CN107854392A

CN107854392A - A kind of brown sugar mildy wash and preparation method thereof

Info

Publication number: CN107854392A
Application number: CN201711053916.3A
Authority: CN
Inventors: 杨菊; 黄振振; 曹波; 刘运花
Original assignee: Guangzhou Bailichen Cosmetics Co Ltd
Current assignee: Guangzhou Bailichen Cosmetics Co Ltd
Priority date: 2017-10-31
Filing date: 2017-10-31
Publication date: 2018-03-30

Abstract

The invention discloses a kind of brown sugar mildy wash and preparation method thereof, its raw material based on 100 parts of total mass fraction, including：10~14 parts of cocounut oil acyl glycine potassium, 1~3 part of sodium methyl cocoyl taurate, 1~3 part of sodium cocoyl glutamate; 8~10 parts of polyethylene glycol, 3~5 parts of cocoamido sodium propionates, 4~5 parts of tax fat agent; 15~18 parts of propane diols, 1.5~2% stabilizers, 1.2~2.0 parts of esters of olive oil PEG 10; 0.1~0.5 part of allantoin; 0.01~0.05 part of dipotassium glycyrrhizinate, 0.5~1.5 part of polyquaternium, 43,30~42 portions of brown sugar; 0.1~0.15 portion of preservative, wherein brown sugar use two kinds of particle diameters.Mildy wash of the present invention has slight particle frosted sense during rubbing, ablation is brought to feel with rubbing, the gradual fine and smooth docile of skin sense, it is more easy to touch inside pore, due to the frosted finish effect of the brown sugar particle of big particle diameter, small particle brown sugar promotes the absorption of nutritional ingredient in brown sugar, and skin water profit is smooth after flushing, salubrious penetrating.

Description

A kind of brown sugar mildy wash and preparation method thereof

Technical field

The present invention relates to commodity technical field, more particularly, to a kind of brown sugar mildy wash and preparation method thereof.

Background technology

The first step of the face cleaning as skin care, the value of follow-up skin care work is determined, existing mildy wash acts on more single One, its usual face cleaning effect is divided into common cleaning, exfoliating, three classes for the treatment of, and substantial amounts of grease can be removed after cleaning or frosted Rubbish, or removing dead skin cutin, or anti-inflammatory are antibacterial, but often single function can vacate sky for the face pollution of a new round again Between, therefore, needing further water and milk frost to carry out moisturizing nourishing later in cleaning, for this problem, the country falls over each other outer research and development Multiple-effect mildy wash.

At present, have by adding natural abrasive or compound abrasive to increase the frosted finish effect of common cleaning mildy wash, but because This abrasive material is mostly insoluble particle, on the one hand, and it is big to skin abrasion, it is not easy to be commonly used；On the other hand, after use Frosted particle turns into a kind of rubbish and burden for needing subsequent treatment.

Skin whitening, moisturizing effect of mildy wash also turns into the research and development focus of current multiple-effect mildy wash, and the amino acid that market is expedited the emergence of is clean Face breast has reached the effect of moisturizing, but it has a greatly reduced quality in terms of cleaning force, in the case of having color make-up residual, easily makes It is not thorough into cleaning.And some mildy wash with white-skinned face function dry decortication then because containing highly basic after easily causing clean skin The problems such as.

The content of the invention

The technical problem to be solved in the present invention is skin water shortage, subalimentation after overcoming to solve existing mildy wash cleaning The problem of, and melanin is dispelled from food level security, prepare a kind of gently exfoliating, cleaning, nourishing, whitening and settle at one go Multiple-effect mildy wash

Another technical problem to be solved by the present invention is that provide the preparation method of the multiple-effect mildy wash.

The purpose of the present invention is achieved through the following technical solutions：

A kind of brown sugar mildy wash is provided, its raw material constituent based on 100 parts of mass fraction, including：13~14 portions of cocounut oil Acyl glycine potassium, 2~3 parts of sodium methyl cocoyl taurates, 2~3 parts of sodium cocoyl glutamates, 8~11 parts of polyethylene glycol, 2 ~3 parts of cocoamido sodium propionates, 4~5 parts of tax fat agent, 15.5~18 parts of propane diols, 1.5~2.5 parts of stabilizers, 1.5~2.5 Part olive oil PEG-10 esters, 0.3~0.8 part of allantoin, 0.01~0.05 part of dipotassium glycyrrhizinate, 0.5~2 part of polyquaternium- 43,36~42 portions of brown sugar, 0.1~0.15 portion of preservative, surplus is propane diols.

Preferably, the polyethylene glycol that described polyethylene glycol includes the degree of polymerization 1450 with the degree of polymerization is 6000, it is further excellent Selection of land, the mass ratio that the polyethylene glycol that the polyethylene glycol of the degree of polymerization 1450 is 6000 with the degree of polymerization adds in formula is 1:(1 ~1.5).

Preferably, described tax fat agent is HE coconut oil glyceride types.

Preferably, described stabilizer is glycerol monohydroxystearate, hydroxy stearic acid or tocopherol.

Described brown sugar uses food grade brown sugar purchased in market.Preferably, the brown sugar that the present invention uses includes two kinds of particle diameters, It is the thin sugar for more than raw sugar and 60 mesh of 40~60 mesh (containing 60 mesh) respectively, the thin sugar preferably more than 60 mesh is 60~100 mesh.Enter Preferably, the brown sugar addition mass ratio of two kinds of particle diameters of thickness is 2 to one step:1.

It is further preferable that the present invention provides a kind of self-control brown sugar, preparation method is as follows：

Fresh cane is squeezed the juice, and is filtrated to get clarification sucrose mix juice, and sucrose mix juice is boiled through 80 DEG C of low temperature, concentrated, obtains Baume The brown sugar solution of 95 ° of degree, low temperature drying lumps at 70 DEG C, crushed 40 mesh sieves：Again grinding screen upper part and excessively 40 mesh sieves, Repeat operation, until all collecting screenings by 40 mesh sieves, cross 60 mesh sieves, it is raw sugar to obtain oversize, and screenings is Thin sugar.

The homemade brown sugar of the present invention, comprising raw sugar and thin sugar, remain most molasses components.Applied to preparation originally Invent the mildy wash, after its compatibility with other key components, synergy becomes apparent, exfoliation, dispel it is black Significantly more effect is obtained in terms of pigment, light print myogenic, smooth acne hole, reparation acne scar.

It is further preferred that the brown sugar addition mass ratio of two kinds of particle diameters of thickness is 2:1.

Preferably, described preservative is that phenmethylol, chlormethylisothiazo,ine ketone, the mixing of methylisothiazolinone are water-soluble Liquid, and the proportion of composing (g/mol) of three kinds of active ingredient is：108.13:149.6:115.15.

Invention also provides the preparation method of described brown sugar mildy wash, comprise the following steps：

S1. by cocounut oil acyl glycine potassium, sodium methyl cocoyl taurate, sodium cocoyl glutamate, polyethylene glycol- 1450th, cocoamido sodium propionate, assign fat agent, propane diols and mixed thoroughly in pot and be heated to 85 DEG C in emulsify, while be slowly added to carefully Brown sugar, stirring at low speed to whole dissolvings；

S2. after dissolving by heating stabilizer, olive oil PEG-10 esters, PEG-4000 completely, step S1 bodies are added In system, moderate-speed mixer is to being completely dissolved；

S3. after the cooling of step S2 systems, allantoin, dipotassium glycyrrhizinate, polyquaternium -43 is added, are stirred, dissolving；

S4. preservative is added after the cooling of step S3 systems, stirred；

S5. continue to stir and cool, add thick ground brown sugar, stirring at low speed is uniform；

S6. the system prepared by step S5 is stood, and is tied cream, is produced.

Step S1 operation can be operated in pot is emulsified.Preferably, heating is heated to 85 DEG C described in step S1.

Preferably, heating is heated to 85 DEG C described in step S2.

Preferably, cooling is to be cooled to less than 65 DEG C described in step S3.

Preferably, cooling is to be cooled to less than 50 DEG C described in step S4.

Preferably, cooling is to be cooled to less than 40 DEG C described in step S5.

Preferably, the time stood described in step S6 is more than 15 minutes.

Beneficial effects of the present invention are as follows：

For the present invention using amino acid surfactant compounding anti-inflammatory bacteriostatic agent, property is gently non-stimulated, crucial by other The compatibility of component, mildy wash not only have common deep layer cleaning effect, and in massage processes, the brown sugar particle slowly melted can Gentle exfoliation is played, and dredges epithelial tissue downright bad in pore, accelerates molasses to be sought with multivitamin isoreactivity The absorption formed point, reach safe removing toxic substances, dispel the food-grade whitening feature of melanin, by long-term use, in brown sugar mildy wash Abundant nutritional ingredient can also light print myogenic, to a certain extent smooth acne hole, reparation acne scar.In particular by the red of different-grain diameter Sugar, there is slight particle frosted sense during rubbing, bring ablation to feel with rubbing, the gradual fine and smooth docile of skin sense, be more easy to contact To inside pore, due to the frosted finish effect of the brown sugar particle of big particle diameter, small particle brown sugar promotes the absorption of nutritional ingredient in brown sugar, Skin water profit is smooth after flushing, salubrious penetrating.

Invention further provides a kind of brown sugar of homemade different-grain diameter, the brown sugar remains most molasses Composition, after its compatibility with other key components, synergy becomes apparent, and exfoliation, dispels melanin, light print life Flesh, smooth acne hole, obtain significantly more effect in terms of repairing acne scar, after continuous use 1 week, skin just show bright and clean silk it is sliding, It is white touched with red, as a result prove, described brown sugar mildy wash, the obvious foster skin whitening of energy, and can be long-term use of.

Mildy wash preparation method provided by the invention is simple, easy to operate, and properties of product are stable, has good economic effect Should, it is adapted to industrial production.

Embodiment

The present invention is further illustrated with reference to specific embodiment.Following being given for example only property of embodiment explanations, it is impossible to manage Solve as limitation of the present invention.Unless stated otherwise, the raw material used in following embodiments is that conventional purchased in market or commercial sources obtain The raw material obtained, unless stated otherwise, the method and apparatus used in following embodiments are method commonly used in the art and set It is standby.

For convenience of description, it is as follows to be exemplified below heretofore described primary raw material source, is purchased in market, but not therefore Limit the scope of the invention.

Cocounut oil acyl glycine potassium, CAS 301341-58-2 are conventional purchased in market；Sodium methyl cocoyl taurate, conventional city Purchase；Sodium cocoyl glutamate, it is conventional purchased in market；Polyethylene glycol -1450, CAS 25322-68-3, it is conventional purchased in market；Polyethylene glycol- 6000, CAS 25322-68-3, it is conventional purchased in market；Cocoamido sodium propionate, it is conventional purchased in market；HE coconut oil glyceride types, CAS Number 68606-18-8, it is conventional purchased in market；Propane diols, CAS 26264-14-2 are conventional purchased in market；Glycerol monohydroxystearate, conventional city Purchase；Hydroxy stearic acid, CAS 1330-70-7, conventional purchased in market, olive oil PEG-10 esters, CAS 103819-46-1 are conventional It is purchased in market；Allantoin, CAS 97-59-6 are conventional purchased in market；Dipotassium glycyrrhizinate, CAS 68797-35-3, it is conventional purchased in market；Polyquaternary amine Salt -43, it is purchased from Shanghai Hong Du Fine Chemical Co., Ltd；Phenmethylol, CAS 100-51-6 are conventional purchased in market；Chloromethyl isothiazole Quinoline ketone, CAS 26172-55-4 are conventional purchased in market；Methylisothiazolinone, CAS 2682-20-4 are conventional purchased in market.

Brown sugar, which can be that conventional brown sugar purchased in market is screened, obtains thin the sugar more than raw sugar and 60 mesh of the mesh of particle diameter 40~60. It can make by oneself.

Preferred self-control brown sugar of the invention, Homemade method are as follows：Take fresh cane to squeeze the juice, be filtrated to get clarification sucrose mix juice, will Sucrose mix juice is boiled through 80 DEG C of low temperature, concentrated, and obtains the brown sugar solution of 95 ° of Baume degrees, and low temperature drying lumps at 70 DEG C, after crushing Cross 40 mesh metallic screens, and grinding screen upper part again, collect screenings, cross 60 mesh metallic screens, it is raw sugar to obtain oversize, under sieve Thing is thin sugar.

Embodiment 1

Brown sugar mildy wash of the present invention is prepared according to following steps：

S1. 13 parts of cocounut oil acyl glycine potassium, 2.5 parts of sodium methyl cocoyl taurates, 2.5 parts of cocounut oil acyl glutamic acid are weighed Sodium, 4.5 parts of polyethylene glycol -1450,4 parts of cocoamido sodium propionates, 5.5 parts assign fat agent, 17.3 parts of propane diols in emulsifying in pot Mix thoroughly and be heated to 85 DEG C, while be slowly added to 26 parts thin sugar, stirring at low speed to whole dissolvings.

S2. weigh 2 parts of stabilizer, 2 parts of olive oil PEG-10 esters, 5.5% PEG-4000 dissolve by heating it is complete Afterwards, it is added in emulsification pot, moderate-speed mixer is to being completely dissolved.

S3. emulsification pot is cooled to 65 DEG C, add 0.5 part of allantoin, 0.01 part of dipotassium glycyrrhizinate, 1.5 parts of polyquaterniums- 43, stirring to dissolving.

S4. emulsification pot temperature is down to 40 DEG C, adds 0.1 portion of preservative and stirs.

S5. continue stirring cooling, add 13 portions of raw sugar, it is vulgar to stir.

S5. knot cream 30min is stood, produces described brown sugar mildy wash.

Embodiment 2

Described brown sugar mildy wash is prepared according to following steps：

S1. 14 parts of cocounut oil acyl glycine potassium, 2 parts of sodium methyl cocoyl taurates, 2 parts of sodium cocoyl glutamates, 5 are weighed Part polyethylene glycol -1450,6 parts of cocoamido sodium propionates, 5 parts of tax fat agent, 15.5 parts of propane diols are mixed thoroughly and added in pot in emulsifying Heat is slowly added to 28 parts thin sugar, stirring at low speed to whole dissolvings to 85 DEG C.

S2. 1.5 parts of stabilizer is weighed, 1.5 parts of olive oil PEG-10 esters, 4% PEG-4000s have dissolved by heating Quan Hou, it is added in emulsification pot, moderate-speed mixer is to being completely dissolved.

S3. emulsification pot is cooled to 65 DEG C, add 0.8 part of allantoin, 0.05 part of dipotassium glycyrrhizinate, 0.5 part of polyquaternium- 43, stirring to dissolving.

S4. emulsification pot temperature is down to 40 DEG C, adds 0.15 portion of preservative and stirs.

S5. continue stirring cooling, add 14 portions of raw sugar, it is vulgar to stir.

S5. knot cream 30min is stood, produces described brown sugar mildy wash.

Embodiment 3

Described brown sugar mildy wash is prepared according to following steps：

S1. 12% cocounut oil acyl glycine potassium, 3 parts of sodium methyl cocoyl taurates, 3 parts of sodium cocoyl glutamates, 3 are weighed Part polyethylene glycol -1450,4.6 parts of cocoamido sodium propionates, 6 parts of tax fat agent, 18 parts of propane diols are mixed thoroughly and added in pot in emulsifying Heat is slowly added to 28 parts thin sugar, stirring at low speed to whole dissolvings to 85 DEG C.

S2. 2.5% stabilizer is weighed, 2.5 parts of olive oil PEG-10 esters, 6 parts of PEG-4000s have dissolved by heating Quan Hou, it is added in emulsification pot, moderate-speed mixer is to being completely dissolved.

S3. emulsification pot is cooled to 65 DEG C, adds 0.3 part of allantoin, 0.03 part of dipotassium glycyrrhizinate, 2 parts of polyquaternium -43, Stirring is extremely dissolved.

S5. continue stirring cooling, add 12 portions of raw sugar, it is vulgar to stir.

S5. knot cream 30min is stood, produces brown sugar mildy wash.

Embodiment 4

Described brown sugar mildy wash is prepared according to following steps：

S1. 14 parts of cocounut oil acyl glycine potassium, 2 parts of sodium methyl cocoyl taurates, 2 parts of sodium cocoyl glutamates, 5 are weighed Part polyethylene glycol -1450,6 parts of cocoamido sodium propionates, 5 parts of tax fat agent, 57.5 parts of propane diols are mixed thoroughly and added in pot in emulsifying Heat is stirred to whole dissolvings to 85 DEG C.

S2. 1.5 parts of stabilizer is weighed, 1.5 parts of olive oil PEG-10 esters, 4 parts of PEG-4000s have dissolved by heating Quan Hou, it is added in emulsification pot, moderate-speed mixer is to being completely dissolved.

S5. knot cream 30min is stood, obtains common mildy wash.

Embodiment 5

Described brown sugar mildy wash is prepared according to following steps：

S1. weigh 14% cocounut oil acyl glycine potassium, 2 sodium methyl cocoyl taurates, 2 parts of sodium cocoyl glutamates, 5 parts Polyethylene glycol -1450,6 parts of cocoamido sodium propionates, 5 parts assign fat agent, 43.5 parts of propane diols and mix thoroughly and heat in emulsifying in pot To 85 DEG C, stir to whole dissolvings.

S4. emulsification pot temperature is down to 40 DEG C, adds the Pericarppium Armeniacae Amarum powder of 0.15 portion of preservative and 14 parts and stirs.

S5. knot cream 30min is stood, obtains frosted mildy wash.

By the mildy wash described in comparing embodiment 1~5, summarize and find, the gained mildy wash foam of embodiment 1~5 is fine and closely woven Abundant, cleaning capacity is relatively strong but does not stimulate gently.The wherein gained mildy wash of embodiment 1~3 carries due to the addition of special brown sugar Brown sugar caramel, color and luster are in caramel brown, have slight particle frosted sense during rubbing, bring ablation to feel with rubbing, skin The gradual fine and smooth docile of sense, is more easy to touch inside pore, due to the frosted finish effect of the brown sugar particle of big particle diameter, brown sugar mildy wash energy Scutellum is slightly peeled off, increases the permeability of skin, promotes the absorption of nutritional ingredient in brown sugar, skin water moistens light after flushing Sliding, salubrious penetrating, after being used continuously 1 week, the bright and clean silk of skin is sliding, white touched with red, as a result proves, described brown sugar mildy wash, energy Obvious foster skin whitening, and can be long-term use of.

The gained mildy wash of comparative example 4, no special odor, skin sense is moist during rubbing, can gently clean table Skin grease, but without frosted finish effect, in terms of skin care without remarkable result；By contrast, comparative example 5 has more strong " frosted " is felt, and is used continuously less than 1 week, engenders serious water shortage symptom, and cutaneous manifestations are slightly damaged, and shows as to smearing Smoothing toner there is a certain degree of stimulate the reaction, the results showed that, such frosted mildy wash is unsuitable long-term use of.

Claims

A kind of 1. brown sugar mildy wash, it is characterised in that its raw material based on 100 parts of total mass fraction, including：10~14 parts of cocounut oil acyls Glycine potassium, 1~3 part of sodium methyl cocoyl taurate, 1~3 part of sodium cocoyl glutamate, 8~10 parts of polyethylene glycol, 3~5 Part cocoamido sodium propionate, 4~5 parts of tax fat agent, 15~18 parts of propane diols, 1.5~2% stabilizers, 1.2~2.0 parts of olive oil PEG-10 esters, 0.1~0.5 part of allantoin, 0.01~0.05 part of dipotassium glycyrrhizinate, 0.5~1.5 part of polyquaternium -43,30 ~42 portions of brown sugar, 0.1~0.15 portion of preservative.
2. brown sugar mildy wash according to claim 1, it is characterised in that described polyethylene glycol include the degree of polymerization 1450 with The degree of polymerization is 6000 polyethylene glycol.
3. brown sugar mildy wash according to claim 1, it is characterised in that described polyethylene glycol include the degree of polymerization 1450 with The mass ratio both polyethylene glycol that the degree of polymerization is 6000 is 1：(1~1.5).
4. brown sugar mildy wash according to claim 1, it is characterised in that described tax fat agent is HE coconut oil glyceride types.
5. brown sugar mildy wash according to claim 1, it is characterised in that described stabilizer be glycerol monohydroxystearate, The one or more of hydroxy stearic acid or tocopherol.
6. brown sugar mildy wash according to claim 1, it is characterised in that described preservative is phenmethylol, the different thiophene of chloromethyl The mixed aqueous solution of oxazoline ketone, methylisothiazolinone；It is preferred that the proportion of composing of three kinds of active ingredient（g/mol）For：108.13: 149.6:115.15。
7. brown sugar mildy wash according to claim 1, it is characterised in that the brown sugar is the brown sugar of two kinds of particle diameters, is respectively Thin the sugar more than raw sugar of 40~60 mesh and 60 mesh；It is preferred that thin sugar more than 60 mesh is 60~100 mesh.
8. according to the brown sugar mildy wash of claim 1 or 7, it is characterised in that the preparation method of the brown sugar is fresh cane Squeeze the juice, be filtrated to get clarification sucrose mix juice, sucrose mix juice is boiled through 80 DEG C of low temperature, concentrated, obtains the brown sugar solution of 95 ° of Baume degrees, Low temperature drying lumps at 70 DEG C, crushed 40 mesh sieves：Again grinding screen upper part, and screenings is collected, 60 mesh sieves are crossed, are obtained Oversize is raw sugar, and screenings is thin sugar.
9. according to the brown sugar mildy wash of claim 7 or 8, it is characterised in that and the brown sugar addition quality of two kinds of particle diameters of thickness Ratio is 2:1.
10. according to the preparation method of any one of the claim 1~9 brown sugar mildy wash, it is characterised in that including following step Suddenly：

S1. by cocounut oil acyl glycine potassium, sodium methyl cocoyl taurate, sodium cocoyl glutamate, polyethylene glycol -1450, coconut palm Oleoyl alanine sodium, assign fat agent, propane diols and mixed thoroughly in pot and be heated to 85 DEG C in emulsifying, while be slowly added to thin brown sugar, Stirring at low speed is to whole dissolvings；

S2. after dissolving by heating stabilizer, olive oil PEG-10 esters class, PEG-4000 completely, step S1 systems are added In, moderate-speed mixer is to being completely dissolved；

S3. after the cooling of step S2 systems, allantoin, dipotassium glycyrrhizinate, polyquaternium -43 is added, are stirred, dissolving；

S4. preservative is added after the cooling of step S3 systems, stirred；

S5. continue to stir and cool, add thick ground brown sugar, stirring at low speed is uniform；

S6. the system prepared by step S5 is stood, and is tied cream, is produced.