CN107737055A - A kind of preparation method of pure natural water lock cosmetics - Google Patents
A kind of preparation method of pure natural water lock cosmetics Download PDFInfo
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- CN107737055A CN107737055A CN201711250472.2A CN201711250472A CN107737055A CN 107737055 A CN107737055 A CN 107737055A CN 201711250472 A CN201711250472 A CN 201711250472A CN 107737055 A CN107737055 A CN 107737055A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Gerontology & Geriatric Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a kind of preparation method of pure natural water lock cosmetics, comprise the following steps：1）Peony essential oil, Angelica Dahurica extract, chrysanthemum extract, almond powder, reed leaf extract, REISH, aloe extract are added into water successively, and is stirred continuously, it is to be mixed uniformly after, allotment water is made；2）Allotment water is placed in fermentation tank, 40 ~ 50 DEG C of keeping temperature in fermentation process, and every three hour stirrings once；3）After fermentation 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needs constantly to be stirred zymotic fluid in encapsulation process；4）Packing is completed, and produces pure natural water lock cosmetics.The preparation process of pure natural water lock cosmetics provided by the invention, does not add preservative, pigment, essence completely, nonirritant to human body skin, and allergic reaction will not occur, meet the needs of different crowd.
Description
Technical field
The present invention relates to cosmetic technical field, in particular to a kind of preparation method of pure natural water lock cosmetics.
Background technology
Skin is the largest organ for being covered in human body surface, due to directly being contacted with external environment, aoxidized, dried,
The stimulation of a variety of tension-causing factors such as ultraviolet, is highly susceptible to injure.Especially all become in winter, the whole metabolism of human body
It is more slow, the metabolism of skin also becomes particularly slow, the cutin of skin epidermis can not eubolism, cutin is deposited in skin
Surface, the cell of epidermis bottom is caused to be oppressed, skin can not absorb nutrition, and metabolic toxicities are accumulated in skin, produce various
Skin problem, inconvenience is produced to people's normal life.
Existing cosmetics in order to extend service life and attract consumer, with the addition of a large amount of preservatives and essence etc.,
Consumer further generates infringement in use, harmful impoliteness to consumer skin.Some are in order to play the cosmetic to get instant result
Effect, chemical article is also added, cause that user's is allergic, carried out more ill effect for the health of skin.
The content of the invention
It is another object of the present invention to provide a kind of metabolism improving skin moisturizing that can cooperate with skin, accelerates skin
The process of toxin expelling, reach to skin repair, anti-ageing, moisturizing effect and be free of the chemical substances such as preservative, pigment, essence, can
Skin toxins are excluded, and allergic reaction will not occur, extend the preparation for including pure natural water lock cosmetics in skin water lock cycle
Method.
A kind of preparation method of pure natural water lock cosmetics, it is characterised in that comprise the following steps：
(1) successively into water add peony essential oil, Angelica Dahurica extract, chrysanthemum extract, almond powder, reed leaf extract,
REISH, aloe extract, and be stirred continuously, it is to be mixed uniformly after, allotment water is made；
(2) allotment water is placed in fermentation tank, 40~50 DEG C of keeping temperature in fermentation process, and stirred every three hours
Once；
(3) after fermenting 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed constantly in encapsulation process
Zymotic fluid is stirred；
(4) packing is completed, and produces pure natural water lock cosmetics.
In order to which the preparation method of the present invention is better achieved, further, in the step (1), raw material is added into water
Process be, successively into water add peony essential oil, Angelica Dahurica extract, chrysanthemum extract, almond powder, reed leaf extract, spirit
Sesame powder, aloe extract, it is stirred continuously during adding component, after the previous component of addition stirs evenly, could adds next
Component.
In order to which the preparation method of the present invention is better achieved, further, the time of fermentation is small for 72 in the step (3)
When.
In order to which the preparation method of the present invention is better achieved, further, the preparation process of the peony essential oil is：Tree peony
Hua Yushui presses 1：In 4 input steamers, first heated with indirect steam, when temperature rises to 70-80 DEG C, be passed through open steam and be heated to
Boiling, about with 30-40 minutes, continue to distill 2.5-3 hours, controlling stream liquid outlet quantity is spend weight 1-2 times, and distillation speed is steamer
The 8-10% of volume, cooling water inflow is controlled, makes efflux head half an hour temperature control after 28-35 DEG C, half an hour to last temperature
At 40-45 DEG C, efflux separates peony oil and peony oil saturation distilled water through oil water separator for degree control, takes out peony oil,
Saturation distilled water flows into multiple fractional distillation column by oil water separator under discrepancy in elevation effect, is heated in the presence of the steam that steamer rises
Evaporate again, then condensed device returns to oil water separator, so distills, evaporates again repeatedly.
In order to which the preparation method of the present invention, further, the Angelica Dahurica extract, chrysanthemum extract, reed is better achieved
The extraction process of reed leaf extract is：Take air-dried raw material, go the removal of impurity, plus 6-10 times measure water refluxing extraction 1-5 times, each 3-
5 hours, filtering, merging filtrate, thick paste is concentrated under reduced pressure into, then adds the 4-5 times of ethanol solution for measuring 75-90%, be sufficiently stirred
Uniformly, 8-20 hours are stood, filtering, decompression filtrate recycling ethanol, reclaims concentrate, produce the extract of above Chinese medicine.
The present invention compared with prior art, has advantages below and beneficial effect：
(1) pure natural water lock cosmetics provided by the invention are by the way that pearl powder, propolis, peony oil, leaflet marine alga are extracted
Thing, butter berry extract and Flos Pelargonii Hortori compounding use, the metabolism improving skin moisturizing of skin can be cooperateed with, accelerate skin
The process of skin toxin expelling, reach to skin repair, anti-ageing, moist effect；
(2) pure natural water lock cosmetics of the invention can beat skin aquaporin, be waken up with the speed of common 7 times of milky lotion
Skin basalis, the mercury that can will be remained originally while moisturizing is repaired, lead, dust together are metabolized out, reach by it is interior to
Outer dredging and reparation, while shining face moisturizing, light spot, improvement sensitiveness skin, pore cleanser cleaning skin, oil-control, water lock are up to
48 hours as long as, skin is maintained without using other species cosmetics；
(3) present invention in pure natural water lock cosmetics preparation process, do not add preservative, pigment, essence completely, produce
The cosmetics gone out are nonirritant to human body skin, and allergic reaction will not occur, and disclosure satisfy that the use demand of different crowd.
Embodiment
For the purpose of the present invention, process conditions and advantage effect is more clearly understood, with reference to following embodiment, to this
Invention is described in further detail, but the implementation of the present invention is not limited to this, is not departing from the above-mentioned technological thought feelings of the present invention
Under condition, according to ordinary skill knowledge and customary means, various replacements and change are made, the model of the present invention all should be included in
In enclosing, specific implementation example described herein is not intended to limit the present invention only to explain the present invention.
Embodiment 1：
The present embodiment discloses a kind of specific preparation process of pure natural water lock cosmetics, comprises the following steps：
(1) successively into water add pearl powder, tocopherol, propolis, peony oil, reed leaf extract, butter berry extract,
Flos Pelargonii Hortori, it is stirred continuously during adding component, after the previous component of addition stirs evenly, next component could be added,
And be stirred continuously, it is to be mixed uniformly after, be made allotment water；
(2) allotment water is placed in fermentation tank, 40~50 DEG C of keeping temperature in fermentation process, and stirred every three hours
Once；
(3) after fermenting 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed constantly in encapsulation process
Zymotic fluid is stirred；
(4) packing is completed, and produces pure natural water lock cosmetics finished product.
Obtained pure natural water lock cosmetics finished product is detected, it is as a result as follows：Pure natural water lock cosmetics are nothing
Color clear solution, color milk is white, light peony essential oil taste, after being sprayed on skin surface, feels very salubrious, and skin sense is good,
Moisture retention water moistens.
Obtained pure natural water lock cosmetics finished product is free of any preservative, therefore period of storage is shorter, after tested,
Shelf storage is within 3 months under normal temperature (15~25 DEG C), in refrigerator in low temperature (0~5 DEG C) refrigerated storage 6 months, will not occur
Rotten, product items organoleptic indicator, physical and chemical index, sanitary index meet national standard.
Obtained pure natural water lock cosmetics finished product is carried out to the resistance to Thermal test of 24 hours under the conditions of 40 ± 1 DEG C, so
After recover room temperature, detection finds that any muddiness do not occur after room temperature is recovered in cosmetics, and the cosmetics after recovery room temperature are each
Item sense index, physical and chemical index, sanitary index meet corresponding national standard.
Obtained pure natural water lock cosmetics finished product is carried out to the cold-resistant test of 24 hours under the conditions of -15 ± 1 DEG C, so
After recover room temperature, detection finds that any muddiness do not occur after room temperature is recovered in cosmetics, and the cosmetics after recovery room temperature are each
Item sense index, physical and chemical index, sanitary index meet corresponding national standard.
The method of specifically used pure natural water lock cosmetics finished product：In use, shaking, face, Ran Houshuan are uniformly sprayed on
Hand pats face skin and promotes to absorb.In order to which effect normally plays, it is proposed that the dosage of 1 week first 3 months 1 bottle of water, make every time sooner or later
With please contact can regard own situation unrestricted choice water after clapping enough 6 times, 3 months.
Using this product, locate to add sun-proof isolated product daytime, without other skin-protection products.
Embodiment 2：
The present embodiment is directed to the pure natural water lock cosmetics finished product that above-described embodiment is prepared, and carries out toxicology test,
Including acute ocular irritation test and multiple skin irritation test.
First, acute ocular irritation test,
1st, tested material：
Pure natural water lock cosmetics finished product is as former state.
2nd, animal and feeding environment
2.1 animal
The healthy big ear rabbit 3 of Japan, regular grade, is provided, before experiment at least by plant of experimental animal administration commission of Sichuan Province
Adapt to 3 days.
2.2 feeding environment
20~22 DEG C of temperature, 40~70%, 12/12 hour light and shade of relative humidity alternately illuminate.Single cage is raised, autonomous drink
Water.Full-valence pellet feed.
3rd, major experimental instrument and reagent
KJ5S3 type hand-held slit-lamp microscopes；
Phosphor strip, specification：Every 1.0mg containing fluorescein sodium, per built-in 10 of box.
4th, test method
Moon 24h before 4.1 experiments, two eyes of experimental animal are checked (including the use of fluorescein sodium inspection).Have
The animal of irritation, corneal defect and conjunctival damage cannot be used for testing.
4.2 gently pull open the palpebra inferior of rabbit side eyes, and tested material 0.1ml is instilled in conjunctival sac, makes upper and lower eyelid
It is passive to close 1s to prevent tested material from losing.To very fast with enough, flow velocity during 30s but not cause the current of animal eye injury to rush
Wash 30s.
4.3 clinical examinations and scoring：Instill again 1 after tested material, 24,48,72h and 4d and 7d enter to animal eyes
Row checks.If 72h does not occur stimulate the reaction, experiment can be terminated.If it find that involve cornea or have other stimulations,
Not recuperator in 7d, to determine that the invertibity of the infringement or irreversibility need to extend time observation, it is usually no more than 21d and provides
7d, 14d, 21d visual report.In addition to corneal, iris, conjunctiva are observed, other detrimental effects should record
And report.
Then press《Cosmetics health specification》Acute eye irritation/corrosion test table Scoring System such as table 1：
The tested material of table one is to Rabbits with Acute eye irritation result (30s flushings)
Tested material is microstimulation to Rabbits with Acute eye irritation.
----------------------------------------------------
2nd, multiple skin irritation test
1st, tested material：
Pure natural water lock cosmetics finished product stoste, 0.5ml/2.5cm × 2.5cm/ is only.
2nd, animal and feeding environment
2.1 animal
The healthy big ear rabbit 4 of Japan, regular grade, male and female, is provided, examination by plant of experimental animal administration commission of Sichuan Province
At least adapted to 3 days before testing.
2.2 feeding environment
20~22 DEG C of temperature, 40~70%, 12/12 hour light and shade of relative humidity alternately illuminate.Single cage is raised, autonomous drink
Water.Full-valence pellet feed.
3. test method
About 24h before experiment, experimental animal back backbone diamond wool is cut, and can not damage epidermis, and unhairing scope is left and right each
About 3cm × 3cm, tested material 0.5ml is taken directly to be applied on skin (area about 2.5cm × 2.5cm), every time smearing 1 time, continuously
14d is smeared, since 2d, cropping before smearing every time, residual tested material is removed with warm water.1 as a child observes result, presses《Change
Cosmetic hygienic practice》(version in 2007) skin irritation/corrosion test table scoring, check plot and trial zone are equally handled, pressed
Every animal average integral daily is calculated according to respective formula, skin irritatin intensity is judged from table.As shown in table 2：
The tested material of table two is to the multiple skin irritation test result of rabbit
Tested material is nonirritant to the multiple skin irritation of rabbit
---------------------------------------------
3rd, toxicology test result shows：
Acute ocular irritation test result：Microstimulation
Multiple skin irritation test result：It is nonirritant
Therefore, can be with this product stimulation harmless to the human body, can be safe to use.
Embodiment 3：
The present embodiment carries out health chemical testing, as a result to pure natural water lock cosmetics finished product made from the inventive method
Such as table 3.
The hygienic chemistry testing result of table three
| Inspection project | Unit | Limitation | Testing result | Individual event conclusion |
| Total plate count | CFU/g | ≤1000 | ＜ 10 | It is qualified |
| Excrement colibacillus group | CFU/g | It must not detect | Do not detect | It is qualified |
| Pseudomonas aeruginosa | CFU/g | It must not detect | Do not detect | It is qualified |
| Staphylococcus aureus | CFU/g | It must not detect | Do not detect | It is qualified |
| Mould saccharomycete counts | CFU/g | ≤100 | ＜ 10 | It is qualified |
| Lead | mg/kg | ≤40 | 13.04 | It is qualified |
| Mercury | mg/kg | ≤1 | 0.015 | It is qualified |
| Arsenic | mg/kg | ≤10 | Do not detect (＜ 0.01) | It is qualified |
Health chemical testing result shows that lead, arsenic, the content of mercury meet national standard in this product, can use safely.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that：Not
A variety of change, modification, replacement and modification can be carried out to these embodiments by departing under the principle and objective of the present invention, of the invention
Scope is limited by claim and its equivalent.
Claims (5)
1. a kind of preparation method of pure natural water lock cosmetics, it is characterised in that comprise the following steps：
（1）Peony essential oil, Angelica Dahurica extract, chrysanthemum extract, almond powder, reed leaf extract, ganoderma lucidum are added into water successively
Powder, aloe extract, and be stirred continuously, it is to be mixed uniformly after, allotment water is made；
（2）Allotment water is placed in fermentation tank, 40 ~ 50 DEG C of keeping temperature in fermentation process, and every three hour stirrings once；
（3）After fermentation 72 hours, zymotic fluid is collected, zymotic fluid is sent into production line packing, needed in encapsulation process constantly to hair
Zymotic fluid is stirred；
（4）Packing is completed, and produces pure natural water lock cosmetics.
2. the preparation method of pure natural water lock cosmetics according to claim 1, it is characterised in that the step（1）In,
The process that Xiang Shuizhong adds raw material is to add peony essential oil, Angelica Dahurica extract, chrysanthemum extract, almond powder, reed into water successively
Reed leaf extract, REISH, aloe extract, it is stirred continuously during adding component, after the previous component of addition stirs evenly,
Next component could be added.
3. the preparation method of pure natural water lock cosmetics according to claim 1 or 2, it is characterised in that the step（3）
The time of middle fermentation is 72 hours.
4. the preparation method of pure natural water lock cosmetics according to claim 1 or 2, it is characterised in that the tree peony essence
Oil preparation process be：Peony presses 1 with water：In 4 input steamers, first heated with indirect steam, temperature rises to 70-80 DEG C
When, it is passed through open steam and is heated to seethe with excitement, about with 30-40 minutes, continue to distill 2.5-3 hours, controlling stream liquid outlet quantity is spends weight
1-2 times, distillation speed be steamer volume 8-10%, control cooling water inflow, make efflux head half an hour temperature control in 28-
35 DEG C, controlled after half an hour to end temperature at 40-45 DEG C, efflux steams peony oil and peony oil saturation through oil water separator
Distilled water separates, and takes out peony oil, and saturation distilled water flows into multiple fractional distillation column by oil water separator under discrepancy in elevation effect, risen in steamer
Heated in the presence of steam and evaporated again, then condensed device returns to oil water separator, so distills, evaporates again repeatedly.
5. the preparation method of pure natural water lock cosmetics according to claim 1 or 2, it is characterised in that the root of Dahurain angelica carries
Thing, chrysanthemum extract, the extraction process of reed leaf extract is taken to be：Air-dried raw material is taken, the removal of impurity is gone, adds 6-10 times to measure water time
Stream extraction 1-5 times, each 3-5 hours, filtering, merging filtrate, is concentrated under reduced pressure into thick paste, and then adding 4-5 times measures 75-90%'s
Ethanol solution, stir, stand 8-20 hours, filtering, decompression filtrate recycling ethanol, reclaim concentrate, produce the above
The extract of Chinese medicine.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711250472.2A CN107737055A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of pure natural water lock cosmetics |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711250472.2A CN107737055A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of pure natural water lock cosmetics |
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| Publication Number | Publication Date |
|---|---|
| CN107737055A true CN107737055A (en) | 2018-02-27 |
Family
ID=61238814
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711250472.2A Withdrawn CN107737055A (en) | 2017-12-01 | 2017-12-01 | A kind of preparation method of pure natural water lock cosmetics |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108785167A (en) * | 2018-07-11 | 2018-11-13 | 王培战 | Root of Dahurain angelica liquid bio fermentate and preparation method thereof and the purposes in terms of cosmetics |
| CN112662478A (en) * | 2021-01-14 | 2021-04-16 | 四川绿色本草科技发展有限公司 | Chrysanthemum essence, oral cleaning product containing chrysanthemum essence and preparation method of oral cleaning product |
-
2017
- 2017-12-01 CN CN201711250472.2A patent/CN107737055A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108785167A (en) * | 2018-07-11 | 2018-11-13 | 王培战 | Root of Dahurain angelica liquid bio fermentate and preparation method thereof and the purposes in terms of cosmetics |
| CN112662478A (en) * | 2021-01-14 | 2021-04-16 | 四川绿色本草科技发展有限公司 | Chrysanthemum essence, oral cleaning product containing chrysanthemum essence and preparation method of oral cleaning product |
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