4) of whitening and moisturizing profit body frost of the present invention and (5); homogenizing also claims homogenate; be the processing procedure of the dispersion micronize made in suspension (or emulsion) system, homogenization, this process plays a part reduce dispersion yardstick and improve dispersion distributing homogeneity simultaneously.Homogenizing carries out mainly through homogenizer, and the instrument used in the present invention is high pressure homogenizer, and pressure is 40000psi, and brand is speed in upper tableland, and production firm is speed light industry Equipment Limited in upper tableland.In addition, the emulsifying pot brand used in the present invention is for many prosperous, and model is RHJ, and production firm is Science and Technology Ltd. of Wuxi City Zhong Wang automatization.
Properties of product evaluation test of the present invention is as follows:
One, irritation test:
Select 2.5 ~ 3kg healthy rabbits 60, a mao 2.5cm2 is shaved at symmetrical 20 places that select, every rabbit back, carries out with own control test method(s), each painting 0.5g product of the present invention, twice daily, left side or right side are smeared at random, observe and the reacting phenomenon of skin after recording 24h, 72h.
Result shows: have no the local excitation such as skin rubefaction, dermexanthesis, water lump reaction after being coated with product 24h, 72h of the present invention, and illustrating that whitening and moisturizing of the present invention moistens body frost is be perfectly safe, without any untoward reaction.
Two, efficacy validation
Select the 25-45 year female volunteers that 240 health colour of skin skin quality are close, test site is Nanchang City, Jiangxi Province, above volunteer selects by ten, Nanchang City, Jiangxi Province hospital dermatology department expert checks conformance with standard, be divided into 12 groups, 11 groups is test group, one group is matched group, often organize 20 people, the product of matched group without whitening and moisturizing component, test group product of the present invention, the colour of skin of colour atla and everyone health of body skin comparison record was used to number before on-test, during on-test, product is acted on whole health, sooner or later respectively once, continuous use three months.Record the colour of skin numbering of everyone health after three months, to everyone numbering, contrast with list before test, colour atla product are called the logical colour of skin of PANTONE coloured silk
tMguide, brand is PANTONE, and model is STG201, and manufacturer is positioned at the U.S..Color logical colour of skin guide [PANTONESkinToneGuide] works out according to the thousands of kinds of actual colours of skin in scientific measurement various human skin type.Aim to reproduce and formulate closest to the entity colour of skin, this color storehouse is the complete visual reference of human skin, and being applicable to any market that the colour of skin is relevant, is the unique international color standard of the exact matching colour of skin.Each coloured silk leads to colour of skin guide numbering and is made up of four alphanumerics, and front two refers to skin colourity or background color, and latter two refer to skin color or brightness.Noon every day, 1-3 point used moisture of skin tester to test the water content of everyone six area skin and record, calculating mean value, six positions comprise last arm, lower arms, shank, thigh, abdominal part and back, moisture of skin tester brand is milikang Mei Likang, model is SK-IV, and manufacturer is Mei Sicheng Science and Technology Ltd. of Shenzhen.
Detailed description of the invention
Embodiment 1-11 is test group, and embodiment 12 is matched group, and every embodiment test number 20 people, used everyone colour of skin of colorimetric card record, use every embodiment product to act on whole health, sooner or later respectively once, use three months continuously before on-test.Record the colour of skin numbering of everyone health after three months, to everyone numbering, contrast with list before test, colour atla product are called the logical colour of skin of PANTONE coloured silk
tMguide, brand is PANTONE, and model is STG201, and manufacturer is positioned at the U.S..Color logical colour of skin guide [PANTONESkinToneGuide] works out according to the thousands of kinds of actual colours of skin in scientific measurement various human skin type.Aim to reproduce and formulate closest to the entity colour of skin, this color storehouse is the complete visual reference of human skin, and being applicable to any market that the colour of skin is relevant, is the unique international color standard of the exact matching colour of skin.Each coloured silk leads to colour of skin guide numbering and is made up of four alphanumerics, and front two refers to skin colourity or background color, and latter two refer to skin color or brightness.Noon every day, 1-3 point used moisture of skin tester to test the water content of everyone six area skin and record, calculating mean value, six positions comprise last arm, lower arms, shank, thigh, abdominal part and back, tester brand is milikang Mei Likang, model is SK-IV, and manufacturer is Mei Sicheng Science and Technology Ltd. of Shenzhen.
Below in conjunction with specific embodiment, the invention will be further described:
Embodiment 1
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 5 parts, 12 parts, Semen Coicis stem, 18 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 5 weight portion, Semen Coicis stem 12 weight portion, extra large silkweed blade 18 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, test after everyone body skin colourity than test before white twice, brightness has all highlighted one to two degree.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 66.5%, 64.6%, 68.5%, 61.8%, 62.9%, 65.6%, 67.5%, 69.4%, 64.5%, 66.6%, 67.1%, 67.2%, 60.9%, 61.2%, 62.6%, 64.3%, 68.6%, 67.8%, 66.4%, 63.8%.
Embodiment 2
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 7 parts, 15 parts, Semen Coicis stem, 12 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 7 weight portion, Semen Coicis stem 15 weight portion, extra large silkweed blade 12 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, test after everyone body skin colourity than test before white twice, brightness has all highlighted one to two degree.
Subject number |
Body skin numbering before test |
Body skin numbering after test |
1 |
4Y02 |
2Y01 |
2 |
4Y03 |
2Y01 |
3 |
4Y04 |
2Y02 |
4 |
4Y02 |
2Y01 |
5 |
4Y02 |
2Y01 |
6 |
4Y03 |
2Y02 |
7 |
4Y04 |
2Y02 |
8 |
4Y04 |
2Y02 |
9 |
4Y02 |
2Y01 |
10 |
4Y02 |
2Y01 |
11 |
4Y02 |
2Y01 |
12 |
4Y03 |
2Y01 |
13 |
4Y03 |
2Y01 |
14 |
4Y04 |
2Y02 |
15 |
4Y04 |
2Y02 |
16 |
4Y04 |
2Y02 |
17 |
4Y02 |
2Y01 |
18 |
4Y02 |
2Y01 |
19 |
4Y03 |
2Y02 |
20 |
4Y02 |
2Y01 |
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 67.1%, 66.8%, 60.9%, 69.0%, 61.9%, 62.1%, 62.3%, 60.9%, 67.7%, 69.1%, 60.7%, 65.0%, 64.8%, 64.3%, 68.3%, 64.6%, 64.0%, 61.1%, 66.3%, 62.5%.
Embodiment 3
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 8 parts, 14 parts, Semen Coicis stem, 16 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 8 weight portion, Semen Coicis stem 14 weight portion, extra large silkweed blade 16 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, test after everyone body skin colourity than test before white twice, brightness has all highlighted one to two degree.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 69.4%, 67.1%, 65.5%, 69.5%, 63.2%, 65.4%, 69.7%, 64.5%, 60.1%, 62.3%, 63.1%, 62.6%, 66.0%, 61.5%, 60.9%, 62.5%, 64.4%, 61.3%, 67.2%, 61.5%.
Embodiment 4
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 6 parts, 13 parts, Semen Coicis stem, 17 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 6 weight portion, Semen Coicis stem 13 weight portion, extra large silkweed blade 17 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, test after everyone body skin colourity than test before white twice, brightness has all highlighted one to two degree.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 67.6%, 60.4%, 66.3%, 64.8%, 63.5%, 65.7%, 63.6%, 69.0%, 64.6%, 65.3%, 64.9%, 68.9%, 62.3%, 66.8%, 68.8%, 65.8%, 67.7%, 66.9%, 61.4%, 67.2%
Embodiment 5
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 9 parts, 10 parts, Semen Coicis stem, 13 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 9 weight portion, Semen Coicis stem 10 weight portion, extra large silkweed blade 13 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, add 10 times more respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, test after everyone body skin colourity than test before white twice, brightness has all highlighted one to two degree.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 61.3%, 62.7%, 61.2%, 67.8%, 65.8%, 62.3%, 67.7%, 60.6%, 66.8%, 64.2%, 69.3%, 61.3%, 61.1%, 63.6%, 61.5%, 60.7%, 68.9%, 64.9%, 64.2%
Embodiment 6
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 5 parts, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after being dried by Caulis et Folium Brassicae campestris fruit 5 weight portion 60 DEG C, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carries out 60 orders and sieves, then adds 10 times to the ethanol containing deionized water of plant weight part, and concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, Caulis et Folium Brassicae campestris fruit extract can be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add triethanolamine 3 weight portion and Caulis et Folium Brassicae campestris fruit extract when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves twice.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 41.1%, 42.0%, 42.8%, 43.9%, 42.9%, 44.6%, 41.6%, 41.4%, 44.1%, 40.1%, 40.6%, 44.7%, 41.7%, 41.2%, 43.3%, 44.0%, 42.1%, 40.0%, 42.4%, 44.7%.
Embodiment 7
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
12 parts, Semen Coicis stem, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after being dried by Semen Coicis stem 12 weight portion 60 DEG C, then carry out 60 orders and sieve, then add 10 times to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, Semen Coicis stem extract can be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add triethanolamine 3 weight portion and Semen Coicis stem extract when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves twice.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 42.9%, 40.6%, 40.3%, 40.1%, 43.2%, 43.9%, 42.4%, 43.4%, 44.6%, 42.2%, 41.3%, 44.6%, 44.1%, 44.7%, 42.2%, 44.3%, 44.6%, 41.1%, 44.8%, 43.1%.
Embodiment 8
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
18 parts, sea silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after being dried by extra large silkweed blade 18 weight portion 60 DEG C, then carry out 60 orders and sieve, then add 10 times to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, extra large silkweed leaf extract can be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add triethanolamine 3 weight portion and extra large silkweed leaf extract when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves twice.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 42.4%, 40.1%, 40.3%, 42.1%, 44.9%, 40.4%, 42.9%, 40.8%, 41.7%, 42.3%, 42.9%, 44.8%, 43.6%, 41.5%, 44.7%, 40.4%, 41.7%, 40.8%, 40.9%, 44.9%.
Embodiment 9
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 5 parts, 12 parts, Semen Coicis stem, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 5 weight portion, Semen Coicis stem 12 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, then add 10 times respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves one to twice.
Subject number |
Body skin numbering before test |
Body skin numbering after test |
1 |
4Y03 |
4Y01 |
2 |
3Y04 |
3Y03 |
3 |
4Y03 |
4Y02 |
4 |
3Y04 |
3Y03 |
5 |
4Y03 |
4Y01 |
6 |
3Y04 |
3Y02 |
7 |
4Y03 |
4Y02 |
8 |
4Y03 |
4Y01 |
9 |
3Y04 |
3Y03 |
10 |
3Y04 |
3Y03 |
11 |
4Y03 |
4Y02 |
12 |
3Y04 |
3Y03 |
13 |
3Y04 |
3Y03 |
14 |
3Y04 |
3Y03 |
15 |
4Y03 |
4Y02 |
16 |
4Y03 |
4Y02 |
17 |
4Y03 |
4Y02 |
18 |
3Y04 |
3Y03 |
19 |
3Y04 |
3Y03 |
20 |
4Y03 |
4Y02 |
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 50.4%, 49.5%, 46.4%, 46.3%, 49.5%, 46.6%, 48.8%, 46.3%, 45.0%, 45.5%, 49.0%, 49.9%, 49.4%, 48.8%, 49.7%, 46.2%, 46.9%, 47.7%, 47.4%, 48.6%.
Embodiment 10
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
Caulis et Folium Brassicae campestris fruit 5 parts, 18 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Caulis et Folium Brassicae campestris fruit 5 weight portion, extra large silkweed blade 18 weight portion respectively 60 DEG C of oven dry, before drying, Caulis et Folium Brassicae campestris fruit does not remove the peel shell, then carry out 60 orders to sieve, then add 10 times respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves one to twice.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 48.6%, 46.4%, 49.1%, 46.6%, 47.8%, 49.7%, 50.2%, 45.0%, 48.3%, 49.7%, 49.2%, 45.9%, 48.8%, 49.3%, 48.0%, 50.2%, 45.9%, 50.6%, 45.7%.
Embodiment 11
A kind of whitening and moisturizing profit body frost containing plant extract of the present invention, be made up of the component comprising following weight portion:
12 parts, Semen Coicis stem, 18 parts, extra large silkweed blade, hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The whitening and moisturizing profit body frost of the present embodiment is completed by following steps:
(1) pulverize after Semen Coicis stem 12 weight portion, extra large silkweed blade 18 weight portion respectively 60 DEG C of oven dry, then carry out 60 orders and sieve, then add 10 times respectively to the ethanol containing deionized water of plant weight part, concentration of alcohol is 75%; Then soak 12 hours under 35 DEG C of conditions; Carry out 40 DEG C of ultrasonic extractions 6 hours, frequency is 20000Hz, get supernatant centrifugal, filter, refluxing ethanol, refilter once, can plant extract be obtained, for subsequent use;
(2) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(3) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(4) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(5) add the plant extract obtained in triethanolamine 3 weight portion and step (1) when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(6) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this whitening and moisturizing profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin does not change, but brightness all improves one to twice.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 45.1%, 50.5%, 49.3%, 46.9%, 48.8%, 49.4%, 47.0%, 50.5%, 47.2%, 49.3%, 47.5%, 47.9%, 48.9%, 45.2%, 48.9%, 48.2%, 50.6%, 45.9%, 48.2%, 45.5%.
Embodiment 12
The present embodiment is matched group, is made up of the component comprising following weight portion:
Hydrolecithin 4 parts, polydimethylsiloxane 10 parts, glyceryl stearate 5 parts, allantoin 3 parts, propylene glycol 10 parts, cetearyl alcohol 7 parts, carbomer 4 parts, 65 parts, water, triethanolamine 3 parts, 4 parts, essence, antiseptic 3 parts.
The profit body frost of the present embodiment is completed by following steps:
(1) allantoin 3 weight portion, propylene glycol 10 weight portion, cetearyl alcohol 7 weight portion, carbomer 4 weight portion, water 65 weight portion are warmed up to 100 DEG C respectively, are incubated 90 ~ 95 DEG C, after mixing, stirring and dissolving is complete, obtains mixed liquor a, for subsequent use;
(2) hydrolecithin 4 weight portion, polydimethylsiloxane 10 weight portion, glyceryl stearate 5 weight portion are warmed up to 60 ~ 70 DEG C respectively, after mixing, stirring and dissolving is complete, obtains mixed liquor b, for subsequent use;
(3) first by mixed liquor a suction emulsifying pot, more slowly by mixed liquor b suction emulsifying pot, homogenizing 15 ~ 20min, insulated and stirred 15 ~ 20min, evacuation is lowered the temperature;
(4) add triethanolamine 3 weight portion when pot to be emulsified is cooled to 55 ~ 60 DEG C, homogenizing 5 ~ 10min, stirs;
(5) add 4 weight portion essence and 3 weight portion antiseptic when pot to be emulsified is cooled to 45 ~ 50 DEG C, stir, namely obtain this profit body frost.
Result of the test:
1,20 people after three months the change of body skin as shown in the table, after test, everyone the body skin colour of skin and brightness do not change.
2, everyone trimestral moisture content of skin meansigma methods of 20 people respectively: 36.0%, 36.8%, 37.9%, 35.4%, 40.2%, 41.3%, 35.2%, 36.7%, 35.9%, 39.3%, 36.5%, 36.4%, 36.1%, 35.7%, 37.8%, 38.2%, 38.5%, 35.6%, 37.4%, 41.1%.