CN107929212A - hair conditioner containing pearl - Google Patents
hair conditioner containing pearl Download PDFInfo
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- CN107929212A CN107929212A CN201711440888.0A CN201711440888A CN107929212A CN 107929212 A CN107929212 A CN 107929212A CN 201711440888 A CN201711440888 A CN 201711440888A CN 107929212 A CN107929212 A CN 107929212A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Life Sciences & Earth Sciences (AREA)
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Abstract
The invention discloses the hair conditioner containing pearl, it is prepared from the following raw materials in parts by weight：Pearl extracting solution 6.0 8.0%, 16 18 alcohol 3.5 4.0%, hexadecyltrimethylammonium chloride 2.5 3.5%, white oil 1.0 2.0%, EDTA 0.1 0.2%, silicone emulsion 1.5 2.0%, dimethicone 0.5 1.0%, softener 0.3 0.5%, jojoba oil 0.3 0.5%, methyl hydroxybenzoate 0.1 0.2%, citric acid 0.5 1.0%, essence 0.1 0.2%, deionized water, surplus.
Description
Technical field
The present invention relates to chemical product technical field, and in particular to the hair conditioner containing pearl.
Background technology
Hair conditioner can form one layer of smooth protective film on hair, effectively prevent moisture scatter and disappear, make healthy hair it is submissive, grow
It is profit, glossy and easily comb.Method exclusively with hair conditioner has been the trend in the whole world, and developed country probably has 80%
Long term consumer uses all kinds of hair conditioner, and in China, this numeral is also rising year by year.
The biological composite that hair is made of cortex, in addition to protein structure, grease and moisture are also to protect hair
Flexible base substance is held, if the grease on hair is removed, hair fragility rapid wear is will result in, dries out and may result in
Hair shaft fracture.Cationic surfactant hexadecyltrimethylammonium chloride can pass through the cation positive charge and hair of itself
Surface negative charge neutralizes, and reduces the repulsive force between cuticula scale.Cationic surfactant provide it is this it is unique in
And function, the electrostatic of hair is reduced, hair is increased soft feeling, it is elegant, and improve the cardability of hair.
Pearl is rare Chinese medicine, and pearl is the outer embrane of female shellfish and the nacre secreted by the epidermal cell of pearl sac
And formed.Pearl has higher medical value, and pearl has bimillennial history as important medicinal material in China.I
State using pearl cosmetic health care be also it is with a long history, the period of Three Kingdoms《Mingyi Bielu》In pearl has just been classified as important medicine
Material, Li Shizhen (1518-1593 A.D.)《Compendium of Materia Medica》, contain " pearl apply face, make us moist good color.Brothers are applied, skin hangnail is removed, face can be changed and gone
It is dim, make the gloss pure white ".
Why pearl has such significant beauty treatment health care efficacy, is that the inclusion enriched by it determines.It is precious according to analysis
The main component of pearl is calcium carbonate, protein, moisture and various trace elements, including iron, aluminium, magnesium, zinc, selenium, copper, manganese, germanium, potassium
With strontium etc., additionally containing porphyrins (PEG) and light base Europe phosphorus amino acid.Calcium therein enters people's physical efficiency and promotes phosphoric acid
The vigor of adenosinase simultaneously has adjusting blood alkaline functional.Glycine, alanine and L-aminobutanedioic acid content highest therein, these ammonia
Base acid is all the class of amino acid that human body cannot synthesize, it is required, especially glycine to maintaining human body nitrogen balance, it
It is the important component of glutathione in human body, and glutathione is proved that cylinder super-oxidation lipid can be removed and is used as important fortune
Defeated instrument assists amino acid disengaging cell.Magnesium, manganese in trace element are needed for some energy conversions of human body and its growth and development
The important activator of enzyme：Zinc is then the confactor of some enzymes, related with growth in humans and intellectual development；Iron is synthesis ferroheme
Essential component.
The yield of present fresh water pearl is growing, and for pearl always for medicinal, conventional use is always to grind pearl
It is used to taking orally or acting on cosmetics into the powder less than 2 μm, which contains a large amount of calcium carbonate not soluble in water, is unfavorable for
Human body absorbs, so the research for soluble pearl powder increasingly causes the interest of people.In existing research, in succession
Water soluble full component pearl powder is investigated, substantially increases the absorptivity of human body, widely to develop the new application of pearl,
The critical pressure of water and critical-temperature are respectively 22.1MPa and 374 DEG C, in f>374 DEG C, p>Under the conditions of 22.1MPa,
The dielectric constant of water is 5-15.It is known as in the water of low temperature pressure into the liquid condition more slightly lower with 22.1MPa than 374.2 DEG C
" subcritical water ".Heat water to more than boiling point, below critical point, and control system pressure makes water remain liquid, this shape
The water of state is referred to as subcritical water, and it is referred to as superheated water and high-temperature water also to have it in the literature.Under usual conditions, water is polar compounds
Thing.Under 505kPa pressure, raise (50-300 DEG C) with temperature, its dielectric constant is decreased to 1 by 70, that is to say, that its property by
It is highly polar to fade to nonpolar, solute can be extracted from high to low by polarity.Under conditions of temperature and pressure is all higher,
The polarity of water reduces, can be with extracting apolar compound；Under conditions of temperature and pressure is all relatively low, the polarity of water improves, can be with
Extract polar compound.During actual extraction, since the influence that influences be not so good as temperature of the pressure to dielectric constant is big, so
Mainly the dielectric constant of water is controlled by adjusting temperature.Due to be without using acid, alkali and catalyst water under high thermal high
Treatment technology, therefore the extracting method of subcritical water is referred to as " green facture ".In addition, extraction can be in the several seconds
Completed in several minutes of short time, so have the advantages that continuous processing can be carried out.Subcritical Water Extraction technology is natural
There is very much prospect in the extraction of the active ingredient in product field.
The content of the invention
The object of the present invention is to provide the hair conditioner containing pearl, is a kind of not only moisturizing but also the New-style Hair Conditioner of anti-dandruff.
The present invention is achieved through the following technical solutions.
Hair conditioner containing pearl, is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl, pure water is added, is handled with high-speed shearing emulsion machine, then with high pressure microjet
Ultra-Micro Grinding Equipment is handled in 25 DEG C, obtains paste serous material；
2) decompose calcareous：The material that upper step is obtained adds hydrochloric acid, and stirring, untill no longer precipitation is produced, is filtered
To precipitation, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds sodium carboxymethylcellulose, will be de-
In oxygen deionized water injection kettle, extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extracted
Terminate, pressure release, extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Pre-treatment described in step 1) of the present invention, preferably by crushing pearl, according to 1:1 weight ratio adds pure water, uses
High-speed shearing emulsion machine handles 10-20min, rotating speed 8000-12000r/min, then with high pressure microjet Ultra-Micro Grinding Equipment
Handled in 25 DEG C, processing pressure 80-120MPa, number of processes is 2-4 times, obtains paste serous material.
Removal described in step 2) is calcareous, and concentration of hydrochloric acid is not so high, preferably the hydrochloric acid of 6mol/L, if selection 12mol/
The hydrochloric acid (36-38%) of L is directly added into pearl powder, then can produce substantial amounts of foam in the solution, illustrate there is substantial amounts of amino acid
Generation, the rate of recovery for making amino acid is reduced.
Addition sodium carboxymethylcellulose described in step 3), is preferably added to equivalent to pearl raw material 0.010-0.015 weight
The sodium carboxymethylcellulose of part.
Hair conditioner of the present invention containing pearl, prepares with reference to the prior art, and A preferably is added thermal agitation to 80
DEG C, until component is completely dissolved；B phases are added sequentially in deionized water, heating stirring is to 80 DEG C, until component is completely molten
Solution；A is added in B phases and emulsifies 20-30min, stirring is cooled to 50 DEG C, adds C phases, continues to be stirred into cream, after filling,
As finished product.
Compared with prior art, advantages of the present invention：
1st, in the prior art, pearl raw material is usually to use pearl powder as raw material, but manually produces medicinal treasure at present
Pearl powder, expensive, pharmacy's sale price, every gram of 2.27 yuan of price, production cycle length, and manpower spend more；Also have using shell
Nacre, extracts nacreous layer powder, cheap, every gram of three points of or so, still, either pearl powder or nacreous layer powder, and directly
Use is connect, the assimilation effect of human body is simultaneously bad.Existing hair conditioner, generally with hexadecyltrimethylammonium chloride and 16-18 alcohol
Coordinate, as moisturizer, but moisture preserving time persistence or not so good, and present invention adds special pearl extracting solution,
Coordinate hexadecyltrimethylammonium chloride and 16-18 alcohol, while moisturizing, can more improve the smooth and flexibility of hair.
2nd, in the prior art, pearl extracting solution (hydrolyzate) is usually used：Crushing-decomposition is calcareous-and hydrolysis-deacidification-goes
Except dissolubility Ca2+- technique that resin removes anions and canons-concentration is crossed, existing technique, step is various, pearl extracting solution (water
Solve liquid) yield it is low, and time-consuming, such as generally uses 112 DEG C of more than back hydrolysis 24h of normal pressure during hydrolysis.And the present invention
Method, combines Subcritical Water Extraction, and technique is simple, the time is short.
3rd, for the present invention when carrying out Subcritical Water Extraction, it is to close that a certain amount of sodium carboxymethylcellulose is added in material
Key, can be to Ca in solution2+Parcel is formed, prevents it from producing precipitation, blocks extraction equipment pipeline.
Embodiment
With embodiment, the invention will be further described below, but the invention is not limited in these embodiments.
Embodiment 1：
Hair conditioner containing pearl, is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl, according to 1:1 weight ratio adds pure water, is handled with high-speed shearing emulsion machine
10min, rotating speed 8000r/min, are then handled, processing pressure is with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C
80MPa, number of processes are 2 times, obtain paste serous material；
2) decompose calcareous：The material that upper step is obtained adds 12mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.010 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Embodiment 2：
Hair conditioner containing pearl, is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl, according to 1:1 weight ratio adds pure water, is handled with high-speed shearing emulsion machine
20min, rotating speed 12000r/min, are then handled, processing pressure is with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C
120MPa, number of processes are 4 times, obtain paste serous material；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.015 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Embodiment 3：
Hair conditioner containing pearl, is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl, according to 1:1 weight ratio adds pure water, is handled with high-speed shearing emulsion machine
15min, rotating speed 10000r/min, are then handled, processing pressure is with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C
100MPa, number of processes are 3 times, obtain paste serous material；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.010 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Comparative example 1：
Formula is prepared with embodiment 3, pearl extracting solution using following methods：
1) pre-treatment：By crushing pearl, according to 1:1 weight ratio adds pure water, is handled with high-speed shearing emulsion machine
15min, rotating speed 10000r/min, are then handled, processing pressure is with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C
100MPa, number of processes are 3 times, obtain paste serous material；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The filtrate that upper step obtains is placed in extraction kettle, deionized deoxygenated water is injected in kettle,
Extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extraction terminates, pressure release, extract flow
Enter in collecting tank and be cooled to room temperature, obtain extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains.
Comparative example 2：
Formula is used with embodiment 3, pearl extracting solution：
Pre-treatment-addition hydrochloric acid decomposes calcareous-suction filtration-precipitation and adds hydrochloric acid, and 112 DEG C of back hydrolysis 24h- heating of normal pressure are gone
Deacidification-mistake resin anion (R.A.) removes Cl-, filtrate freezing and crystallizing remove CaCl2- cross resin and remove anions and canons-is concentrated to give.
Comparative example 3：
Formula is replaced with embodiment 3, pearl extracting solution with pearl powder.
Experimental example：
1st, moisturizing rate：It will be placed in the sample after constant weight in the silica gel drier that RH is 81%, 3,5,7 and of standing time
24h, weighs the quality of sample after placing respectively.Every group of experiment sets 3 repetitions.
Calculation formula：
Moisturizing rate (Rr)=Hn/H0× 100%
H0To add amount of moisture, HnFor amount of moisture after placement.
The embodiment obtained using the method for the present invention is substantially better than comparative example.
2nd, counter-bending rigidity test
Every sample is fixed on the positioning device, sends out the other end horizontal stretching of fiber, and horizontal displacement claims bending length L,
During test, platform is moved downward with speed O.0lmm/s, passes through the measurement shown in microbalance in counter-bending rigidity testing instrument
The numerical value of power, since balance clasp joint triggers fiber and is allowed to bend, the ratio between power/displacement is expressed as F/D.Wherein F is curved power
For amount (in units of mg), D is curved distance (in units of mm).
Bending resistance stiffness R=FL3/3D(mg·mm2)
During the hair conditioner processing hair that comparative example obtains, the bending resistance stiffness of hair is larger, and hair bending resistance stiffness is relatively low
When illustrate that hair is easier to bend, that is, our usually said more soft hairs, embodiment 3 can improve the soft of hair
It is soft, and it is substantially better than comparative example.
Claims (4)
1. the hair conditioner containing pearl, it is characterised in that be prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl, pure water is added, is handled with high-speed shearing emulsion machine, then with high pressure microjet ultra micro
Disintegrating apparatus is handled in 25 DEG C, obtains paste serous material；
2) decompose calcareous：The material that upper step is obtained adds hydrochloric acid, and stirring, untill no longer precipitation is produced, it is heavy to be obtained by filtration
Form sediment, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, sodium carboxymethylcellulose is added, deoxidation is gone
In ionized water injection kettle, extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extraction knot
Beam, pressure release, extract are flowed into collecting tank and are cooled to room temperature, and obtain extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
2. the hair conditioner according to claim 1 containing pearl, it is characterised in that：Pre-treatment described in step 1), be by
Crushing pearl, according to 1:1 weight ratio adds pure water, and 10-20min, rotating speed 8000- are handled with high-speed shearing emulsion machine
12000r/min, is then handled, processing pressure 80-120MPa with high pressure microjet Ultra-Micro Grinding Equipment in 25 DEG C, place
It is 2-4 times to manage number, obtains paste serous material.
3. the hair conditioner according to claim 1 containing pearl, it is characterised in that：Decomposition described in step 2) is calcareous, salt
Acid concentration is 6mol/L.
4. the hair conditioner according to claim 1 containing pearl, it is characterised in that：Addition carboxymethyl described in step 3) is fine
The plain sodium of dimension, adds the sodium carboxymethylcellulose equivalent to pearl raw material 0.010-0.015 parts by weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711440888.0A CN107929212A (en) | 2017-12-27 | 2017-12-27 | hair conditioner containing pearl |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711440888.0A CN107929212A (en) | 2017-12-27 | 2017-12-27 | hair conditioner containing pearl |
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| Publication Number | Publication Date |
|---|---|
| CN107929212A true CN107929212A (en) | 2018-04-20 |
Family
ID=61940455
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711440888.0A Pending CN107929212A (en) | 2017-12-27 | 2017-12-27 | hair conditioner containing pearl |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050137A (en) * | 1988-10-25 | 1991-03-27 | 江西省农业科普服务部 | Produce the method for Margarita liquid by the nacre powder |
| CN1131016A (en) * | 1995-12-20 | 1996-09-18 | 复旦大学 | Technique for hydrolization of pearl by physical method |
| CN102113991A (en) * | 2011-01-13 | 2011-07-06 | 浙江长生鸟珍珠生物科技有限公司 | Toning lotion containing pearl water extract and preparation method |
| KR20170025121A (en) * | 2015-08-27 | 2017-03-08 | 주식회사 카나 | Method of manufacturing a mask pack cosmetic composition |
| CN106963696A (en) * | 2017-05-18 | 2017-07-21 | 黄裕才 | A kind of hair conditioner |
| CN107362074A (en) * | 2017-09-14 | 2017-11-21 | 王雷 | A kind of preparation method of algae hair conditioner |
-
2017
- 2017-12-27 CN CN201711440888.0A patent/CN107929212A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1050137A (en) * | 1988-10-25 | 1991-03-27 | 江西省农业科普服务部 | Produce the method for Margarita liquid by the nacre powder |
| CN1131016A (en) * | 1995-12-20 | 1996-09-18 | 复旦大学 | Technique for hydrolization of pearl by physical method |
| CN102113991A (en) * | 2011-01-13 | 2011-07-06 | 浙江长生鸟珍珠生物科技有限公司 | Toning lotion containing pearl water extract and preparation method |
| KR20170025121A (en) * | 2015-08-27 | 2017-03-08 | 주식회사 카나 | Method of manufacturing a mask pack cosmetic composition |
| CN106963696A (en) * | 2017-05-18 | 2017-07-21 | 黄裕才 | A kind of hair conditioner |
| CN107362074A (en) * | 2017-09-14 | 2017-11-21 | 王雷 | A kind of preparation method of algae hair conditioner |
Non-Patent Citations (1)
| Title |
|---|
| 潘炳炎: "《珍珠加工技术》", 30 September 1988, 农业出版社 * |
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