CN107714616A

CN107714616A - A kind of moisturizing, crease-resistant daily pad pasting composition and preparation method thereof

Info

Publication number: CN107714616A
Application number: CN201711180790.6A
Authority: CN
Inventors: 柳继成
Original assignee: Shanghai He Xuan Brand Management Co Ltd
Current assignee: Shanghai He Xuan Brand Management Co Ltd
Priority date: 2017-11-23
Filing date: 2017-11-23
Publication date: 2018-02-23

Abstract

The present invention relates to a kind of moisturizing, crease-resistant daily pad pasting composition, eye microcirculation is improved by natural marine conotoxin, suppress eye contraction and play significant anti-wrinkle effect, with three kinds of collagen synergy, deeply preserving moisture, strengthen anti-wrinkle effect, glycerine, propane diols, Chondrus crispus extract, 1, 2 hexylene glycols, glycine betaine and allantoin etc. strengthen moisturizing and moisturizing effect, ceramide, tocopherol acetate water lock moisturizing, the repair for strengthening the composition to skin is used in combination in glucose and allantoin, consolidate moisturizing, crease-resistant beneficial effect, also iris action of the skin to extraneous ultraviolet radiation etc. is strengthened.The moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, according to each chemical property and effect, using specific addition step and order by merging, it is uniformly dispersed, the skin care system of stable system, the moisturizing of composition, crease-resistant skin care effect is set farthest to be played.

Description

A kind of moisturizing, crease-resistant daily pad pasting composition and preparation method thereof

Technical field

The invention belongs to daily use chemicals technical field, and in particular to a kind of moisturizing, crease-resistant daily pad pasting composition and its preparation Method.

Background technology

Age increases, seasonal variations and sunlight, air pollution and frequently using various factors such as electronic products Cause skin corium collapse, moisture-retaining capacity decline, the various problems such as dry skin aging.Especially eye part skin, it is human body skin The most weak position of skin, skin is thin, lean, and lack flexibility fiber and collagen structure, and long-term use eye is improper and radiates, be empty The influence of gas pollution etc., easily cause the various skin symptoms such as dry eye part skin, microgroove and pouch.

Daytime is the clear-headed stage that body energy is used, should be based on " defence " to eye maintenance, sun-proof, moisturizing, antioxygen Change the important goal for being referred to as eye maintenance in the daytime, and night is physiological function rest period for nursing of self-discipline, the eye of one day tired out Portion's skin requires supplementation with more nutritional ingredients, eye skin is releived and maintenance.

But the eyeware products and solution for lenses and contact lenses that in the market is common, including eye patch mostly not because of the day and night nursing demand of skin and Design is made a distinction in nutritional ingredient, even if causing what can not be metabolized in eye patch containing beneficial nutritional ingredient in skin It is absorbed and used in cycle, can causes eye nutritional ingredient process because nutrition can not be rapidly absorbed on the contrary, forms fat Grain etc., is unfavorable for the nursing of eye skin on the contrary.

The content of the invention

Based on problem above, it is an object of the invention to provide a kind of moisturizing, crease-resistant daily pad pasting composition.

Another object of the present invention is to provide a kind of preparation method of the composition.

The technical scheme is that：

The present invention provides a kind of moisturizing, crease-resistant daily pad pasting composition, including following components in percentage by weight：

Hydrolyzed wheat protein 0.1-0.5%, hydrolytic collagen 0.1-0.5%, hydrolytic soya bean protein 0.1-0.5%, natural sea Foreign conotoxin 2-5%, ceramide 0.1-0.5%, tocopherol acetate 0.5-1%, glycerine 2-5%, propane diols 2-5%, 1,2- hexylene glycol 0.4-0.7%, glycine betaine 0.5-1%, Chondrus crispus extract 0.1-0.5%, allantoin 0.1-0.2%, Glucose 0.1-0.5%, hydrolecithin 0.1-0.5% and EDETATE SODIUM 0.01-0.02%；Excess water.

According to the moisturizing of the present invention, crease-resistant daily pad pasting composition, it is preferred that the component also includes acrylic acid (ester) Class/C10-30 alkylol acrylamide acid esters cross-linked polymers 0.1-0.5%, xanthans 0.1-0.5% and budding short stalk enzyme polysaccharide 2- 3%.

Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers in above component have moisturizing, emulsification, increasing Thick and film forming effect；Xanthans also has the function that stable, thickening and emulsification；The short stalk enzyme polysaccharide of sprouting have thickening and into The effect of film.Above weight than component as the moisture-keeping crease-shedding composition component add, described composition can be made Dispersed and have suitable mobility, suitably the active ingredient as eye patch carries out the production of daily pad pasting.

According to the moisturizing of the present invention, crease-resistant daily pad pasting composition, it is preferred that the component also includes triethanolamine 0.1-0.5%.

According to the moisturizing of the present invention, crease-resistant daily pad pasting composition, it is preferred that the component also includes para hydroxybenzene second Ketone 0.3-0.7% and essence 0.001-0.004%.

The present invention also provides a kind of moisturizing, the preparation method of crease-resistant daily pad pasting composition, the preparation method Comprise the following steps：

(1) water is heated, adds glycerine, propane diols, EDETATE SODIUM, glycine betaine, allantoin, xanthans, third while stirring Olefin(e) acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme polysaccharide, are well mixed, obtain the first mixing Thing；

(2) homogeneous and emulsification are carried out successively in the first mixture for obtaining step (1)；

(3) first mixture for completing emulsification is cooled to less than 45 DEG C, 1,2- of input hexylene glycols, glucose and hydrogen Change lecithin, be well mixed, obtain the second mixture；

(4) second mixture is cooled, input natural marine conotoxin, hydrolyzed wheat protein, hydrolytic collagen, water Soybean protein, Chondrus crispus extract, ceramide and tocopherol acetate are solved, is well mixed, obtains the daily pad pasting Composition.

According to moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, it is preferred that in step (1), Heat water to 80-85 DEG C.

According to moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, it is preferred that in step (2), Homogenizing time is 3-5min, then in 80-85 DEG C of emulsified 15-20min.

According to moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, it is preferred that in step (2), Mixing speed in emulsion process is 50-70r/min.

According to moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, it is preferred that in step (4), Second mixture is cooled to less than 40 DEG C.

When including parahydroxyacet-ophenone and essence according to moisturizing of the present invention, crease-resistant daily pad pasting composition, institute Preparation method is stated to comprise the following steps：

(1) heat water to 80-85 DEG C, while stirring add glycerine, propane diols, EDETATE SODIUM, glycine betaine, allantoin, Xanthans, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme polysaccharide, are well mixed, obtain To the first mixture；

(2) homogeneous 3-5min is first carried out in the first mixture for obtaining step (1), then in 80-85 DEG C of emulsified 15- 20min, it is 50-70r/min to keep the speed of agitator in emulsion process；

(3) first mixture for completing emulsification is cooled to less than 45 DEG C, put into 1,2- hexylene glycols, triethanolamine, Glucose, hydrolecithin, parahydroxyacet-ophenone and essence, it is well mixed, obtains the second mixture；

(4) second mixture is cooled to less than 40 DEG C, input natural marine conotoxin, hydrolyzed wheat protein, Hydrolytic collagen, hydrolytic soya bean protein, Chondrus crispus extract, ceramide and tocopherol acetate, it is well mixed, obtains institute State daily pad pasting composition.

In order to facilitate understanding moisturizing of the present invention, the technical scheme of crease-resistant daily pad pasting composition, to part material group Divide and be briefly described：

Natural marine conotoxin：Rich in aspartic acid, arginine, serine, alanine, glutamic acid, proline, sweet ammonia Acid, lysine, histidine, tryptophan, cystine and dipeptides diaminobutyryl benzyl amide diacetin, can significantly improve eye Portion's microcirculation, mitigate livid ring around eye, suppress the contraction of eye muscle, so as to reach the effect for mitigating wrinkle.

Three kinds of hydrolyzed wheat protein, hydrolytic collagen, hydrolytic soya bean protein collagen compoundings, form protect on a skin surface Moist diaphragm, promote sticking together for epidermal cell epimatrix, keep the tight of epidermis lipid monofilm, improve cell Protein level, promote the synthesis of collagen, so as to cooperative reinforcing anti-wrinkle effect.

Ceramide and tocopherol acetate promote skin metabolism, prevent pigment deposition, improve skin elasticity；And god Close with the structure of matter of keratoderma through acid amides, the water that can be penetrated into quickly in skin, and cuticula combines, and is formed a kind of Network structure, moisture is pinned, repair skin barrier, skin care.

Glucose has photoprotection, prevents ultraviolet to be directed through skin, can be calm with depigmentaton, repairs skin.

I.e. described moisturizing, crease-resistant daily pad pasting composition, shunk, played by improving eye microcirculation, suppressing eye Anti-wrinkle effect, with three kinds of collagen synergy, play deeply preserving moisture, crease-resistant technique effect, ceramide and tocopherol Acetic acid esters is combined, and not only acts as the effect of moisturizing skin, moreover it is possible to network structure is combined to form with the water in keratoderma, Moisture is pinned, not easily runs off the active ingredient in the moisturizing, crease-resistant daily pad pasting composition, permanent effect；In addition, also It is used in combination by glucose and allantoin, further enhances repair of the composition to skin, is consolidated moisturizing, resists The beneficial effect of wrinkle, also strengthen iris action of the skin to extraneous ultraviolet radiation etc..

The all components raw material that the present invention relates to is embodied in《Cosmetic material Names Catalogue (2015 is used Version)》In.

Beneficial effects of the present invention are：

The moisturizing provided by the invention, crease-resistant daily pad pasting composition, pass through the correlation of corresponding percentage by weight Component, significant anti-wrinkle effect is played by improving eye microcirculation, suppressing eye contraction, is made with three kinds of collagens joints With, deeply preserving moisture, enhancing anti-wrinkle effect, glycerine, propane diols, Chondrus crispus extract, 1,2- hexylene glycols, glycine betaine and allantois Element etc. strengthens moisturizing and moisturizing effect, ceramide, tocopherol acetate water lock moisturizing, and glucose and allantoin are used in combination and increased Strong repair of the composition to skin, consolidates moisturizing, crease-resistant beneficial effect, also strengthens skin to extraneous ultraviolet spoke The iris action penetrated etc..

Moisturizing of the present invention, the preparation method of crease-resistant daily pad pasting composition, according to each composition chemically Matter and corresponding effect, using specific addition step and order by merging, it is uniformly dispersed, the skin care body of stable system System, allows the skin care moisturizing of the composition, crease-resistant skin care effect farthest to be utilized and played.

Embodiment

To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below Detailed description.Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Base Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned Other embodiment, belong to the scope that the present invention is protected.

Embodiment 1

Hydrolyzed wheat protein 0.1%, hydrolytic collagen 0.5%, hydrolytic soya bean protein 0.1%, natural marine conotoxin 5%th, ceramide 0.1%, tocopherol acetate 1%, glycerine 2%, propane diols 5%, 1,2- hexylene glycols 0.4%, glycine betaine 1%th, Chondrus crispus extract 0.1%, allantoin 0.2%, glucose 0.1%, hydrolecithin 0.5% and EDETATE SODIUM 0.01%；Excess water.

Above-mentioned moisturizing, the preparation method of crease-resistant daily pad pasting composition, comprise the following steps：

(1) water is put into aqueous phase pot and is heated to 85 DEG C, insulation, add glycerine, propane diols, EDTA bis- while stirring Sodium, glycine betaine, allantoin, xanthans, it is well mixed, obtains the first mixture；

(2) the first mixture vacuum for obtaining step (1) is pumped into emulsification pot, first homogeneous 3min, then the breast at 85 DEG C Change 15min, the mixing speed in emulsion process is 70r/min；

Embodiment 2

Hydrolyzed wheat protein 0.5%, hydrolytic collagen 0.1%, hydrolytic soya bean protein 0.5%, natural marine conotoxin 2%th, ceramide 0.5%, tocopherol acetate 0.5%, glycerine 5%, propane diols 2%, 1,2- hexylene glycols 0.7%, glycine betaine 0.5%th, Chondrus crispus extract 0.5%, allantoin 0.1%, glucose 0.5%, hydrolecithin 0.1%, EDETATE SODIUM 0.02%th, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.1%, xanthans 0.5% and budding short stalk enzyme Polysaccharide 2%；Excess water.

(1) water is put into aqueous phase pot and is heated to 80 DEG C, insulation, add glycerine, propane diols, EDTA bis- while stirring Sodium, glycine betaine, allantoin, xanthans, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme Polysaccharide, it is well mixed, obtains the first mixture；

(2) the first mixture vacuum for obtaining step (1) is pumped into emulsification pot, first homogeneous 5min, then the breast at 80 DEG C Change 20min, the mixing speed in emulsion process is 50r/min；

Embodiment 3

Hydrolyzed wheat protein 0.4%, hydrolytic collagen 0.2%, hydrolytic soya bean protein 0.3%, natural marine conotoxin 2%th, ceramide 0.2%, tocopherol acetate 0.8%, glycerine 3%, propane diols 2%, 1,2- hexylene glycols 0.6%, three ethanol Amine 0.1%, glycine betaine 0.5%, Chondrus crispus extract 0.3%, allantoin 0.1%, glucose 0.5%, hydrolecithin 0.1%th, EDETATE SODIUM 0.02%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.5%, xanthans 0.1% and budding short stalk enzyme polysaccharide 3%；Excess water.

(1) water is put into aqueous phase pot and is heated to 85 DEG C, insulation, add glycerine, propane diols, EDTA bis- while stirring Sodium, glycine betaine, allantoin, xanthans, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme Polysaccharide, it is well mixed, obtains the first mixture；

(3) first mixture for completing emulsification is cooled to less than 45 DEG C, put into 1,2- hexylene glycols, triethanolamine, Glucose and hydrolecithin, it is well mixed, obtains the second mixture；

Embodiment 4

Hydrolyzed wheat protein 0.3%, hydrolytic collagen 0.4%, hydrolytic soya bean protein 0.3%, natural marine conotoxin 4%th, ceramide 0.3%, tocopherol acetate 0.7%, glycerine 3%, propane diols 4%, 1,2- hexylene glycols 0.6%, three ethanol Amine 0.5%, glycine betaine 0.6%, Chondrus crispus extract 0.2%, allantoin 0.15%, glucose 0.4%, hydrolecithin 0.2%th, EDETATE SODIUM 0.01%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.2%, xanthans 0.3% and budding short stalk enzyme polysaccharide 2%, parahydroxyacet-ophenone 0.3%, essence 0.004%, excess water.

(1) water is put into aqueous phase pot and is heated to 82 DEG C, insulation, add glycerine, propane diols, EDTA bis- while stirring Sodium, glycine betaine, allantoin, xanthans, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme Polysaccharide, it is well mixed, obtains the first mixture；

(2) the first mixture vacuum for obtaining step (1) is pumped into emulsification pot, first homogeneous 4min, then the breast at 84 DEG C Change 17min, the mixing speed in emulsion process is 60r/min；

Embodiment 5

Hydrolyzed wheat protein 0.1%, hydrolytic collagen 0.3%, hydrolytic soya bean protein 0.25%, natural marine conotoxin 2%th, ceramide 0.3%, tocopherol acetate 0.7%, glycerine 4%, propane diols 2%, 1,2- hexylene glycols 0.6%, three ethanol Amine 0.2%, glycine betaine 0.6%, Chondrus crispus extract 0.3%, allantoin 0.1%, glucose 0.2%, hydrolecithin 0.2%th, EDETATE SODIUM 0.01%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.1%, xanthans 0.5%th, sprout short stalk enzyme polysaccharide 2%, parahydroxyacet-ophenone 0.7% and essence 0.001%；Excess water.

Embodiment 6

Hydrolyzed wheat protein 0.2%, hydrolytic collagen 0.3%, hydrolytic soya bean protein 0.5%, natural marine conotoxin 3%th, ceramide 0.2%, tocopherol acetate 0.8%, glycerine 5%, propane diols 3%, 1,2- hexylene glycols 0.5%, three ethanol Amine 0.2%, glycine betaine 0.6%, Chondrus crispus extract 0.3%, allantoin 0.1%, glucose 0.2%, hydrolecithin 0.2%th, EDETATE SODIUM 0.01%, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer 0.1%, xanthans 0.25%th, sprout short stalk enzyme polysaccharide 2%, parahydroxyacet-ophenone 0.6% and essence 0.003%；Excess water.

(2) the first mixture vacuum for obtaining step (1) is pumped into emulsification pot, first homogeneous 4min, then the breast at 85 DEG C Change 17min, the mixing speed in emulsion process is 50r/min；

Experimental example

1st, it is more than one full year of life that 100 18 are collected, the female volunteers below 60 one full year of life, all volunteers have because of long-term use Electronic product, the symptom such as eye dryness, microgroove, pouch caused by irregular and air pollution etc. of living.

Above-mentioned 100 volunteers are divided into two groups, one group is experimental group, uses the group described in containing the embodiment of the present invention 6 The daily pad pasting of compound；One group is blank control group (having placebo effect).

2nd, application method

After early morning face cleaning, 20min is sticked with eye patch respectively, remaining liq is then gently massaged into and is completely absorbed.Often Regular 3 times of week, during which without using other skin care item.After persistently using 3 months, the improvement situation of eye part skin is counted.As a result such as Under：

It is effective：Eye part skin water content significantly raises, microgroove substantially subtract it is light, pouch be obviously reduced in addition disappear；

Effectively：Periocualr skin water content raises, and microgroove, which has, subtracts light trend, and pouch reduces；

It is invalid：Eye part skin water content, microgroove and pouch do not have significant change.

Table 1

	Effective/%	Effectively/%	Invalid/%	Total effective rate/%
					Experimental group	27	17	6	88
Control group	0	3	47	6

As can be seen from Table 1, adhered to the composition containing the present invention after sticking 3 months, improve skin microgroove and pouch Total effective rate up to 88%, and found in statistics, for the female group of 18-30 year, use the daily of the present composition Pad pasting sticked after effective percentage up to more than 98%.

Thus, it can be known that the moisturizing of the present invention, crease-resistant daily pad pasting composition, for long-term use of electronic product, are received Solar radiation and caused by eye dryness, microgroove and pouch be significantly improved effect, to the female group between 18-30 year The improvement result of eye skin problem be especially apparent.

The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all be contained Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.

Claims

1. a kind of moisturizing, crease-resistant daily pad pasting composition, it is characterised in that including following components in percentage by weight：

Hydrolyzed wheat protein 0.1-0.5%, hydrolytic collagen 0.1-0.5%, hydrolytic soya bean protein 0.1-0.5%, natural sea potato Spiral shell toxin 2-5%, ceramide 0.1-0.5%, tocopherol acetate 0.5-1%, glycerine 2-5%, propane diols 2-5%, 1,2- Hexylene glycol 0.4-0.7%, glycine betaine 0.5-1%, Chondrus crispus extract 0.1-0.5%, allantoin 0.1-0.2%, grape Sugared 0.1-0.5%, hydrolecithin 0.1-0.5% and EDETATE SODIUM 0.01-0.02%；Surplus is water.

2. moisturizing according to claim 1, crease-resistant daily pad pasting composition, it is characterised in that also including acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers 0.1-0.5%, xanthans 0.1-0.5% and budding short stalk enzyme polysaccharide 2-3%.

3. moisturizing according to claim 2, crease-resistant daily pad pasting composition, it is characterised in that also including triethanolamine 0.1-0.5%.

4. moisturizing according to claim 3, crease-resistant daily pad pasting composition, it is characterised in that also including para hydroxybenzene Ethyl ketone 0.3-0.7% and essence 0.001-0.004%.

5. moisturizing according to claim 2, the preparation method of crease-resistant daily pad pasting composition, it is characterised in that described Preparation method comprises the following steps：

(1) water is heated, adds glycerine, propane diols, EDETATE SODIUM, glycine betaine, allantoin, xanthans, acrylic acid while stirring (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme polysaccharide, are well mixed, obtain the first mixture；

(2) the first mixture for obtaining step (1) carries out homogeneous and emulsification；

(3) first mixture for completing emulsification is cooled to less than 45 DEG C, 1,2- of input hexylene glycols, glucose and hydrogenation ovum Phosphatide, it is well mixed, obtains the second mixture；

(4) second mixture is cooled, input natural marine conotoxin, hydrolyzed wheat protein, hydrolytic collagen, hydrolysis are big Legumin, Chondrus crispus extract, ceramide and tocopherol acetate, it is well mixed, obtains the daily pad pasting combination Thing.

6. preparation method according to claim 5, it is characterised in that in step (1), heat water to 80-85 DEG C.

7. preparation method according to claim 5, it is characterised in that in step (2), homogenizing time 3-5min, so Afterwards in 80-85 DEG C of emulsified 15-20min.

8. preparation method according to claim 5, it is characterised in that in step (2), the stirring speed in emulsion process Spend for 50-70r/min.

9. preparation method according to claim 5, it is characterised in that in step (4), second mixture is cooled To less than 40 DEG C.

10. moisturizing according to claim 4, the preparation method of crease-resistant daily pad pasting composition, it is characterised in that described Preparation method comprises the following steps：

(1) 80-85 DEG C is heated water to, adds glycerine, propane diols, EDETATE SODIUM, glycine betaine, allantoin, xanthan while stirring Glue, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers and budding short stalk enzyme polysaccharide, are well mixed, obtain the One mixture；

(3) first mixture for completing emulsification is cooled to less than 45 DEG C, 1,2- of input hexylene glycols, triethanolamine, grape Sugar, hydrolecithin, parahydroxyacet-ophenone and essence, it is well mixed, obtains the second mixture；

(4) second mixture is cooled to less than 40 DEG C, input natural marine conotoxin, hydrolyzed wheat protein, hydrolysis Collagen, hydrolytic soya bean protein, Chondrus crispus extract, ceramide and tocopherol acetate, it is well mixed, obtains the day With pad pasting composition.