CN107935682A - Production method of microbial fertilizer with comprehensive nutrition and rich humus - Google Patents

Production method of microbial fertilizer with comprehensive nutrition and rich humus Download PDF

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Publication number
CN107935682A
CN107935682A CN201711166396.7A CN201711166396A CN107935682A CN 107935682 A CN107935682 A CN 107935682A CN 201711166396 A CN201711166396 A CN 201711166396A CN 107935682 A CN107935682 A CN 107935682A
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rich
humus
comprehensive
production method
mixed
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CN107935682B (en
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孙仁贵
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Woda Agricultural Technology Co ltd
Xinjiang Black Key Acid Fertilizer Co ltd
Xinjiang Standard Spectrum Testing Engineering Technology Co ltd
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Maanshan Xinzhou Grape Specialized Cooperative
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

A production method of a microbial fertilizer with comprehensive nutrition and rich humus is characterized by comprising the steps of preparing porous particles, preparing biogas slurry chelating liquid, preparing a fertilizer inner core by using the porous particles and decomposed biogas residues as raw materials, spraying the biogas slurry chelating liquid in vacuum, and coating by using gamma-glutamic acid and gelatin as coating slow-release agents to obtain the microbial fertilizer with comprehensive nutrition and rich humus. The microbial fertilizer with comprehensive nutrition and rich humus can promote healthy growth of organisms and greatly increase yield of crops; but also has the capability of loosening soil and increasing the reserved water of the soil.

Description

A kind of nutrition is comprehensive and is rich in the production method of the microbial manure of humus
Technical field
The invention belongs to fertilizer field, and in particular to a kind of nutrition is comprehensive and is rich in the producer of the microbial manure of humus Method.
Background technology
Although the application of chemical fertilizer promotes the raising of crop yield, if but long-term a large amount of administrations, soil will be destroyed Structure, cause soil fertility to decline, and is not only decreased obviously yield increase effect, or even pollutes the environment.Compared with chemical fertilizer, microorganism Fertilizer has obvious advantage in terms of improving utilization rate of fertilizer, increase crop yield and preserving the ecological environment.Carry out in a deep going way micro- Bio-feritlizer is studied, for realizing that agricultural sustainable development has very important significance.
The content of the invention
A kind of nutrition it is an object of the invention to provide improvement soil hardening, increasing both production and income is comprehensive and rich in humus The production method of microbial manure.
In order to realize above-mentioned purpose, present invention employs following technical solution:
A kind of nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that it includes, porous particle Preparation, prepared by biogas slurry chelating liquid, prepare fertilizer inner core by raw material of porous particle and decomposed biogas residue, airless spraying biogas slurry chelates Liquid, then using gamma-glutamic acid and gelatin as coated slow release formulation, coating, obtains nutrition comprehensively and is rich in the microbial manure of humus.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that its specific step Suddenly it is:
(1)Flyash and bentonite are mixed, ultramicro grinding is carried out to 160-180 mesh sieves are crossed, adds water, regulation system water content For 25-30%, 40-60min is stirred with the stir speed (S.S.) of 250-300r/min, to the paste of substantially uniformity, is then squeezed into thickness The sheet of 2cm;
(2)By step(1)Obtained flaky material is put into 550-600 DEG C of high temperature kiln roasting 3-5h, cools down, and crushes, mistake 20-40 mesh sieves, then 15-20min is cleaned using ultrasonic cleaning agent, filter, drying, obtains porous particle;
(3)Urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate are uniformly mixed, 60-80 mesh is crushed, obtains mixed-powder; Mixed-powder, EM bacteria agent are added in biogas slurry again, magnetic agitation 60min, makes it fully dissolve under the conditions of 50 DEG C, adjusts body The pH of system to 6, adds EDTA and OP-10, continues magnetic agitation 30min, obtains biogas slurry chelating liquid;
(4)Porous particle, decomposed biogas residue are uniformly mixed, is transferred in comminutor and is granulated, obtains fertilizer inner core;By poly- γ-paddy Propylhomoserin is added in stirring container, adds deionized water, stirs evenly the Polyurethane-epoxy resin aqueous solution for being configured to 2-4%;By gelatin It is added in stirring container, adds deionized water to submerge gelatin, is placed in 40-45 DEG C of water bath with thermostatic control, it is complete to mix to gelatin Fully dissolved, adds deionized water constant volume, is configured to the aqueous gelatin solution of 2-4%;
(5)Fertilizer inner core is added in vacuum deposition apparatus under normal pressure, starts to extract vacuum and causes air, when pressure is reduced to During 0.02-0.04MPa, start to spray biogas slurry chelating liquid, mixed organization continuous mixed fertilizer inner core during spraying, to spray It is even;After spraying mixing stops, pressure is constantly raised until normal pressure, starts mixing spraying Polyurethane-epoxy resin aqueous solution and gelatin water The mixed solution of solution, after spraying, starts the hot wind that air blower rouses 40-50 DEG C, continues to mix 15-20min, obtain nutrition Microbial manure comprehensive and rich in humus.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that step(1)In Flyash and bentonitic mass ratio are 1:1.2-1.5.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that step(3)In Biogas slurry, urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate, EM bacteria agent, the mass ratio of EDTA and OP-10 are 1:0.22- 0.25:0.18-0.2:0.15-0.18:0.1-0.12:0.1-0.12:0.04-0.05:0.02-0.03:0.01-0.012.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that step(4)In Porous particle, decomposed biogas residue mass ratio be 1:3-4.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that step(5)In Fertilizer inner core, biogas slurry chelating liquid, the mass ratio of mixed solution of Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution be 1:0.3- 0.4:0.2-0.3.
The nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that step(5)'s The mass ratio of Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution is 1 in mixed solution:1.
By above-mentioned technical solution, the beneficial effects of the invention are as follows:
The present invention prepares porous particle with flyash and bentonite material, then is mixed with fertilizer inner core with decomposed biogas residue, not only Solve the problems, such as fine coal ash fouling, and the ability that soil reserves moisture can be increased with fluffy soil;It is rich at the same time in biogas residue Humus, can not only provide nutrient needed for plant growth, improve soil, can also improve crop quality, improve crop yield, promote Into high crop yield stable yields, preservation of fertility, while utilization rate of fertilizer can be improved, reduce production cost.The present invention uses vacuum Biogas slurry chelating liquid is sprayed on fertilizer inner core by spraying technology, adds load capacity of the biogas slurry chelating liquid on fertilizer inner core;Together When biogas slurry in contain organic substance, active ingredient, hormonal substance, strengthens the drought-resistant ability of crop, strengthens crop freezing tolerance, The quality of crop can also effectively be improved, improve root system of plant surrounding environment, soil is improved, chronic administration chemical fertilizer can be solved and brought Soil hardening problem.EM bacteria agent is added in fertilizer of the present invention, soil micro-ecosystem system can be improved, mitigate or reduce plant The generation of pest and disease damage.The present invention uses gamma-glutamic acid and gelatin as coated slow release formulation, forms coating layer, efficiently reduces activity Material is influenced by outside environmental elements, controls the rate of release of core.The nutrition of the present invention is micro- comprehensively and rich in humus Bio-feritlizer, not only can promote the health of living organism to grow up strong and sturdy, significantly promote crop yield;And there is fluffy soil Earth, increase soil reserve the ability of moisture.
Embodiment
The nutrition of the present embodiment is comprehensive and is rich in the production method of the microbial manure of humus, it is concretely comprised the following steps:
(1)Flyash and bentonite are mixed, ultramicro grinding is carried out to 160 mesh sieves are crossed, adds water, regulation system water content is 30%, 60min is stirred with the stir speed (S.S.) of 300r/min, to the paste of substantially uniformity, is then squeezed into the sheet of thick 2cm;
(2)By step(1)Obtained flaky material is put into 600 DEG C of high temperature kiln roasting 4h, cools down, and crushes, and crosses 40 mesh sieves, Again using ultrasonic cleaning agent cleaning 20min, filter, drying, obtains porous particle;
(3)Urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate are uniformly mixed, 80 mesh is crushed, obtains mixed-powder;Again Mixed-powder, EM bacteria agent are added in biogas slurry, magnetic agitation 60min, makes it fully dissolve under the conditions of 50 DEG C, regulation system PH to 6, add EDTA and OP-10, continue magnetic agitation 30min, obtain biogas slurry chelating liquid;
(4)Porous particle, decomposed biogas residue are uniformly mixed, is transferred in comminutor and is granulated, obtains fertilizer inner core;By poly- γ-paddy Propylhomoserin is added in stirring container, adds deionized water, stir evenly be configured to 2% Polyurethane-epoxy resin aqueous solution;By gelatin plus Enter into stirring container, add deionized water to submerge gelatin, be placed in 45 DEG C of waters bath with thermostatic control, it is completely molten to mix to gelatin Solution, adds deionized water constant volume, is configured to 4% aqueous gelatin solution;
(5)Fertilizer inner core is added in vacuum deposition apparatus under normal pressure, starts to extract vacuum and causes air, when pressure is reduced to During 0.04MPa, start to spray biogas slurry chelating liquid, mixed organization continuous mixed fertilizer inner core during spraying, to spray uniformly;Spraying After mixing stops, pressure is constantly raised until normal pressure, starts the mixed of mixing spraying Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution Solution is closed, after spraying, starts the hot wind of 50 DEG C of air blower drum, continues to mix 20min, nutrition is obtained comprehensively and is rich in humic The microbial manure of matter.
The step of the present embodiment(1)Middle flyash and bentonitic mass ratio are 1:1.2.
The step of the present embodiment(3)Middle biogas slurry, urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate, EM bacteria agent, The mass ratio of EDTA and OP-10 is 1:0.25:0.2:0.18:0.12:0.1:0.05:0.03:0.01.
The step of the present embodiment(4)In porous particle, decomposed biogas residue mass ratio be 1:4.
The step of the present embodiment(5)In fertilizer inner core, biogas slurry chelating liquid, Polyurethane-epoxy resin aqueous solution and gelatin it is water-soluble The mass ratio of the mixed solution of liquid is 1:0.4:0.2.
The step of the present embodiment(5)Mixed solution in the mass ratio of Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution be 1:1.

Claims (7)

1. a kind of nutrition is comprehensive and is rich in the production method of the microbial manure of humus, it is characterised in that it includes, porous Prepared by the preparation of grain, biogas slurry chelating liquid, fertilizer inner core, airless spraying biogas slurry chela are prepared as raw material using porous particle and decomposed biogas residue Liquid is closed, then using gamma-glutamic acid and gelatin as coated slow release formulation, coating, obtains nutrition comprehensively and be rich in the microorganism fertilizer of humus Material.
2. the nutrition according to claims 1 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, it is concretely comprised the following steps:
(1)Flyash and bentonite are mixed, ultramicro grinding is carried out to 160-180 mesh sieves are crossed, adds water, regulation system water content For 25-30%, 40-60min is stirred with the stir speed (S.S.) of 250-300r/min, to the paste of substantially uniformity, is then squeezed into thickness The sheet of 2cm;
(2)By step(1)Obtained flaky material is put into 550-600 DEG C of high temperature kiln roasting 3-5h, cools down, and crushes, mistake 20-40 mesh sieves, then 15-20min is cleaned using ultrasonic cleaning agent, filter, drying, obtains porous particle;
(3)Urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate are uniformly mixed, 60-80 mesh is crushed, obtains mixed-powder; Mixed-powder, EM bacteria agent are added in biogas slurry again, magnetic agitation 60min, makes it fully dissolve under the conditions of 50 DEG C, adjusts body The pH of system to 6, adds EDTA and OP-10, continues magnetic agitation 30min, obtains biogas slurry chelating liquid;
(4)Porous particle, decomposed biogas residue are uniformly mixed, is transferred in comminutor and is granulated, obtains fertilizer inner core;By poly- γ-paddy Propylhomoserin is added in stirring container, adds deionized water, stirs evenly the Polyurethane-epoxy resin aqueous solution for being configured to 2-4%;By gelatin It is added in stirring container, adds deionized water to submerge gelatin, is placed in 40-45 DEG C of water bath with thermostatic control, it is complete to mix to gelatin Fully dissolved, adds deionized water constant volume, is configured to the aqueous gelatin solution of 2-4%;
(5)Fertilizer inner core is added in vacuum deposition apparatus under normal pressure, starts to extract vacuum and causes air, when pressure is reduced to During 0.02-0.04MPa, start to spray biogas slurry chelating liquid, mixed organization continuous mixed fertilizer inner core during spraying, to spray It is even;After spraying mixing stops, pressure is constantly raised until normal pressure, starts mixing spraying Polyurethane-epoxy resin aqueous solution and gelatin water The mixed solution of solution, after spraying, starts the hot wind that air blower rouses 40-50 DEG C, continues to mix 15-20min, obtain nutrition Microbial manure comprehensive and rich in humus.
3. the nutrition according to claims 2 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, step(1)Middle flyash and bentonitic mass ratio are 1:1.2-1.5.
4. the nutrition according to claims 2 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, step(3)Middle biogas slurry, urea, calcium superphosphate, Diammonium phosphate (DAP), magnesium sulfate, zinc sulfate, EM bacteria agent, EDTA and OP-10 Mass ratio is 1:0.22-0.25:0.18-0.2:0.15-0.18:0.1-0.12:0.1-0.12:0.04-0.05:0.02-0.03: 0.01-0.012。
5. the nutrition according to claims 2 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, step(4)In porous particle, decomposed biogas residue mass ratio be 1:3-4.
6. the nutrition according to claims 2 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, step(5)In fertilizer inner core, biogas slurry chelating liquid, the mixed solution of Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution Mass ratio is 1:0.3-0.4:0.2-0.3.
7. the nutrition according to claims 2 is comprehensive and is rich in the production method of the microbial manure of humus, its feature It is, step(5)Mixed solution in the mass ratio of Polyurethane-epoxy resin aqueous solution and aqueous gelatin solution be 1:1.
CN201711166396.7A 2017-11-21 2017-11-21 Production method of microbial fertilizer with comprehensive nutrition and rich humus Active CN107935682B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108586087A (en) * 2018-07-17 2018-09-28 王亚 A kind of long-acting slow-release Liquid organic fertilizer and preparation method thereof
CN114538992A (en) * 2022-04-11 2022-05-27 重庆农笑农业发展有限公司 Efficient water-soluble microbial compound fertilizer

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CN104557282A (en) * 2014-12-24 2015-04-29 福建佳玛驰生态科技有限公司 Special inorganic fertilizer for peanut and preparation method thereof
CN106431773A (en) * 2016-12-05 2017-02-22 黄璜 Preparation method of ficus carica fertilizer for early growth stage
CN107082726A (en) * 2017-05-11 2017-08-22 河南龙之锦农业发展有限公司 A kind of preparation method of flue-cured tobacco fertilizer special for organic using wormcast as matrix
CN107129349A (en) * 2017-04-19 2017-09-05 明光市农源农作物专业合作社 One kind load carbon-based magnetic biological fertilizer of ferroso-ferric oxide biomass and preparation method thereof
CN107285889A (en) * 2017-07-27 2017-10-24 望江县农旺农业专业合作社 A kind of preparation method of paddy rice-dedicated fertilizer
CN107324892A (en) * 2017-07-26 2017-11-07 望江县乡缘农业有限责任公司 A kind of Rice Cropping sterilization sustained release compoiste fertilizer
CN107353144A (en) * 2017-06-27 2017-11-17 安徽省瑞森生物科技有限责任公司 It is a kind of can desinsection compound Acetamiprid marine alga base charing granulated fertilizer preparation method

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104557282A (en) * 2014-12-24 2015-04-29 福建佳玛驰生态科技有限公司 Special inorganic fertilizer for peanut and preparation method thereof
CN106431773A (en) * 2016-12-05 2017-02-22 黄璜 Preparation method of ficus carica fertilizer for early growth stage
CN107129349A (en) * 2017-04-19 2017-09-05 明光市农源农作物专业合作社 One kind load carbon-based magnetic biological fertilizer of ferroso-ferric oxide biomass and preparation method thereof
CN107082726A (en) * 2017-05-11 2017-08-22 河南龙之锦农业发展有限公司 A kind of preparation method of flue-cured tobacco fertilizer special for organic using wormcast as matrix
CN107353144A (en) * 2017-06-27 2017-11-17 安徽省瑞森生物科技有限责任公司 It is a kind of can desinsection compound Acetamiprid marine alga base charing granulated fertilizer preparation method
CN107324892A (en) * 2017-07-26 2017-11-07 望江县乡缘农业有限责任公司 A kind of Rice Cropping sterilization sustained release compoiste fertilizer
CN107285889A (en) * 2017-07-27 2017-10-24 望江县农旺农业专业合作社 A kind of preparation method of paddy rice-dedicated fertilizer

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108586087A (en) * 2018-07-17 2018-09-28 王亚 A kind of long-acting slow-release Liquid organic fertilizer and preparation method thereof
CN114538992A (en) * 2022-04-11 2022-05-27 重庆农笑农业发展有限公司 Efficient water-soluble microbial compound fertilizer

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