CN107937094A - 一种高附着性耐磨自动化机械设备用润滑脂及其制备 - Google Patents

一种高附着性耐磨自动化机械设备用润滑脂及其制备 Download PDF

Info

Publication number
CN107937094A
CN107937094A CN201711128872.6A CN201711128872A CN107937094A CN 107937094 A CN107937094 A CN 107937094A CN 201711128872 A CN201711128872 A CN 201711128872A CN 107937094 A CN107937094 A CN 107937094A
Authority
CN
China
Prior art keywords
parts
adhesion
lubricating grease
resisting
automated machine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711128872.6A
Other languages
English (en)
Inventor
李逊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUXI ZHONGKE SUHUI AUTOMATION TECHNOLOGY CO LTD
Original Assignee
WUXI ZHONGKE SUHUI AUTOMATION TECHNOLOGY CO LTD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WUXI ZHONGKE SUHUI AUTOMATION TECHNOLOGY CO LTD filed Critical WUXI ZHONGKE SUHUI AUTOMATION TECHNOLOGY CO LTD
Priority to CN201711128872.6A priority Critical patent/CN107937094A/zh
Publication of CN107937094A publication Critical patent/CN107937094A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/04—Elements
    • C10M2201/041—Carbon; Graphite; Carbon black
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/10—Compounds containing silicon
    • C10M2201/105—Silica
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02—Hydroxy compounds
    • C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/126—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic
    • C10M2207/1265—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids monocarboxylic used as thickening agent
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/289—Partial esters containing free hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/401—Fatty vegetable or animal oils used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/109—Polyethers, i.e. containing di- or higher polyoxyalkylene groups esterified
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/12—Polysaccharides, e.g. cellulose, biopolymers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/08—Amides
    • C10M2215/082—Amides containing hydroxyl groups; Alkoxylated derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2225/00—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2225/04—Organic macromolecular compounds containing phosphorus as ingredients in lubricant compositions obtained by phosphorisation of macromolecualr compounds not containing phosphorus in the monomers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/061—Esters derived from boron
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
    • C10M2227/06—Organic compounds derived from inorganic acids or metal salts
    • C10M2227/065—Organic compounds derived from inorganic acids or metal salts derived from Ti or Zr
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2050/00—Form in which the lubricant is applied to the material being lubricated
    • C10N2050/10—Semi-solids; greasy

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

本发明公开了一种高附着性耐磨自动化机械设备用润滑脂，其由以下重量份数的原料组成：高附着性基础油50~80份、钛酸酯偶联剂1~3份、椰油酸二乙醇酰胺2~6份、石墨粉1~3份、季戊四醇酯20~30份、蓖麻油烷醇酰胺硼酸酯1~3份、脂肪酸聚氧乙烯酯2~5份、气相二氧化硅3~7份、鲸蜡醇3~6份、羟甲基纤维素0.5~1.5份、羟丙基二淀粉磷酸酯1~4份、其他功能助剂1~2份。本发明采用附着性、耐磨性良好的原料，可在较长时间内保持润滑部位的润滑，而且工艺简单，便于大规模工业化生产和使用，所得润滑脂综合润滑性能良好，具有较高的经济价值和社会价值，适合工业化生产和大批量的自动化设备使用。

Description

一种高附着性耐磨自动化机械设备用润滑脂及其制备
技术领域
本发明涉及润滑脂技术领域，尤其是涉及一种高附着性耐磨自动化机械设备用润滑脂及其制备方法。
背景技术
科技的不断发展带动了自动化技术的不断进步，至今，自动化设备广泛用于工农业、军事、科学研究、交通运输业、商业、医疗、服务和家电等方面。自动化技术不仅可以把人从繁重的体力劳动、部分脑力劳动以及危险、恶劣的工作环境中解放出来，同时可以扩展人的器官功能，极大地提高劳动生产率，增强人类认知世界和改造世界的能力。自动化机械设备在使用、运行过程中，许多零件的运转需要使用大量的油脂润滑，现有的用于自动化设备的润滑脂存在的问题为，其涂覆后的附着性较差，尤其是自动化设备在使用过程中由于机械摩擦不断产生热量，导致润滑油脂温度不断升高产生滴落，这种现象不仅容易导致润滑部位的润滑性失效，需要经常补加润滑剂，增加了工人工作量且容易因遗漏导致设备机械性磨损，而且容易导致环境污染，降低工作效率，影响了自动化机械设备的正常运转。
发明内容
针对现有技术不足，本发明提供了一种自动化设备用的高附着性、高耐磨性的润滑脂及其制备方法。
本发明解决上述技术问题采用的技术方案为：一种高附着性耐磨自动化机械设备用润滑脂，其由以下原料组成：高附着性基础油、稠化剂、钛酸酯偶联剂、椰油酸二乙醇酰胺、石墨粉、季戊四醇酯、蓖麻油烷醇酰胺硼酸酯、脂肪酸聚氧乙烯酯、气相二氧化硅、鲸蜡醇、羟甲基纤维素、羟丙基二淀粉磷酸酯、其他功能助剂；
所述的原料的重量份数为：高附着性基础油50~80份、钛酸酯偶联剂1~3份、椰油酸二乙醇酰胺2~6份、石墨粉1~3份、季戊四醇酯20~30份、蓖麻油烷醇酰胺硼酸酯1~3份、脂肪酸聚氧乙烯酯2~5份、气相二氧化硅3~7份、鲸蜡醇3~6份、羟甲基纤维素0.5~1.5份、羟丙基二淀粉磷酸酯1~4份、其他功能助剂1~2份。
进一步地，所述的高附着性基础油为棕榈油和动物獾油，其质量份比为5~10:1。
进一步地，所述的稠化剂为锂皂、钙皂或锂钙复合皂稠化剂。
进一步地，所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，包括以下步骤：将稠化剂、50~70%量的高附着性基础油置于皂化釜中混合后，于80~100℃皂化反应2~4h，加入剩余高附着性基础油继续保温反应0.5~1h，升温至160~180℃并保温10min后转移至调和釜冷却回流，冷却至70~80℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
与现有技术相比，本发明具备的有益效果为：本发明提供的一种高附着性耐磨自动化机械设备用润滑脂及其制备，采用附着性、耐磨性良好的原料，可在较长时间内保持润滑部位的润滑，而且工艺简单，便于大规模工业化生产和使用，所得润滑脂综合润滑性能良好，具有较高的经济价值和社会价值，适合工业化生产和大批量的自动化设备使用。
具体实施方式
下面结合具体实施例对本发明做进一步的说明。
实施例1：一种高附着性耐磨自动化机械设备用润滑脂，其由以下原料组成：高附着性基础油、钛酸酯偶联剂、椰油酸二乙醇酰胺、石墨粉、季戊四醇酯、蓖麻油烷醇酰胺硼酸酯、脂肪酸聚氧乙烯酯、气相二氧化硅、鲸蜡醇、羟甲基纤维素、羟丙基二淀粉磷酸酯、其他功能助剂；
所述的原料的重量份数为：高附着性基础油65份、钛酸酯偶联剂2份、椰油酸二乙醇酰胺4份、石墨粉2份、季戊四醇酯25份、蓖麻油烷醇酰胺硼酸酯2份、脂肪酸聚氧乙烯酯4份、气相二氧化硅5份、鲸蜡醇5份、羟甲基纤维素1份、羟丙基二淀粉磷酸酯2份、其他功能助剂1.5份。
进一步地，所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为4:2:1。
进一步地，所述的稠化剂为锂皂稠化剂。
进一步地，所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，包括以下步骤：将稠化剂、60%量的高附着性基础油置于皂化釜中混合后，于90℃皂化反应3h，加入剩余高附着性基础油继续保温反应45min，升温至170℃并保温10min后转移至调和釜冷却回流，冷却至75℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
实施例2：一种高附着性耐磨自动化机械设备用润滑脂，其由以下重量份数的原料组成：高附着性基础油50份、钛酸酯偶联剂1份、椰油酸二乙醇酰胺2份、石墨粉1份、季戊四醇酯20份、蓖麻油烷醇酰胺硼酸酯1份、脂肪酸聚氧乙烯酯2份、气相二氧化硅3份、鲸蜡醇3份、羟甲基纤维素0.5份、羟丙基二淀粉磷酸酯1份、其他功能助剂1份。
进一步地，所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为3:1:1；所述的稠化剂为钙皂稠化剂；所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，包括以下步骤：将稠化剂、50%量的高附着性基础油置于皂化釜中混合后，于80℃皂化反应2h，加入剩余高附着性基础油继续保温反应0.5h，升温至160℃并保温10min后转移至调和釜冷却回流，冷却至70℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
实施例3：一种高附着性耐磨自动化机械设备用润滑脂，其由以下重量份数的原料组成：高附着性基础油80份、钛酸酯偶联剂3份、椰油酸二乙醇酰胺6份、石墨粉3份、季戊四醇酯30份、蓖麻油烷醇酰胺硼酸酯3份、脂肪酸聚氧乙烯酯5份、气相二氧化硅7份、鲸蜡醇6份、羟甲基纤维素1.5份、羟丙基二淀粉磷酸酯4份、其他功能助剂2份。
进一步地，所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为5: 3:1；所述的稠化剂为锂钙复合皂稠化剂；所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，包括以下步骤：将稠化剂、70%量的高附着性基础油置于皂化釜中混合后，于100℃皂化反应4h，加入剩余高附着性基础油继续保温反应1h，升温至180℃并保温10min后转移至调和釜冷却回流，冷却至80℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
实施例4：一种高附着性耐磨自动化机械设备用润滑脂，其由以下重量份数的原料组成：高附着性基础油60份、钛酸酯偶联剂3份、椰油酸二乙醇酰胺2份、石墨粉1份、季戊四醇酯30份、蓖麻油烷醇酰胺硼酸酯1份、脂肪酸聚氧乙烯酯5份、气相二氧化硅3份、鲸蜡醇6份、羟甲基纤维素0.5份、羟丙基二淀粉磷酸酯1份、其他功能助剂2份。
进一步地，所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为5:1:1；所述的稠化剂为锂皂稠化剂；所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，包括以下步骤：将稠化剂、55%量的高附着性基础油置于皂化釜中混合后，于95℃皂化反应3.5h，加入剩余高附着性基础油继续保温反应50min，升温至165℃并保温10min后转移至调和釜冷却回流，冷却至70℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
实施例5：一种高附着性耐磨自动化机械设备用润滑脂，其由以下重量份数的原料组成：高附着性基础油70份、钛酸酯偶联剂1.5份、椰油酸二乙醇酰胺5份、石墨粉2.5份、季戊四醇酯26份、蓖麻油烷醇酰胺硼酸酯2.5份、脂肪酸聚氧乙烯酯4份、气相二氧化硅6份、鲸蜡醇4份、羟甲基纤维素0.8份、羟丙基二淀粉磷酸酯3份、其他功能助剂1.5份。
进一步地，所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为9:4:2；所述的稠化剂为锂皂稠化剂；所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，其具体步骤同实施例1。
对上述实施例1-5得到的润滑脂进行标准测试，结果显示，上述实施例1-5得到的润滑脂的工作锥入度为270~180（0.1mm），滴点为245~255℃，四球法抗磨性能0.45~0.53mm，润滑脂润滑性和附着性较好，制备方法简单，是一种适合工业化生产和大批量自动化设备使用的润滑脂。
应当指出的是，上述实施例所揭示的内容，仅为本发明较佳实施例的数种，但凡本领域技术人员采用的局部变更、变化，或对本发明所揭示的技术内容的部分修饰，而源于本发明的技术本质且为熟习该项技艺的人所不加创造性思维易于推知获得的，皆不脱离本发明的专利权范畴。

Claims (5)

1.一种高附着性耐磨自动化机械设备用润滑脂，其特征在于，由以下原料组成：高附着性基础油、钛酸酯偶联剂、椰油酸二乙醇酰胺、石墨粉、季戊四醇酯、蓖麻油烷醇酰胺硼酸酯、脂肪酸聚氧乙烯酯、气相二氧化硅、鲸蜡醇、羟甲基纤维素、羟丙基二淀粉磷酸酯、其他功能助剂；
所述的原料的重量份数为：高附着性基础油50~80份、钛酸酯偶联剂1~3份、椰油酸二乙醇酰胺2~6份、石墨粉1~3份、季戊四醇酯20~30份、蓖麻油烷醇酰胺硼酸酯1~3份、脂肪酸聚氧乙烯酯2~5份、气相二氧化硅3~7份、鲸蜡醇3~6份、羟甲基纤维素0.5~1.5份、羟丙基二淀粉磷酸酯1~4份、其他功能助剂1~2份。
2.根据权利要求1所述的一种高附着性耐磨自动化机械设备用润滑脂，其特征在于：所述的高附着性基础油为棕榈油、大豆油和氢化蓖麻油，其质量份比为3~5:1~3:1。
3.根据权利要求1所述的一种高附着性耐磨自动化机械设备用润滑脂，其特征在于：所述的稠化剂为锂皂、钙皂或锂钙复合皂稠化剂。
4.根据权利要求1所述的一种高附着性耐磨自动化机械设备用润滑脂，其特征在于：所述的其他功能助剂为抗氧剂、消泡剂、防锈剂、降凝剂的复合。
5.权利要求1-4任一项所述的一种高附着性耐磨自动化机械设备用润滑脂的制备方法，其特征在于，包括以下步骤：将稠化剂、50~70%量的高附着性基础油置于皂化釜中混合后，于80~100℃皂化反应2~4h，加入剩余高附着性基础油继续保温反应0.5~1h，升温至160~180℃并保温10min后转移至调和釜冷却回流，冷却至70~80℃时加入其余原料，保温均化研磨，脱气处理，冷却至常温后得到本发明的润滑脂。
CN201711128872.6A 2017-11-15 2017-11-15 一种高附着性耐磨自动化机械设备用润滑脂及其制备 Pending CN107937094A (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711128872.6A CN107937094A (zh) 2017-11-15 2017-11-15 一种高附着性耐磨自动化机械设备用润滑脂及其制备

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711128872.6A CN107937094A (zh) 2017-11-15 2017-11-15 一种高附着性耐磨自动化机械设备用润滑脂及其制备

Publications (1)

Publication Number Publication Date
CN107937094A true CN107937094A (zh) 2018-04-20

Family

ID=61931147

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711128872.6A Pending CN107937094A (zh) 2017-11-15 2017-11-15 一种高附着性耐磨自动化机械设备用润滑脂及其制备

Country Status (1)

Country Link
CN (1) CN107937094A (zh)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107815339A (zh) * 2017-11-15 2018-03-20 无锡中科苏惠自动化技术有限公司 高附着性耐磨自动化机械设备用润滑油及其制备方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1699528A (zh) * 2005-05-24 2005-11-23 吴兴和 通用减磨润滑油添加剂及制备方法
CN103497812A (zh) * 2013-08-29 2014-01-08 中国石油化工股份有限公司 一种生物降解型膨润土润滑脂组合物及制备方法
CN104531272A (zh) * 2014-12-08 2015-04-22 邯郸派瑞化工科技有限公司 一种电气石辅助二硫化钼类润滑添加剂及其制备方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1699528A (zh) * 2005-05-24 2005-11-23 吴兴和 通用减磨润滑油添加剂及制备方法
CN103497812A (zh) * 2013-08-29 2014-01-08 中国石油化工股份有限公司 一种生物降解型膨润土润滑脂组合物及制备方法
CN104531272A (zh) * 2014-12-08 2015-04-22 邯郸派瑞化工科技有限公司 一种电气石辅助二硫化钼类润滑添加剂及其制备方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
孙建林: "《材料成形摩擦与润滑》", 31 July 2007, 国防工业出版社 *
李有良等: "《工业炸药生产技术》", 30 April 2016, 北京理工大学出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107815339A (zh) * 2017-11-15 2018-03-20 无锡中科苏惠自动化技术有限公司 高附着性耐磨自动化机械设备用润滑油及其制备方法

Similar Documents

Publication Publication Date Title
CN103981004B (zh) 极压复合铝基润滑脂组合物及制备方法
CN103897781A (zh) 1206润滑脂
CN104073327A (zh) 乳化切削液、切削稀释液及其制备和使用方法
CN105062643B (zh) 硼酸磷酸脂肪酯及其制备方法和用该酯制备微量润滑油
CN104450130A (zh) 金属切削液及其制备方法
CN104263476A (zh) 生物可降解微量润滑油及其制备方法
CN104450120A (zh) 一种半合成金属拉丝润滑液及制备方法
CN107474917A (zh) 一种石墨烯润滑油及其制备方法
CN103361151A (zh) 一种润滑剂组合物及其制备方法和用该组合物配制微量润滑剂
CN108085097A (zh) 一种高温设备润滑油
CN104818103B (zh) 汽车用低碳钢件冷挤压成形润滑剂及其制备方法
CN105950268A (zh) 一种含石墨烯添加剂的金属加工多功能润滑剂及其制备方法
CN108130168A (zh) 一种高温锂基脂及其制备方法
CN107937094A (zh) 一种高附着性耐磨自动化机械设备用润滑脂及其制备
CN104120017B (zh) 一种渗透力强防锈性能好的水基切削液及其制备方法
CN113493716B (zh) 润滑脂组合物及其制备方法
CN104073322A (zh) 金属加工液及其制备方法
CN110734804B (zh) 一种纳米切削油及其制备方法和应用
CN102618377A (zh) 空调用铜螺纹管轧制润滑液、制备方法及使用方法
CN102936530B (zh) 一种齿轮加工微量切削液
CN107815339A (zh) 高附着性耐磨自动化机械设备用润滑油及其制备方法
CN105154195B (zh) 一种极压复合锂基润滑脂组合物
CN108998176A (zh) 一种铝合金切削液及其制备方法
CN107880981A (zh) 一种用于自动化机械设备的生物基润滑脂及其制备方法
CN1743438A (zh) 冲压模具及金属拉丝模具适用的耐高温耐重负荷的润滑剂

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180420

WD01 Invention patent application deemed withdrawn after publication