CN107753766A - A kind of preparation method of Processed Product of Rhizoma Gastrodiae - Google Patents
A kind of preparation method of Processed Product of Rhizoma Gastrodiae Download PDFInfo
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- CN107753766A CN107753766A CN201711185732.2A CN201711185732A CN107753766A CN 107753766 A CN107753766 A CN 107753766A CN 201711185732 A CN201711185732 A CN 201711185732A CN 107753766 A CN107753766 A CN 107753766A
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- Prior art keywords
- rhizoma gastrodiae
- hours
- constant temperature
- steamed
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/898—Orchidaceae (Orchid family)
- A61K36/8988—Gastrodia
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
Abstract
The present invention relates to kind of a Technology of Processing Chinese Herbal Medicines field, and in particular to a kind of preparation method of Processed Product of Rhizoma Gastrodiae；Rhizoma Gastrodiae raw material is steamed to the saturating heart, then will be steamed to the rhizoma Gastrodiae freezing of the saturating heart, be finally dried in vacuo and produce Processed Product of Rhizoma Gastrodiae；The present invention is on the basis of the conventional lyophilized technique of existing freeze-drying gastrodia elata piece, it is to add the step of being steamed rhizoma Gastrodiae raw material to the saturating heart before freezing, the step serves key effect to solving " existing freeze-drying tablet is frangible, and there is the technical problem of white powder material on surface "；Also freezing and the parameter of process of vacuum drying are improved in invention, the step of cooperation is steamed to the saturating heart, so as to get instant rhizoma Gastrodiae freeze-drying tablet intensity it is high, surface is smooth；For the exocuticle yellow-white for the instant gastrodia elata slice that the present invention is prepared to yellowish-brown, some tops remain rufous to the bud of dark-brown parrot mouth shape or residual stem foot；Section is white to canescence, it is seen that white or faint yellow tendon and vessel point projection, gas is micro-, sweet.
Description
Technical field
The present invention relates to kind of a Technology of Processing Chinese Herbal Medicines field, and in particular to a kind of preparation method of Processed Product of Rhizoma Gastrodiae.
Background technology
Rhizoma Gastrodiae is in irregular lumps or strip and block, and size has, long 5~10 centimetres, 1.5~5 centimetres of diameter.Table
Face yellowish-brown, or micro-strip brown.There is fine and closely woven vertical wrinkle, all to have strumae, the prominent tip of knurl has the sagging disk of dark brown more
Shape bud scar.Main root lower end is slightly thick, and knurl is dashed forward larger, and upward tapered knurl is prominent smaller, and often there is one section of bavin matter stem foot on top.Bottom has substantially
Root trace or fibrous root residual.Matter is hard, is not easily broken, section yellow-white, has the small oil drop being dispersed in, center crack, conduit
Group's radiation arrangement, forming layer ring-type.Gas is fragrant special, and sweet and slightly bitter taste is pungent, slightly mucus.With individual big neat, surface yellowish-brown is disconnected
Face yellow-white, the solid person of matter are preferred.Rushed down with tonifying middle-Jiao and Qi, strengthening the spleen and stomach, eliminate dampness and have diuretic effect, antiemetic, hidroschesis, antiabortive function.It is main
Control：The middle deficiency of vital energy is weak, indigestion caused by dysfunction of the spleen, oedema turgor, vomiting dysentery, fetal irritability, the disease such as physically weak spontaneous perspiration.
At present, Processed Product of Rhizoma Gastrodiae mainly has rhizoma Gastrodiae block, gastrodia elata slice and Rhizoma Gastrodiae powder；Rhizoma Gastrodiae block and gastrodia elata slice quality are hard, can not
Directly take, it is necessary to soak for a long time；Rhizoma Gastrodiae powder stickiness is big, not soluble in water.So rhizoma Gastrodiae drink made under such processing procedure
Piece is unfavorable for taking for the elderly.
The content of the invention
It is an object of the invention to provide a kind of preparation method of Processed Product of Rhizoma Gastrodiae, it is frangible to solve existing freeze-drying tablet, and surface
There is the technical problem of white powder material.
To solve above-mentioned technical problem, the present invention uses following technical scheme：
A kind of preparation method of the preparation method of Processed Product of Rhizoma Gastrodiae, comprises the following steps：
Rhizoma Gastrodiae raw material is steamed to the saturating heart, then will be steamed to the rhizoma Gastrodiae freezing of the saturating heart, be finally dried in vacuo and produce Processed Product of Rhizoma Gastrodiae.
Further, steaming into saturating heart step, it is 15-30min rhizoma Gastrodiae raw material to be steamed to the time of saturating heart boiling.
Further, in freezing step, rhizoma Gastrodiae tablet raw material is refrigerated to -45 °C.
Further, it is vacuum drying to concretely comprise the following steps：
S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time
- 20 °C are freely heated up to, afterwards constant temperature 2 hours；
S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；
S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；
S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Compared with prior art, the present invention at least has the advantages that：
1. the present invention on the basis of the conventional lyophilized technique of existing freeze-drying gastrodia elata piece, is to add to enter rhizoma Gastrodiae raw material before freezing
The step of row is steamed to the saturating heart, " existing freeze-drying tablet is frangible, and the technology that there is white powder material on surface is asked to solving for the step
Topic " serves key effect.
2. also being improved in invention the parameter of freezing and process of vacuum drying, cooperation is steamed to the step of the saturating heart
Suddenly, so as to get instant rhizoma Gastrodiae freeze-drying tablet intensity it is high, surface is smooth.
3. the exocuticle yellow-white for the instant gastrodia elata slice that the present invention is prepared to yellowish-brown, some tops remains reddish brown
Color to dark-brown parrot mouth shape bud or residual stem foot；Section is white to canescence, it is seen that white or faint yellow tendon and vessel point projection,
Gas is micro-, sweet.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1
A kind of preparation method of the preparation method of Processed Product of Rhizoma Gastrodiae, comprises the following steps：
Rhizoma Gastrodiae raw material is steamed to the saturating heart, then will be steamed to the rhizoma Gastrodiae freezing of the saturating heart, be finally dried in vacuo and produce Processed Product of Rhizoma Gastrodiae.
The exocuticle yellow-white for the instant gastrodia elata slice that the present invention is prepared to yellowish-brown, some tops remains rufous
To the bud or residual stem foot of dark-brown parrot mouth shape；Section is white to canescence, it is seen that white or faint yellow tendon and vessel point projection, gas
It is micro-, it is sweet.
Embodiment 2
On the basis of embodiment 1, steaming into saturating heart step, rhizoma Gastrodiae raw material is being steamed to the time of saturating heart boiling and be
15min, the present invention are to add to enter rhizoma Gastrodiae raw material before freezing on the basis of the conventional lyophilized technique of existing freeze-drying gastrodia elata piece
The step of row is steamed to the saturating heart, " existing freeze-drying tablet is frangible, and the technology that there is white powder material on surface is asked to solving for the step
Topic " serves key effect.
Embodiment 3
On the basis of embodiment 1, steaming into saturating heart step, rhizoma Gastrodiae raw material is being steamed to the time of saturating heart boiling and be
22min, the present invention are to add to enter rhizoma Gastrodiae raw material before freezing on the basis of the conventional lyophilized technique of existing freeze-drying gastrodia elata piece
The step of row is steamed to the saturating heart, " existing freeze-drying tablet is frangible, and the technology that there is white powder material on surface is asked to solving for the step
Topic " serves key effect.
Embodiment 4
On the basis of embodiment 1, steaming into saturating heart step, rhizoma Gastrodiae raw material is being steamed to the time of saturating heart boiling and be
30min, the present invention are to add to enter rhizoma Gastrodiae raw material before freezing on the basis of the conventional lyophilized technique of existing freeze-drying gastrodia elata piece
The step of row is steamed to the saturating heart, " existing freeze-drying tablet is frangible, and the technology that there is white powder material on surface is asked to solving for the step
Topic " serves key effect.
Embodiment 5
On the basis of embodiment 1-4, in freezing step, rhizoma Gastrodiae tablet raw material is refrigerated to -45 °C, also to freezing in the present invention
And the parameter of process of vacuum drying is improved, cooperation the step of steaming to the saturating heart, so as to get instant rhizoma Gastrodiae freeze-drying tablet
Intensity is high, and surface is smooth.
Embodiment 6
It is vacuum drying to concretely comprise the following steps on the basis of embodiment 1-5：
S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time
- 20 °C are freely heated up to, afterwards constant temperature 2 hours；
S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；
S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；
S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Also the parameter of freezing and process of vacuum drying is improved in the present invention, cooperation is steamed to the step of the saturating heart
Suddenly, so as to get instant rhizoma Gastrodiae freeze-drying tablet intensity it is high, surface is smooth.
Embodiment 7
A kind of preparation method of the preparation method of Processed Product of Rhizoma Gastrodiae, comprises the following steps：
Rhizoma Gastrodiae raw material is steamed to the saturating heart, steamed into saturating heart step, rhizoma Gastrodiae raw material is steamed to saturating heart boiling when
Between be 15min.
Then it will steam to the rhizoma Gastrodiae freezing of the saturating heart, in freezing step, rhizoma Gastrodiae tablet raw material be refrigerated to -45 °C.
Finally it is dried in vacuo and produces Processed Product of Rhizoma Gastrodiae, it is vacuum drying to concretely comprise the following steps：
S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time
- 20 °C are freely heated up to, afterwards constant temperature 2 hours；
S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；
S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；
S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Embodiment 8
A kind of preparation method of the preparation method of Processed Product of Rhizoma Gastrodiae, comprises the following steps：
Rhizoma Gastrodiae raw material is steamed to the saturating heart, steamed into saturating heart step, rhizoma Gastrodiae raw material is steamed to saturating heart boiling when
Between be 22min.
It will finally steam to the rhizoma Gastrodiae freezing of the saturating heart, in freezing step, rhizoma Gastrodiae tablet raw material be refrigerated to -45 °C.
Then it is dried in vacuo and produces Processed Product of Rhizoma Gastrodiae, it is vacuum drying to concretely comprise the following steps：
S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time
- 20 °C are freely heated up to, afterwards constant temperature 2 hours；
S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；
S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；
S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Embodiment 9
A kind of preparation method of the preparation method of Processed Product of Rhizoma Gastrodiae, comprises the following steps：
Rhizoma Gastrodiae raw material is steamed to the saturating heart, steamed into saturating heart step, rhizoma Gastrodiae raw material is steamed to saturating heart boiling when
Between be 30min.
Then it will steam to the rhizoma Gastrodiae freezing of the saturating heart, in freezing step, rhizoma Gastrodiae tablet raw material be refrigerated to -45 °C.
Finally it is dried in vacuo and produces Processed Product of Rhizoma Gastrodiae, it is vacuum drying to concretely comprise the following steps：
S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time
- 20 °C are freely heated up to, afterwards constant temperature 2 hours；
S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；
S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；
S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；
S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；
S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Although reference be made herein to invention has been described for multiple explanatory embodiments of the invention, however, it is to be understood that
Those skilled in the art can be designed that a lot of other modifications and embodiment, and these modifications and embodiment will fall in this Shen
Please be within disclosed spirit and spirit.More specifically, can be to master in the range of disclosure and claim
The building block and/or layout for inscribing composite configuration carry out a variety of variations and modifications.Except what is carried out to building block and/or layout
Outside modification and improvement, to those skilled in the art, other purposes also will be apparent.
Claims (4)
- A kind of 1. preparation method of Processed Product of Rhizoma Gastrodiae, it is characterised in that：Comprise the following steps：Rhizoma Gastrodiae raw material is steamed to the saturating heart, then will be steamed to the rhizoma Gastrodiae freezing of the saturating heart, be finally dried in vacuo and produce Processed Product of Rhizoma Gastrodiae.
- A kind of 2. preparation method of Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that：Steaming to saturating heart step In, it is 15-30min rhizoma Gastrodiae raw material to be steamed to the time of saturating heart boiling.
- A kind of 3. preparation method of Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that：In freezing step, by day Numb tablet raw material is refrigerated to -45 °C.
- A kind of 4. preparation method of Processed Product of Rhizoma Gastrodiae according to claim 1, it is characterised in that：Vacuum drying specific steps For：S1, after rhizoma Gastrodiae tablet raw material is refrigerated into preset temperature, start to vacuumize, when vacuum reaches 20 Pa, start for the first time - 20 °C are freely heated up to, afterwards constant temperature 2 hours；S2, second, are freely heated up to -10 °C, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；S3, third time, -5 °C are freely heated up to, afterwards constant temperature 2 hours, air pressure is maintained at 5Pa；S4, the 4th time, be heated up to 5 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 10Pa；S5, the 5th time, be heated up to 15 °C within the uniform velocity 2 hours, afterwards constant temperature 2 hours, air pressure is maintained at 15Pa；S6, the 6th time, be freely heated up to 25 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；S7, the 7th time, be freely heated up to 35 °C, afterwards constant temperature 3 hours, air pressure is maintained at 20Pa；S8, vacuum control is closed, do not keep atmospheric pressure value, continue constant temperature after 2 hours, drying terminates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711185732.2A CN107753766A (en) | 2017-11-23 | 2017-11-23 | A kind of preparation method of Processed Product of Rhizoma Gastrodiae |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711185732.2A CN107753766A (en) | 2017-11-23 | 2017-11-23 | A kind of preparation method of Processed Product of Rhizoma Gastrodiae |
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| CN107753766A true CN107753766A (en) | 2018-03-06 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1632434A (en) * | 2004-12-30 | 2005-06-29 | 周强 | Freeze drying and processing method for gastrodia tuber |
| CN103623250A (en) * | 2013-12-10 | 2014-03-12 | 程从友 | Preparation technology of active freeze-dried rhizoma gastrodiae |
| CN104721593A (en) * | 2015-04-02 | 2015-06-24 | 贵州同威生物科技有限公司 | Fresh gastrodia elata freeze-dried powder and preparation method thereof |
| CN105213813A (en) * | 2015-07-30 | 2016-01-06 | 昆明理工大学 | A kind of Rhizoma Gastrodiae alternating temperature drying means |
| CN105641474A (en) * | 2016-01-19 | 2016-06-08 | 腾冲秋实科贸有限公司 | Rhizoma gastrodiae processing method |
-
2017
- 2017-11-23 CN CN201711185732.2A patent/CN107753766A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1632434A (en) * | 2004-12-30 | 2005-06-29 | 周强 | Freeze drying and processing method for gastrodia tuber |
| CN103623250A (en) * | 2013-12-10 | 2014-03-12 | 程从友 | Preparation technology of active freeze-dried rhizoma gastrodiae |
| CN104721593A (en) * | 2015-04-02 | 2015-06-24 | 贵州同威生物科技有限公司 | Fresh gastrodia elata freeze-dried powder and preparation method thereof |
| CN105213813A (en) * | 2015-07-30 | 2016-01-06 | 昆明理工大学 | A kind of Rhizoma Gastrodiae alternating temperature drying means |
| CN105641474A (en) * | 2016-01-19 | 2016-06-08 | 腾冲秋实科贸有限公司 | Rhizoma gastrodiae processing method |
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