CN107099152A - A kind of radiation proof new material and preparation method thereof - Google Patents
A kind of radiation proof new material and preparation method thereof Download PDFInfo
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- CN107099152A CN107099152A CN201710350931.8A CN201710350931A CN107099152A CN 107099152 A CN107099152 A CN 107099152A CN 201710350931 A CN201710350931 A CN 201710350931A CN 107099152 A CN107099152 A CN 107099152A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L89/00—Compositions of proteins; Compositions of derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
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Abstract
The invention discloses a kind of radiation proof new material, the radiation proof new material includes the component of following mass parts：26 parts of organosilicon, 28 parts of dipentaerythritol, 13 parts of sodium hydroxide, 0.5 1.0 parts of cosolvent, 28 parts of aqueous acrylic emulsion, 35 parts of ethyl acetate, 5 15 parts of toluene, 35 parts of tributoxyethyl phosphate, 13 parts of fire retardant, 26 parts of styrene-butadiene latex, 5 15 parts of ethoxy ethanol, 26 parts of dimethyl ether, 79 parts of collagen, 9 15 parts of polyphenol.The invention provides a kind of radiation proof new material and preparation method thereof, the vigor of the radioresistance molecule of the new material and selection are strong through row, with good function affect, the formula of material is simple, cheap, and preparation technology is simple, realize cost-effective and reduce labor intensity, meet actual operation requirements.
Description
Technical field
The present invention relates to a kind of radiation proof new material and preparation method thereof, belong to new material and fabricating technology field.
Background technology
New material refers to some newly-developed or researching and developing, having preeminent performance materials, with than traditional material more
For excellent performance.New material technology is then the will according to people, is processed by physical study, design of material, material, experiment is commented
A series of research process such as valency, create the technology for the new material that can meet various needs.With scientific technological advance, people
On the basis of traditional material, according to the achievement in research of modern science and technology, new material is developed.New material is metal material by component
Material, inorganic non-metallic material（Such as ceramics, gallium arsenide semiconductor）, high-molecular organic material, the major class of advanced composite material four.Press
Material property is divided into structural material and functional material.Structural material mainly uses the mechanics and physicochemical property of material, to meet
The performance requirement such as high intensity, high rigidity, high rigidity, high temperature resistant, wear-resisting, anti-corrosion, Flouride-resistani acid phesphatase；Functional material mainly uses material
The effects such as the electricity, magnetic, sound, the photo-thermal that have, to realize certain function, such as semi-conducting material, magnetic material, light-sensitive material, temperature-sensitive
Material, stealth material and manufacture atom bomb, nuclear material of hydrogen bomb etc..New material acts on great in national defense construction.For example, ultrapure
Silicon, GaAs are succeeded in developing, and cause the birth of extensive and super large-scale integration, make the operational speed of a computer from per second several
Bring up to more than 10,000,000,000 times per second for 100000 times；The operating temperature of materials for aeroengines often improves 100 DEG C, and thrust can increase 24%；
Stealth material energy electromagnetic wave absorption or the infra-red radiation for reducing weaponry, make enemy's detection system be difficult to find etc..21 generation
One of Main way of discipline development in science and technology is the development and application of new material.The research of new material, is that the mankind are recognized physical property
Know and application is marched to deeper.
The research of new material is always the main body of China's scientific research project, if it is possible to research and develop that a composition is simple, raw material is honest and clean
Valency, and the green wood material formula and the simple preparation technology of flow of good result can be reached, will be the big contribution of the mankind.
The content of the invention
The present invention, should exactly in view of the deficienciess of the prior art, provide a kind of radiation proof new material and preparation method thereof
New material has good function effect, and the formula of material is simple, cheap, and preparation technology is simple, realizes and saves into
This meets actual operation requirements with reducing labor intensity.
To solve the above problems, the technical solution used in the present invention is as follows：
A kind of radiation proof new material, the radiation proof new material includes the component of following mass parts：2-6 parts of organosilicon, two seasons penta
2-8 parts of tetrol, 1-3 parts of sodium hydroxide, 0.5-1.0 parts of cosolvent, 2-8 parts of aqueous acrylic emulsion, 3-5 parts of ethyl acetate, first
5-15 parts of benzene, 3-5 parts of tributoxyethyl phosphate, 1-3 parts of fire retardant, 2-6 parts of styrene-butadiene latex, 5-15 parts of ethoxy ethanol, two
2-6 parts of methyl ether, 7-9 parts of collagen, 9-15 parts of polyphenol.
As the improvement of above-mentioned technical proposal, the content of component of the radiation proof new material is 4 parts of organosilicon, two seasons penta
5 parts of tetrol, 2 parts of sodium hydroxide, 0.75 part of cosolvent, 5 parts of aqueous acrylic emulsion, 4 parts of ethyl acetate, 10 parts of toluene, phosphoric acid
It is three 4 parts of butoxyethyls, 2 parts of fire retardant, 4 parts of styrene-butadiene latex, 10 parts of ethoxy ethanol, 4 parts of dimethyl ether, 8 parts of collagen, many
12 parts of phenol.
Specifically, a kind of preparation method of radiation proof new material is as follows：
Step（1）：By above-mentioned organosilicon, dipentaerythritol, sodium hydroxide, aqueous acrylic emulsion, ethyl acetate, tricresyl phosphate fourth
Epoxide ethyl ester, fire retardant, styrene-butadiene latex, dimethyl ether, collagen are proportionally added into homogenizer, are divided in whipping process
Add twice with the cosolvent got ready, mixer rotating speed 600-800rpm makes mixing material temperature be raised to 135 DEG C；
Step（2）：By step（1）Material in high speed mixer is released, and is added in low-speed mixer and is cooled, and is added simultaneously
The ethoxy ethanol and toluene of preheated processing, polyphenol is added when temperature drops to 65 degree, is stirred for 8-12 minutes, is well mixed
After discharge；
Step（3）：By step（2）The material being stirred is put into single screw extrusion machine, 135-160 DEG C of rotating speed 12- of plasticization temperature
16rpm, material of the present invention is produced by hot-forming twice, then through air-cooled.
Compared with prior art, implementation result of the invention is as follows by the present invention：
The invention provides a kind of radiation proof new material and preparation method thereof, the vigor of the radioresistance molecule of the new material and selection
Strong through row, with good function affect, the formula of material is simple, cheap, and preparation technology is simple, realizes section
About cost meets actual operation requirements with reducing labor intensity.
Note：Radiation proof new material produced by the present invention tool extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and
Enhance the radiation proof new material tensile strength and fracture elongation is big.
Embodiment
Illustrate present disclosure below in conjunction with specific embodiments.
Embodiment 1
A kind of radiation proof new material, the radiation proof new material includes the component of following mass parts：2 parts of organosilicon, two seasons penta 4
2 parts of alcohol, 1 part of sodium hydroxide, 0.5 part of cosolvent, 2 parts of aqueous acrylic emulsion, 3 parts of ethyl acetate, 5 parts of toluene, tricresyl phosphate fourth
3 parts of epoxide ethyl ester, 1 part of fire retardant, 2 parts of styrene-butadiene latex, 5 parts of ethoxy ethanol, 2 parts of dimethyl ether, 7 parts of collagen, polyphenol 9
Part.
Specifically, a kind of preparation method of radiation proof new material is as follows：
Step（1）：By above-mentioned organosilicon, dipentaerythritol, sodium hydroxide, aqueous acrylic emulsion, ethyl acetate, tricresyl phosphate fourth
Epoxide ethyl ester, fire retardant, styrene-butadiene latex, dimethyl ether, collagen are proportionally added into homogenizer, are divided in whipping process
Add twice with the cosolvent got ready, mixer rotating speed 600rpm makes mixing material temperature be raised to 135 DEG C；
Step（2）：By step（1）Material in high speed mixer is released, and is added in low-speed mixer and is cooled, and is added simultaneously
The ethoxy ethanol and toluene of preheated processing, polyphenol is added when temperature drops to 65 degree, is stirred for 8 minutes, after being well mixed
Discharging；
Step（3）：By step（2）The material being stirred is put into single screw extrusion machine, 135 DEG C of rotating speed 12rpm of plasticization temperature, warp
It is hot-forming after twice, then produce material of the present invention through air-cooled.
The vigor of the radioresistance molecule of material of the present invention and selection are strong through row, with good function affect,
The formula of material is simple, cheap, and preparation technology is simple, realizes cost-effective with reducing labor intensity, satisfaction reality
Use requirement.
Note：Radiation proof new material produced by the present invention tool extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and
Enhance the radiation proof new material tensile strength and fracture elongation is big.
Embodiment 2
A kind of radiation proof new material, the radiation proof new material includes the component of following mass parts, the radiation proof new material
Content of component is 4 parts of organosilicon, 5 parts of dipentaerythritol, 2 parts of sodium hydroxide, 0.75 part of cosolvent, aqueous acrylic emulsion 5
Part, 4 parts of ethyl acetate, 10 parts of toluene, 4 parts of tributoxyethyl phosphate, 2 parts of fire retardant, 4 parts of styrene-butadiene latex, ethoxy ethanol
10 parts, 4 parts of dimethyl ether, 8 parts of collagen, 12 parts of polyphenol.
Specifically, a kind of preparation method of radiation proof new material is as follows：
Step（1）：By above-mentioned organosilicon, dipentaerythritol, sodium hydroxide, aqueous acrylic emulsion, ethyl acetate, tricresyl phosphate fourth
Epoxide ethyl ester, fire retardant, styrene-butadiene latex, dimethyl ether, collagen are proportionally added into homogenizer, are divided in whipping process
Add twice with the cosolvent got ready, mixer rotating speed 700rpm makes mixing material temperature be raised to 135 DEG C；
Step（2）：By step（1）Material in high speed mixer is released, and is added in low-speed mixer and is cooled, and is added simultaneously
The ethoxy ethanol and toluene of preheated processing, polyphenol is added when temperature drops to 65 degree, is stirred for 10 minutes, after being well mixed
Discharging；
Step（3）：By step（2）The material being stirred is put into single screw extrusion machine, 150 DEG C of rotating speed 14rpm of plasticization temperature, warp
It is hot-forming after twice, then produce material of the present invention through air-cooled.
The vigor of the radioresistance molecule of material of the present invention and selection are strong through row, with good function affect,
The formula of material is simple, cheap, and preparation technology is simple, realizes cost-effective with reducing labor intensity, satisfaction reality
Use requirement.
Note：Radiation proof new material produced by the present invention tool extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and
Enhance the radiation proof new material tensile strength and fracture elongation is big.
Embodiment 3
A kind of radiation proof new material, the radiation proof new material includes 6 parts of component organosilicon, the dipentaerythritol of following mass parts
8 parts, 3 parts of sodium hydroxide, 1.0 parts of cosolvent, 8 parts of aqueous acrylic emulsion, 5 parts of ethyl acetate, 15 parts of toluene, tricresyl phosphate fourth oxygen
5 parts of base ethyl ester, 3 parts of fire retardant, 6 parts of styrene-butadiene latex, 15 parts of ethoxy ethanol, 6 parts of dimethyl ether, 9 parts of collagen, polyphenol 15
Part.
Specifically, a kind of preparation method of radiation proof new material is as follows：
Step（1）：By above-mentioned organosilicon, dipentaerythritol, sodium hydroxide, aqueous acrylic emulsion, ethyl acetate, tricresyl phosphate fourth
Epoxide ethyl ester, fire retardant, styrene-butadiene latex, dimethyl ether, collagen are proportionally added into homogenizer, are divided in whipping process
Add twice with the cosolvent got ready, mixer rotating speed 800rpm makes mixing material temperature be raised to 135 DEG C；
Step（2）：By step（1）Material in high speed mixer is released, and is added in low-speed mixer and is cooled, and is added simultaneously
The ethoxy ethanol and toluene of preheated processing, polyphenol is added when temperature drops to 65 degree, is stirred for 12 minutes, after being well mixed
Discharging；
Step（3）：By step（2）The material being stirred is put into single screw extrusion machine, 160 DEG C of rotating speed 16rpm of plasticization temperature, warp
It is hot-forming after twice, then produce material of the present invention through air-cooled.
The vigor of the radioresistance molecule of material of the present invention and selection are strong through row, with good function affect,
The formula of material is simple, cheap, and preparation technology is simple, realizes cost-effective with reducing labor intensity, satisfaction reality
Use requirement.
Note：Radiation proof new material produced by the present invention tool extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and
Enhance the radiation proof new material tensile strength and fracture elongation is big.
Above content is made for the present invention in conjunction with specific embodiments describes in detail, it is impossible to assert that the present invention is specific real
Apply and be only limitted to these explanations.For those skilled in the art, before present inventive concept is not departed from
Put, some simple deduction or replace can also be made, the scope of protection of the invention should be all considered as belonging to.
Claims (3)
1. a kind of radiation proof new material, it is characterised in that：The radiation proof new material includes the component of following mass parts：Organosilicon
2-6 parts, 2-8 parts of dipentaerythritol, 1-3 parts of sodium hydroxide, 0.5-1.0 parts of cosolvent, 2-8 parts of aqueous acrylic emulsion, acetic acid
3-5 parts of ethyl ester, 5-15 parts of toluene, 3-5 parts of tributoxyethyl phosphate, 1-3 parts of fire retardant, 2-6 parts of styrene-butadiene latex, ethyoxyl second
5-15 parts of alcohol, 2-6 parts of dimethyl ether, 7-9 parts of collagen, 9-15 parts of polyphenol.
2. a kind of radiation proof new material according to claim 1, it is characterised in that：The mass parts group of the radiation proof new material
It is divided into 4 parts of organosilicon, 5 parts of dipentaerythritol, 2 parts of sodium hydroxide, 0.75 part of cosolvent, 5 parts of aqueous acrylic emulsion, acetic acid second
4 parts of ester, 10 parts of toluene, 4 parts of tributoxyethyl phosphate, 2 parts of fire retardant, 4 parts of styrene-butadiene latex, 10 parts of ethoxy ethanol, diformazan
4 parts of ether, 8 parts of collagen, 12 parts of polyphenol.
3. a kind of preparation method of radiation proof new material according to claim 1-2, it is characterised in that：The preparation method is such as
Under：
Step（1）：By above-mentioned organosilicon, dipentaerythritol, sodium hydroxide, aqueous acrylic emulsion, ethyl acetate, tricresyl phosphate fourth
Epoxide ethyl ester, fire retardant, styrene-butadiene latex, dimethyl ether, collagen are proportionally added into homogenizer, are divided in whipping process
Add twice with the cosolvent got ready, mixer rotating speed 600-800rpm makes mixing material temperature be raised to 135 DEG C；
Step（2）：By step（1）Material in high speed mixer is released, and is added in low-speed mixer and is cooled, and is added simultaneously
The ethoxy ethanol and toluene of preheated processing, polyphenol is added when temperature drops to 65 degree, is stirred for 8-12 minutes, is well mixed
After discharge；
Step（3）：By step（2）The material being stirred is put into single screw extrusion machine, 135-160 DEG C of rotating speed 12- of plasticization temperature
16rpm, material of the present invention is produced by hot-forming twice, then through air-cooled.
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| CN201710350931.8A CN107099152A (en) | 2017-05-18 | 2017-05-18 | A kind of radiation proof new material and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722767A (en) * | 2017-11-07 | 2018-02-23 | 广西小草信息产业有限责任公司 | A kind of radiation proof new material and preparation method thereof |
| CN107868373A (en) * | 2017-11-16 | 2018-04-03 | 芜湖领航新材料科技有限公司 | A kind of radiation proof new material |
| CN109181348A (en) * | 2018-09-28 | 2019-01-11 | 桐城市双港森科塑料厂 | A kind of radiation protection new material |
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| CN105199283A (en) * | 2015-10-30 | 2015-12-30 | 太仓市天合新材料科技有限公司 | Novel radiation-proof material |
| CN106243573A (en) * | 2016-08-29 | 2016-12-21 | 裴寿益 | A kind of radiation proof material |
| CN106380724A (en) * | 2016-08-30 | 2017-02-08 | 裴寿益 | New radiation-shielding composite material |
| CN106497087A (en) * | 2016-11-24 | 2017-03-15 | 安徽省天乐塑业有限公司 | A kind of edible soybean protein isolate packaging film and preparation method thereof |
-
2017
- 2017-05-18 CN CN201710350931.8A patent/CN107099152A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105199283A (en) * | 2015-10-30 | 2015-12-30 | 太仓市天合新材料科技有限公司 | Novel radiation-proof material |
| CN106243573A (en) * | 2016-08-29 | 2016-12-21 | 裴寿益 | A kind of radiation proof material |
| CN106380724A (en) * | 2016-08-30 | 2017-02-08 | 裴寿益 | New radiation-shielding composite material |
| CN106497087A (en) * | 2016-11-24 | 2017-03-15 | 安徽省天乐塑业有限公司 | A kind of edible soybean protein isolate packaging film and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107722767A (en) * | 2017-11-07 | 2018-02-23 | 广西小草信息产业有限责任公司 | A kind of radiation proof new material and preparation method thereof |
| CN107868373A (en) * | 2017-11-16 | 2018-04-03 | 芜湖领航新材料科技有限公司 | A kind of radiation proof new material |
| CN109181348A (en) * | 2018-09-28 | 2019-01-11 | 桐城市双港森科塑料厂 | A kind of radiation protection new material |
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