CN107929213A - It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation - Google Patents
It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation Download PDFInfo
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- CN107929213A CN107929213A CN201711440936.6A CN201711440936A CN107929213A CN 107929213 A CN107929213 A CN 107929213A CN 201711440936 A CN201711440936 A CN 201711440936A CN 107929213 A CN107929213 A CN 107929213A
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- hair
- pearl
- extraction
- reparation
- dyed
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
Abstract
It is used for the invention discloses a kind of after having hair dyed to the pearl hair conditioner of hair reparation, is prepared from the following raw materials in parts by weight：Pearl extracting solution 6.0 8.0%, salicylic acid 0.4 0.5%, thymol 0.05 0.10%, hexadecyltrimethylammonium chloride 2.0 3.0%, glycerine 2.0 3.0%, sodium chloride 2.0 3.0%, guar gum 1.0 1.5%, silicone emulsion 1.5 2.0%, dimethicone 0.5 1.0%, jojoba oil 0.3 0.5%, methyl hydroxybenzoate 0.1 0.2%, citric acid 0.5 1.0%, essence 0.1 0.2%, deionized water, surplus.
Description
Technical field
The present invention relates to chemical product technical field, and in particular to a kind of to be used to take care of hair to the pearl of hair reparation after having hair dyed
Element.
Background technology
As the improvement of people's living standards, the number and frequency of hair dyeing are increasing sharply.The main component of hair is
Protein, compared with other protein, the Nature comparison torpescence of hair protein matter.But hair is to boiling water, acid, alkali, oxidant
It is more sensitive with reducing agent.Some Oxidizing and Reducing Agents are used during hair dyeing.They are all some acid or alkali
The chemicals of property.Hair is also possible to contact vapor for a long time in the process.Therefore, during hair dyeing, it is above-mentioned because
Element can all damage hair.
Hair conditioner can form one layer of smooth protective film on hair, effectively prevent moisture scatter and disappear, make healthy hair it is submissive, grow
It is profit, glossy and easily comb.Method exclusively with hair conditioner has been the trend in the whole world, and developed country probably has 80%
Long term consumer uses all kinds of hair conditioner, and in China, this numeral is also rising year by year.
Pearl is rare Chinese medicine, and pearl is the outer embrane of female shellfish and the nacre secreted by the epidermal cell of pearl sac
And formed.Pearl has higher medical value, and pearl has bimillennial history as important medicinal material in China.I
State using pearl cosmetic health care be also it is with a long history, the period of Three Kingdoms《Mingyi Bielu》In pearl has just been classified as important medicine
Material, Li Shizhen (1518-1593 A.D.)《Compendium of Materia Medica》, contain " pearl apply face, make us moist good color.Brothers are applied, skin hangnail is removed, face can be changed and gone
It is dim, make the gloss pure white ".
Why pearl has such significant beauty treatment health care efficacy, is that the inclusion enriched by it determines.It is precious according to analysis
The main component of pearl is calcium carbonate, protein, moisture and various trace elements, including iron, aluminium, magnesium, zinc, selenium, copper, manganese, germanium, potassium
With strontium etc., additionally containing porphyrins (PEG) and light base Europe phosphorus amino acid.Calcium therein enters people's physical efficiency and promotes phosphoric acid
The vigor of adenosinase simultaneously has adjusting blood alkaline functional.Glycine, alanine and L-aminobutanedioic acid content highest therein, these ammonia
Base acid is all the class of amino acid that human body cannot synthesize, it is required, especially glycine to maintaining human body nitrogen balance, it
It is the important component of glutathione in human body, and glutathione is proved that cylinder super-oxidation lipid can be removed and is used as important fortune
Defeated instrument assists amino acid disengaging cell.Magnesium, manganese in trace element are needed for some energy conversions of human body and its growth and development
The important activator of enzyme：Zinc is then the confactor of some enzymes, related with growth in humans and intellectual development；Iron is synthesis ferroheme
Essential component.
The yield of present fresh water pearl is growing, and for pearl always for medicinal, conventional use is always to grind pearl
It is used to taking orally or acting on cosmetics into the powder less than 2 μm, which contains a large amount of calcium carbonate not soluble in water, is unfavorable for
Human body absorbs, so the research for soluble pearl powder increasingly causes the interest of people.In existing research, in succession
Water soluble full component pearl powder is investigated, substantially increases the absorptivity of human body, widely to develop the new application of pearl,
The critical pressure of water and critical-temperature are respectively 22.1MPa and 374 DEG C, in f>374 DEG C, p>Under the conditions of 22.1MPa,
The dielectric constant of water is 5-15.It is known as in the water of low temperature pressure into the liquid condition more slightly lower with 22.1MPa than 374.2 DEG C
" subcritical water ".Heat water to more than boiling point, below critical point, and control system pressure makes water remain liquid, this shape
The water of state is referred to as subcritical water, and it is referred to as superheated water and high-temperature water also to have it in the literature.Under usual conditions, water is polar compounds
Thing.Under 505kPa pressure, raise (50-300 DEG C) with temperature, its dielectric constant is decreased to 1 by 70, that is to say, that its property by
It is highly polar to fade to nonpolar, solute can be extracted from high to low by polarity.Under conditions of temperature and pressure is all higher,
The polarity of water reduces, can be with extracting apolar compound；Under conditions of temperature and pressure is all relatively low, the polarity of water improves, can be with
Extract polar compound.During actual extraction, since the influence that influences be not so good as temperature of the pressure to dielectric constant is big, so
Mainly the dielectric constant of water is controlled by adjusting temperature.Due to be without using acid, alkali and catalyst water under high thermal high
Treatment technology, therefore the extracting method of subcritical water is referred to as " green facture ".In addition, extraction can be in the several seconds
Completed in several minutes of short time, so have the advantages that continuous processing can be carried out.Subcritical Water Extraction technology is natural
There is very much prospect in the extraction of the active ingredient in product field.
The content of the invention
It is used for the object of the present invention is to provide a kind of after having hair dyed to the pearl hair conditioner of hair reparation.
The present invention is achieved through the following technical solutions.
It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation, it is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl；
2) decompose calcareous：The material that upper step is obtained adds hydrochloric acid, and stirring, untill no longer precipitation is produced, is filtered
To precipitation, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds sodium carboxymethylcellulose, will be de-
In oxygen deionized water injection kettle, extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extracted
Terminate, pressure release, extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Crushing described in step 1) of the present invention, is preferably crushed to granularity and is less than 3mm.
Removal described in step 2) is calcareous, and concentration of hydrochloric acid is not so high, preferably the hydrochloric acid of 6mol/L, if selection 12mol/
The hydrochloric acid (36-38%) of L is directly added into pearl powder, then can produce substantial amounts of foam in the solution, illustrate there is substantial amounts of amino acid
Generation, the rate of recovery for making amino acid is reduced.
Addition sodium carboxymethylcellulose described in step 3), is preferably added to equivalent to pearl raw material 0.010-0.015 weight
The sodium carboxymethylcellulose of part.
It is of the present invention a kind of for, to the pearl hair conditioner of hair reparation, being prepared after having hair dyed with reference to the prior art, it is excellent
A is added thermal agitation to 80 DEG C by choosing, until component is completely dissolved；B phases are added sequentially in deionized water, heating stirring to 80
DEG C, until component is completely dissolved；A is added in B phases and emulsifies 20-30min, stirring is cooled to 50 DEG C, adds C phases, continues
Cream is stirred into, is finished product after filling.
Compared with prior art, advantages of the present invention：
1st, in the prior art, pearl raw material is usually to use pearl powder as raw material, but manually produces medicinal treasure at present
Pearl powder, expensive, pharmacy's sale price, every gram of 2.27 yuan of price, production cycle length, and manpower spend more；Also have using shell
Nacre, extracts nacreous layer powder, cheap, every gram of three points of or so, still, either pearl powder or nacreous layer powder, and directly
Use is connect, the assimilation effect of human body is simultaneously bad.Existing hair conditioner, much uses glycerine to add as moisturizing, the usage amount of glycerine
It is bigger, 10-20% or so, as moisturizer, but moisture preserving time persistence or not so good, and present invention adds special
Pearl extracting solution, coordinate a small amount of glycerine, while moisturizing, can more improve the smooth and flexibility of hair.
2nd, in the prior art, pearl extracting solution (hydrolyzate) is usually used：Crushing-decomposition is calcareous-and hydrolysis-deacidification-goes
Except dissolubility Ca2+- technique that resin removes anions and canons-concentration is crossed, existing technique, step is various, pearl extracting solution (water
Solve liquid) yield it is low, and time-consuming, such as generally uses 112 DEG C of more than back hydrolysis 24h of normal pressure during hydrolysis.And the present invention
Method, combines Subcritical Water Extraction, and technique is simple, the time is short.
3rd, for the present invention when carrying out Subcritical Water Extraction, it is to close that a certain amount of sodium carboxymethylcellulose is added in material
Key, can be to Ca in solution2+Parcel is formed, prevents it from producing precipitation, blocks extraction equipment pipeline.
Embodiment
With embodiment, the invention will be further described below, but the invention is not limited in these embodiments.
Embodiment 1：
It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation, it is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：Crushing pearl to granularity is less than 3mm；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.010 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Embodiment 2：
It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation, it is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：Crushing pearl to granularity is less than 3mm；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.015 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Embodiment 3：
It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation, it is prepared from the following raw materials in parts by weight：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：Crushing pearl to granularity is less than 3mm；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, adds the carboxymethyl of 0.010 parts by weight
Sodium cellulosate, deionized deoxygenated water is injected in kettle, is extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, during extraction
Between 5-10min, extraction terminates, pressure release, and extract is flowed into collecting tank and is cooled to room temperature, and obtains extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
Comparative example 1：
Formula is prepared with embodiment 3, pearl extracting solution using following methods：
1) pre-treatment：Crushing pearl to granularity is less than 3mm；
2) decompose calcareous：The material that upper step is obtained adds 6mol/L hydrochloric acid, stirs, untill no longer precipitation is produced,
Precipitation is obtained by filtration, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The filtrate that upper step obtains is placed in extraction kettle, deionized deoxygenated water is injected in kettle,
Extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extraction terminates, pressure release, extract flow
Enter in collecting tank and be cooled to room temperature, obtain extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains.
Comparative example 2：
Formula is used with embodiment 3, pearl extracting solution：
Crushing-addition hydrochloric acid decomposes calcareous-suction filtration-precipitation and adds hydrochloric acid, and 112 DEG C of back hydrolysis 24h- heating of normal pressure remove
Acid-cross resin anion (R.A.) removal Cl-, filtrate freezing and crystallizing remove CaCl2- cross resin and remove anions and canons-is concentrated to give.
Comparative example 3：
Formula is replaced with embodiment 3, pearl extracting solution with pearl powder.
Experimental example：
1st, moisturizing rate：It will be placed in the sample after constant weight in the silica gel drier that RH is 81%, 3,5,7 and of standing time
24h, weighs the quality of sample after placing respectively.Every group of experiment sets 3 repetitions.
Calculation formula：
Moisturizing rate (Rr)=Hn/H0× 100%
H0To add amount of moisture, HnFor amount of moisture after placement.
The embodiment obtained using the method for the present invention is substantially better than comparative example.
2nd, shampoo and hair conditioner handle the influence to being damaged hair cuticle in 3 months.
2.1 material
2.1.1 research object and packet share 50 dye originator voluntary participation this researchs, are divided into shampoo group and hair care
Plain group, every group of 10 people.All participants are sampled in laggard wardrobe hair of having hair dyed, then receives hair conditioner and handles 1 time, there are 10
The alone shampoo (shampoo group) in 3 months afterwards, another 10X4 is continuing with shampoo+hair conditioner (hair conditioner
Group).All participants are women, age 25-50 Sui.Every participant did not received hair dyeing in nearest 1 year, and through skin
Section doctor, which checks, to be confirmed without hair follicle disease.
2.1.2 instrument JSM-6300 scanning electron microscope (JEOL, Japan).
2.2 method
2.2.1 sample collection provides the hair washing of same brand, embodiment 3, comparative example for every participant.Hair takes
Before sample is set in hair dyeing respectively.After hair dyeing at once, 1,2,3 month after used hair washing product.When collecting hair swatch, choose whole
Hair, is collected in dedicated polybag and indicates name, age, materials time and hair dyeing or hair dyeing mode by everyone 2.
2.2.2 after sample preparation cleans the sample gathered with distilled water, the hair shaft of 1cm long is taken at bullet root 5cm,
It is fixed on after to be dried with double faced adhesive tape on objective table, coating conductive paste.Scanning electron microscopic observation is carried out after metal spraying.
2.2.3 hair cuticle scoring samples this central sections, i.e., at hair near-end 5.5cm, is observed under scanning electron microscope every
The form of a hair cuticle.Normal hair cuticle is parallel to be covered in hair shaft surface in an orderly manner just as fish scale (or imbrication), when it is damaged
When hindering, hair cuticle cannot tightly be covered in hair shaft surface and tilt.Angle, or hair cuticle edge are formed with the major axis of hair shaft
Integrality destroyed.By the discussion of this problem panel of expert, difference is given according to the angle between hair cuticle and hair shaft
Score value：0 point；0 ° -45 ° are 1 point；45 ° -90 ° are 2 points；>90 ° are 3 points.40 hairs in each sample counting same horizontal line
Cuticle, gained total score score for total hair cuticle.Score value is higher, shows that hair cuticle damage is more serious.
2.3 statistical method
All data input computer, and statistical analysis is completed with SPSSl3.0 softwares.As a result with Represent, two groups
Between compare and examined using t.Comparison among groups uses variance analysis.
1 month after the hair dyeing of shampoo group, although only carrying out 1 hair conditioner processing, the damage of hair sample hair cuticle is average
Integration reduces, the no significant difference (P compared with before having hair dyed>0.05).But 2nd month and 3rd month thereafter is maos small
Skin lesion extent is gradually increasing again, and especially at 3rd month, hair cuticle lesion extent difference compared with having hair dyed or hair dyeing is preceding has system
Meter learns meaning (P<0.01).
1 month hair cuticle lesion extent has just returned to the level (P before hair dyeing after the hair dyeing of hair conditioner group>0.05).To the 3rd
A month, hair cuticle lesion extent was compared with before hair dyeing or hair dyeing, no significant difference (P>0.05).To 3 groups of embodiment and
Between comparative example group hair cuticle lesion extent it was found that, 3 groups of hair cuticle lesion extents of embodiment are significantly less than comparative example group (P<
0.01), and this species diversity is gradually increased for 3rd month from l-.
Claims (4)
1. a kind of be used for after having hair dyed to the pearl hair conditioner of hair reparation, it is characterised in that by the raw material system of following weight proportion
Into：
The pearl extracting solution, is prepared by the following preparation method：
1) pre-treatment：By crushing pearl；
2) decompose calcareous：The material that upper step is obtained adds hydrochloric acid, and stirring, untill no longer precipitation is produced, it is heavy to be obtained by filtration
Form sediment, precipitation is washed with aliquots of deionized water；
3) Subcritical Water Extraction：The precipitation that upper step obtains is placed in extraction kettle, sodium carboxymethylcellulose is added, deoxidation is gone
In ionized water injection kettle, extracted, 130-140 DEG C of extraction temperature, pressure 5-8MPa, extraction time 5-10min, extraction knot
Beam, pressure release, extract are flowed into collecting tank and are cooled to room temperature, and obtain extract；
4) Ca is removed2+、Cl-：Extract is successively removed into remaining Ca by anions and canons resin2+、Cl-, obtain filtrate；
5) concentrate：The filtrate that upper step is obtained concentrates, and is concentrated into 10 times of raw material weight, obtains pearl extracting solution.
2. a kind of it is used for according to claim 1 after having hair dyed to the pearl hair conditioner of hair reparation, it is characterised in that：Step
1) crushing described in, is crushed to granularity and is less than 3mm.
3. a kind of it is used for according to claim 1 after having hair dyed to the pearl hair conditioner of hair reparation, it is characterised in that：Step
2) decomposition described in is calcareous, concentration of hydrochloric acid 6mol/L.
4. a kind of it is used for according to claim 1 after having hair dyed to the pearl hair conditioner of hair reparation, it is characterised in that：Step
3) the addition sodium carboxymethylcellulose described in, adds the carboxymethyl cellulose equivalent to pearl raw material 0.010-0.015 parts by weight
Sodium.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711440936.6A CN107929213A (en) | 2017-12-27 | 2017-12-27 | It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711440936.6A CN107929213A (en) | 2017-12-27 | 2017-12-27 | It is a kind of to be used for after having hair dyed to the pearl hair conditioner of hair reparation |
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| CN107929213A true CN107929213A (en) | 2018-04-20 |
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Citations (6)
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|---|---|---|---|---|
| CN1050137A (en) * | 1988-10-25 | 1991-03-27 | 江西省农业科普服务部 | Produce the method for Margarita liquid by the nacre powder |
| CN1131016A (en) * | 1995-12-20 | 1996-09-18 | 复旦大学 | Technique for hydrolization of pearl by physical method |
| CN102113991A (en) * | 2011-01-13 | 2011-07-06 | 浙江长生鸟珍珠生物科技有限公司 | Toning lotion containing pearl water extract and preparation method |
| KR20170025121A (en) * | 2015-08-27 | 2017-03-08 | 주식회사 카나 | Method of manufacturing a mask pack cosmetic composition |
| CN106963696A (en) * | 2017-05-18 | 2017-07-21 | 黄裕才 | A kind of hair conditioner |
| CN107362074A (en) * | 2017-09-14 | 2017-11-21 | 王雷 | A kind of preparation method of algae hair conditioner |
-
2017
- 2017-12-27 CN CN201711440936.6A patent/CN107929213A/en active Pending
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|---|---|---|---|---|
| CN1050137A (en) * | 1988-10-25 | 1991-03-27 | 江西省农业科普服务部 | Produce the method for Margarita liquid by the nacre powder |
| CN1131016A (en) * | 1995-12-20 | 1996-09-18 | 复旦大学 | Technique for hydrolization of pearl by physical method |
| CN102113991A (en) * | 2011-01-13 | 2011-07-06 | 浙江长生鸟珍珠生物科技有限公司 | Toning lotion containing pearl water extract and preparation method |
| KR20170025121A (en) * | 2015-08-27 | 2017-03-08 | 주식회사 카나 | Method of manufacturing a mask pack cosmetic composition |
| CN106963696A (en) * | 2017-05-18 | 2017-07-21 | 黄裕才 | A kind of hair conditioner |
| CN107362074A (en) * | 2017-09-14 | 2017-11-21 | 王雷 | A kind of preparation method of algae hair conditioner |
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| 潘炳炎: "《珍珠加工技术》", 30 September 1988, 农业出版社 * |
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Application publication date: 20180420 |