CN107956109A - 一种羊毛织物的抗菌防缩整理工艺 - Google Patents
一种羊毛织物的抗菌防缩整理工艺 Download PDFInfo
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Abstract
本发明公开了一种羊毛织物的抗菌防缩整理工艺，所述工艺包括前处理、抗菌整理及防缩整理等步骤。(1)本发明所述整理工艺主要采用浸渍处理的方式，通过一系列的前处理步骤能够很容易的将抗菌、防缩整理液整理于羊毛织物的表面；(2)本发明所述整理工艺整理后的羊毛织物具有良好的抗菌和防缩性能，且重复水洗后织物的抗菌耐久性和尺寸稳定性较好。
Description
技术领域
本发明属于纺织技术领域，涉及一种功能性羊毛织物，具体为一种羊毛织物的抗菌防缩整理工艺。
背景技术
在适宜的温湿度环境中，天然纤维尤其是蛋白质纤维成为了微生物生长的良好媒介。纺织品中微生物的大量生长能够引起纺织品降解，产生斑点，不良气味等，对纺织品进行抗菌整理是解决这些问题的理想方法之一。抗菌整理能使细菌致死或抑制其生长。
目前，羊毛织物的研究取得了较大进展，例如应用重金属微粒银或重金属络合物、甲壳素、生物溶菌酶、阳离子季铵盐等抗菌剂对羊毛进行抗菌整理，但由于羊毛本身的特殊结构及其化学组成，通常未经预处理的羊毛纺织品无法直接与具有抗菌活性的整理剂结合反应。因为这种技术难点，抗菌羊毛纺织品未能大规模商品化。
发明内容
本发明解决的技术问题：为了克服现有技术的缺陷，获得一种易于将抗菌、防缩等整理剂整理于羊毛织物表面，且能够稳定结合的工艺，本发明提供了羊毛织物的抗菌防缩整理工艺。
技术方案：一种羊毛织物的抗菌防缩整理工艺，所述工艺包括以下步骤：
(1)将羊毛织物置于质量分数为16％～40％的氢氧化钠水溶液中，在常温条件下进行碱化反应1.5～4小时，反应结束后，加入体积分数为4％～11％的盐酸中和残余的氢氧化钠，去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的羊毛织物浸渍于整理液A中，织物与整理液A的浴比为1:25～30，反应温度为25～35℃，pH为8.0～8.5，反应时间为30～60min，结束后去离子水漂洗，并80℃烘干；
(3)将步骤(2)整理后的羊毛织物浸渍于整理液B中，织物与整理液B的浴比为1:40～50，反应温度为40～50℃，反应时间为25～40min，结束后立即置于烘箱中烘干。
优选的，步骤(1)中所述羊毛织物面密度为165g/m2。
优选的，步骤(2)中所述整理液A，按重量份计包括硫酸氢钾复合盐15～26份、亚硫酸钠8～19份、表面活性剂Triton X-100 1～3份、水35～60份。
优选的，所述亚硫酸钠的质量浓度为8～11g/L。
优选的，步骤(3)中所述整理液B，按重量份计包括聚六亚甲基双胍14～28份、表面活性剂Triton X-100 1～3份、水40～70份。
优选的，所述表面活性剂Triton X-100的质量分数为0.1～0.3％。
有益效果：(1)本发明所述整理工艺主要采用浸渍处理的方式，通过一系列的前处理步骤能够很容易的将抗菌、防缩整理液整理于羊毛织物的表面；(2)本发明所述整理工艺整理后的羊毛织物具有良好的抗菌和防缩性能，且重复水洗后织物的抗菌耐久性和尺寸稳定性较好。
具体实施方式
实施例1
一种羊毛织物的抗菌防缩整理工艺，所述工艺包括以下步骤：
(1)将羊毛织物置于质量分数为16％的氢氧化钠水溶液中，在常温条件下进行碱化反应1.5小时，反应结束后，加入体积分数为4％的盐酸中和残余的氢氧化钠，去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的羊毛织物浸渍于整理液A中，织物与整理液A的浴比为1:25，反应温度为25℃，pH为8.0，反应时间为30min，结束后去离子水漂洗，并80℃烘干；
(3)将步骤(2)整理后的羊毛织物浸渍于整理液B中，织物与整理液B的浴比为1:40，反应温度为40℃，反应时间为25min，结束后立即置于烘箱中烘干。
步骤(1)中所述羊毛织物面密度为165g/m2。
步骤(2)中所述整理液A，按重量份计包括硫酸氢钾复合盐15份、亚硫酸钠8份、表面活性剂Triton X-100 1份、水35份。
所述亚硫酸钠的质量浓度为8g/L。
步骤(3)中所述整理液B，按重量份计包括聚六亚甲基双胍14份、表面活性剂Triton X-1001份、水40份。
所述表面活性剂Triton X-100的质量分数为0.1％。
实施例2
一种羊毛织物的抗菌防缩整理工艺，所述工艺包括以下步骤：
(1)将羊毛织物置于质量分数为28％的氢氧化钠水溶液中，在常温条件下进行碱化反应2.5小时，反应结束后，加入体积分数为7％的盐酸中和残余的氢氧化钠，去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的羊毛织物浸渍于整理液A中，织物与整理液A的浴比为1:28，反应温度为30℃，pH为8.3，反应时间为45min，结束后去离子水漂洗，并80℃烘干；
(3)将步骤(2)整理后的羊毛织物浸渍于整理液B中，织物与整理液B的浴比为1:45，反应温度为45℃，反应时间为30min，结束后立即置于烘箱中烘干。
步骤(1)中所述羊毛织物面密度为165g/m2。
步骤(2)中所述整理液A，按重量份计包括硫酸氢钾复合盐20份、亚硫酸钠12份、表面活性剂Triton X-100 2份、水45份。
所述亚硫酸钠的质量浓度为10g/L。
步骤(3)中所述整理液B，按重量份计包括聚六亚甲基双胍20份、表面活性剂Triton X-1002份、水50份。
所述表面活性剂Triton X-100的质量分数为0.2％。
实施例3
一种羊毛织物的抗菌防缩整理工艺，所述工艺包括以下步骤：
(1)将羊毛织物置于质量分数为40％的氢氧化钠水溶液中，在常温条件下进行碱化反应4小时，反应结束后，加入体积分数为11％的盐酸中和残余的氢氧化钠，去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的羊毛织物浸渍于整理液A中，织物与整理液A的浴比为1:30，反应温度为35℃，pH为8.5，反应时间为60min，结束后去离子水漂洗，并80℃烘干；
(3)将步骤(2)整理后的羊毛织物浸渍于整理液B中，织物与整理液B的浴比为1:50，反应温度为50℃，反应时间为40min，结束后立即置于烘箱中烘干。
步骤(1)中所述羊毛织物面密度为165g/m2。
步骤(2)中所述整理液A，按重量份计包括硫酸氢钾复合盐26份、亚硫酸钠19份、表面活性剂Triton X-100 3份、水60份。
所述亚硫酸钠的质量浓度为11g/L。
步骤(3)中所述整理液B，按重量份计包括聚六亚甲基双胍28份、表面活性剂Triton X-1003份、水70份。
所述表面活性剂Triton X-100的质量分数为0.3％。
对实施例1～3所述工艺整理获得的羊毛织物进行性能测试，结果如下表所示：
Claims (6)
1.一种羊毛织物的抗菌防缩整理工艺，其特征在于，所述工艺包括以下步骤：
(1)将羊毛织物置于质量分数为16％～40％的氢氧化钠水溶液中，在常温条件下进行碱化反应1.5～4小时，反应结束后，加入体积分数为4％～11％的盐酸中和残余的氢氧化钠，去离子水反复洗涤，自然晾干；
(2)将步骤(1)处理后的羊毛织物浸渍于整理液A中，织物与整理液A的浴比为1:25～30，反应温度为25～35℃，pH为8.0～8.5，反应时间为30～60min，结束后去离子水漂洗，并80℃烘干；
(3)将步骤(2)整理后的羊毛织物浸渍于整理液B中，织物与整理液B的浴比为1:40～50，反应温度为40～50℃，反应时间为25～40min，结束后立即置于烘箱中烘干。
2.根据权利要求1所述的一种羊毛织物的抗菌防缩整理工艺，其特征在于，步骤(1)中所述羊毛织物面密度为165g/m2。
3.根据权利要求1所述的一种羊毛织物的抗菌防缩整理工艺，其特征在于，步骤(2)中所述整理液A，按重量份计包括硫酸氢钾复合盐15～26份、亚硫酸钠8～19份、表面活性剂Triton X-100 1～3份、水35～60份。
4.根据权利要求3所述的一种羊毛织物的抗菌防缩整理工艺，其特征在于，所述亚硫酸钠的质量浓度为8～11g/L。
5.根据权利要求1所述的一种羊毛织物的抗菌防缩整理工艺，其特征在于，步骤(3)中所述整理液B，按重量份计包括聚六亚甲基双胍14～28份、表面活性剂Triton X-100 1～3份、水40～70份。
6.根据权利要求3或5所述的一种羊毛织物的抗菌防缩整理工艺，其特征在于，所述表面活性剂Triton X-100的质量分数为0.1～0.3％。
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