CN107779877A - A kind of metal-polishing liquid and preparation method thereof - Google Patents
A kind of metal-polishing liquid and preparation method thereof Download PDFInfo
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- CN107779877A CN107779877A CN201711165427.7A CN201711165427A CN107779877A CN 107779877 A CN107779877 A CN 107779877A CN 201711165427 A CN201711165427 A CN 201711165427A CN 107779877 A CN107779877 A CN 107779877A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
- C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
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Abstract
The invention provides a kind of preparation method of metal-polishing liquid, comprise the following steps：（1）Chitosan/attapulgite clay compounded particulate is prepared；（3）80 120 parts of 15 parts of silicon powder, 25 parts of ball-type silicones micro mist, chitosan/4 8 parts of attapulgite particulate, 36 parts of cysteine, 12 parts of APES, 25 parts of citric acid, 12 parts of cocounut oil acyl diethanol amine, 13 parts of sodium cocoyl glutamate, 15 parts of poly-aspartate, 26 parts of tallow amine APEO and water are weighed by weight；（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed; ball milling; then cysteine, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine APEO and water are added; it is mixed evenly, produces a kind of metal-polishing liquid.This polishing fluid effect is good, and environmental pollution is small.
Description
Technical field
The present invention relates to polishing fluid, and in particular to a kind of metal-polishing liquid.
Background technology
The processing of metal surface has many kinds of ways and meanses, such as plating, electrophoresis, chemical treatment, surface polishing.Chemistry
Polishing is the chemical attack under a kind of specific condition, and it is metal surface is reached whole by controlling the dissolving of metal selective
Gentle bright process of metal working, is constantly subjected to the attention of people, still, wants steel substrate and reaches comprehensive brightness effect
And clearly word and pattern are kept, this proposes requirements at the higher level to surface with chemical polishing technology, wherein just including chemical polishing solution.Gold
Category utensil, which shapes rear surface, would generally adhere to one layer of greasy dirt or other chemicals, utensil using after a period of time by using
The corrosion of environment, rusty stain can be produced on surface, in order to attractive in appearance and increase the service life, commonly use special metal cleaner or polishing
The dirt on surface is cleared up in agent.But existing polishing agent, which exists, returns the problems such as rust is fast, and applicable metal species are narrow, cleaning is not thorough,
Contain fluorine compounds or phosphorus-containing compound, environmental pollution in many polishing agents.And the polishing agent that in the market is commonly used is with solid
Based on, i.e. antiscuffing paste, labor intensity is big when in use for this product, not complete enough to fine-structured surface processing.
The content of the invention
Technical problems to be solved：It is an object of the invention to provide a kind of metal-polishing liquid and preparation method thereof, the polishing
Agent can not only make metal surface keep gloss to become clear, and also have the function that cleaning-nursing, derusting stain and maintenance decontamination, be a variety of
The ideal chose of metallic article cleaning maintenance.
Technical scheme：A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）Chitosan and attapulgite mixing and ball milling 30-60min are then dissolved in 1-1.5wt% acetum, mixed
Liquid stirs 3000-6000r/h at 40 DEG C, disperses 1h and obtains viscous composite, wherein chitosan, attapulgite and acetic acid is molten
The mass ratio of liquid is 2.5-3:2-4:40-50；
（2）Viscous composite is added into atoleine and 1-4h is stirred at room temperature in sorbitan fatty ester, then
Add formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
2-5h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite repeatedly, atoleine, loses
The mass ratio of water sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 75-90:65-85:0.15-0.3:5-7:4-8；
（3）Weigh by weight silicon powder 1-5 parts, ball-type silicones micro mist 2-5 parts, chitosan/attapulgite particulate 4-8 parts,
Cysteine 3-6 parts, APES 1-2 parts, citric acid 2-5 parts, cocounut oil acyl diethanol amine 1-2 parts, cocounut oil acyl paddy
Propylhomoserin sodium 1-3 parts, poly-aspartate 1-5 parts, tallow amine APEO 2-6 parts and water 80-120 parts；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 5-10min, then added
Cysteine, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, ox
Fat amine APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Further, the preparation method of described a kind of metal-polishing liquid, step（1）The average deacetylation of middle chitosan
≥90%。
Further, the preparation method of described a kind of metal-polishing liquid, step（1）Middle attapulgite is acidifying concave convex rod
Soil, the preparation method for being acidified attapulgite are then ground 200 mesh sieve with 37% salt acid soak 24h by attapulgite, most
After be eluted with water.
Further, the preparation method of described a kind of metal-polishing liquid, step（1）Middle chitosan and attapulgite mixing
Ball milling 40-60min, is then dissolved in 1.5wt% acetum, and mixed liquor stirs 4000-5000r/h at 40 DEG C, disperses
The mass ratio of 1h acquisition viscous composites, wherein chitosan, attapulgite and acetum is 2.5:2-3:42-48.
Further, the preparation method of described a kind of metal-polishing liquid, step（2）Middle viscous composite, liquid stone
The mass ratio of wax, sorbitan fatty ester, formaldehyde and glutaraldehyde is 78-85:70-85:0.22-0.28:6-7:5-6.
Further, the preparation method of described a kind of metal-polishing liquid, step（3）Silicon powder 2-4 is weighed by weight
Part, ball-type silicones micro mist 2-4 parts, chitosan/attapulgite particulate 5-7 parts, cysteine 4-5 parts, alkylphenol-polyethenoxy
Ether 1-2 parts, citric acid 3-5 parts, cocounut oil acyl diethanol amine 1-1.5 parts, sodium cocoyl glutamate 1.5-2.4 parts, poly-aspartate
2-4 parts, tallow amine APEO 3-5 parts and water 90-110 parts.
Further, the preparation method of described a kind of metal-polishing liquid, step（4）Middle Ball-milling Time is 8min.
Beneficial effect：The glossiness and wetting flow leveling of the polishing of the polishing agent of the present invention are more excellent, and cut is gone
Except rate is high, the greasy dirt and rust staining of metal surface can be effectively removed, improves metal surface gloss, the polishing agent composition safety collar
Protect, and preparation method is simple, is adapted to promote.
Embodiment
Embodiment 1
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 30min, it is then dissolved in 1wt% acetum, mixed liquor is 40
3000r/h is stirred at DEG C, disperses the mass ratio that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
For 2.5:2:40；
（2）Viscous composite is added into atoleine and 1h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
2h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 75:85:0.15:7:4；
（3）1 part of silicon powder, 5 parts of ball-type silicones micro mist, chitosan/4 parts of attapulgite particulate, half Guang ammonia are weighed by weight
6 parts of acid, 1 part of APES, 2 parts of citric acid, 2 parts of cocounut oil acyl diethanol amine, 1 part of sodium cocoyl glutamate, poly- day
80 parts of 1 part of winter propylhomoserin, 6 parts of tallow amine APEO and water；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 5min, then add half Guang
Propylhomoserin, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine
APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Embodiment 2
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 60min, it is then dissolved in 1.5wt% acetum, mixed liquor exists
6000r/h is stirred at 40 DEG C, disperses the quality that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
Than for 3:4:50；
（2）Viscous composite is added into atoleine and 4h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
5h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 90:65:0.3:5:8；
（3）5 parts of silicon powder, 2 parts of ball-type silicones micro mist, chitosan/8 parts of attapulgite particulate, half Guang ammonia are weighed by weight
3 parts of acid, 2 parts of APES, 5 parts of citric acid, 1 part of cocounut oil acyl diethanol amine, 3 parts of sodium cocoyl glutamate, poly- day
120 parts of 5 parts of winter propylhomoserin, 2 parts of tallow amine APEO and water；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 10min, then add half
Cystine, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow
Amine APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Embodiment 3
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 40min, it is then dissolved in 1.2wt% acetum, mixed liquor exists
4000r/h is stirred at 40 DEG C, disperses the quality that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
Than for 2.5:2:48；
（2）Viscous composite is added into atoleine and 1h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
5h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 78:85:0.22:6:6；
（3）4 parts of silicon powder, 2 parts of ball-type silicones micro mist, chitosan/5 parts of attapulgite particulate, half Guang ammonia are weighed by weight
It is 4 parts of acid, 2 parts of APES, 5 parts of citric acid, 1 part of cocounut oil acyl diethanol amine, 1.5 parts of sodium cocoyl glutamate, poly-
110 parts of 2 parts of aspartic acid, 3 parts of tallow amine APEO and water；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 8min, then add half Guang
Propylhomoserin, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine
APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Embodiment 4
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 60min, it is then dissolved in 1.4wt% acetum, mixed liquor exists
5000r/h is stirred at 40 DEG C, disperses the quality that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
Than for 2.5:3:42；
（2）Viscous composite is added into atoleine and 4h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
2h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 85:70:0.28:7:5；
（3）2 parts of silicon powder, 4 parts of ball-type silicones micro mist, chitosan/7 parts of attapulgite particulate, half Guang ammonia are weighed by weight
Acid 5 parts, 1 part of APES, 3 parts of citric acid, 1.5 parts of cocounut oil acyl diethanol amine, 2.4 parts of sodium cocoyl glutamate,
90 parts of 4 parts of poly-aspartate, 5 parts of tallow amine APEO and water；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 8min, then add half Guang
Propylhomoserin, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine
APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Embodiment 5
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 50min, it is then dissolved in 1.5wt% acetum, mixed liquor exists
4500r/h is stirred at 40 DEG C, disperses the quality that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
Than for 2.5:2.8:45；
（2）Viscous composite is added into atoleine and 2h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
4h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 82:76:0.25:6:6；
（3）3 parts of silicon powder, 3 parts of ball-type silicones micro mist, chitosan/6 parts of attapulgite particulate, half Guang ammonia are weighed by weight
5 parts of acid, 1.5 parts of APES, 4 parts of citric acid, 1.2 parts of cocounut oil acyl diethanol amine, sodium cocoyl glutamate 1.8
Part, 3 parts of poly-aspartate, 4 parts of tallow amine APEO and 100 parts of water；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 8min, then add half Guang
Propylhomoserin, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine
APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Comparative example 1
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）1 part of silicon powder, 5 parts of ball-type silicones micro mist, 2 parts of chitosan, 4 parts of attapulgite particulate, half Guang are weighed by weight
It is 6 parts of propylhomoserin, 1 part of APES, 2 parts of citric acid, 2 parts of cocounut oil acyl diethanol amine, 1 part of sodium cocoyl glutamate, poly-
80 parts of 1 part of aspartic acid, 6 parts of tallow amine APEO and water；
（2）Silicon powder, ball-type silicones micro mist, chitosan, attapulgite particulate are mixed, ball milling 5min, then add half Guang
Propylhomoserin, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, tallow amine
APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
Comparative example 2
A kind of preparation method of metal-polishing liquid, comprises the following steps：
（1）By chitosan and attapulgite mixing and ball milling 60min, it is then dissolved in 1.5wt% acetum, mixed liquor exists
6000r/h is stirred at 40 DEG C, disperses the quality that 1h obtains viscous composite, wherein chitosan, attapulgite and acetum
Than for 3:4:50；
（2）Viscous composite is added into atoleine and 4h, Ran Houjia is stirred at room temperature in sorbitan fatty ester
Enter formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
5h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite, atoleine, dehydration repeatedly
The mass ratio of sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 90:65:0.3:5:8；
（3）5 parts of silicon powder, chitosan/8 parts of attapulgite particulate, 3 parts of cysteine, alkyl phenol polyoxy second are weighed by weight
120 parts of 2 parts of alkene ether, 5 parts of citric acid, 1 part of cocounut oil acyl diethanol amine, 3 parts of sodium cocoyl glutamate, 5 parts of poly-aspartate and water；
（4）Silicon powder and chitosan/attapulgite particulate are mixed, ball milling 10min, then add cysteine, alkyl phenol gathers
Oxygen vinethene, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate and water, are mixed evenly, i.e.,
Obtain a kind of metal-polishing liquid.
Polishing fluid made from embodiment 1-5 and comparative example 1-2 and commercially available polishing fluid are used in aluminum alloy material surface,
Its using effect is as shown in table 1, and the glossiness of the polishing of this polishing agent and wetting flow leveling compare as can be seen from Table 1
Excellent, cut clearance is high.
The property indices of 1 metal-polishing liquid of the present invention of table
Claims (7)
1. a kind of preparation method of metal-polishing liquid, it is characterised in that comprise the following steps：
（1）Chitosan and attapulgite mixing and ball milling 30-60min are then dissolved in 1-1.5wt% acetum, mixed
Liquid stirs 3000-6000r/h at 40 DEG C, disperses 1h and obtains viscous composite, wherein chitosan, attapulgite and acetic acid is molten
The mass ratio of liquid is 2.5-3:2-4:40-50；
（2）Viscous composite is added into atoleine and 1-4h is stirred at room temperature in sorbitan fatty ester, then
Add formaldehyde and be warming up to 60 DEG C, adjust and stabilising system pH is 10, add glutaraldehyde after reacting 1h and be warming up to 70 DEG C, reaction
2-5h, then extraction washing obtains chitosan/attapulgite clay compounded particulate, wherein viscous composite repeatedly, atoleine, loses
The mass ratio of water sorbitan fatty acid ester, formaldehyde and glutaraldehyde is 75-90:65-85:0.15-0.3:5-7:4-8；
（3）Weigh by weight silicon powder 1-5 parts, ball-type silicones micro mist 2-5 parts, chitosan/attapulgite particulate 4-8 parts,
Cysteine 3-6 parts, APES 1-2 parts, citric acid 2-5 parts, cocounut oil acyl diethanol amine 1-2 parts, cocounut oil acyl paddy
Propylhomoserin sodium 1-3 parts, poly-aspartate 1-5 parts, tallow amine APEO 2-6 parts and water 80-120 parts；
（4）Silicon powder, ball-type silicones micro mist and chitosan/attapulgite particulate are mixed, ball milling 5-10min, then added
Cysteine, APES, citric acid, cocounut oil acyl diethanol amine, sodium cocoyl glutamate, poly-aspartate, ox
Fat amine APEO and water, are mixed evenly, and produce a kind of metal-polishing liquid.
A kind of 2. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（1）Middle chitosan
Average deacetylation >=90%.
A kind of 3. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（1）Middle concave convex rod
Soil for acidifying attapulgite, be acidified attapulgite preparation method be by attapulgite with 37% salt acid soak 24h, Ran Houyan
Honed 200 mesh sieve, is finally eluted with water.
A kind of 4. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（1）Middle chitosan
With attapulgite mixing and ball milling 40-60min, it is then dissolved in 1.5wt% acetum, mixed liquor stirs at 40 DEG C
4000-5000r/h, disperse 1h and obtain viscous composite, wherein chitosan, the mass ratio of attapulgite and acetum is
2.5:2-3:42-48。
A kind of 5. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（2）Middle viscosity is multiple
The mass ratio of condensation material, atoleine, sorbitan fatty ester, formaldehyde and glutaraldehyde is 78-85:70-85:0.22-
0.28:6-7:5-6。
A kind of 6. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（3）By weight
Weigh silicon powder 2-4 parts, ball-type silicones micro mist 2-4 parts, chitosan/attapulgite particulate 5-7 parts, cysteine 4-5 parts, alkane
Base phenol polyethenoxy ether 1-2 parts, citric acid 3-5 parts, cocounut oil acyl diethanol amine 1-1.5 parts, sodium cocoyl glutamate 1.5-2.4
Part, poly-aspartate 2-4 parts, tallow amine APEO 3-5 parts and water 90-110 parts.
A kind of 7. preparation method of metal-polishing liquid according to claim 1, it is characterised in that：Step（4）During middle ball milling
Between be 8min.
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| CN101933906A (en) * | 2010-08-20 | 2011-01-05 | 淮阴工学院 | Preparation method of controlled-release drug-carried composite microsphere with small particle size and high mechanical strength |
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| CN103642397A (en) * | 2013-11-25 | 2014-03-19 | 大连创达技术交易市场有限公司 | Water-soluble light polishing agent used for plastics |
| CN105349999A (en) * | 2015-11-19 | 2016-02-24 | 苏州捷德瑞精密机械有限公司 | Environment-friendly polishing solution and preparation method thereof |
| CN105344329A (en) * | 2015-11-30 | 2016-02-24 | 武汉科技大学 | Graphene oxide and chitosan microsphere and preparation method thereof |
| CN106318222A (en) * | 2016-08-18 | 2017-01-11 | 江苏锦阳不锈钢制品有限公司 | Method for preparing high-precision polishing solution |
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2017
- 2017-11-21 CN CN201711165427.7A patent/CN107779877A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101933906A (en) * | 2010-08-20 | 2011-01-05 | 淮阴工学院 | Preparation method of controlled-release drug-carried composite microsphere with small particle size and high mechanical strength |
| CN102516882A (en) * | 2011-12-19 | 2012-06-27 | 德米特（苏州）电子环保材料有限公司 | Method for making resin lens polishing solution of alumina matrix |
| CN103642397A (en) * | 2013-11-25 | 2014-03-19 | 大连创达技术交易市场有限公司 | Water-soluble light polishing agent used for plastics |
| CN105349999A (en) * | 2015-11-19 | 2016-02-24 | 苏州捷德瑞精密机械有限公司 | Environment-friendly polishing solution and preparation method thereof |
| CN105344329A (en) * | 2015-11-30 | 2016-02-24 | 武汉科技大学 | Graphene oxide and chitosan microsphere and preparation method thereof |
| CN106318222A (en) * | 2016-08-18 | 2017-01-11 | 江苏锦阳不锈钢制品有限公司 | Method for preparing high-precision polishing solution |
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Application publication date: 20180309 |