CN107771945A - A kind of formula milk and its manufacture method for helping to improve middle-aged and old sleep qualities - Google Patents
A kind of formula milk and its manufacture method for helping to improve middle-aged and old sleep qualities Download PDFInfo
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- CN107771945A CN107771945A CN201711025825.9A CN201711025825A CN107771945A CN 107771945 A CN107771945 A CN 107771945A CN 201711025825 A CN201711025825 A CN 201711025825A CN 107771945 A CN107771945 A CN 107771945A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/16—Agglomerating or granulating milk powder; Making instant milk powder; Products obtained thereby
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1522—Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1526—Amino acids; Peptides; Protein hydrolysates; Nucleic acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/156—Flavoured milk preparations ; Addition of fruits, vegetables, sugars, sugar alcohols or sweeteners
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/158—Milk preparations; Milk powder or milk powder preparations containing additives containing vitamins or antibiotics
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Abstract
A kind of formula milk and its production method for helping to improve middle-aged and old sleep qualities, formula composition is by weight percentage, basic ingredient is made a living one or more sum >=70% in newborn ox/sheep, full-cream ox/goat milk powder, skimmed milk power, desalted whey powder, PURE WHEY and lactose, lactoalbumin=0.3~3, tealeaves theanine=0.1~1.0, casein hydrolysate peptides=0.05~0.5, Wild jujube seeds extract=0.1~1.The one or more of following material are additionally added in formula composition:WPC=1~10, oligoisomaltose=5~12, maltodextrin=5~20, calcium carbonate=0.8~1.8.Processing step includes:After all nutriment mixed dissolutions such as lactogenesis/whole milk powder and skimmed milk power, WPC, tealeaves theanine, lactoalbumin, dairy products original washing powder is formed after homogeneous, sterilization, concentration, spray drying, then carries out the formula milk that packaging is made required.
Description
Technical field
The present invention is formula milk processing and fabricating technical field, and being related to a kind of helps to improve middle-aged and old sleep qualities
Formula milk and its manufacture method.
Background technology
It is extremely important with health to physical recovery to possess a good sleep.But with the increase at age, the elderly
Sleep quality has the trend being gradually reduced.Research shows, in more than 60 years old the elderly the prevalence rate of sleep-disorder be 30%~
40%, its illness rate increases and increased with the age.Sleep it is bad health is damaged, body immune function reduction, add
Fast aging and decrease of memory.
The content of the invention
The present invention is intended to provide a kind of formula milk and its manufacture method for helping to improve middle-aged and old sleep qualities, food
With the milk powder sleep quality can be allowed bad or insomnia crowd helps improve sleep quality and can be eaten for a long time.
Technical scheme:
A kind of formula milk for helping to improve middle-aged and old sleep qualities, formula form by weight percentage, basic ingredient
Ox/sheep of making a living is newborn, the one or more in full-cream ox/goat milk powder, skimmed milk power, desalted whey powder, PURE WHEY and lactose
Sum >=70%, lactoalbumin=0.3~3, tealeaves theanine=0.1~1.0, casein hydrolysate peptides=0.05~0.5, spina date seed carry
Take thing=0.1~1.
The one or more of following material can also be added in formula composition:WPC=1~10, it is oligomeric different
Maltose=5~12, maltodextrin=5~20, calcium carbonate=0.8~1.8.
A certain amount of composite nutrient can also be added in formula milk.The vitamin that composite nutrient usually contains has dimension
It is several in raw plain A, vitamin B1, vitamin B6, vitamin C, vitamin D, vitamin E, folic acid and L carnitines;
Generally conserved in composite nutrient several in the trace element such as iron, magnesium, zinc, manganese, sodium.
This product is not suitable for infant and used.
According to a kind of manufacture for helping to improve the formula milk of middle-aged and old sleep qualities of above-mentioned formula compositing range
Method, comprise the following steps that:
(1)Dispensing and pretreatment:By setting formula composition, the sequencing into the bulk raw material in dispensing shear cylinder is followed successively by
Desalted whey powder, lactose, fresh milk or whole milk powder, skimmed milk power, PURE WHEY, oligoisomaltose, tealeaves theanine, breast
Albumin, 35~70 DEG C of water temperature;Compounded in the small powder pill tank of belt stirrer with 10~20 times, 40~60 DEG C of dissolved in purified water
Shearing tank is added after mineral matter, fully dissolving;Again with 10~20 times, 25~50 DEG C of dissolved in purified water B B-complexes, stirring 3~
It is slowly added to after 5min in constant volume tank.
(2)Homogeneous:40~60 DEG C of homogenizing temperature, 10~25Mpa of pressure.
(3)Sterilization:85~95 DEG C, 10~15s of time of sterilization temperature, feed temperature control is below 20 DEG C after sterilization.
(4)Concentration:90~110 DEG C of sterilization temperature during concentration, 10~20s of time;Be concentrated in vacuo discharge concentration control with
The square Baume degrees of milk powder 9~21, dense 20~55 DEG C of milk drop temperature.
(5)Spray drying:110~185 DEG C of EAT, 60~90 DEG C of temperature of outgoing air, goes out powder temperature≤25 DEG C, product water
Divide≤4.0%.
(6)Packaging:Finished product, product moisture≤5.0%.
Inventive principle:
Lactoalbumin helps to alleviate pressure and improves sleep, improves abstract visual memory.Clinical research shows, lactoalbumin
In α-la contain substantial amounts of tryptophan, tryptophan is the precursor substance of serotonin in the brain, and serotonin has help
The ability that human body eases off the pressure, so α-la can improve the sleep of trophic disturbance crowd.
The substantial amounts of tealeaves theanine of naturally occurring in green tea.Tealeaves theanine is a kind of amino of unique free form
Acid, its active amino acid are L-thiamine.L-thiamine is a kind of relaxant, mood can be promoted to loosen, and make for good health sleep.
Theanine can suppress nerve cell death caused by transient cerebral ischemia, have protective effect to nerve cell, and it can reduce MDA contents
So as to reduce lipid peroxidation, promote the function of central cholinergic system, reach raising memory, the purpose of anti-aging.
Casein hydrolysate peptides are ten peptides that casein hydrolysis obtain, and have antianxiety or antidepressant effect.It can increase
Strong memory, the state of mind is improved, is focused on, sleep quality decline is improved, alleviates pressure, control body weight, beautifying face and moistering lotion.
The anti-fatigue effect that addition casein hydrolysate peptides milk powder is evaluated by zoopery shows:Casein hydrolysate peptides and addition casein
The milk powder of range of hydrolysed peptides extends mouse swimming time, reduces blood lactase acid, urea nitrogen content, improves hepatic glycogen content, show
Certain antifatigue effect, the generation of delay fatigue.
Spina date seed is traditional Chinese medicine simply, has tranquilizing soporific, antitumor, regulation blood fat and other effects.Chinese earliest one
Portion's medicine book《Sheng Nong's herbal classic》Described in:" bowl spares benefit liver, hard muscles and bones, help the work(of cloudy gas, all spina date seed." Ming Dynasty's Li Shizhen
《Compendium of Materia Medica》Described in, " ripe with treatment, insomnia due to insufficiency of the gallbladder-qi, the disease of polydipsia abnormal sweating for jujube kernel;Raw to be slept well with treatment gallbladder-heat, all foot is fainted cloudy few
Positive medicine.Spina date seed is the seed of wild jujube, can make after processing medicinal, and it contains alkaloid, several amino acids and metallic element
Deng composition, the effect such as antitoxic heart-soothing and sedative, bowl spares nourishing the liver, arrest sweating can be played, to illnesss such as restlessness of asrhenia type and insomnia, palpitation with fear palpitation, physically weak spontaneous perspirations
There is preferable therapeutic effect.
This product is not suitable for infant and used.
Beneficial effects of the present invention:The present invention adds lactoalbumin, tealeaves theanine, casein hydrolysis in formula milk
Peptide(Light peptide), Spine Date Seed/extract, sleep quality can be made bad or insomnia people crowd improves and sleep quality and can grown
Phase eats non-toxic side effect.
Embodiment
Illustrate with reference to embodiments.
Embodiment 1
Formula milk, composition are by weight percentage:Skimmed milk power 30, whole milk powder(Contained with dosage during lactogenesis by dry
Amount conversion)30, desalted whey powder 20, WPC 5, oligoisomaltose 5, maltodextrin 5, calcium carbonate 1.5, milky white egg
White 1, tealeaves theanine 0.8, casein hydrolysate peptides 0.2, Wild jujube seeds extract 1, after the dissolving of above material mixing, add containing dimension
The nutrient bag 0.5 of raw element and trace element(Containing vitamin A, vitamin D, vitamin E, vitamin, iron, magnesium, zinc, left-handed meat
Alkali), in 50 degrees Celsius of mixing, the then homogeneous under the conditions of 45 degrees Celsius of temperature, pressure 18Mpa, then high temperature sterilization, then concentrate,
It is spray-dried to obtain milk powder original washing powder 100KG again, then be packaged into different size help sleep milk powder.
(1)Dispensing and pretreatment:By the formula of each product, into the bulk raw material in dispensing shear cylinder sequencing according to
It is secondary for desalted whey powder, lactose, whole milk powder, skimmed milk power, oligoisomaltose, maltodextrin, lactoalbumin, tealeaves tea ammonia
Acid, casein hydrolysate peptides, Wild jujube seeds extract, calcium carbonate etc., 55 DEG C of water temperature.With 15 in the small powder pill tank of belt stirrer
Again, 50 DEG C of dissolved in purified water compounding mineral matters, if fully shear tank after dissolving;Again with 10 times, 25 DEG C of dissolved in purified water it is compound
Vitamin, it is slowly added in constant volume tank after mixing time 5min.
(2)Homogeneous:Temperature 50 C, homogenization pressure 18Mpa.
(3)Sterilization:91 DEG C, time 12s of sterilization temperature, feed temperature control is below 20 DEG C after sterilization.
(4)Concentration:105 DEG C of sterilization temperature during concentration, time 16s;It is concentrated in vacuo:Product material discharge concentration control with
The square Baume degrees of milk powder 15, dense 35 DEG C of milk drop temperature.
(5)Spray drying:EAT:165 DEG C, temperature of outgoing air:70 DEG C, go out 20 DEG C of powder temperature, product moisture 3.5%.
(6)Packaging:Finished product, the % of product moisture 3.5.
Embodiment 2
Formula milk, composition are by weight percentage:Full-cream goat milk powder 40, skimmed milk power 20, maltodextrin 10, desalted whey
Powder 10, WPC 5, oligoisomaltose 9.8, calcium carbonate 1, lactoalbumin 2.5, tealeaves theanine 0.5, casein water
Solve peptide 0.1, Wild jujube seeds extract 0.5.After the dissolving of above material mixing, the nutrient bag containing vitamin and trace element is added
0.5(Containing vitamin A, vitamin D, vitamin E, vitamin, iron, magnesium, zinc, l-cn), mixed at 50 DEG C, then in temperature
45 DEG C, homogeneous under the conditions of pressure 18Mpa, then high temperature sterilization, then concentrate, then be spray-dried to obtain milk powder original washing powder, then be packaged into not
Same specification helps sleep goat milk powder.
(1)Dispensing and pretreatment:By the formula of each product, into the bulk raw material in dispensing shear cylinder sequencing according to
It is secondary for desalted whey powder, lactose, whole milk powder, skimmed milk power, oligoisomaltose, lactoalbumin, tealeaves theanine, casein
Range of hydrolysed peptides, Wild jujube seeds extract, calcium carbonate etc., 52 DEG C of water temperature.In the small powder pill tank of belt stirrer with 10 times, 40 DEG C it is pure
Water dissolving compounding mineral matter, fully adds shearing tank after dissolving;Again with 10 times, 25 DEG C of dissolved in purified water B B-complexes, stirring
It is slowly added to after 5min in constant volume tank.
(2)Homogeneous:40 DEG C of temperature, homogenization pressure 12Mpa.
(3)Sterilization:91 DEG C, time 12s of sterilization temperature, feed temperature control is below 20 DEG C after sterilization.
(4)Concentration:103 DEG C of sterilization temperature during concentration, time 16s;It is concentrated in vacuo:Product material discharge concentration control with
The square Baume degrees of milk powder 15, dense 30 DEG C of milk drop temperature.
(5)Spray drying:EAT:155 DEG C, temperature of outgoing air:65 DEG C, go out 20 DEG C of powder temperature, product moisture 3.0%.
(6)Packaging:Finished product, the %. of product moisture 3.0.
Embodiment 3
Formula milk, composition are by weight percentage:Whole milk powder(Converted with dosage during lactogenesis by dry matter content)28, take off
Fat milk powder 22, desalted whey powder 25, oligoisomaltose 10, maltodextrin 12, PURE WHEY 1, calcium carbonate 0.8, milky white egg
White 0.1, tealeaves theanine 0.2, casein hydrolysate peptides 0.3, Wild jujube seeds extract 0.1.After the dissolving of above material mixing, addition contains
There is the nutrient bag 0.5 of vitamin, mineral trace element(Containing vitamin A, vitamin D, vitamin E, vitamin, iron, magnesium,
Zinc, l-cn), in 50 DEG C of mixing, the then homogeneous under the conditions of temperature 50 C, pressure 18Mpa, then high temperature sterilization, then concentrate,
It is spray-dried to obtain milk powder original washing powder again, is then packaged into inner wrapping, produces matching somebody with somebody for a kind of women beauty fat reducing and healthy reproduction
Square goat milk powder.
(1)Dispensing and pretreatment:By the formula of each product, into the bulk raw material in dispensing shear cylinder sequencing according to
It is secondary for desalted whey powder, lactose, whole milk powder, skimmed milk power, oligoisomaltose, lactoalbumin, tealeaves theanine, casein
Range of hydrolysed peptides, Wild jujube seeds extract, calcium carbonate etc., 60 DEG C of water temperature.In the small powder pill tank of belt stirrer with 20 times, 60 DEG C it is pure
Water dissolving compounding mineral matter, if fully shear tank after dissolving;Again with 20 times, 40 DEG C of dissolved in purified water B B-complexes, stirring
It is slowly added to after 3min in constant volume tank.
(2)Homogeneous:Temperature 60 C, homogenization pressure 25Mpa.
(3)Sterilization:95 DEG C, time 15s of sterilization temperature, feed temperature control is below 20 DEG C after sterilization.
(4)Concentration:106 DEG C of sterilization temperature during concentration, time 10s;It is concentrated in vacuo:Product material discharge concentration control with
The square Baume degrees of milk powder 18, dense 50 DEG C of milk drop temperature.
(5)Spray drying:EAT:178 DEG C, temperature of outgoing air:85 DEG C, go out 20 DEG C of powder temperature, product moisture 2.5%.
(6)Packaging:Finished product, the % of product moisture 2.5.
Claims (3)
- A kind of 1. formula milk for helping to improve middle-aged and old sleep qualities, it is characterised in that:Formula composition percentage by weight Than meter, basic ingredient is made a living in newborn ox/sheep, full-cream ox/goat milk powder, skimmed milk power, desalted whey powder, PURE WHEY and lactose One or more sum >=70%, lactoalbumin=0.3~3, tealeaves theanine=0.1~1.0, casein hydrolysate peptides=0.05~ 0.5, Wild jujube seeds extract=0.1~1.
- A kind of 2. formula milk for helping to improve middle-aged and old sleep qualities according to claim 1, it is characterised in that: The one or more of following material are additionally added in formula composition:WPC=1~10, oligoisomaltose=5~12, Maltodextrin=5~20, calcium carbonate=0.8~1.8.
- 3. a kind of formula milk for helping to improve middle-aged and old sleep qualities of compositing range is formulated according to claim 1 or 2 Production method, comprise the following steps that:(1)Dispensing and pretreatment:By setting formula composition, the sequencing into the bulk raw material in dispensing shear cylinder is followed successively by Desalted whey powder, lactose, fresh milk or whole milk powder, skimmed milk power, PURE WHEY, oligoisomaltose, tealeaves theanine, breast Albumin, 35~70 DEG C of water temperature;Compounded in the small powder pill tank of belt stirrer with 10~20 times, 40~60 DEG C of dissolved in purified water Shearing tank is added after mineral matter, fully dissolving;Again with 10~20 times, 25~50 DEG C of dissolved in purified water B B-complexes, stirring 3~ It is slowly added to after 5min in constant volume tank;(2)Homogeneous:40~60 DEG C of homogenizing temperature, 10~25Mpa of pressure;(3)Sterilization:85~95 DEG C, 10~15s of time of sterilization temperature, feed temperature control is below 20 DEG C after sterilization;(4)Concentration:90~110 DEG C of sterilization temperature during concentration, 10~20s of time;Discharge concentration control is concentrated in vacuo in laboratory milk The Baume degrees of powder 9~21, dense 20~55 DEG C of milk drop temperature;(5)Spray drying:110~185 DEG C of EAT, 60~90 DEG C of temperature of outgoing air go out powder temperature≤25 DEG C, and product moisture≤ 4.0%;(6)Packaging:Finished product, product moisture≤5.0%.
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Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110623073A (en) * | 2019-10-15 | 2019-12-31 | 卜球 | Formula milk powder beneficial to body height and preparation method thereof |
CN110651830A (en) * | 2019-09-29 | 2020-01-07 | 澳优乳业(中国)有限公司 | Modified milk powder for improving sleep and preparation method thereof |
CN110651827A (en) * | 2019-11-07 | 2020-01-07 | 吴元昱 | Sleep-aiding pre-sleep yoghourt and preparation method thereof |
CN111670953A (en) * | 2019-03-10 | 2020-09-18 | 王莉 | Camel milk powder and small molecular peptide formula milk powder |
CN111869731A (en) * | 2020-07-24 | 2020-11-03 | 杭州利项科技有限公司 | Milk powder capable of improving sleep quality and production equipment and production method thereof |
CN112042757A (en) * | 2020-09-15 | 2020-12-08 | 四川金汇源农业科技有限责任公司 | Milk powder formula beneficial to improving sleep and preparation method thereof |
CN112136898A (en) * | 2020-09-21 | 2020-12-29 | 上海民河生物科技有限公司 | Formula milk powder for improving sleep and nourishing brain to calm nerves and preparation method thereof |
CN112189711A (en) * | 2020-10-30 | 2021-01-08 | 广州市美素力营养品有限公司 | Milk powder for assisting in reducing hypertension, hyperglycemia and hyperlipidemia of middle-aged and old people |
CN113349381A (en) * | 2021-06-02 | 2021-09-07 | 橡果美健实业投资股份有限公司 | Food composition capable of relieving depression and preparation method thereof |
CN113575692A (en) * | 2021-08-06 | 2021-11-02 | 西安百跃羊乳集团有限公司 | Goat milk powder for promoting sleep and preparation method thereof |
CN113995017A (en) * | 2021-10-28 | 2022-02-01 | 江西人之初乳品营养有限公司 | Modified milk powder for improving sleep and preparation method thereof |
CN114009509A (en) * | 2021-11-15 | 2022-02-08 | 吴兆盈 | Formula milk powder capable of improving immunity, strengthening muscles and bones and assisting sleep and preparation method of formula milk powder |
CN115299501A (en) * | 2022-08-11 | 2022-11-08 | 美庐生物科技股份有限公司 | Preparation method of milk powder for improving sleep and product thereof |
CN115669945A (en) * | 2022-10-24 | 2023-02-03 | 上海艾斯顿医疗科技有限公司 | Liposome-coated polypeptide with neurotrophic effect, and preparation method and application thereof |
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Cited By (16)
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CN111670953A (en) * | 2019-03-10 | 2020-09-18 | 王莉 | Camel milk powder and small molecular peptide formula milk powder |
CN110651830B (en) * | 2019-09-29 | 2023-03-24 | 澳优乳业(中国)有限公司 | Modified milk powder for improving sleep and preparation method thereof |
CN110651830A (en) * | 2019-09-29 | 2020-01-07 | 澳优乳业(中国)有限公司 | Modified milk powder for improving sleep and preparation method thereof |
CN110623073A (en) * | 2019-10-15 | 2019-12-31 | 卜球 | Formula milk powder beneficial to body height and preparation method thereof |
CN110651827A (en) * | 2019-11-07 | 2020-01-07 | 吴元昱 | Sleep-aiding pre-sleep yoghourt and preparation method thereof |
CN111869731A (en) * | 2020-07-24 | 2020-11-03 | 杭州利项科技有限公司 | Milk powder capable of improving sleep quality and production equipment and production method thereof |
CN112042757A (en) * | 2020-09-15 | 2020-12-08 | 四川金汇源农业科技有限责任公司 | Milk powder formula beneficial to improving sleep and preparation method thereof |
CN112136898A (en) * | 2020-09-21 | 2020-12-29 | 上海民河生物科技有限公司 | Formula milk powder for improving sleep and nourishing brain to calm nerves and preparation method thereof |
CN112189711A (en) * | 2020-10-30 | 2021-01-08 | 广州市美素力营养品有限公司 | Milk powder for assisting in reducing hypertension, hyperglycemia and hyperlipidemia of middle-aged and old people |
CN113349381A (en) * | 2021-06-02 | 2021-09-07 | 橡果美健实业投资股份有限公司 | Food composition capable of relieving depression and preparation method thereof |
CN113575692A (en) * | 2021-08-06 | 2021-11-02 | 西安百跃羊乳集团有限公司 | Goat milk powder for promoting sleep and preparation method thereof |
CN113995017A (en) * | 2021-10-28 | 2022-02-01 | 江西人之初乳品营养有限公司 | Modified milk powder for improving sleep and preparation method thereof |
CN114009509A (en) * | 2021-11-15 | 2022-02-08 | 吴兆盈 | Formula milk powder capable of improving immunity, strengthening muscles and bones and assisting sleep and preparation method of formula milk powder |
CN115299501A (en) * | 2022-08-11 | 2022-11-08 | 美庐生物科技股份有限公司 | Preparation method of milk powder for improving sleep and product thereof |
CN115669945A (en) * | 2022-10-24 | 2023-02-03 | 上海艾斯顿医疗科技有限公司 | Liposome-coated polypeptide with neurotrophic effect, and preparation method and application thereof |
CN115669945B (en) * | 2022-10-24 | 2024-03-08 | 上海艾斯顿医疗科技有限公司 | Liposome-coated polypeptide with neurotrophic effect, and preparation method and application thereof |
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