CN107898731A - A kind of aloe moisturizing lotion and preparation method thereof - Google Patents

A kind of aloe moisturizing lotion and preparation method thereof Download PDF

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Publication number
CN107898731A
CN107898731A CN201711462871.5A CN201711462871A CN107898731A CN 107898731 A CN107898731 A CN 107898731A CN 201711462871 A CN201711462871 A CN 201711462871A CN 107898731 A CN107898731 A CN 107898731A
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aloe
moisturizing lotion
stirring
water
preparation
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段华勇
苏茂
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Shenzhen City Yaan Technology Co Ltd
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Shenzhen City Yaan Technology Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/342—Alcohols having more than seven atoms in an unbroken chain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55—Phosphorus compounds
    • A61K8/553—Phospholipids, e.g. lecithin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67—Vitamins
    • A61K8/678—Tocopherol, i.e. vitamin E
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/82—Preparation or application process involves sonication or ultrasonication

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Biophysics (AREA)
  • Molecular Biology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of aloe moisturizing lotion and preparation method thereof, the percentage by weight of each raw material of aloe moisturizing lotion is：Aloe extract 5 10%, octadecyl alcolol 5 10%, atoleine 5 10%, certain herbaceous plants with big flowers acid glyceride 2 6%, octadecyl alcolol Ethoxylate 1 4%, vitamin E 1.5 4.5%, phosphatidase 0 .5 1.2%, allantoin 0.5 1.2%, glucan 1 4%, xanthans 2 6%, arachidic alcohol 1 6%, isobutanol 3 8%, glycerine 5 10%, essence 0.5 1.2%, surplus are water；Scientific formulation, using ultrasonic extraction, the moisturizing ingredient in aloe is sufficiently extracted, extraction time is short and extraction efficiency is high；The preparation method of aloe moisturizing lotion is simple, and emulsifying effectiveness is good, and obtained aloe moisturizing lotion is creamy white, and after skin wiping, under 25 DEG C of air conditioner surroundings, the percentage of water loss of 10h only has 8%, and water loss is slow, and moistening effect is good.

Description

A kind of aloe moisturizing lotion and preparation method thereof
Technical field
The invention belongs to cosmetic field, and in particular to a kind of aloe moisturizing lotion and preparation method thereof.
Background technology
Aloe (scientific name：Aloe vera) it is the perennial normal of A Fu flowers section (also known as Asphodelaceae, Eremurus chinensis section) Aloe Green herbaceous plant, leafage is raw, big and plump, in seat shape or is born in stem top, and the normal lanceolar of leaf or the short width of leaf, there is sharp tooth at edge Thorn.Inflorescence is umbrella shape, total shape, spike, cone etc., and color is in red, yellow or tool redness of the skin or complexion spot, six, petal, six pieces of gynoecium.Perianth The more joints of base portion are into tubular.
The polysaccharide and multivitamin contained in aloe has human skin good nutrition, moistens, whitening effect.Emerald green leaf reed Luxuriant growth is the Fresh leaf of aloe of the direct beauty of optimum, i.e. aloe barbadensis Miller, it have make skin contraction, softness, moisturizing, anti-inflammatory, The performance of bleaching.Hardening, angling, the effect for improving scar are also released, can not only prevent small wrinkle, pouch, cutis laxa, also Skin wet, tender and lovely can be kept, at the same time it can also treat scytitis, to acne, freckle, acne and scald, knife wound, worm Stinging etc. also has the effect of fine.It is similarly effective to hair, hair can be made to keep moistening smooth, pre-Anti-hair loss.
The content of the invention
It is an object of the invention to provide a kind of aloe moisturizing lotion and preparation method thereof, method is simple, and emulsifying effectiveness is good, system The aloe moisturizing lotion obtained is creamy white,
The purpose of the present invention can be achieved through the following technical solutions：
A kind of aloe moisturizing lotion, the percentage by weight of each raw material are：Aloe extract 5-10%, octadecyl alcolol 5-10%, liquid Body paraffin 5-10%, certain herbaceous plants with big flowers acid glyceride 2-6%, octadecyl alcolol Ethoxylate 1-4%, vitamin E 1.5-4.5%, phosphatidase 0 .5- 1.2%th, allantoin 0.5-1.2%, glucan 1-4%, xanthans 2-6%, arachidic alcohol 1-6%, isobutanol 3-8%, glycerine 5- 10%th, essence 0.5-1.2%, surplus are water.
Further, the extracting method of the aloe extract is：After taking fresh aloe leaf to clean, be put into ball mill into Row crushes, and the asparagus juice connection aloe slag after crushing is put into mixer, and side stirring just adds solvent, and agitated liquid, which flows into, to be held In device, the container for holding aloe liquid is then put into ultrasound in ultrasonic cell disruptor and obtains aloe crude extract, is then adopted Column chromatography for separation, purification and drying to obtain aloe extract are carried out with silicagel column.
Further, the solvent is 50% diethyl ether solution, and the mass ratio of fresh aloe and solvent is 1:5-10.
Further, the ultrasonic power is 200-250W, ultrasonic time 10-15min.
Further, the eluant, eluent that the column chromatography uses is methanol：Water=7.5-8.5:1.
A kind of preparation method of aloe moisturizing lotion, specifically includes following steps：
(1) octadecyl alcolol, atoleine, certain herbaceous plants with big flowers acid glyceride, octadecyl alcolol Ethoxylate, vitamin E, the phosphorus of mass parts are weighed Fat, allantoin, glucan, xanthans arachidic alcohol, isobutanol and glycerine are added in stirring in water bath device, and stirring is so that each raw material is molten Solution is uniformly mixed；
(2) weigh the aloe extract of mass parts and water is added in another stirring in water bath device, stirring is so that aloe extraction Thing is substantially dissolved in water, be then slowly added to step (1) while stirring made from mixed liquor, continue to stir after addition, Obtain mixed emulsion；
(3) mixed emulsion made from step (2) is put into homogenizer and carries out homogeneous；
(4) after homogeneous, take out homogenizing fluid stirring cooling, add essence, be uniformly mixed, be cooled to room temperature to obtain the final product To aloe moisturizing lotion.
Further, the bath temperature of the stirring in water bath device described in step (1) is 75-85 DEG C, mixing time 20-35min.
Further, the bath temperature of the stirring in water bath device described in step (2) is 75-85 DEG C, stirs 10-15min.
Further, the homogenizing time described in step (3) is 1-3min.
Further, the cooling temperature described in step (4) is 45-50 DEG C.
Beneficial effects of the present invention：
A kind of aloe moisturizing lotion of the offer of the present invention, scientific formulation, using ultrasonic extraction, by the moisturizing in aloe Component sufficiently extracts, and extraction time is short and extraction efficiency is high；The preparation method of aloe moisturizing lotion is simple, emulsifying effectiveness Good, obtained aloe moisturizing lotion is creamy white, and after skin wiping, under 25 DEG C of air conditioner surroundings, the percentage of water loss of 10h only has 8%, water loss is slow, and moistening effect is good.
Embodiment
The technical solution in the embodiment of the present invention will be clearly and completely described below, it is clear that described implementation Example is only part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this area is common All other embodiment that technical staff is obtained without creative efforts, belongs to the model that the present invention protects Enclose.
Embodiment 1
A kind of aloe moisturizing lotion, the weight of each raw material are：Aloe extract 5g, octadecyl alcolol 5g, atoleine 5g, certain herbaceous plants with big flowers acid are sweet Grease 2g, octadecyl alcolol Ethoxylate 1g, vitamin E 1.5g, phosphatidase 0 .5g, allantoin 0.5g, bextran 45 g, xanthans 2g, Arachidic alcohol 1g, isobutanol 8g, glycerine 10g, essence 0.5g, water 54g；
The extracting method of the aloe extract is：After taking fresh aloe leaf 100g to clean, it is put into ball mill and carries out Crush, the asparagus juice connection aloe slag after crushing is put into mixer, side stirring just adds 50% diethyl ether solution 500g, stirs After mixing 30min, in liquid inlet container, then the container for holding aloe liquid is put into ultrasonic cell disruptor, ultrasonic work( Rate is 200W, and ultrasonic time 10min, that is, obtain aloe crude extract, then using silicagel column carry out column chromatography for separation, purification and Drying to obtain aloe extract；The eluant, eluent that the column chromatography uses is methanol：Water=7.5:1；
The preparation method of aloe moisturizing lotion is：
(1) octadecyl alcolol, atoleine, certain herbaceous plants with big flowers acid glyceride, octadecyl alcolol Ethoxylate, vitamin E, the phosphorus of mass parts are weighed Fat, allantoin, glucan, xanthans arachidic alcohol, isobutanol and glycerine are added in stirring in water bath device, and bath temperature is 75 DEG C, Mixing time is 20min so that each dissolution of raw material is uniformly mixed；
(2) weigh the aloe extract of mass parts and water is added in another stirring in water bath device, bath temperature is 75 DEG C, is stirred It is 10min to mix the time so that aloe extract is substantially dissolved in water, and it is obtained to be then slowly added to step (1) while stirring Mixed liquor, continues to stir 10min after addition, obtains mixed emulsion；
(3) mixed emulsion made from step (2) is put into homogenizer and carries out homogeneous 1min；
(4) after homogeneous, when taking-up homogenizing fluid stirring is cooled to 45 DEG C, essence is added, stirring 15min is uniformly mixed, It is cooled to room temperature and obtains aloe moisturizing lotion, obtained aloe moisturizing lotion is creamy white, after skin wiping, in 22 DEG C of air-conditioning Under environment, the percentage of water loss of 10h is 6%, and water loss is slow, and moistening effect is good.
Embodiment 2
A kind of aloe moisturizing lotion, the weight of each raw material are：Aloe extract 10g, octadecyl alcolol 10g, atoleine 6g, certain herbaceous plants with big flowers acid Glyceride 6g, octadecyl alcolol Ethoxylate 1g, vitamin E 2g, phosphatidase 1 .2g, allantoin 1.2g, glucan 1g, xanthans 3g, Arachidic alcohol 5g, isobutanol 3g, glycerine 5g, essence 1.0g, water 44.6g；
The extracting method of the aloe extract is：After taking fresh aloe leaf 100g to clean, it is put into ball mill and carries out Crushing, the asparagus juice connection aloe slag after crushing is put into mixer, side stirring just adds 50% diethyl ether solution 1000g, After stirring 60min, in liquid inlet container, then the container for holding aloe liquid is put into ultrasonic cell disruptor, ultrasound Power is 250W, and ultrasonic time 15min, that is, obtain aloe crude extract, then carries out column chromatography for separation, purification using silicagel column The aloe extract with drying to obtain；The eluant, eluent that the column chromatography uses is methanol：Water=8.5:1；
The preparation method of aloe moisturizing lotion is：
(1) octadecyl alcolol, atoleine, certain herbaceous plants with big flowers acid glyceride, octadecyl alcolol Ethoxylate, vitamin E, the phosphorus of mass parts are weighed Fat, allantoin, glucan, xanthans arachidic alcohol, isobutanol and glycerine are added in stirring in water bath device, and bath temperature is 85 DEG C, Mixing time is 35min so that each dissolution of raw material is uniformly mixed；
(2) weigh the aloe extract of mass parts and water is added in another stirring in water bath device, bath temperature is 85 DEG C, is stirred It is 15min to mix the time so that aloe extract is substantially dissolved in water, and it is obtained to be then slowly added to step (1) while stirring Mixed liquor, continues to stir 15min after addition, obtains mixed emulsion；
(3) mixed emulsion made from step (2) is put into homogenizer and carries out homogeneous 3min；
(4) after homogeneous, when taking-up homogenizing fluid stirring is cooled to 50 DEG C, essence is added, stirring 20min is uniformly mixed, It is cooled to room temperature and obtains aloe moisturizing lotion, obtained aloe moisturizing lotion is creamy white, after skin wiping, in 25 DEG C of air-conditioning Under environment, the percentage of water loss of 10h is 8%, and water loss is slow, and moistening effect is good.
Embodiment 3
A kind of aloe moisturizing lotion, the weight of each raw material are：Aloe extract 7g, octadecyl alcolol 7g, atoleine 8g, certain herbaceous plants with big flowers acid are sweet Grease 5g, octadecyl alcolol Ethoxylate 4g, vitamin E 4g, phosphatidase 0 .6g, allantoin 0.6g, glucan 2g, xanthans 5g, flower Raw alcohol 2g, isobutanol 5g, glycerine 6g, essence 0.6g, water 43.2g；
The extracting method of the aloe extract is：After taking fresh aloe leaf 100g to clean, it is put into ball mill and carries out Crush, the asparagus juice connection aloe slag after crushing is put into mixer, side stirring just adds 50% diethyl ether solution 800g, stirs After mixing 40min, in liquid inlet container, then the container for holding aloe liquid is put into ultrasonic cell disruptor, ultrasonic work( Rate is 220W, and ultrasonic time 12min, that is, obtain aloe crude extract, then using silicagel column carry out column chromatography for separation, purification and Drying to obtain aloe extract；The eluant, eluent that the column chromatography uses is methanol：Water=8:1；
The preparation method of aloe moisturizing lotion is：
(1) octadecyl alcolol, atoleine, certain herbaceous plants with big flowers acid glyceride, octadecyl alcolol Ethoxylate, vitamin E, the phosphorus of mass parts are weighed Fat, allantoin, glucan, xanthans arachidic alcohol, isobutanol and glycerine are added in stirring in water bath device, and bath temperature is 82 DEG C, Mixing time is 30min so that each dissolution of raw material is uniformly mixed；
(2) weigh the aloe extract of mass parts and water is added in another stirring in water bath device, bath temperature is 82 DEG C, is stirred It is 12min to mix the time so that aloe extract is substantially dissolved in water, and it is obtained to be then slowly added to step (1) while stirring Mixed liquor, continues to stir 12min after addition, obtains mixed emulsion；
(3) mixed emulsion made from step (2) is put into homogenizer and carries out homogeneous 2min；
(4) after homogeneous, when taking-up homogenizing fluid stirring is cooled to 48 DEG C, essence is added, stirring 16min is uniformly mixed, It is cooled to room temperature and obtains aloe moisturizing lotion, obtained aloe moisturizing lotion is creamy white, after skin wiping, in 28 DEG C of air-conditioning Under environment, the percentage of water loss of 10h is 10%, and water loss is slow, and moistening effect is good.
Above content is only to design example and explanation of the invention, affiliated those skilled in the art Various modifications or additions are done to described specific embodiment or are substituted in a similar way, without departing from invention Design or surmount scope defined in the claims, be within the scope of protection of the invention.

Claims (10)

  1. A kind of 1. aloe moisturizing lotion, it is characterised in that：The percentage by weight of each raw material is：Aloe extract 5-10%, octadecyl alcolol 5-10%, atoleine 5-10%, certain herbaceous plants with big flowers acid glyceride 2-6%, octadecyl alcolol Ethoxylate 1-4%, vitamin E 1.5- 4.5%th, phosphatidase 0 .5-1.2%, allantoin 0.5-1.2%, glucan 1-4%, xanthans 2-6%, arachidic alcohol 1-6%, isobutyl Alcohol 3-8%, glycerine 5-10%, essence 0.5-1.2%, surplus are water.
  2. A kind of 2. aloe moisturizing lotion according to claim 1, it is characterised in that：The extracting method of the aloe extract For：After taking fresh aloe leaf to clean, it is put into ball mill and is crushed, the asparagus juice connection aloe slag after crushing is put into stirring In machine, side stirring just adds solvent, and agitated liquid is flowed into container, and the container for holding aloe liquid then is put into supersonic cell Ultrasound obtains aloe crude extract in pulverizer, then carries out column chromatography for separation, purification and drying to obtain using silicagel column Aloe extract.
  3. A kind of 3. aloe moisturizing lotion according to claim 2, it is characterised in that：The ether that the solvent is 50% is molten The mass ratio of liquid, fresh aloe and solvent is 1:5-10.
  4. A kind of 4. aloe moisturizing lotion according to claim 2, it is characterised in that：The ultrasonic power is 200-250W, Ultrasonic time is 10-15min.
  5. A kind of 5. aloe moisturizing lotion according to claim 2, it is characterised in that：What the column chromatography used washes De- agent is methanol：Water=7.5-8.5:1.
  6. A kind of 6. preparation method of aloe moisturizing lotion, it is characterised in that：Specifically include following steps：
    (1) weigh the octadecyl alcolols of mass parts, atoleine, certain herbaceous plants with big flowers acid glyceride, octadecyl alcolol Ethoxylate, vitamin E, phosphatide, Allantoin, glucan, xanthans arachidic alcohol, isobutanol and glycerine are added in stirring in water bath device, and stirring is so that each dissolution of raw material It is uniformly mixed；
    (2) weigh the aloe extract of mass parts and water is added in another stirring in water bath device, stirring is so that aloe extract fills Point be dissolved in water, be then slowly added to step (1) while stirring made from mixed liquor, continue to stir after addition, obtain Mixed emulsion；
    (3) mixed emulsion made from step (2) is put into homogenizer and carries out homogeneous；
    (4) after homogeneous, homogenizing fluid stirring cooling is taken out, essence is added, is uniformly mixed, is cooled to room temperature and obtains reed Luxuriant growth moisture retention liquid.
  7. A kind of 7. preparation method of aloe moisturizing lotion according to claim 6, it is characterised in that：Water described in step (1) The bath temperature for bathing blender is 75-85 DEG C, mixing time 20-35min.
  8. A kind of 8. preparation method of aloe moisturizing lotion according to claim 6, it is characterised in that：Water described in step (2) The bath temperature for bathing blender is 75-85 DEG C, stirs 10-15min.
  9. A kind of 9. preparation method of aloe moisturizing lotion according to claim 6, it is characterised in that：It is equal described in step (3) The matter time is 1-3min.
  10. A kind of 10. preparation method of aloe moisturizing lotion according to claim 6, it is characterised in that：It is cold described in step (4) But temperature is 45-50 DEG C.
CN201711462871.5A 2017-12-28 2017-12-28 A kind of aloe moisturizing lotion and preparation method thereof Pending CN107898731A (en)

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Application Number Priority Date Filing Date Title
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1424331A (en) * 2002-12-30 2003-06-18 北京工商大学 Extraction of acetylized mannan from aloe juice
CN103083214A (en) * 2013-02-27 2013-05-08 上海莱博生物科技有限公司 Aloe moisturizing lotion and application thereof
CN105055271A (en) * 2015-07-21 2015-11-18 刘振标 Aloe nutritive emulsion
CN105520874A (en) * 2015-12-21 2016-04-27 太仓张根木生物科技有限公司 Aloe moisturizing lotion

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1424331A (en) * 2002-12-30 2003-06-18 北京工商大学 Extraction of acetylized mannan from aloe juice
CN103083214A (en) * 2013-02-27 2013-05-08 上海莱博生物科技有限公司 Aloe moisturizing lotion and application thereof
CN105055271A (en) * 2015-07-21 2015-11-18 刘振标 Aloe nutritive emulsion
CN105520874A (en) * 2015-12-21 2016-04-27 太仓张根木生物科技有限公司 Aloe moisturizing lotion

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