CN107713008A - A kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method - Google Patents
A kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method Download PDFInfo
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- CN107713008A CN107713008A CN201710927167.6A CN201710927167A CN107713008A CN 107713008 A CN107713008 A CN 107713008A CN 201710927167 A CN201710927167 A CN 201710927167A CN 107713008 A CN107713008 A CN 107713008A
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- fried pearl
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- cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
- A24D3/048—Tobacco smoke filters characterised by their shape or structure containing additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/04—Starch derivatives, e.g. crosslinked derivatives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/04—Starch derivatives, e.g. crosslinked derivatives
- C08L3/06—Esters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/04—Starch derivatives, e.g. crosslinked derivatives
- C08L3/08—Ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L3/00—Compositions of starch, amylose or amylopectin or of their derivatives or degradation products
- C08L3/04—Starch derivatives, e.g. crosslinked derivatives
- C08L3/10—Oxidised starch
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Grain Derivatives (AREA)
Abstract
The invention discloses a kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method, the quick-fried pearl compound wall materialses include two layers, and internal layer is specific hot melt adhesive material, after specific hot melt adhesive is heated into molten condition, it is placed in 50 90 DEG C of storage tanks and is incubated, this is compound wall materialses internal layer.Outer layer is made up of quickly dissolving agar, locust bean gum, converted starch and deionized water, and its proportioning is：2~10：0.5~5：5~30：55~92.5, by the mixed-powder of quickly dissolving agar, locust bean gum and converted starch, quick stirring is added in 80 ± 5 DEG C of deionized waters to being completely dissolved, mixing time is 0.5-1 hour, vacuumize to be placed in heating insulation layer storage tank after de-bubble and be incubated, this glue is compound wall materialses outer layer；The present invention quick-fried pearl compound wall materialses point are inside and outside two layers, and internal layer be water impermeable membrane, can effectively obstruct inner core liquid and water-soluble essence exosmoses, and it is solid and have the shell of hardness that outer layer can assign quick-fried pearl, beneficial to explosion.
Description
Technical field
The invention belongs to quick-fried pearl technical field, and in particular to a kind of quick-fried Zhu Bi of inanimacy cigarette for wrapping up water-soluble essence
Material and preparation method.
Background technology
Cigarette is to wrap into essence in soft capsule with quick-fried pearl, is put into filter tip, and capsule is extruded by it using hand before suction
Essence therein is discharged, while increase operation is interesting, the overall organoleptic quality of tobacco product can be improved.This is required
Quick-fried pearl possesses the characteristics of " shape circle, pinching loud, liquid-impermeable ".
In the prior art, using the molten quick-fried pearl of essence of oil to be common, because cigarette will be far more than the molten perfume (or spice) of oil with the species of water-soluble essence
Essence, to develop the product of more appropriate client colony taste demands, the quick-fried pearl that can wrap up water-soluble essence is developed into the industry
Focus.Patent of invention CN103815541 A disclose a kind of three layers of cigarette quick-fried pearl capsule with diuresis promoting function and preparation method thereof, are related to one kind three
Layer cigarette quick-fried pearl capsule with diuresis promoting function and preparation method thereof, its capsule shells are two layers, and internal layer is sodium alginate complex compound, and outer layer is wax material
Material；Patent of invention CN103815542 B disclose a kind of four layers of cigarette capsule with diuresis promoting function and preparation method thereof, are related to a kind of four layers of cigarette and use
Capsule with diuresis promoting function and preparation method thereof, its capsule shells are three layers, and interior one layer is sodium alginate complex compound, and interior two layers are wax material, outside
Layer is again sodium alginate complex compound；The wax material layer that above patent uses is to be easy to rupture, and this can cause the conjunction of finished product
Lattice rate is extremely low, even if will not also play the effect of significantly improving in wax coat outer wrapping sodium alginate layer again.Apply for a patent CN
104479870 A disclose cigarette capsule with diuresis promoting function that a kind of complex salt is wall material and preparation method thereof, and it is wall to be related to a kind of complex salt
Cigarette capsule with diuresis promoting function of material and preparation method thereof, its inner core liquid are molded with inwall by sodium alginate, and sodium alginate is running into divalence
It can be molded immediately after ion, but with the extension of time, due to ion motion, the sodium alginate in its inner core liquid also can be slowly
Shaping solidification, so capsule with diuresis promoting function has the risk that significant conversion is solid pearl, and the risk is uncontrollable, and in addition, it is made
Wax material covering is similarly difficult to play the effect for preventing water translocation.
The needs of to meet industry development present situation and client's difference religious belief, the quick-fried pearl wall material (such as gelatin) of animality
It is national or even disabled at some because its special animal origin has not been praised highly gradually, therefore develop the quick-fried Zhu Bi of inanimacy
Material material can be more suitable for the quick stable development of industry.Quick-fried pearl wall material is inanimacy raw material used in the present invention, is met
Industry development trend.
PUR (English name：HotGlue) it is high polymer material, its physical state changes with temperature in certain temperature range
Become and change, it is nonpoisonous and tasteless, belong to environmental-protecting chemical product.The species of PUR is a lot, and present invention selection softening point is low, water resistance
Good, stability height, use can be heated repeatedly, the specific hot melt adhesive after film forming with certain intensity and toughness, as quick-fried Zhu Bi
Material can play the effect of fabulous barrier moisture extravasation.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide a kind of inanimacy cigarette for wrapping up water-soluble essence with quick-fried
Pearl wall material and preparation method.
To achieve the above object, the quick-fried pearl wall material of the inanimacy cigarette provided by the invention for wrapping up water-soluble essence, it is special
Sign is：Comprising inside and outside two layers, internal layer is hot melt adhesive film, obstructs moisture, to prevent water point and soluble perfume to moving outside
Move；Outer layer is made up of quickly dissolving agar, locust bean gum, converted starch, 80 ± 5 DEG C of deionized waters, the quickly dissolving agar, locust bean
80 ± 5 DEG C of glue, converted starch deionized water quality ratios are 2~10：0.5~5：5~30：55~92.5.
Preferably, the quickly dissolving agar of the outer layer：Locust bean gum：Converted starch：80 ± 5 DEG C of deionized water quality
Than for 3~8：1.5~4：10~25：63~85.5.
The present invention also provides a kind of inanimacy cigarette for wrapping up water-soluble essence preparation method of quick-fried pearl wall material, and it includes
Following steps：
(1) after internal layer specific hot melt adhesive powder/grain being heated into thawing, it is placed in the storage tank with heating interlayer, interlayer
50-90 DEG C is heated to steam, and insulation, gained hot melt adhesive liquid is that can wrap up the quick-fried pearl wall material of the inanimacy cigarette of water-soluble essence
Internal layer；
(2) according to the above ratio, after outer skin materials are well mixed, insulated and stirred 0.5-1 hours are dissolved into glue, vacuumize
It is placed in 80 DEG C of storage tanks, is incubated after de-bubble, gained glue is that can wrap up the quick-fried pearl wall material of the inanimacy cigarette of water-soluble essence
Outer layer.
The advantage of the invention is that：The present invention is used using specific hot melt adhesive as the inanimacy cigarette that can wrap up water-soluble essence
The internal layer of quick-fried pearl wall material, because such a high polymer material is waterproof, has certain intensity and toughness, can effectively prevent moisture and
Soluble perfume moves outside, it is ensured that the shaping of the quick-fried pearl of water-soluble essence is included, and the stability stored for a long time；Outer layer is using speed
Molten agar, locust bean gum and converted starch are compound, because this three kinds of plant colloids have fabulous synergistic function, can assign quick-fried
Pearl certain intensity and brittleness, ensure quick-fried pearl " that pinches breaks, pinches loud ".Water-soluble essence is wrapped up using what this compound wall materials made
Inanimacy cigarette have great improvement in terms of water preventing ability, weatherability, hardness and brittleness with quick-fried pearl.
Embodiment
With reference to embodiment, the present invention is described in further detail, but they do not form to the present invention and limited.
Embodiment 1
A kind of inanimacy cigarette for wrapping up water-soluble essence is made up of with quick-fried pearl wall material, internal layer extraordinary EVA hot-melt adhesive, outside
Layer is made up of the raw material of following components and parts by weight：2 parts of quickly dissolving agar, 0.5 part of locust bean gum, 5 parts of converted starch, deionization
92.5 parts of water.Specifically preparation method is：After internal layer specific hot melt adhesive powder/grain is heated into thawing, it is placed in heating interlayer
In storage tank, interlayer is heated to 75 DEG C with steam, and insulation, gained hot melt adhesive liquid is the inanimacy cigarette that can wrap up water-soluble essence
With the inner layer material of quick-fried pearl wall material；2 parts of quickly dissolving agars, 0.5 part of locust bean gum, 5 portions of converted starches are mixed to join 92.5 parts
In the deionized water of 80 DEG C of insulations, it is incubated quick stirring and is dissolved into uniform glue in 0.5 hour, 80 DEG C of storages are placed in after vacuumizing de-bubble
It is incubated in batch can, gained glue is the cladding material for the quick-fried pearl wall material of inanimacy cigarette that can wrap up water-soluble essence.Use
The quick-fried pearl pill dripping machines of DWJSY-III drop into quick-fried pearl.The obtained a diameter of 3.5mm of quick-fried pearl, internal layer thickness are 80um, and outer layer thickness is
150um, compression strength 11.5N.Quick-fried pearl is easier to pinch brokenly, and the clear and melodious sound can be sent when pinching mother-in-law.Dry quick-fried pearl is statically placed in suction
Water paper 24 hours, whole process slightly seep water phenomenon generation.
Embodiment 2
A kind of quick-fried pearl wall material of inanimacy cigarette for wrapping up water-soluble essence, internal layer are made up of extraordinary PA PURs, outside
Layer is made up of the raw material of following components and parts by weight：10 parts of quickly dissolving agar, 5 parts of locust bean gum, 30 parts of converted starch, deionization
55 parts of water.Specifically preparation method is：After internal layer specific hot melt adhesive powder/grain is heated into thawing, the storage with heating interlayer is placed in
In batch can, interlayer is heated to 50-90 DEG C with steam, and insulation, gained hot melt adhesive liquid is the inanimacy that can wrap up water-soluble essence
The inner layer material of the quick-fried pearl wall material of cigarette；10 parts of quickly dissolving agars, 5 parts of locust bean gums, 30 portions of converted starches are mixed to join 55 parts
In the deionized water of 80 DEG C of insulations, it is incubated quick stirring and is dissolved into uniform glue in 1 hour, 80 DEG C of storings are placed in after vacuumizing de-bubble
It is incubated in tank, gained glue is the cladding material for the quick-fried pearl wall material of inanimacy cigarette that can wrap up water-soluble essence.Use
The quick-fried pearl pill dripping machines of DWJSY-III drop into quick-fried pearl.The obtained a diameter of 3.5mm of quick-fried pearl, internal layer thickness are 100um, outer layer thickness
For 280um, compression strength 15N.Quick-fried pearl is less susceptible to pinch brokenly, and sound is smaller when pinching brokenly.Dry quick-fried pearl is statically placed in blotting paper
24 hours, whole process produced without infiltration phenomenon.
Embodiment 3
A kind of quick-fried pearl wall material of inanimacy cigarette for wrapping up water-soluble essence, internal layer are made up of extraordinary PET PURs, outside
Layer is made up of the raw material of following components and parts by weight：4 parts of quickly dissolving agar, 2 parts of locust bean gum, 15 parts of converted starch, deionization
79 parts of water.Specifically preparation method is：After internal layer specific hot melt adhesive powder/grain is heated into thawing, the storage with heating interlayer is placed in
In batch can, interlayer is heated to 50-90 DEG C with steam, and insulation, gained hot melt adhesive liquid is the inanimacy that can wrap up water-soluble essence
The inner layer material of the quick-fried pearl wall material of cigarette；4 parts of quickly dissolving agars, 2 parts of locust bean gums, 15 portions of converted starches are mixed to join 79 part 80
In the deionized water of DEG C insulation, it is incubated quick stirring and is dissolved into uniform glue in 0.6 hour, 80 DEG C of storings are placed in after vacuumizing de-bubble
It is incubated in tank, gained glue is the cladding material for the quick-fried pearl wall material of inanimacy cigarette that can wrap up water-soluble essence.Use
The quick-fried pearl pill dripping machines of DWJSY-III drop into quick-fried pearl.The obtained a diameter of 2.5mm of quick-fried pearl, internal layer thickness are 60um, and outer layer thickness is
180um, compression strength 13N.Quick-fried pearl can send the clear and melodious sound when pinching brokenly.Dry quick-fried pearl is statically placed in blotting paper 24 hours,
Whole process produces almost without infiltration phenomenon.
Embodiment 4
A kind of quick-fried pearl wall material of inanimacy cigarette for wrapping up water-soluble essence, internal layer are made up of extraordinary TPU PURs, outside
Layer is made up of the raw material of following components and parts by weight：6 parts of quickly dissolving agar, 2.5 parts of locust bean gum, 20 parts of converted starch, go from
Sub- 71.5 parts of water.Specifically preparation method is：After internal layer specific hot melt adhesive powder/grain is heated into thawing, it is placed in heating interlayer
Storage tank in, interlayer is heated to 50-90 DEG C with steam, insulation, and gained hot melt adhesive liquid is can wrap up water-soluble essence non-dynamic
The inner layer material of the quick-fried pearl wall material of physical property cigarette；6 parts of quickly dissolving agars, 2.5 parts of locust bean gums, 25 portions of converted starches are mixed to join
In the deionized water of 66.5 parts of 80 DEG C of insulations, it is incubated quick stirring and is dissolved into uniform glue in 0.8 hour, be placed in after vacuumizing de-bubble
It is incubated in 80 DEG C of storage tanks, gained glue is the cladding material for the quick-fried pearl wall material of inanimacy cigarette that can wrap up water-soluble essence.
Quick-fried pearl is dropped into using the quick-fried pearl pill dripping machines of DWJSY-III.The obtained a diameter of 2.5mm of quick-fried pearl, internal layer thickness are 100um, outer layer
Thickness is 200um, compression strength 13.5N.Quick-fried pearl can send the clear and melodious sound when pinching brokenly.Dry quick-fried pearl is statically placed in blotting paper
24 hours, whole process produced without infiltration phenomenon.
Claims (4)
1. a kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method, its compound wall materialses internal layer is hot melt
Glue；
Wherein, the extraordinary thermosol is any one or a few in EVA, PA, PET, PE, PES, TPU class.
2. a kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method, its compound wall materialses outer layer be by with
Lower component and the raw material of parts by weight composition：
Wherein, described quickly dissolving agar viscosity is 5-20mpa.s, intensity 400-1500g/cm2；
Described locust bean gum viscosity is 1000-3000mpa.s；
The converted starch is oxidized starch, acid treated starches, esterified and cross-linked starch, one kind in crosslinking etherified starch or several
Kind.
A kind of 3. wrap up water-soluble essence or inanimacy cigarette quick-fried pearl compound wall materialses and preparation method thereof, it is characterised in that its
Preparation method comprises the following steps that：
(1) after the extraordinary thermosol in above-mentioned formula being heated into molten condition, it is placed in 50-90 DEG C of storage tank and is incubated, this heat
Melten gel liquid is internal layer of the cigarette with quick-fried pearl compound wall materialses；
(2) 2~10 parts of quickly dissolving agar in above-mentioned formula, 0.5~5 part of locust bean gum and 5~30 portions of converted starches are mixed
It is dissolved in after closing uniformly in 55~92.5 parts of 80 ± 5 DEG C of deionized waters, stirring 0.5-1 hours are dissolved into glue, after vacuumizing de-bubble
It is placed in 80 DEG C of storage tanks and is incubated, this glue is outer layer of the cigarette with quick-fried pearl compound wall materialses.
4. a kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method according to claim 3,
It is characterized in that：Glue in the step (2), be by quickly dissolving agar, locust bean gum be respectively adopted 80 ± 5 DEG C of deionized waters,
Stirring is dissolved into quickly dissolving agar solution, locust bean gum solution and converted starch solution for 0.5~1 hour or by quickly dissolving agar, locust tree
Bean gum and converted starch be added in 80 ± 5 DEG C of deionized waters simultaneously, is stirred 0.5~1 hour and is dissolved into mixing sol solution.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710927167.6A CN107713008A (en) | 2017-10-09 | 2017-10-09 | A kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method |
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| CN201710927167.6A CN107713008A (en) | 2017-10-09 | 2017-10-09 | A kind of the inanimacy cigarette for wrapping up water-soluble essence quick-fried pearl wall material and preparation method |
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| CN107713008A true CN107713008A (en) | 2018-02-23 |
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Cited By (5)
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| CN109892690A (en) * | 2019-04-17 | 2019-06-18 | 云南中烟工业有限责任公司 | A kind of cigarette graphene-based complex microsphere and preparation method thereof |
| CN110140796A (en) * | 2019-05-16 | 2019-08-20 | 湖南尔康保健食品有限公司 | A kind of quick-fried pearl sugar and preparation method thereof |
| CN111436651A (en) * | 2019-01-16 | 2020-07-24 | 深圳波顿香料有限公司 | Blasting bead for cigarette and preparation method thereof |
| CN112641130A (en) * | 2020-12-25 | 2021-04-13 | 福建金闽再造烟叶发展有限公司 | Cigarette bead blasting quality control method |
| CN113325128A (en) * | 2021-05-28 | 2021-08-31 | 四川中烟工业有限责任公司 | Method for detecting moisture of surface skin of blasting bead |
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| CN113325128A (en) * | 2021-05-28 | 2021-08-31 | 四川中烟工业有限责任公司 | Method for detecting moisture of surface skin of blasting bead |
| CN113325128B (en) * | 2021-05-28 | 2022-10-21 | 四川中烟工业有限责任公司 | Method for detecting moisture of surface skin of blasting bead |
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