CN107737057A - A kind of preparation method of toxin-expelling and face nourishing cosmetics - Google Patents
A kind of preparation method of toxin-expelling and face nourishing cosmetics Download PDFInfo
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- CN107737057A CN107737057A CN201711252545.1A CN201711252545A CN107737057A CN 107737057 A CN107737057 A CN 107737057A CN 201711252545 A CN201711252545 A CN 201711252545A CN 107737057 A CN107737057 A CN 107737057A
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- expelling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Biotechnology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of preparation method of toxin-expelling and face nourishing cosmetics, comprise the following steps：1）Rosa Damascana, Rhizoma Gastrodiae extract, angelica extract, coixlacrymajobi powder, leaflet crab apple extract, REISH, Fructus Cucumidis sativi extract are added into water successively, and is stirred continuously, it is to be mixed uniformly after, allotment water is made；2）Allotment water is placed in fermentation tank, 40 ~ 50 DEG C of keeping temperature in fermentation process, and every three hour stirrings once；3）After fermentation 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needs constantly to be stirred zymotic fluid in encapsulation process；4）Packing is completed, and produces toxin-expelling and face nourishing cosmetics.The preparation process of toxin-expelling and face nourishing cosmetics provided by the invention, do not add preservative, pigment, essence completely, it is nonirritant to human body skin, allergic reaction will not occur, meet the needs of different crowd.
Description
Technical field
The present invention relates to cosmetic technical field, in particular to a kind of preparation method of toxin-expelling and face nourishing cosmetics.
Background technology
Skin is the largest organ for being covered in human body surface, due to directly being contacted with external environment, aoxidized, dried,
The stimulation of a variety of tension-causing factors such as ultraviolet, is highly susceptible to injure.Especially all become in winter, the whole metabolism of human body
It is more slow, the metabolism of skin also becomes particularly slow, the cutin of skin epidermis can not eubolism, cutin is deposited in skin
Surface, the cell of epidermis bottom is caused to be oppressed, skin can not absorb nutrition, and metabolic toxicities are accumulated in skin, produce various
Skin problem, inconvenience is produced to people's normal life.
Existing cosmetics in order to extend service life and attract consumer, with the addition of a large amount of preservatives and essence etc.,
Consumer further generates infringement in use, harmful impoliteness to consumer skin.Some are in order to play the cosmetic to get instant result
Effect, chemical article is also added, cause that user's is allergic, carried out more ill effect for the health of skin.
The content of the invention
It is another object of the present invention to provide a kind of metabolism improving skin moisturizing that can cooperate with skin, accelerates skin
The process of toxin expelling, reach to skin repair, anti-ageing, moisturizing effect and be free of the chemical substances such as preservative, pigment, essence, can
Skin toxins are excluded, and allergic reaction will not occur, extend the preparation side for including toxin-expelling and face nourishing cosmetics in skin water lock cycle
Method.
A kind of preparation method of toxin-expelling and face nourishing cosmetics, it is characterised in that comprise the following steps：
(1) Rosa Damascana, Rhizoma Gastrodiae extract, angelica extract, coixlacrymajobi powder, the extraction of leaflet Malus spectabilis are added into water successively
Thing, REISH, Fructus Cucumidis sativi extract, and be stirred continuously, it is to be mixed uniformly after, allotment water is made；
(2) allotment water is placed in fermentation tank, 40~50 DEG C of keeping temperature in fermentation process, and stirred every three hours
Once；
(3) after fermenting 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed constantly in encapsulation process
Zymotic fluid is stirred；
(4) packing is completed, and produces toxin-expelling and face nourishing cosmetics.
In order to which the preparation method of the present invention is better achieved, further, in the step (1), raw material is added into water
Process be, successively into water add Rosa Damascana, Rhizoma Gastrodiae extract, angelica extract, coixlacrymajobi powder, leaflet crab apple extract,
REISH, Fructus Cucumidis sativi extract, it is stirred continuously during adding component, after the previous component of addition stirs evenly, under could adding
One component.
In order to which the preparation method of the present invention is better achieved, further, the time of fermentation is small for 72 in the step (3)
When.
In order to which the preparation method of the present invention is better achieved, further, the preparation process of the Rosa Damascana is：Rose
Hua Yushui presses 1：In 4 input steamers, first heated with indirect steam, when temperature rises to 70-80 DEG C, be passed through open steam and be heated to
Boiling, about with 30-40 minutes, continue to distill 2.5-3 hours, controlling stream liquid outlet quantity is spend weight 1-2 times, and distillation speed is steamer
The 8-10% of volume, cooling water inflow is controlled, makes efflux head half an hour temperature control after 28-35 DEG C, half an hour to last temperature
At 40-45 DEG C, efflux separates attar of rose and attar of rose saturation distilled water through oil water separator for degree control, takes out attar of rose,
Saturation distilled water flows into multiple fractional distillation column by oil water separator under discrepancy in elevation effect, is heated in the presence of the steam that steamer rises
Evaporate again, then condensed device returns to oil water separator, so distills, evaporates again repeatedly.
It is further, the Rhizoma Gastrodiae extract, angelica extract, small in order to which the preparation method of the present invention is better achieved
The extraction process of leaf crab apple extract is：Take air-dried raw material, go the removal of impurity, plus 6-10 times measure water refluxing extraction 1-5 times, every time
3-5 hours, filtering, merging filtrate, thick paste is concentrated under reduced pressure into, then adds the 4-5 times of ethanol solution for measuring 75-90%, fully stir
Mix uniformly, stand 8-20 hours, filtering, decompression filtrate recycling ethanol, reclaim concentrate, produce the extract of above Chinese medicine.
The present invention compared with prior art, has advantages below and beneficial effect：
(1) toxin-expelling and face nourishing cosmetics provided by the invention by by pearl powder, propolis, attar of rose, leaflet marine algae extract,
Butter berry extract and Flos Pelargonii Hortori compounding use, the metabolism improving skin moisturizing of skin can be cooperateed with, accelerate skin
The process of toxin expelling, reach to skin repair, anti-ageing, moist effect；
(2) toxin-expelling and face nourishing cosmetics of the invention can beat skin aquaporin, and flesh is waken up with the speed of common 7 times of milky lotion
Skin basalis, the mercury that can will be remained originally while moisturizing is repaired, lead, dust together are metabolized out, reached from inside to outside
Dredging and reparation, while shining face moisturizing, light spot, improvement sensitiveness skin, pore cleanser cleaning skin, oil-control, water lock are up to 48
As long as hour, skin is maintained without using other species cosmetics；
(3) present invention in toxin-expelling and face nourishing cosmetics preparation process, do not add preservative, pigment, essence completely, produce
Cosmetics it is nonirritant to human body skin, allergic reaction will not occur, disclosure satisfy that the use demand of different crowd.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this
Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention
Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in
In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1：
The present embodiment discloses a kind of specific preparation process of toxin-expelling and face nourishing cosmetics, comprises the following steps：
(1) pearl powder, tocopherol, propolis, attar of rose, leaflet crab apple extract, butter fruit extraction are added into water successively
Thing, Flos Pelargonii Hortori, it is stirred continuously during adding component, after the previous component of addition stirs evenly, next group could be added
Point, and be stirred continuously, it is to be mixed uniformly after, allotment water is made；
(2) allotment water is placed in fermentation tank, 40~50 DEG C of keeping temperature in fermentation process, and stirred every three hours
Once；
(3) after fermenting 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed constantly in encapsulation process
Zymotic fluid is stirred；
(4) packing is completed, and produces toxin-expelling and face nourishing cosmetics finished product.
Obtained toxin-expelling and face nourishing cosmetics finished product is detected, it is as a result as follows：Toxin-expelling and face nourishing cosmetics are colourless
Bright solution, color milk is white, light Rosa Damascana taste, after being sprayed on skin surface, feels very salubrious, skin sense is good, moisturizing
Water moistens.
Obtained toxin-expelling and face nourishing cosmetics finished product is free of any preservative, therefore period of storage is shorter, after tested, normal
Shelf storage is within 3 months under warm (15~25 DEG C), in refrigerator in low temperature (0~5 DEG C) refrigerated storage 6 months, will not become
Matter, product items organoleptic indicator, physical and chemical index, sanitary index meet national standard.
Obtained toxin-expelling and face nourishing cosmetics finished product is carried out under the conditions of 40 ± 1 DEG C to the resistance to Thermal test of 24 hours, then
Recover room temperature, detection finds that any muddiness do not occur after room temperature is recovered in cosmetics, and it is every to recover the cosmetics after room temperature
Sense index, physical and chemical index, sanitary index meet corresponding national standard.
Obtained toxin-expelling and face nourishing cosmetics finished product is carried out under the conditions of -15 ± 1 DEG C to the cold-resistant test of 24 hours, then
Recover room temperature, detection finds that any muddiness do not occur after room temperature is recovered in cosmetics, and it is every to recover the cosmetics after room temperature
Sense index, physical and chemical index, sanitary index meet corresponding national standard.
The method of specifically used toxin-expelling and face nourishing cosmetics finished product：In use, shaking, face is uniformly sprayed on, then both hands
Face skin is patted to promote to absorb.In order to which effect normally plays, it is proposed that the dosage of 1 week first 3 months 1 bottle of water, use every time sooner or later,
Please contact can regard own situation unrestricted choice water after clapping enough 6 times, 3 months.
Using this product, locate to add sun-proof isolated product daytime, without other skin-protection products.
Embodiment 2：
The present embodiment is directed to the toxin-expelling and face nourishing cosmetics finished product that above-described embodiment is prepared, and carries out toxicology test, bag
Include acute ocular irritation test and multiple skin irritation test.
First, acute ocular irritation test,
1st, tested material：
Toxin-expelling and face nourishing cosmetics finished product is as former state.
2nd, animal and feeding environment
2.1 animal
The healthy big ear rabbit 3 of Japan, regular grade, is provided, before experiment at least by plant of experimental animal administration commission of Sichuan Province
Adapt to 3 days.
2.2 feeding environment
20~22 DEG C of temperature, 40~70%, 12/12 hour light and shade of relative humidity alternately illuminate.Single cage is raised, autonomous drink
Water.Full-valence pellet feed.
3rd, major experimental instrument and reagent
KJ5S3 type hand-held slit-lamp microscopes；
Phosphor strip, specification：Every 1.0mg containing fluorescein sodium, per built-in 10 of box.
4th, test method
Moon 24h before 4.1 experiments, two eyes of experimental animal are checked (including the use of fluorescein sodium inspection).Have
The animal of irritation, corneal defect and conjunctival damage cannot be used for testing.
4.2 gently pull open the palpebra inferior of rabbit side eyes, and tested material 0.1ml is instilled in conjunctival sac, makes upper and lower eyelid
It is passive to close 1s to prevent tested material from losing.To very fast with enough, flow velocity during 30s but not cause the current of animal eye injury to rush
Wash 30s.
4.3 clinical examinations and scoring：Instill again 1 after tested material, 24,48,72h and 4d and 7d enter to animal eyes
Row checks.If 72h does not occur stimulate the reaction, experiment can be terminated.If it find that involve cornea or have other stimulations,
Not recuperator in 7d, to determine that the invertibity of the infringement or irreversibility need to extend time observation, it is usually no more than 21d and provides
7d, 14d, 21d visual report.In addition to corneal, iris, conjunctiva are observed, other detrimental effects should record
And report.
Then press《Cosmetics health specification》Acute eye irritation/corrosion test table Scoring System such as table 1：
The tested material of table one is to Rabbits with Acute eye irritation result (30s flushings)
Tested material is microstimulation to Rabbits with Acute eye irritation.
2nd, multiple skin irritation test
1st, tested material：
Toxin-expelling and face nourishing cosmetics finished product stoste, 0.5ml/2.5cm × 2.5cm/ is only.
2nd, animal and feeding environment
2.1 animal
The healthy big ear rabbit 4 of Japan, regular grade, male and female, is provided, examination by plant of experimental animal administration commission of Sichuan Province
At least adapted to 3 days before testing.
2.2 feeding environment
20~22 DEG C of temperature, 40~70%, 12/12 hour light and shade of relative humidity alternately illuminate.Single cage is raised, autonomous drink
Water.Full-valence pellet feed.
3. test method
About 24h before experiment, experimental animal back backbone diamond wool is cut, and can not damage epidermis, and unhairing scope is left and right each
About 3cm × 3cm, tested material 0.5ml is taken directly to be applied on skin (area about 2.5cm × 2.5cm), every time smearing 1 time, continuously
14d is smeared, since 2d, cropping before smearing every time, residual tested material is removed with warm water.1 as a child observes result, presses《Change
Cosmetic hygienic practice》(version in 2007) skin irritation/corrosion test table scoring, check plot and trial zone are equally handled, pressed
Every animal average integral daily is calculated according to respective formula, skin irritatin intensity is judged from table.As shown in table 2：
The tested material of table two is to the multiple skin irritation test result of rabbit
Tested material is nonirritant to the multiple skin irritation of rabbit
3rd, toxicology test result shows：
Acute ocular irritation test result：Microstimulation
Multiple skin irritation test result：It is nonirritant
Therefore, can be with this product stimulation harmless to the human body, can be safe to use.
Embodiment 3：
The present embodiment carries out health chemical testing, as a result such as to toxin-expelling and face nourishing cosmetics finished product made from the inventive method
Table 3.
The hygienic chemistry testing result of table three
| Inspection project | Unit | Limitation | Testing result | Individual event conclusion |
| Total plate count | CFU/g | ≤1000 | ＜ 10 | It is qualified |
| Excrement colibacillus group | CFU/g | It must not detect | Do not detect | It is qualified |
| Pseudomonas aeruginosa | CFU/g | It must not detect | Do not detect | It is qualified |
| Staphylococcus aureus | CFU/g | It must not detect | Do not detect | It is qualified |
| Mould saccharomycete counts | CFU/g | ≤100 | ＜ 10 | It is qualified |
| Lead | mg/kg | ≤40 | 13.04 | It is qualified |
| Mercury | mg/kg | ≤1 | 0.015 | It is qualified |
| Arsenic | mg/kg | ≤10 | Do not detect (＜ 0.01) | It is qualified |
Health chemical testing result shows that lead, arsenic, the content of mercury meet national standard in this product, can use safely.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that：Not
A variety of change, modification, replacement and modification can be carried out to these embodiments by departing under the principle and objective of the present invention, of the invention
Scope is limited by claim and its equivalent.
Claims (5)
1. a kind of preparation method of toxin-expelling and face nourishing cosmetics, it is characterised in that comprise the following steps：
（1）Rosa Damascana, Rhizoma Gastrodiae extract, angelica extract, coixlacrymajobi powder, leaflet crab apple extract, spirit are added into water successively
Sesame powder, Fructus Cucumidis sativi extract, and be stirred continuously, it is to be mixed uniformly after, allotment water is made；
（2）Allotment water is placed in fermentation tank, 40 ~ 50 DEG C of keeping temperature in fermentation process, and every three hour stirrings once；
（3）After fermentation 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed in encapsulation process constantly to hair
Zymotic fluid is stirred；
（4）Packing is completed, and produces toxin-expelling and face nourishing cosmetics.
2. the preparation method of toxin-expelling and face nourishing cosmetics according to claim 1, it is characterised in that the step（1）In, to
The process that raw material is added in water is to add Rosa Damascana, Rhizoma Gastrodiae extract, angelica extract, coixlacrymajobi powder, leaflet into water successively
Crab apple extract, REISH, Fructus Cucumidis sativi extract, it is stirred continuously during adding component, after the previous component of addition stirs evenly,
Next component could be added.
3. the preparation method of toxin-expelling and face nourishing cosmetics according to claim 1 or 2, it is characterised in that the step（3）In
The time of fermentation is 72 hours.
4. the preparation method of toxin-expelling and face nourishing cosmetics according to claim 1 or 2, it is characterised in that the Rosa Damascana
Preparation process be：Rose presses 1 with water：In 4 input steamers, first heated with indirect steam, when temperature rises to 70-80 DEG C,
It is passed through open steam to be heated to seethe with excitement, about with 30-40 minutes, continues to distill 2.5-3 hours, controlling stream liquid outlet quantity is to spend the 1- of weight
2 times, distillation speed is the 8-10% of steamer volume, controls cooling water inflow, makes efflux head half an hour temperature control at 28-35 DEG C,
Controlled after half an hour to end temperature at 40-45 DEG C, efflux is through oil water separator by attar of rose and attar of rose saturation distilled water
Separate, take out attar of rose, saturation distilled water flows into multiple fractional distillation column by oil water separator under discrepancy in elevation effect, in the steam that steamer rises
In the presence of heated and evaporated again, then condensed device returns to oil water separator, so distills, evaporates again repeatedly.
5. the preparation method of toxin-expelling and face nourishing cosmetics according to claim 1 or 2, it is characterised in that the rhizoma Gastrodiae extraction
Thing, angelica extract, the extraction process of leaflet crab apple extract are：Air-dried raw material is taken, the removal of impurity is gone, adds 6-10 times to measure water time
Stream extraction 1-5 times, each 3-5 hours, filtering, merging filtrate, is concentrated under reduced pressure into thick paste, and then adding 4-5 times measures 75-90%'s
Ethanol solution, stir, stand 8-20 hours, filtering, decompression filtrate recycling ethanol, reclaim concentrate, produce the above
The extract of Chinese medicine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711252545.1A CN107737057A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of toxin-expelling and face nourishing cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711252545.1A CN107737057A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of toxin-expelling and face nourishing cosmetics |
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| Publication Number | Publication Date |
|---|---|
| CN107737057A true CN107737057A (en) | 2018-02-27 |
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ID=61238837
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711252545.1A Withdrawn CN107737057A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of toxin-expelling and face nourishing cosmetics |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN106619446A (en) * | 2016-12-06 | 2017-05-10 | 四川自然菲科技有限公司 | Composition capable of expelling toxin and beautifying skin, skin-care lotion capable of expelling toxin and beautifying skin and preparation method thereof |
-
2017
- 2017-12-01 CN CN201711252545.1A patent/CN107737057A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104004589A (en) * | 2013-10-31 | 2014-08-27 | 菏泽中禾健元生物科技有限公司 | Producing method of peony essential oil |
| CN106619446A (en) * | 2016-12-06 | 2017-05-10 | 四川自然菲科技有限公司 | Composition capable of expelling toxin and beautifying skin, skin-care lotion capable of expelling toxin and beautifying skin and preparation method thereof |
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Application publication date: 20180227 |
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