CN107929108A - A kind of preparation method of high moisturizing moisturizing seaweed mask - Google Patents
A kind of preparation method of high moisturizing moisturizing seaweed mask Download PDFInfo
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- CN107929108A CN107929108A CN201711252047.7A CN201711252047A CN107929108A CN 107929108 A CN107929108 A CN 107929108A CN 201711252047 A CN201711252047 A CN 201711252047A CN 107929108 A CN107929108 A CN 107929108A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/56—Compounds, absorbed onto or entrapped into a solid carrier, e.g. encapsulated perfumes, inclusion compounds, sustained release forms
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a kind of preparation method of high moisturizing moisturizing seaweed mask, using seaweed as nutritional ingredient raw material, the transport agent using graphene oxide as nutritional ingredient, comprises the following steps the facial mask：（1）Produce nutrient solution,（2）Load graphene oxide,（3）Allotment,（4）Infiltration and（5）Packaging sterilizing.The present invention is suitable for sensitiveness skin crowd, does not add any artificial synthesized additive being irritating to the skin；Skin is high to the absorption efficiency of active ingredient, is conducive to moisturizing；The preparation process of facial mask is simple, environmentally protective.
Description
Technical field
The present invention relates to facial mask technical field, more particularly, to a kind of preparation method of high moisturizing moisturizing seaweed mask.
Background technology
In recent years, with the raising of people's living standard, the mankind increasingly focus on maintaining oneself, various health products,
Skin care item emerge in an endless stream.Facial mask is a kind of carrier of face beautifying health keeping product, is a classification in skin care item, and it is also most that its is most basic
Important purpose is to make up makeup removing and the still insufficient cleaning that washes one's face, and coordinates other essential ingredients to realize it on this basis
Its maintenance function, such as replenishing water and preserving moisture, whitening and anti-aging, Sage Extract etc..Seaweed is mainly by protein, polysaccharide, food
The composition of nutritive substances such as fibres, vitamin, amino acid and aliphatic acid.Wherein methionine, cystine are enriched, and can prevent skin
Skin is dried, and dry skin can be made to improve fat secretion rich in gloss, Oily.In conclusion fully natural green of the present invention,
Do not stimulate gently, moistening effect is good.
Up to the present, the relevant report of existing many moisture saver mask in the prior art, such as：
The Chinese patent of Application No. CN201510575120.9 discloses a kind of moisture saver mask and preparation method thereof, the moisturizing
Facial mask includes the raw material of following parts by weight：5-10 parts of Fructus Cucumidis sativi extract, 1-6 parts of Passion flower P.E, flores sambuci extract 2-5
Part, 1-6 parts of Gotu Kola P.E, 10-20 parts of aloe meat extract, 1-5 parts of ginseng extract, 5-10 parts of saualane, pawpaw egg
White 1-2 parts of enzyme, 2-6 parts of olive oil, 1-5 parts of vitamin B6.The moisture saver mask formula of the invention is reasonable, and moistening effect is good, takes effect
Time is short, safe.
The Chinese patent application of Application No. CN201710075675.6 discloses a kind of guarantor containing Radix et Caulis Opuntiae Dillenii extract
Wet facial mask, the moisture saver mask include：（1）Mask substrate；With（2）Facial mask essence, the facial mask essence include：（a）Water
Soluble surfactant, the thickener make viscosity of the facial mask essence with 1mPa s to 5000mPa s；With（b）0.1wt%、
The moisture-keeping composition of 30wt%, the moisture-keeping composition include polyalcohol, Semen Coicis extract, turn round thorn Cactus Pedicel extract；With
（c）Aqueous carrier.The moisture saver mask can promote aquaporin to express, the moisture supply of lifting skin from inside to outside, also
It can promote the synthesis of epidermal protein and cortex, strengthen the barrier function of skin, prevent moisture loss, lift skin hydration and skin
Skin reflecting feel, has synergistic moisture-keeping function.
But facial mask complicated component of the prior art, the change stimulated often is produced to skin containing artificial synthesized possibility
Study point, and abundant facial mask nutritional ingredient is not easy to be absorbed by the body, and has not only caused to waste again so that the moisturizing moisturizing effect of facial mask
Difference, can not meet the needs of people.
The content of the invention
The present invention is to overcome in the prior art, and it is poor that the nutritional ingredient of facial mask is not easy moisturizing moisturizing effect caused by absorbing
The problem of, there is provided a kind of preparation method of high moisturizing moisturizing seaweed mask, using natural seaweed active ingredient, with graphite oxide
Alkene makees carrier, effectively transports nutritional ingredient intracellular, reaches the effect of efficient replenishing water and preserving moisture.
To achieve these goals, the present invention uses following technical scheme：
A kind of preparation method of high moisturizing moisturizing seaweed mask, the facial mask is using seaweed as nutritional ingredient raw material, with graphite oxide
Alkene is the transport agent of nutritional ingredient.In seaweed is mainly protein, fat, vitamin, trace element and carbon aquation
Contain algal polysaccharides in compound etc., wherein seaweed, abundant hydroxyl makes seaweed mask have the characteristics that vicidity and moisture retention, sea
Protein content about 8% in algae, these materials have skin a kind of natural affinity, replenishing water and preserving moisture effect are played to skin.Stone
The specific surface area (up to 2600m2.g-1) of black alkene, is used as pharmaceutical carrier after modifying graphene oxide with polyethylene glycol, has height
Effect carries the effect of medicine, so as to transport the abundant protein in seaweed, protein is not only rested on skin surface, rapidly transports
Egg output white matter enters into the cell, so as to fulfill the purpose of the efficient absorption efficient moisture-retention of skin.
Preferably, a kind of preparation method of high moisturizing moisturizing seaweed mask comprises the following steps：
（1）Produce nutrient solution：Fresh seaweed is ground into rotten shape, its nutritional ingredient is refined with the method for SCF-CO 2, obtains
To nutrient solution；Contain colloid in the nutrient solution completed if extracting, enzymolysis liquid enzymolysis must be added, pass through the side of SCF-CO 2
Method prepares that nutrient solution, which is easily absorbed by the skin, nutrition is most is retained, do not stimulate gently, carry the light Hai Xiang of seaweed
Taste, moistening effect are notable；
（2）Load graphene oxide：Added into graphene oxide in polyethylene glycol and graphene solution is made, by graphene solution
Add in nutrient solution, hydro-thermal method reacts to obtain the nutrient solution of load graphene；Polyethylene glycol is nontoxic, nonirritant, mildly bitter flavor, tool
There are the characteristics such as good water solubility it is applied in cosmetic industry.Polyethylene glycol can be uniformly dispersed oxygen in hydro-thermal method reaction
Graphite alkene, while react with graphene oxide, functionalization graphene is obtained, makes graphene oxide functionalization that there is medicine
Carrier function, then loads to the active ingredient in nutrient solution on functionalization graphene, and whole process passes through one step of hydro-thermal method
Complete, and process is environmentally protective；
（3）Allotment：By step（2）The nutrient solution of middle acquisition is with colloid by weight 10：1-25：1 is deployed into colloidal solution；
（4）Infiltration：By face paper infiltration 15-60 minutes in above-mentioned colloidal solution；
（5）Packaging sterilizing：The facial mask infiltrated is fitted into aseptic package bag and is sealed and with sterilizing under high pressure.Using skill of the present invention
Seaweed mask made of art scheme have it is environmentally protective, gentle, be easy to be absorbed by the skin, component is simple, suitable for sensitiveness flesh
It is skin crowd, cheap and easy to get, there are extensive market prospects.
Preferably, step（1）In, extraction carries out at room temperature.
Preferably, step（2）Described in graphene solution concentration be 2-20mg/L.
It is preferably, rapid（2）In, the weight ratio of graphene solution and nutrient solution is 1-50:100.
Preferably, step（2）In, the hydro-thermal method carries out in reaction kettle, reacts 10-48h at 180-300 DEG C.
Preferably, step（3）In, the colloid is sodium alginate, density 1.0-1.1g/cm3.
Preferably, step（5）In, the operating pressure of the sterilizing is 300-500 atmospheric pressure, sterilization time 30-
40min。
Therefore, the present invention has the advantages that：（1）Suitable for sensitiveness skin crowd, any manually conjunction is not added
Into the additive being irritating to the skin；（2）Skin is high to the absorption efficiency of active ingredient, is conducive to moisturizing；（3）Technique letter
It is single, it is environmentally protective.
Embodiment
The present invention is described in further detail with reference to embodiment.Graphene oxide and poly- in the present invention
Ethylene glycol is medical grade, is commercial products.
Embodiment 1：
A kind of preparation method of high moisturizing moisturizing seaweed mask, comprises the following steps：
（1）Produce nutrient solution：Fresh seaweed is ground into rotten shape, refines its nutrition with the method for SCF-CO 2 at room temperature
Component, obtains nutrient solution；
（2）Load graphene oxide：It is molten that the graphene that concentration is 2mg/L is made in addition polyethylene glycol into graphene oxide
Liquid, graphene solution is added in nutrient solution, and the weight ratio of graphene solution and nutrient solution is 1：100, the hydro-thermal method at 180 DEG C
48h is reacted, obtains the nutrient solution of load graphene；
（3）Allotment：By step（2）The nutrient solution of middle acquisition and the sodium alginate colloid by weight 10 that density is 1.0g/cm3：1
Ratio be deployed into colloidal solution；
（4）Infiltration：By face paper infiltration 15 minutes in above-mentioned colloidal solution；
（5）Packaging sterilizing：The facial mask infiltrated is fitted into aseptic package bag and is sealed and with sterilizing under high pressure, the work pressure of sterilizing
Power is 300 atmospheric pressure, sterilization time 40min.
Embodiment 2：
A kind of preparation method of high moisturizing moisturizing seaweed mask, comprises the following steps：
（1）Produce nutrient solution：Fresh seaweed is ground into rotten shape, refines its nutrition with the method for SCF-CO 2 at room temperature
Component, obtains nutrient solution；
（2）Load graphene oxide：It is molten that the graphene that concentration is 20mg/L is made in addition polyethylene glycol into graphene oxide
Liquid, graphene solution is added in nutrient solution, and the weight ratio of graphene solution and nutrient solution is 1：50, the hydro-thermal method at 300 DEG C
10h is reacted, obtains the nutrient solution of load graphene；
（3）Allotment：By step（2）The nutrient solution of middle acquisition and the sodium alginate colloid by weight 25 that density is 1.1g/cm3：1
Ratio be deployed into colloidal solution；
（4）Infiltration：By face paper infiltration 60 minutes in above-mentioned colloidal solution；
（5）Packaging sterilizing：The facial mask infiltrated is fitted into aseptic package bag and is sealed and with sterilizing under high pressure, the work pressure of sterilizing
Power is 500 atmospheric pressure, sterilization time 30min.
Embodiment 3：
A kind of preparation method of high moisturizing moisturizing seaweed mask, comprises the following steps：
（1）Produce nutrient solution：Fresh seaweed is ground into rotten shape, refines its nutrition with the method for SCF-CO 2 at room temperature
Component, obtains nutrient solution；
（2）Load graphene oxide：It is molten that the graphene that concentration is 10mg/L is made in addition polyethylene glycol into graphene oxide
Liquid, graphene solution is added in nutrient solution, and the weight ratio of graphene solution and nutrient solution is 1：75, the hydro-thermal method at 250 DEG C
25h is reacted, obtains the nutrient solution of load graphene；
（3）Allotment：By step（2）The nutrient solution of middle acquisition and the sodium alginate colloid by weight 20 that density is 1.05g/cm3：
1 ratio is deployed into colloidal solution；
（4）Infiltration：By face paper infiltration 30 minutes in above-mentioned colloidal solution；
（5）Packaging sterilizing：The facial mask infiltrated is fitted into aseptic package bag and is sealed and with sterilizing under high pressure, the work pressure of sterilizing
Power is 400 atmospheric pressure, sterilization time 35min.
Clinical case：
Some volunteers are randomly selected to verify seaweed mask moistening effect that technical solution of the present invention is prepared：
Case 1：Mr. Wang, female, 28 years old, under the conditions of local weather bureau issue Data Air relative humidity is 20%, takes facial mask
After 16 minutes, face continue moisturizing 30 it is small when.
Case 2：So-and-so is applied, female, 20 years old, under the conditions of local weather bureau issue Data Air relative humidity is 32%, takes
After facial mask 15 minutes, face continue moisturizing 18 it is small when.
Case 3：The Qin so-and-so, man, 23 years old, under the conditions of local weather bureau issue Data Air relative humidity is 50%, takes
Facial mask after ten minutes, face continue moisturizing 20 it is small when.
Case 4：Clock so-and-so, female, 30 years old, under the conditions of local weather bureau issue Data Air relative humidity is 46%, takes
Facial mask after twenty minutes, face continue moisturizing 16 it is small when.
Case 5：Zhang, female, 34 years old, under the conditions of local weather bureau issue Data Air relative humidity is 58%, takes
Facial mask after twenty minutes, face continue moisturizing 22 it is small when.
Above volunteer is skin discomfort phenomenon occur.
Claims (8)
1. a kind of preparation method of high moisturizing moisturizing seaweed mask, it is characterized in that, the facial mask using seaweed as nutritional ingredient raw material,
Transport agent using graphene oxide as nutritional ingredient.
2. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 1, it is characterized in that, including following step
Suddenly：
Produce nutrient solution：Fresh seaweed is ground into rotten shape, uses supercritical CO2The method of extraction refines its nutritional ingredient, is sought
Nutrient solution；
Load graphene oxide：Added into graphene oxide in polyethylene glycol and graphene solution be made, by graphene solution plus
Enter in nutrient solution, hydro-thermal method reacts to obtain the nutrient solution of load graphene；
（3）Allotment：By step（2）The nutrient solution of middle acquisition is with colloid by weight 10：1-25：1 is deployed into colloidal solution；
（4）Infiltration：By face paper infiltration 15-60 minutes in above-mentioned colloidal solution；
（5）Packaging sterilizing：The facial mask infiltrated is fitted into aseptic package bag and is sealed and with sterilizing under high pressure.
3. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2, it is characterized in that, step（1）In,
Extraction carries out at room temperature.
4. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2, it is characterized in that, step（2）In
The graphene solution concentration is 2-20mg/L.
5. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2, it is characterized in that, step（2）In,
The weight ratio of graphene solution and nutrient solution is 1-50:100.
6. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2, it is characterized in that, step（2）In,
The hydro-thermal method carries out in reaction kettle, reacts 10-48h at 180-300 DEG C.
7. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2, it is characterized in that, step（3）In,
The colloid is sodium alginate, density 1.0-1.1g/cm3。
8. a kind of preparation method of high moisturizing moisturizing seaweed mask according to claim 2-7 any one, it is characterized in that,
Step（5）In, the operating pressure of the sterilizing is 300-500 atmospheric pressure, sterilization time 30-40min.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711252047.7A CN107929108A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of high moisturizing moisturizing seaweed mask |
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| CN201711252047.7A CN107929108A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of high moisturizing moisturizing seaweed mask |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110327263A (en) * | 2019-08-09 | 2019-10-15 | 汉西(厦门)科技有限公司 | It is a kind of for improving the graphene facial mask and preparation method of dry skin problem of rough |
| CN113599279A (en) * | 2021-09-06 | 2021-11-05 | 天津富勤科技股份有限公司 | Graphene oxide and titanium dioxide composite photocatalyst, cleaning mask and preparation method of cleaning mask |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105686957A (en) * | 2016-03-20 | 2016-06-22 | 吉林大学 | Electro-spinning nanofiber mask with core-shell structure and preparation method thereof |
| CN106821852A (en) * | 2017-02-22 | 2017-06-13 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of facial mask |
-
2017
- 2017-12-01 CN CN201711252047.7A patent/CN107929108A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105287248A (en) * | 2015-11-18 | 2016-02-03 | 张建刚 | Graphene oxide mask and preparation method thereof |
| CN105686957A (en) * | 2016-03-20 | 2016-06-22 | 吉林大学 | Electro-spinning nanofiber mask with core-shell structure and preparation method thereof |
| CN106821852A (en) * | 2017-02-22 | 2017-06-13 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of facial mask |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110327263A (en) * | 2019-08-09 | 2019-10-15 | 汉西(厦门)科技有限公司 | It is a kind of for improving the graphene facial mask and preparation method of dry skin problem of rough |
| CN113599279A (en) * | 2021-09-06 | 2021-11-05 | 天津富勤科技股份有限公司 | Graphene oxide and titanium dioxide composite photocatalyst, cleaning mask and preparation method of cleaning mask |
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