CN107754372A - The separation equipment of the active ingredient of natural drug - Google Patents

The separation equipment of the active ingredient of natural drug Download PDF

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Publication number
CN107754372A
CN107754372A CN201711158018.4A CN201711158018A CN107754372A CN 107754372 A CN107754372 A CN 107754372A CN 201711158018 A CN201711158018 A CN 201711158018A CN 107754372 A CN107754372 A CN 107754372A
Authority
CN
China
Prior art keywords
pot
solvent extraction
active ingredient
reaction vessel
filter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201711158018.4A
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Chinese (zh)
Inventor
程真勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Chengdu Fowles Medical Technology Co Ltd
Original Assignee
Chengdu Fowles Medical Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chengdu Fowles Medical Technology Co Ltd filed Critical Chengdu Fowles Medical Technology Co Ltd
Priority to CN201711158018.4A priority Critical patent/CN107754372A/en
Publication of CN107754372A publication Critical patent/CN107754372A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

The invention discloses the separation equipment of the active ingredient of natural drug, including pot for solvent extraction, the bottom of the pot for solvent extraction is provided with heater, thermometer, at least one feed tube connected with pot for solvent extraction is set in the side wall of pot for solvent extraction, the pot for solvent extraction is internally provided with hollow filter ball, the ball wall of the filter ball is filter screen, the rotating shaft placed vertically is connected with above filter ball, the drive device of drive shaft rotation is connected with the top of rotating shaft, multiple drain pipes are provided with below pot for solvent extraction, the top of the drain pipe connects with pot for solvent extraction, the bottom of drain pipe is communicated with reaction vessel, reaction vessel is placed on magnetic stirring apparatus, the control valve of control drain pipe conducting is provided with inside all drain pipes.The present invention can just extract plurality of active ingredients by changing the solvent added in pot for solvent extraction, solve the problems, such as the extraction that active ingredient is carried out to peach leaf.

Description

The separation equipment of the active ingredient of natural drug
Technical field
The present invention relates to a kind of extraction element, and in particular to the separation equipment of the active ingredient of natural drug.
Background technology
Peach leaf is the leaf of rosaceous plant peach (Prunus.persica (L) Batsch), and the whole nation is extensively distributed.Peach leaf has There is good medical value, in peach leaf among the people as the existing history remote of folk prescription for treating for example disease such as prickly heat.In Herbal chemistry is analyzed, and peach leaf contains lycopene (lycopene), naringenin (Naringenin) and quininic acid (Quinic The effective medicinal components such as acid).
The Development volue of peach leaf is considerable, but the utilization of peach leaf still are limited in Traditional Chinese Medicine method at this stage, Various decoctions and decoction are mainly made into Chinese medicine to treat various diseases.Peach leaf is allowed to certainly after fruit harvesting at present So come off in orchard as fertilizer, not yet carry out the industrialized production development of extracts active ingredients, main cause is to fail so far Economically and reasonably extraction process is worked out, peach leaf extracts active ingredients are come out into the bulk drug or health products as pharmaceuticals industry The functional component of industry.
The content of the invention
Traditional equipment for decocting Chinese traditional herb medicines can not extract the active ingredient in peach leaf during the technical problems to be solved by the invention, Purpose is the separation equipment for the active ingredient for providing natural drug, solves the problems, such as the extraction that active ingredient is carried out to peach leaf.
The present invention is achieved through the following technical solutions:
The separation equipment of the active ingredient of natural drug, including pot for solvent extraction, the bottom of the pot for solvent extraction are provided with heating dress Put, thermometer, at least one feed tube connected with pot for solvent extraction is set in the side wall of pot for solvent extraction, the pot for solvent extraction is internally provided with Hollow filter ball, the ball wall of the filter ball is filter screen, and the rotating shaft placed vertically, the top of rotating shaft are connected with above filter ball Portion is connected with the drive device of drive shaft rotation, and multiple drain pipes, the top of the drain pipe are provided with below pot for solvent extraction Connected with pot for solvent extraction, the bottom of drain pipe is communicated with reaction vessel, and reaction vessel is placed on magnetic stirring apparatus, all drain pipes Inside is provided with the control valve of control drain pipe conducting.
Pot for solvent extraction is used to extract the plurality of active ingredients in peach leaf, reaction vessel and magnetic stirring apparatus cooperation pair in the present invention The filtrate extracted in pot for solvent extraction carries out concentration and obtains natural constituent;The present invention realization principle be:The present invention is traditional The improvement in structure has been carried out to pot for solvent extraction on pot for solvent extraction, reaction vessel is with the addition of on pot for solvent extraction, can be timely and effectively right A variety of filtrates are concentrated, and shorten the drain time of pot for solvent extraction, improve the production efficiency of pot for solvent extraction;The present invention changes leaching Carry the agitating device inside tank;The present invention uses container containing of the filter ball as peach leaf powder, does not interfere with molten in pot for solvent extraction Agent contact with peach leaf powder, in rotating shaft rotary course, the contact area of peach leaf powder and solvent can be increased, additionally it is possible to right Filter residue is filtered, and is easy to separate filter residue and filtrate, and the separation of filter residue and filtrate is difficult in existing pot for solvent extraction, and separation is endless Entirely;The present invention realization principle be:By peach leaf powder in filter ball, the first solvent is added into pot for solvent extraction, opens and adds Thermal, while the drive device of opening of rotary shaft, rotating shaft rotation drive filter ball rotation so that peach leaf powder and the first solvent Fully contact and dissolve, after a period of time, the solution in pot for solvent extraction is passed into a reaction vessel and carries out concentration and obtains the A kind of active ingredient;After liquid in pot for solvent extraction is drained, second of solvent is added into pot for solvent extraction and carries out second of active ingredient Extraction, it is identical with the first extracts active ingredients step;A kind of upper active ingredient is in concentration process, it becomes possible to lower one kind Active ingredient is extracted, and extraction efficiency is high, and time cost is few.The present invention just can by changing the solvent added in pot for solvent extraction Plurality of active ingredients is extracted, solves the problems, such as the extraction that active ingredient is carried out to peach leaf;The present invention is by peach leaf powder using filtering Ball loads, and the rate of filtration is fast, it is not necessary to uses single filter;The present invention has connected pot for solvent extraction with reaction vessel Come, another active ingredient is extracted while a kind of active ingredient can be extracted, production efficiency is high.
The reaction vessel is the flask with upper lid, and connection reaction vessel and the external world are provided with the upper lid of reaction vessel Steam pipe.Steam pipe is used to discharge caused steam in reaction vessel concentration process, is easy to condense and collect steam.
The inner bottom part of pot for solvent extraction is provided with the filter for coating pot for solvent extraction bottom surface completely, and the filter is located at filter ball Between drain pipe.Filter serves further filtration, improves the purity of filtrate.
Three feed tubes are provided with the pot for solvent extraction, three drain pipes are provided with below pot for solvent extraction.It is general in peach leaf Lycopene, naringenin, quininic acid these three active ingredients are extracted, three feed tubes are provided with pot for solvent extraction, separate solubilizer, Be advantageous to keep the purity of solvent, avoid cross-infection between different solvents.
The drive device of rotating shaft is motor.
The present invention compared with prior art, has the following advantages and advantages:
1st, the separation equipment of the active ingredient of natural drug of the present invention just can by changing the solvent added in pot for solvent extraction Plurality of active ingredients is extracted, solves the problems, such as the extraction that active ingredient is carried out to peach leaf;
2nd, the separation equipment of the active ingredient of natural drug of the present invention loads peach leaf powder using filter ball, crosses filtering velocity Degree is fast, it is not necessary to uses single filter;
3rd, the separation equipment of the active ingredient of natural drug of the present invention connects pot for solvent extraction with reaction vessel, Neng Gouti Another active ingredient is extracted while taking a kind of active ingredient, production efficiency is high.
Brief description of the drawings
Accompanying drawing described herein is used for providing further understanding the embodiment of the present invention, forms one of the application Point, do not form the restriction to the embodiment of the present invention.In the accompanying drawings:
Fig. 1 is schematic structural view of the invention.
Mark and corresponding parts title in accompanying drawing:
1- pot for solvent extraction, 2- heaters, 3- thermometers, 4- feed tubes, 5- filter balls, 6- rotating shafts, 7- drain pipes, 8- reactions Container, 9- magnetic stirring apparatus, 10- control valves, 11- filters.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment and accompanying drawing, to this Invention is described in further detail, and exemplary embodiment of the invention and its explanation are only used for explaining the present invention, do not make For limitation of the invention.
Embodiment 1
As shown in figure 1, the separation equipment of the active ingredient of natural drug of the present invention, including pot for solvent extraction 1, the pot for solvent extraction 1 Bottom be provided with heater 2, thermometer 3, at least one feed liquor connected with pot for solvent extraction 1 is set in the side wall of pot for solvent extraction 1 Pipe 4, the pot for solvent extraction 1 are internally provided with hollow filter ball 5, and the ball wall of the filter ball 5 is filter screen, the top of filter ball 5 The rotating shaft 6 placed vertically is connected with, the top of rotating shaft 6 is connected with the drive device of the rotation of drive shaft 6, the lower section of pot for solvent extraction 1 Multiple drain pipes 7 are provided with, the top of the drain pipe 7 connects with pot for solvent extraction 1, and the bottom of drain pipe 7 is communicated with reaction vessel 8, reaction vessel 8 is placed on magnetic stirring apparatus 9, and the control valve that control drain pipe 7 turns on is provided with inside all drain pipes 7 10.Three feed tubes 4 are provided with the pot for solvent extraction 1, the lower section of pot for solvent extraction 1 is provided with three drain pipes 7.The driving of rotating shaft 6 Device is motor.The inner bottom part of pot for solvent extraction 1 is provided with the filter 11 for coating the bottom surface of pot for solvent extraction 1 completely, the filter 11 Between filter ball 5 and drain pipe 7.
Pot for solvent extraction is used to extract the plurality of active ingredients in peach leaf, reaction vessel and magnetic stirring apparatus cooperation pair in the present invention The filtrate extracted in pot for solvent extraction carries out concentration and obtains natural constituent;The present invention realization principle be:The present invention is traditional The improvement in structure has been carried out to pot for solvent extraction on pot for solvent extraction, reaction vessel is with the addition of on pot for solvent extraction, can be timely and effectively right A variety of filtrates are concentrated, and shorten the drain time of pot for solvent extraction, improve the production efficiency of pot for solvent extraction;The present invention changes leaching Carry the agitating device inside tank;The present invention uses container containing of the filter ball as peach leaf powder, does not interfere with molten in pot for solvent extraction Agent contact with peach leaf powder, in rotating shaft rotary course, the contact area of peach leaf powder and solvent can be increased, additionally it is possible to right Filter residue is filtered, and is easy to separate filter residue and filtrate, and the separation of filter residue and filtrate is difficult in existing pot for solvent extraction, and separation is endless Entirely;The present invention realization principle be:By peach leaf powder in filter ball, the first solvent is added into pot for solvent extraction, opens and adds Thermal, while the drive device of opening of rotary shaft, rotating shaft rotation drive filter ball rotation so that peach leaf powder and the first solvent Fully contact and dissolve, after a period of time, the solution in pot for solvent extraction is passed into a reaction vessel and carries out concentration and obtains the A kind of active ingredient;After liquid in pot for solvent extraction is drained, second of solvent is added into pot for solvent extraction and carries out second of active ingredient Extraction, it is identical with the first extracts active ingredients step;A kind of upper active ingredient is in concentration process, it becomes possible to lower one kind Active ingredient is extracted, and extraction efficiency is high, and time cost is few.The present invention just can by changing the solvent added in pot for solvent extraction Plurality of active ingredients is extracted, solves the problems, such as the extraction that active ingredient is carried out to peach leaf;The present invention is by peach leaf powder using filtering Ball loads, and the rate of filtration is fast, it is not necessary to uses single filter;The present invention has connected pot for solvent extraction with reaction vessel Come, another active ingredient is extracted while a kind of active ingredient can be extracted, production efficiency is high.
Embodiment 2
Based on embodiment 1, the reaction vessel 8 is the flask with upper lid, and connection is provided with the upper lid of reaction vessel 8 Reaction vessel 8 and extraneous steam pipe.Steam pipe is used to discharge caused steam in reaction vessel concentration process, is easy to condensation simultaneously Collect steam.
Above-described embodiment, the purpose of the present invention, technical scheme and beneficial effect are carried out further Describe in detail, should be understood that the embodiment that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc., all should include Within protection scope of the present invention.

Claims (5)

1. the separation equipment of the active ingredient of natural drug, including pot for solvent extraction (1), it is characterised in that the bottom of the pot for solvent extraction (1) Portion is provided with heater (2), thermometer (3), sets and at least one is connected with pot for solvent extraction (1) in the side wall of pot for solvent extraction (1) Feed tube (4), the pot for solvent extraction (1) are internally provided with hollow filter ball (5), and the ball wall of the filter ball (5) is filter screen, mistake The rotating shaft (6) placed vertically is connected with above filter bulb (5), the driving of drive shaft (6) rotation is connected with the top of rotating shaft (6) Device, multiple drain pipes (7) is provided with below pot for solvent extraction (1), the top of the drain pipe (7) connects with pot for solvent extraction (1), gone out The bottom of liquid pipe (7) is communicated with reaction vessel (8), and reaction vessel (8) is placed on magnetic stirring apparatus (9), all drain pipes (7) Inside is provided with the control valve (10) of control drain pipe (7) conducting.
2. the separation equipment of the active ingredient of natural drug according to claim 1, it is characterised in that the reaction vessel (8) it is the flask with upper lid, connection reaction vessel (8) and extraneous steam pipe is provided with the upper lid of reaction vessel (8).
3. the separation equipment of the active ingredient of natural drug according to claim 1, it is characterised in that pot for solvent extraction (1) Inner bottom part is provided with the filter (11) for coating pot for solvent extraction (1) bottom surface completely, the filter (11) be located at filter ball (5) with Between drain pipe (7).
4. the separation equipment of the active ingredient of natural drug according to claim 1, it is characterised in that the pot for solvent extraction (1) three feed tubes (4) are provided with, three drain pipes (7) are provided with below pot for solvent extraction (1).
5. the separation equipment of the active ingredient of natural drug according to claim 1, it is characterised in that the drive of rotating shaft (6) Dynamic device is motor.
CN201711158018.4A 2017-11-20 2017-11-20 The separation equipment of the active ingredient of natural drug Withdrawn CN107754372A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711158018.4A CN107754372A (en) 2017-11-20 2017-11-20 The separation equipment of the active ingredient of natural drug

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711158018.4A CN107754372A (en) 2017-11-20 2017-11-20 The separation equipment of the active ingredient of natural drug

Publications (1)

Publication Number Publication Date
CN107754372A true CN107754372A (en) 2018-03-06

Family

ID=61280160

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711158018.4A Withdrawn CN107754372A (en) 2017-11-20 2017-11-20 The separation equipment of the active ingredient of natural drug

Country Status (1)

Country Link
CN (1) CN107754372A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111359255A (en) * 2020-03-31 2020-07-03 山东博奥克生物科技有限公司 Resveratrol tablet and processing production equipment thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111359255A (en) * 2020-03-31 2020-07-03 山东博奥克生物科技有限公司 Resveratrol tablet and processing production equipment thereof
CN111359255B (en) * 2020-03-31 2021-12-21 山东博奥克生物科技有限公司 Resveratrol tablet and processing production equipment thereof

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Application publication date: 20180306