CN107823141A - A kind of preparation method of deer blood freeze-dried powder - Google Patents
A kind of preparation method of deer blood freeze-dried powder Download PDFInfo
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- CN107823141A CN107823141A CN201711193384.3A CN201711193384A CN107823141A CN 107823141 A CN107823141 A CN 107823141A CN 201711193384 A CN201711193384 A CN 201711193384A CN 107823141 A CN107823141 A CN 107823141A
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- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/141—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers
- A61K9/145—Intimate drug-carrier mixtures characterised by the carrier, e.g. ordered mixtures, adsorbates, solid solutions, eutectica, co-dried, co-solubilised, co-kneaded, co-milled, co-ground products, co-precipitates, co-evaporates, co-extrudates, co-melts; Drug nanoparticles with adsorbed surface modifiers with organic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
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Abstract
The invention belongs to deer blood deep process technology field, more particularly to a kind of preparation method of deer blood freeze-dried powder.A kind of preparation method of deer blood freeze-dried powder, comprises the following steps:(1) blood anticoagulant agent solution is prepared, deer blood is placed in and collects in tub tank, it is standby;(2) deer blood is collected, is injected into the collection tub tank of blood anticoagulant agent solution and stirs;(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, it is placed in the refrigerator-freezer or icebox of energy cryogenic refrigeration;(4) the blood ice cube of freezing is taken out into knock fritter, dries, obtain the loose shape product of deer blood;(5) the dried loose shape product of deer blood is taken out, crushes, obtain deer blood freeze-dried powder.The method ensure that the protein consistency of deer blood dry powder, physiological activator are not destroyed, the recovery of water alcohol well, keeps the characteristic of deer blood.
Description
Technical field
The invention belongs to deer blood deep process technology field, more particularly to a kind of preparation method of deer blood freeze-dried powder.
Background technology
Sika deer (Cervus NIppon Tem minck) also known as flower deer, belongs to Cervidae deer category, approximately has water with sika deer
Deer and red deer.
Spotted deers are distributed more widely in China, and more provinces and regions from northeast North China to East China south China have, but due to length
Phase is hunted and the ecological environment of deer existence is compressed, and wild quantity is reduced year by year.It is reported that present only Heilungkiang, Jilin, river
There is wild presence the provinces and regions such as north, Shanxi, Jiangsu, Zhejiang, Jiangxi, Guangdong, Guangxi, Taiwan, but quantity is few.
Deer disposition is docile, is easy to raise, there is raising in the zoo of most provincial, and municipal levels.Since reform and opening-up, create at home
It is very fast to do the development of artificial feeding deer field.Up to over one hundred, the kind deer field of hundred Sub-scales reaches number for kind deer fields more than hundred scales
Ten thousand, rare deer product is maintained at certain level, be unlikely to cause special rare.
Wild deer lives in mixed forest more, near upland meadow and purlieu.Winter lives in mountain region Nan Po and low more
Depression side, the more place activities in Shao Shu wilderness of spring and autumn, summer is often movable in closeer woods, is being wild open fields sooner or later
With the place activity of humidity, the sense of hearing and smell are flourishing, and action is brisk, easily frightened, and doe happiness is gregarious, stag Chang Duju, only exists
Breeding season is just and doe is gregarious, and doe gives birth to a tire every year, and most per one, tire, minority is raw 2,9 months pregnancy periods.
Deer can claim whole body to be all precious, pilose antler, deer bone, deer blood, deer tire, deer placenta, deer horn, deer's sinew, deer's tail, the deer heart, deer
Each position such as kidney can nearly all be used as medicine.Deer blood is made medicinal, occurs name doctor SUN Si miao in ancient times earliest《Qianjin Yi Fang * food therapys》
In.Spitted blood for governance wasting pain in the back, palpitation and insomnia, impotence due to deficiency of the kidney, consumptive lung disease, the inferior disease of uterine bleeding band.Ming Dynasty's Li Shizhen《Herbal guiding principle
Mesh》Record, deer blood cures mainly impotence, and qi-restoratives, only pain in the back, nosebleed epistaxis, injured, mad dog hinder.Tuberculosis is controlled with wine clothes to spit blood.Big qi-restoratives damage,
Benefiting essence-blood, solution pest poison.
Modern medicine research shows that deer blood can enhance metabolism, and build up health, and promotes body totality function effect, right
Neurasthenia, has a sleepless night and to plant the effect of deficient favourable.Constituent analysis to deer blood, it was demonstrated that composition is more and complicated, is rich in deer blood
A variety of human bodies need amino acid and various trace elements and several physiological active substances needed by human, such as the free-fat of lipid
Acid, sterol, glycolipid, phosphatide, hormone, purine, vitamin, polysaccharide, r globulin, hepatocuprein, gluathione oxidizing ferment and
The creatine phosphokinase related to heart body, A2 hydroxybutyric acids Guang hydrogen enzyme and creatine phosphokinase, multiple enzyme etc..
The application of deer blood, important at present is the form using traditional deer blood meal and deer-blood wine, is prepared by raw material of deer blood
Deer blood polypeptide method has more achievement in research, but its commercialized product is still rare.
Deer blood, the about 7-9% of percentage of liveweight in deer body, the blood volume that can be collected when butchering and bloodletting mode and Tu Qianlu feelings
Not-ready status is relevant, and suspension type bloodletting can collect some more than horizontal lying-type bloodletting, face and butcher the mood of deer and steadily collected much than fear
A bit.Face before killing the 55-65% for being emotionally stable and blood total amount being collected with hanging or bloodletting;If not the above situation, general
The 35-45% of total blood volume can be collected into.Thus it is possible to the deer blood being collected into is not a lot, moreover the amount of slaughtering of deer and it is not so good as cattle and sheep
Pig is so much and can not concentrate animal-slaughtering in fixed place.The butchering amount of deer is few and scattered, and therefore, it is necessary that usually collection, which freezes stand-by,
's.The deer blood meal of gained is freeze-dried, can ensure that its protein consistency, active material is not destroyed, and the restoration of water alcohol is good,
Maintain the speciality of fresh deer blood, you can the raw material of deer hemepeptide can be prepared again by preparing various traditional deer blood products.
The information for being disclosed in the background section is merely intended to understanding of the increase to the general background of the present invention, without answering
It has been the prior art well known to persons skilled in the art when being considered as recognizing or implying the information structure in any form.
The content of the invention
To overcome above-mentioned deficiency, the present invention provides a kind of preparation method of deer blood freeze-dried powder, and this method can ensure that deer blood is done
The protein consistency of powder, physiological activator are not destroyed, and the recovery of water alcohol well, keeps the characteristic of deer blood.
Technical scheme provided by the invention is as follows:
A kind of preparation method of deer blood freeze-dried powder, comprises the following steps:
(1) using the bloodletting mode that can collect deer blood more as far as possible, calculate the deer blood volume being collected into, add blood anticoagulant
Agent, deionized water dissolving blood anticoagulant is added, obtain blood anticoagulant agent solution, be placed in deer blood and collect in tub tank, it is standby;
(2) deer blood is collected immediately when slaughtering deer, is injected into the collection tub tank of blood anticoagulant agent solution and is fully stirred
Mix uniformly;
(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, be placed in can cryogenic refrigeration ice
In cabinet or icebox, it is refrigerated to -36 DEG C and is kept for 1-2 hours;
(4) the blood ice cube of freezing is taken out into knock fritter, is dried in Zhi Yu rotation type microwave vacuum dryers, work as freezing
After the drying moisture content < 8% of blood, terminate drying, obtain the loose shape product of deer blood;
(5) the dried loose shape product of deer blood is taken out, crushed, obtain deer blood freeze-dried powder, sampling is to be checked, as early as possible will production
Product move on to relative humidity less than in 50% Room, are packed by fixed ginseng.
Preferably, the blood anticoagulant described in step (1) is trisodium citrate, its addition is the 4- of deer blood weight
5‰。
Preferably, the addition for removing centrifugal water described in step (1) is 5-10 times of trisodium citrate weight.
(vacuum of 4) Zhong rotation type microwave vacuum dryers is 0.06-0.085Mpa, temperature control 58 preferably, step
℃。
Preferably, the granularity of the deer blood freeze-dried powder described in step (5) is 80-100 mesh.
Compared with prior art, the present invention has the advantages that:
(1) method technique of the invention is simple, easily operated, is coupled with refrigerator and microwave vacuum dryer instead of costliness
All-in-one is freeze-dried, equipment investment more than 60% can be saved;Same material and quantity, which are dried, reaches same moisture content, we
2/3 when method ratio is saved with refrigeration integrated machine.
(2) the method ensure that the protein consistency of deer blood dry powder, physiological activator are not destroyed, water alcohol
Recovery well, keep deer blood characteristic.
(3) method of the invention can be used for freezing deer brain, deer marrow, internal organ etc., and it is pre- to be that these materials need to carry out pulp
Could so it be operated after processing.
Embodiment
Following examples do not limit the present invention to be better understood from the present invention.Experimental method in following embodiments,
Unless otherwise specified, it is conventional method.
Embodiment 1:
A kind of preparation method of deer blood freeze-dried powder, comprises the following steps:
(1) using the bloodletting mode that can collect deer blood more as far as possible, calculate the deer blood volume being collected into, add blood anticoagulant
Agent, deionized water dissolving blood anticoagulant is added, obtain blood anticoagulant agent solution, be placed in deer blood and collect in tub tank, it is standby;
Described blood anticoagulant is trisodium citrate, and its addition is the 4 ‰ of deer blood weight;The described addition for removing centrifugal water is
5 times of trisodium citrate weight;
(2) deer blood is collected immediately when slaughtering deer, is injected into the collection tub tank of blood anticoagulant agent solution and is fully stirred
Mix uniformly;
(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, be placed in can cryogenic refrigeration ice
In cabinet or icebox, it is refrigerated to -36 DEG C and is kept for 1 hour;
(4) the blood ice cube of freezing is taken out into knock fritter, is dried in Zhi Yu rotation type microwave vacuum dryers, work as freezing
After the drying moisture content < 8% of blood, terminate drying, obtain the loose shape product of deer blood;Suo Shu rotation type micro-wave vacuums
The vacuum of machine is 0.06Mpa, 58 DEG C of temperature control;
(5) the dried loose shape product of deer blood is taken out, crushed, obtain deer blood freeze-dried powder, sampling is to be checked, as early as possible will production
Product move on to relative humidity less than in 50% Room, are packed by fixed ginseng;The granularity of described deer blood freeze-dried powder is 80 mesh.
Embodiment 2:
A kind of preparation method of deer blood freeze-dried powder, comprises the following steps:
(1) using the bloodletting mode that can collect deer blood more as far as possible, calculate the deer blood volume being collected into, add blood anticoagulant
Agent, deionized water dissolving blood anticoagulant is added, obtain blood anticoagulant agent solution, be placed in deer blood and collect in tub tank, it is standby;
Described blood anticoagulant is trisodium citrate, and its addition is the 5 ‰ of deer blood weight;The described addition for removing centrifugal water is
10 times of trisodium citrate weight;
(2) deer blood is collected immediately when slaughtering deer, is injected into the collection tub tank of blood anticoagulant agent solution and is fully stirred
Mix uniformly;
(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, be placed in can cryogenic refrigeration ice
In cabinet or icebox, it is refrigerated to -36 DEG C and is kept for 2 hours;
(4) the blood ice cube of freezing is taken out into knock fritter, is dried in Zhi Yu rotation type microwave vacuum dryers, work as freezing
After the drying moisture content < 8% of blood, terminate drying, obtain the loose shape product of deer blood;Suo Shu rotation type micro-wave vacuums
The vacuum of machine is 0.085Mpa, 58 DEG C of temperature control;
(5) the dried loose shape product of deer blood is taken out, crushed, obtain deer blood freeze-dried powder, sampling is to be checked, as early as possible will production
Product move on to relative humidity less than in 50% Room, are packed by fixed ginseng;The granularity of described deer blood freeze-dried powder is 100 mesh.
Embodiment 3:
A kind of preparation method of deer blood freeze-dried powder, comprises the following steps:
(1) using the bloodletting mode that can collect deer blood more as far as possible, calculate the deer blood volume being collected into, add blood anticoagulant
Agent, deionized water dissolving blood anticoagulant is added, obtain blood anticoagulant agent solution, be placed in deer blood and collect in tub tank, it is standby;
Described blood anticoagulant is trisodium citrate, and its addition is the 4.5 ‰ of deer blood weight;The described addition for removing centrifugal water
For 8 times of trisodium citrate weight;
(2) deer blood is collected immediately when slaughtering deer, is injected into the collection tub tank of blood anticoagulant agent solution and is fully stirred
Mix uniformly;
(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, be placed in can cryogenic refrigeration ice
In cabinet or icebox, it is refrigerated to -36 DEG C and is kept for 1.5 hours;
(4) the blood ice cube of freezing is taken out into knock fritter, is dried in Zhi Yu rotation type microwave vacuum dryers, work as freezing
After the drying moisture content < 8% of blood, terminate drying, obtain the loose shape product of deer blood;Suo Shu rotation type micro-wave vacuums
The vacuum of machine is 0.08Mpa, 58 DEG C of temperature control;
(5) the dried loose shape product of deer blood is taken out, crushed, obtain deer blood freeze-dried powder, sampling is to be checked, as early as possible will production
Product move on to relative humidity less than in 50% Room, are packed by fixed ginseng;The granularity of described deer blood freeze-dried powder is 90 mesh.
The deer blood freeze-dried powder being prepared using method in embodiment 1-3 is detected, the results are shown in Table 1.
The testing result of deer blood freeze-dried powder is prepared in the method for the present invention of table 1
As shown in Table 1, the protein for the deer blood freeze-dried powder that method of the invention is prepared is more than 78%, amino acid drop
Solution rate is below 55%, and the color and luster of deer blood freeze-dried powder is pink.
The description of the foregoing specific illustrative embodiment to the present invention is to illustrate and the purpose of illustration.These descriptions
It is not wishing to limit the invention to disclosed precise forms, and it will be apparent that according to above-mentioned teaching, can be much changed
And change.The purpose of selecting and describing the exemplary embodiment is that explain that the certain principles of the present invention and its reality should
With so that those skilled in the art can realize and utilize the present invention a variety of exemplaries and
Various chooses and changes.The scope of the present invention is intended to be limited by claims and its equivalents.
Claims (5)
1. a kind of preparation method of deer blood freeze-dried powder, it is characterised in that comprise the following steps:
(1) using the bloodletting mode that can collect deer blood more as far as possible, calculate the deer blood volume being collected into, add blood anticoagulant, then
Deionized water dissolving blood anticoagulant is added, obtains blood anticoagulant agent solution, deer blood is placed in and collects in tub tank, it is standby;
(2) deer blood is collected immediately when slaughtering deer, is injected into the collection tub tank of blood anticoagulant agent solution and is sufficiently stirred
It is even;
(3) blood for consolidating anti-freezing, loaded in open kiver, blood depth < 250mm, be placed in can cryogenic refrigeration refrigerator-freezer or
In icebox, it is refrigerated to -36 DEG C and is kept for 1-2 hours;
(4) the blood ice cube of freezing is taken out into knock fritter, is dried in Zhi Yu rotation type microwave vacuum dryers, work as frozen blood
Drying moisture content < 8% after, terminate drying, obtain the loose shape product of deer blood;
(5) the dried loose shape product of deer blood is taken out, crushed, obtain deer blood freeze-dried powder, sampling is to be checked, as early as possible moves product
It is less than to relative humidity in 50% Room, is packed by fixed ginseng.
2. the preparation method of deer blood freeze-dried powder according to claim 1, it is characterised in that the blood described in step (1)
Anti-coagulants is trisodium citrate, and its addition is the 4-5 ‰ of deer blood weight.
3. the preparation method of deer blood freeze-dried powder according to claim 1, it is characterised in that described in step (1) go from
The addition of edema with the heart involved is 5-10 times of trisodium citrate weight.
4. the preparation method of deer blood freeze-dried powder according to claim 1, it is characterised in that step (4) Zhong rotation type microwaves
The vacuum of vacuum drier is 0.06-0.085Mpa, 58 DEG C of temperature control.
5. the preparation method of deer blood freeze-dried powder according to claim 1, it is characterised in that the deer blood described in step (5)
The granularity of freeze-dried powder is 80-100 mesh.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110354141A (en) * | 2019-07-05 | 2019-10-22 | 安徽省泽华国药饮片有限公司 | A kind of preparation method of deer blood freeze-dried powder |
CN114306388A (en) * | 2021-11-30 | 2022-04-12 | 江西纳弗堂制药有限公司 | Deer fetus freeze-dried decoction pieces and preparation method thereof |
CN115043872A (en) * | 2022-06-17 | 2022-09-13 | 哈尔滨工业大学 | Method for extracting deer blood phospholipid and application thereof |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110354141A (en) * | 2019-07-05 | 2019-10-22 | 安徽省泽华国药饮片有限公司 | A kind of preparation method of deer blood freeze-dried powder |
CN114306388A (en) * | 2021-11-30 | 2022-04-12 | 江西纳弗堂制药有限公司 | Deer fetus freeze-dried decoction pieces and preparation method thereof |
CN115043872A (en) * | 2022-06-17 | 2022-09-13 | 哈尔滨工业大学 | Method for extracting deer blood phospholipid and application thereof |
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Application publication date: 20180323 |