CN107964335A - A kind of wood furniture extinguishing waterborn preparation method for coating - Google Patents
A kind of wood furniture extinguishing waterborn preparation method for coating Download PDFInfo
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- CN107964335A CN107964335A CN201711052328.8A CN201711052328A CN107964335A CN 107964335 A CN107964335 A CN 107964335A CN 201711052328 A CN201711052328 A CN 201711052328A CN 107964335 A CN107964335 A CN 107964335A
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- wood furniture
- coating
- preparation
- extinguishing waterborn
- waterborne
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
- C09D163/10—Epoxy resins modified by unsaturated compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2217—Oxides; Hydroxides of metals of magnesium
- C08K2003/2224—Magnesium hydroxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
- C08K2003/321—Phosphates
- C08K2003/322—Ammonium phosphate
- C08K2003/323—Ammonium polyphosphate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The invention discloses a kind of wood furniture extinguishing waterborn preparation method for coating, include the following steps：Waterborne epoxy acrylate resin, waterborne polyurethane modified epoxy resin, emulsifying agent, levelling agent, defoamer, water are uniformly mixing to obtain prefabricated material；Catalyst, waterborne curing agent, epoxidized soybean oil, ammonium polyphosphate, expanded graphite, magnesium hydroxide, powdered whiting, vermiculite power, blanc fixe, calcined kaolin, anti-settling agent, dispersant are added into prefabricated material and is uniformly mixing to obtain wood furniture extinguishing waterborn coating.Preparation method of the present invention is simple; the coating adhesion of gained water paint is strong; paint film is plentiful, non-yellowing embrittlement, without organic solvent; and good heat dissipation effect; excellent fireproof performance, comprehensive performance is superior, has good protective effect to wood furniture; long-time service rear surface will not peeling, occur fire when also can effectively prevent fires.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of wood furniture extinguishing waterborn preparation method for coating.
Background technology
The phosphorus content of ammonium polyphosphate is up to 30-32%, and nitrogenous is 14-16%, is excellent fire retardant, its most prominent spy
Life smoke when sign is burning is extremely low, does not produce hydrogen halides.Coating equally has excellent fire resistance made of ammonium polyphosphate
Energy.
Wood furniture has the characteristics of attractive and durable, rich classical beauty, is the first choice of many Home furniture finishings.But
The fire resistance of existing wood furniture covering with paint coating is not high, cannot effectively prevent fires when fire occurs, it would be highly desirable to solve.
The content of the invention
Based on technical problem existing for background technology, the present invention proposes a kind of wood furniture extinguishing waterborn coating preparation
Method, preparation method is simple, and the coating adhesion of gained water paint is strong, and paint film is plentiful, non-yellowing embrittlement, without organic molten
Agent, and good heat dissipation effect, excellent fireproof performance, comprehensive performance is superior, has good protective effect to wood furniture, for a long time
Using rear surface will not peeling, occur fire when also can effectively prevent fires.
A kind of wood furniture extinguishing waterborn preparation method for coating proposed by the present invention, includes the following steps：
S1, by waterborne epoxy acrylate resin, waterborne polyurethane modified epoxy resin, emulsifying agent, levelling agent, defoaming
Agent, water are uniformly mixing to obtain prefabricated material；
S2, add catalyst, waterborne curing agent, epoxidized soybean oil, ammonium polyphosphate, expanded graphite, hydrogen-oxygen into prefabricated material
Change magnesium, powdered whiting, vermiculite power, blanc fixe, calcined kaolin, anti-settling agent, dispersant and be uniformly mixing to obtain wooden family
Tool uses extinguishing waterborn coating.
Preferably, emulsifying agent is stearoyl lactate, stearyl lactate, diacetyl tartarate monoglyceride, Sucrose Fatty Acid Ester
Fat ester, distillation monoglyceride, ethoxylated dodecyl alcohol, phenethyl phenol polyethenoxy ether, one kind of fatty amide polyoxyethylene ether
It is or two or more.
Preferably, levelling agent is sulfonated oil, Nekal BX, soybean lecithin, thio-alcohol, hydrazides and mercaptan acetals
It is two or more.
Preferably, defoamer is benzyl carbinol oleate, Laurate alcohol ester phenylacetate, dimethicone, high-carbon alcohol fatty acid ester
Compound, polyoxyethylene polyoxypropylene pentaerythrite ether, polyoxyethylene polyoxy propyl alcohol amidogen ether, polypropylene glycerol aether one kind or
It is two or more.
Preferably, dispersant is stearmide, vinyl bis-stearamides, glyceryl monostearate, three glycerol stearates
Ester, barium stearate, calcium stearate, ethylene-acrylic acid copolymer, ethylene-vinyl acetate copolymer, polyethylene glycol 200, poly- second two
The one or more of alcohol 400.
Preferably, in S1, waterborne epoxy acrylate resin, the weight ratio of waterborne polyurethane modified epoxy resin are 90-
110：30-40.
Preferably, in S1, waterborne epoxy acrylate resin, emulsifying agent, levelling agent, defoamer, the weight ratio of water are 90-
110：2-4：3-5：2-4：150-190.
Preferably, in S2, ammonium polyphosphate, expanded graphite, magnesium hydroxide, powdered whiting, vermiculite power, blanc fixe,
The weight ratio of calcined kaolin is 8-16：12-18：10-20：8-14：4-8：12-20：8-16.
Preferably, it is prefabricated material, catalyst, waterborne curing agent, epoxidized soybean oil, ammonium polyphosphate, anti-settling agent, scattered in S2
The weight ratio of agent is 200-220：1-2：2-4：4-8：8-16：8-12：4-8.
Coating adhesion of the present invention is strong, and paint film is plentiful, non-yellowing embrittlement, without organic solvent, and also good heat dissipation effect, resistance
Excellent performance is fired, comprehensive performance is superior, has good protective effect to wood furniture, long-time service rear surface will not rise
Skin, occurs also can effectively prevent fires during fire.
The present invention is acted synergistically using waterborne epoxy acrylate resin, waterborne polyurethane modified epoxy resin, water of arranging in pairs or groups
Property curing agent and ammonium polyphosphate, not only mutual degree of scatter is high, but also fire resistance is fabulous, and thermal stability is excellent, Gu
Compact in paint film is good after change, and pliability is splendid, and adhesive force is excellent, can balance the brittleness of water-based Epocryl, can incite somebody to action
Coating is firmly locked on wood surface, while is free of organic solvent, and safety and environmental protection is free from environmental pollution；Ammonium polyphosphate and expansion stone
Ink, magnesium hydroxide, powdered whiting, vermiculite power, blanc fixe, calcined kaolin synergistic effect, not only fillibility is good, makes this
The hardness and wear resistance of invention can be excellent, and is compounded with emulsifying agent, good leveling property, and it is former with other can effectively to strengthen above-mentioned raw materials
The combination power of material, greatly enhances the adhesive force between coating and timber plate.
The coating layer thickness of gained water paint of the invention is 1.8-2.2mm；When the fiery temperature of the back of the body is 500 DEG C, coating exists
It is not blistering in 150min, do not change；The furniture for scribbling water paint obtained by the present invention is soaked in water, undercoating is unchanged within 7 days,
Strong adhesive force, does not occur obscission.
Embodiment
In the following, technical scheme is described in detail by specific embodiment.
Embodiment 1
A kind of wood furniture extinguishing waterborn preparation method for coating, includes the following steps：
S1, by 90kg waterborne epoxy acrylates resin, 40kg waterborne polyurethane modified epoxy resins, 2kg emulsifying agents,
5kg levelling agents, 2kg defoamers, 190kg water are uniformly mixing to obtain prefabricated material；
S2, add 2kg catalyst, 2kg waterborne curing agents, 8kg epoxidized soybean oils, 8kg polyphosphoric acids into the prefabricated material of 200kg
Ammonium, 18kg expanded graphites, 10kg magnesium hydroxides, 14kg powdered whitings, 4kg vermiculite powers, 20kg blanc fixes, 8kg calcinings
Kaolin, 12kg anti-settling agents, 4kg dispersants are uniformly mixing to obtain wood furniture extinguishing waterborn coating.
Embodiment 2
A kind of wood furniture extinguishing waterborn preparation method for coating, includes the following steps：
S1, by 110kg waterborne epoxy acrylates resin, 30kg waterborne polyurethane modified epoxy resins, 4kg emulsifying agents,
3kg levelling agents, 4kg defoamers, 150kg water are uniformly mixing to obtain prefabricated material；
S2, add 1kg catalyst, 4kg waterborne curing agents, 4kg epoxidized soybean oils, the poly- phosphorus of 16kg into the prefabricated material of 220kg
Sour ammonium, 12kg expanded graphites, 20kg magnesium hydroxides, 8kg powdered whitings, 8kg vermiculite powers, 12kg blanc fixes, 16kg are forged
Burn kaolin, 8kg anti-settling agents, 8kg dispersants and be uniformly mixing to obtain wood furniture extinguishing waterborn coating.
Embodiment 3
A kind of wood furniture extinguishing waterborn preparation method for coating, includes the following steps：
S1, by 95kg waterborne epoxy acrylates resin, 38kg waterborne polyurethane modified epoxy resins, 2.5kg emulsifying agents,
4.5kg levelling agents, 2.5kg defoamers, 180kg water are uniformly mixing to obtain prefabricated material；
S2, add 1.8kg catalyst, 2.5kg waterborne curing agents, 7kg epoxidized soybean oils, 10kg into the prefabricated material of 205kg
Ammonium polyphosphate, 16kg expanded graphites, 12kg magnesium hydroxides, 12kg powdered whitings, 5kg vermiculite powers, 18kg blanc fixes,
10kg calcined kaolins, 11kg anti-settling agents, 5kg dispersants are uniformly mixing to obtain wood furniture extinguishing waterborn coating.
Embodiment 4
A kind of wood furniture extinguishing waterborn preparation method for coating, includes the following steps：
S1, by 105kg waterborne epoxy acrylates resin, 32kg waterborne polyurethane modified epoxy resins, 3.5kg emulsify
Agent, 3.5kg levelling agents, 3.5kg defoamers, 160kg water are uniformly mixing to obtain prefabricated material；
S2, add 1.2kg catalyst, 3.5kg waterborne curing agents, 5kg epoxidized soybean oils, 14kg into the prefabricated material of 215kg
Ammonium polyphosphate, 14kg expanded graphites, 18kg magnesium hydroxides, 10kg powdered whitings, 7kg vermiculite powers, 14kg blanc fixes,
14kg calcined kaolins, 10kg anti-settling agents, 7kg dispersants are uniformly mixing to obtain wood furniture extinguishing waterborn coating.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (9)
1. a kind of wood furniture extinguishing waterborn preparation method for coating, it is characterised in that include the following steps：
S1, by waterborne epoxy acrylate resin, waterborne polyurethane modified epoxy resin, emulsifying agent, levelling agent, defoamer, water
It is uniformly mixing to obtain prefabricated material；
S2, into prefabricated material add catalyst, waterborne curing agent, epoxidized soybean oil, ammonium polyphosphate, expanded graphite, magnesium hydroxide,
Powdered whiting, vermiculite power, blanc fixe, calcined kaolin, anti-settling agent, dispersant are uniformly mixing to obtain wood furniture resistance
Fire water paint.
2. wood furniture extinguishing waterborn preparation method for coating according to claim 1, it is characterised in that emulsifying agent is tristearin
Acyl lactylate, stearyl lactate, diacetyl tartarate monoglyceride, sucrose fatty ester, distillation monoglyceride, laruyl alcohol polyoxy second
Alkene ether, phenethyl phenol polyethenoxy ether, the one or more of fatty amide polyoxyethylene ether.
3. wood furniture extinguishing waterborn preparation method for coating according to claim 1, it is characterised in that levelling agent is sulfonation
Oil, Nekal BX, soybean lecithin, thio-alcohol, hydrazides and mercaptan acetals it is two or more.
4. wood furniture extinguishing waterborn preparation method for coating according to claim 1, it is characterised in that defoamer is benzene second
The fatty acid ester compounded thing of alcohol oleate, Laurate alcohol ester phenylacetate, dimethicone, higher alcohols, polyoxyethylene polyoxypropylene season penta
Four alcohol ethers, polyoxyethylene polyoxy propyl alcohol amidogen ether, the one or more of polypropylene glycerol aether.
5. wood furniture extinguishing waterborn preparation method for coating according to claim 1, it is characterised in that dispersant is tristearin
Acid amides, vinyl bis-stearamides, glyceryl monostearate, glyceryl tristearate, barium stearate, calcium stearate, ethene-the third
Olefin(e) acid copolymer, ethylene-vinyl acetate copolymer, polyethylene glycol 200, the one or more of polyethylene glycol 400.
6. according to any one of claim 1-5 wood furniture extinguishing waterborn preparation method for coating, it is characterised in that S1
In, waterborne epoxy acrylate resin, the weight ratio of waterborne polyurethane modified epoxy resin are 90-110：30-40.
7. according to any one of claim 1-6 wood furniture extinguishing waterborn preparation method for coating, it is characterised in that S1
In, waterborne epoxy acrylate resin, emulsifying agent, levelling agent, defoamer, the weight ratio of water are 90-110：2-4：3-5：2-4：
150-190。
8. according to any one of claim 1-7 wood furniture extinguishing waterborn preparation method for coating, it is characterised in that S2
In, ammonium polyphosphate, expanded graphite, magnesium hydroxide, powdered whiting, vermiculite power, blanc fixe, the weight ratio of calcined kaolin
For 8-16：12-18：10-20：8-14：4-8：12-20：8-16.
9. according to any one of claim 1-8 wood furniture extinguishing waterborn preparation method for coating, it is characterised in that S2
In, prefabricated material, catalyst, waterborne curing agent, epoxidized soybean oil, ammonium polyphosphate, anti-settling agent, the weight ratio of dispersant are 200-
220：1-2：2-4：4-8：8-16：8-12：4-8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711052328.8A CN107964335A (en) | 2017-10-30 | 2017-10-30 | A kind of wood furniture extinguishing waterborn preparation method for coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711052328.8A CN107964335A (en) | 2017-10-30 | 2017-10-30 | A kind of wood furniture extinguishing waterborn preparation method for coating |
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| Publication Number | Publication Date |
|---|---|
| CN107964335A true CN107964335A (en) | 2018-04-27 |
Family
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|---|---|---|---|
| CN201711052328.8A Withdrawn CN107964335A (en) | 2017-10-30 | 2017-10-30 | A kind of wood furniture extinguishing waterborn preparation method for coating |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108976995A (en) * | 2018-08-07 | 2018-12-11 | 安徽昌发实业有限公司 | A kind of wicker products high-quality water paint |
| CN108977021A (en) * | 2018-06-08 | 2018-12-11 | 浙江安吉朝辉新材料有限公司 | A kind of aqueous woodware paint |
| CN110791155A (en) * | 2019-12-04 | 2020-02-14 | 中国民用航空总局第二研究所 | High-temperature-resistant flame-retardant material and film forming preparation method thereof |
| CN110982387A (en) * | 2019-12-27 | 2020-04-10 | 常州市华菱新材料有限公司 | Water-based epoxy coating with good adhesive force and corrosion resistance on surface of metal substrate and preparation method thereof |
| CN112870772A (en) * | 2021-01-14 | 2021-06-01 | 江苏赛欧信越消泡剂有限公司 | Acid-resistant defoaming agent and preparation method thereof |
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| CN101486863A (en) * | 2008-01-18 | 2009-07-22 | 深圳市海川实业股份有限公司 | Environment friendly waterborne paint and preparation thereof |
| CN102732134A (en) * | 2012-07-11 | 2012-10-17 | 扬州大学 | Acrylate-grafted epoxy-polyurethane water-based woodwork coating |
| CN106366844A (en) * | 2016-08-27 | 2017-02-01 | 安徽省金盾涂料有限责任公司 | High-adhesion epoxy paint with excellent mechanical properties |
-
2017
- 2017-10-30 CN CN201711052328.8A patent/CN107964335A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101486863A (en) * | 2008-01-18 | 2009-07-22 | 深圳市海川实业股份有限公司 | Environment friendly waterborne paint and preparation thereof |
| CN102732134A (en) * | 2012-07-11 | 2012-10-17 | 扬州大学 | Acrylate-grafted epoxy-polyurethane water-based woodwork coating |
| CN106366844A (en) * | 2016-08-27 | 2017-02-01 | 安徽省金盾涂料有限责任公司 | High-adhesion epoxy paint with excellent mechanical properties |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108977021A (en) * | 2018-06-08 | 2018-12-11 | 浙江安吉朝辉新材料有限公司 | A kind of aqueous woodware paint |
| CN108976995A (en) * | 2018-08-07 | 2018-12-11 | 安徽昌发实业有限公司 | A kind of wicker products high-quality water paint |
| CN108976995B (en) * | 2018-08-07 | 2020-09-15 | 安徽昌发实业有限公司 | High-quality water-based paint for wicker products |
| CN110791155A (en) * | 2019-12-04 | 2020-02-14 | 中国民用航空总局第二研究所 | High-temperature-resistant flame-retardant material and film forming preparation method thereof |
| CN110982387A (en) * | 2019-12-27 | 2020-04-10 | 常州市华菱新材料有限公司 | Water-based epoxy coating with good adhesive force and corrosion resistance on surface of metal substrate and preparation method thereof |
| CN110982387B (en) * | 2019-12-27 | 2021-08-20 | 常州市华菱新材料有限公司 | Water-based epoxy coating with good adhesive force and corrosion resistance on surface of metal substrate and preparation method thereof |
| CN112870772A (en) * | 2021-01-14 | 2021-06-01 | 江苏赛欧信越消泡剂有限公司 | Acid-resistant defoaming agent and preparation method thereof |
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Application publication date: 20180427 |
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