CN104726199A - Water-bearing capsule and preparation method thereof - Google Patents
Water-bearing capsule and preparation method thereof Download PDFInfo
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- CN104726199A CN104726199A CN201510063713.7A CN201510063713A CN104726199A CN 104726199 A CN104726199 A CN 104726199A CN 201510063713 A CN201510063713 A CN 201510063713A CN 104726199 A CN104726199 A CN 104726199A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- Chemical Kinetics & Catalysis (AREA)
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- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Medicinal Preparation (AREA)
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Abstract
The invention relates to a water-bearing capsule and a preparation method thereof. The water-bearing capsule consists of a water-based capsule core and a solid capsule shell wrapping the water-based capsule core, wherein the solid capsule shell consists of a hydrophobic membrane layer, a powder wrapping layer and a modified wax layer from outside in sequentially, and the strength of the solid capsule shell reaches 0.5-2.2kg. The water-bearing capsule can significantly reduce multiple harmful ingredients in smoke, reduces harms of a cigarette, and has the efficacy of improving a cigarette smoking moist feeling; the characteristic odor type can be endowed to the cigarette; in addition, the solid capsule shell of the water-bearing capsule is great in strength and difficult to break, so that stable water holding and quality guaranteeing effects of the cigarette are ensured; and the above benefits have very positive significance in improving the cigarette quality.
Description
[technical field]
The invention belongs to technical field of cigarette processing, more specifically, the present invention relates to a kind of containing capsule with diuresis promoting function, also relate to the described preparation method containing capsule with diuresis promoting function.
[background technology]
At present, there is the fashion trend of quick-fried pearl, capsule cigarette in domestic cigarette market.By adding capsule in cigarette filter, squeeze broken capsule before suction, release essence, promotes the mouthfeel of suction.But capsule cigarettes all is on the market all use hydrophilic gel softgel shell layer parcel oiliness essence, on moisture content of flue gas adopting without impact without exception.And the raising of flue gas moisture, can soft flue gas cigarette fragrant, reduce pungency, obviously improve the suction quality of cigarette, improve suction moisture feeling.In addition, existing essence spice for cigarette mostly is water-soluble substances, can only be water-soluble, can not be dissolved in oil-based solvent, and therefore the capsule smoked sheet capsule essence kind that can use and scope are greatly reduced on the market, and available essence is very limited.Meanwhile, water is a kind of good solvent, can dissolve many objectionable constituent in flue gas, reduces the harm of cigarette.
Therefore develop a kind of brand-new capsule with diuresis promoting function, make up the deficiency of existing oiliness soft capsule.The CN 201410059720.5 of Hubei Zhongyan Industry Co., Ltd's application discloses a kind of three layers of capsule with diuresis promoting function.It wraps up water-based essence with sodium alginate complex compound, then wraps up with wax.But comparatively speaking, processing units is complicated, simultaneously outer field wax insufficient strength, easily broken, the volatilization of moisture in capsule with diuresis promoting function can be caused.Their another part application CN 201410059949.9 discloses four layers of capsule with diuresis promoting function and preparation method thereof.The protective membrane being raw material by increase sodium alginate reduces breaking of wax layer, thus adds production cost.As can be seen here, they do not solve capsule circularity and wax layer strength problem, and they do not possess the function of parcel essence powder.
[summary of the invention]
[technical problem that will solve]
The object of this invention is to provide a kind of containing capsule with diuresis promoting function.
Another object of the present invention is to provide the described preparation method containing capsule with diuresis promoting function.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of containing capsule with diuresis promoting function.
Described is made up of the solid gums softgel shell of water-based capsule-core with the described water-based capsule-core of parcel containing capsule with diuresis promoting function;
Described solid gums softgel shell is that the tactic hydrophilic film of ecto-entad, pulvis integument and modified waxes layer form;
The weight ratio of described water-based capsule-core, hydrophilic film, pulvis integument and modified waxes layer is 5.0 ~ 50.0:0.1 ~ 5.0:1.0 ~ 30.0:0.1 ~ 5.0.
According to a preferred embodiment of the present invention, described water-based capsule-core is made up of 59 ~ 99 parts by weight of deionized water, 0 ~ 40 weight part honey or glucose, 0 ~ 31 parts by wt NaCl, 0 ~ 30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1 ~ 2 weight part sanitas.
According to another preferred embodiment of the present invention, described hydrophilic film is made up of 10 ~ 41 weight part sodium alginates, 0 ~ 41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin and 1 ~ 3 weight part sanitas.
According to another preferred embodiment of the present invention, described sanitas is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate.
According to another preferred embodiment of the present invention, described parcel bisque is made up of 0.8 ~ 1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1 ~ 3 weight part calcium chloride, calcium carbonate or calcium lactate and 0.1 ~ 0.5 parts by weight Corn starch, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh or sodium carbonate.
According to another preferred embodiment of the present invention, described modified waxes layer is made up of 4 ~ 7 weight part beeswaxs, Microcrystalline Wax or paraffin, 1 ~ 10 parts of EVA, 1 ~ 4 weight account polyethylene, polypropylene, polyisoprene or polyvinyl acetate (PVA), 0 ~ 2 weight part tuno gum and 0 ~ 35 weight part gutta-percha.
According to another preferred embodiment of the present invention, the intensity of described solid gums softgel shell is 0.5 ~ 2.2kg.
The invention still further relates to the described preparation method containing capsule with diuresis promoting function.The step of this preparation method is as follows:
A, preparation water-based capsule-core
0 ~ 40 weight part honey or glucose, 0 ~ 31 parts by wt NaCl, 0 ~ 30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1 ~ 2 weight part sanitas are dissolved in 59 ~ 99 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
4 ~ 7 weight part beeswaxs, Microcrystalline Wax or paraffin, 1 ~ 10 parts of EVA, 1 ~ 4 weight account polyethylene, polypropylene, polyisoprene, polyvinyl acetate (PVA) or styrene-butadiene rubber(SBR), 0 ~ 2 weight part tuno gum are mixed with 0 ~ 35 weight part gutta-percha, then heating and melting, obtains a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 20 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 100 ~ 150 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 15 ~ 20 parts by weight of deionized water, 0.8 ~ 1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1 ~ 3 weight part calcium chloride, calcium carbonate or calcium lactate, then W-Gum, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh powder or sodium carbonate powder is sprayed, warm air drying again, so form pulvis integument on aqueous solution kernel; Aforesaid operations repeats, until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 82 ~ 246 parts by weight of deionized water, 10 ~ 41 weight part sodium alginates, 0 ~ 41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin, 1 ~ 3 weight part sanitas; then 3 ~ 10min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
According to another preferred embodiment of the present invention, described sanitas is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate..
According to another preferred embodiment of the present invention, the step preparing aqueous solution kernel is as follows:
Use a kind of transparent glass bucket or the transparent glass bucket of oil circulation device is installed bottom it, at glass tank bottom filling silicone oil, its silicone oil height is 3/5 of transparent glass bucket height, adds liquid modified waxes on the surface at described silicone oil, and its modified waxes height is 1/8 of transparent glass bucket height;
Use conventional water dropper that water-based capsule-core is added drop-wise in liquid modified wax, form one deck modified waxes rete on the surface at water-based capsule-core, then by silicone oil, bottom glass tank, obtain aqueous solution kernel.
In more detail the present invention will be described below.
The present invention relates to a kind of containing capsule with diuresis promoting function.
Described is made up of the solid gums softgel shell of water-based capsule-core with the described water-based capsule-core of parcel containing capsule with diuresis promoting function;
Described solid gums softgel shell is that the tactic hydrophilic film of ecto-entad, pulvis integument and modified waxes layer form.
The weight ratio of described water-based capsule-core, hydrophilic film, pulvis integument and modified waxes layer is 5.0 ~ 50.0:0.1 ~ 5.0:1.0 ~ 30.0:0.1 ~ 5.0.
According to the present invention, if the amount of water-based capsule-core is less than 5.0, and when the weight ratio of other layer remains unchanged, then there will be the situation that capsule is not easily pinched brokenly; If the amount of water-based capsule-core is greater than 50.0, then there will be capsule size bigger than normal, be unfavorable for the problem of filter stick compound; Therefore, the amount of water-based capsule-core is 5.0 ~ 50.0 is appropriate.
Similarly, if the amount of hydrophilic film is less than 0.1, and when the weight ratio of other layer remains unchanged, then there will be capsule intensity inadequate, the flaky problem of pulvis integument; If the amount of hydrophilic film is greater than 5.0, then there will be the situation that capsule is not easily pinched brokenly; Therefore, the amount of hydrophilic film is 0.1 ~ 5.0 is rational.
If the amount of pulvis integument is less than 1.0, and when the weight ratio of other layer remains unchanged, then there will be capsule circularity inadequate, be unfavorable for the problem of filter stick compound; If the amount of pulvis integument is greater than 30.0, then there will be capsule size bigger than normal, be unfavorable for the problem of filter stick compound; Therefore, the amount of pulvis integument is 1.0 ~ 30.0 is rational.
If the amount of modified waxes layer is less than 0.1, and when the weight ratio of other layer remains unchanged, then there will be aqueous solution kernel easily broken, the not easily problem of subsequent disposal; If the amount of modified waxes layer is greater than 5.0, then can be unfavorable for the operation that truncates of aqueous solution kernel; Therefore, the amount of modified waxes layer is 0.1 ~ 5.0 is feasible.
In the present invention, according to Industry methods, adopt instrumental test, the intensity of described solid gums softgel shell is 0.5 ~ 2.2kg.
According to the present invention, the effect of described water-based capsule-core is mainly, for cigarette provides moisture, fragrance, to improve the suction mouthfeel of smoker.Described water-based capsule-core is made up of 59-99 parts by weight of deionized water, 0-40 weight part honey or glucose, 0-31 parts by wt NaCl, the acid of 0-30 parts by weight of lemon, water-soluble lemon essence or tobacco extract and 1-2 weight part sanitas.
Wherein, honey, glucose, sodium-chlor and citric acid are all the products that people know, water-soluble lemon essence and tobacco extract that the present invention uses also are all extensive product solds in the market, the water-soluble lemon essence such as sold with the taste essence of trade(brand)name taste by the taste essence and flavoring agent company limited of Hangzhou taste; The tobacco extract sold with trade(brand)name yunyan extract by Guangzhou daily use chemicals Chemical Co., Ltd..
Described sanitas is the important component in cigarette products, obvious impact is had on cigarette quality, the sanitas that the present invention uses is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate, and they are all extensive product solds in the market.
According to the present invention, the effect of described hydrophilic film is mainly fixing pulvis integument, promotes capsule intensity.
Described hydrophilic film is made up of 10-41 weight part sodium alginate, 0-41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin and 1-3 weight part sanitas.
In hydrophilic film of the present invention, when the amount of other component is in described scope, if the amount of sodium alginate is less than 10 weight parts, then there will be pelletized capsule surface gel growth excessively slow, the problem that gel-strength is inadequate; If the amount of sodium alginate is greater than 41 weight parts, then there will be gel growth too fast, the problem that capsule crushing strength is bigger than normal; Therefore, the amount of sodium alginate is 10-41 weight part is feasible.Similarly, when the amount of other component is in described scope, if the amount of gelatin etc. is greater than 41 weight parts, then there will be gelatin viscosity bigger than normal, not easily dispersed with stirring, the problem that finished capsule product intensity is bigger than normal; Therefore, the amount of gelatin etc. is 0-41 weight part is feasible.
The sodium alginate that the present invention uses and gelatin etc. are product solds in the market, the sodium alginate such as sold with trade(brand)name bright moon by Qingdao Mingyue Marine Alga Group Corp., Ltd.; The gelling gum sold with trade(brand)name Fu Feng by Fu Feng Group Co., Ltd.The sanitas used in this step is identical with previously described, does not repeat them here.
According to the present invention, the effect of described pulvis integument is mainly the circularity promoting capsule, gives the function of parcel essence powder.
Described parcel bisque is made up of 0.8-1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1-3 weight part calcium chloride, calcium carbonate or calcium lactate and 0.1-0.5 parts by weight Corn starch, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh or sodium carbonate.
In parcel bisque of the present invention, when the amount of other component is in described scope, if the amount of PEG-200 etc. is less than 0.8 weight part, then there will be aqueous solution core surface hydrophobicity too strong, the problem that pulvis not easily wraps up; If the amount of PEG-200 etc. is greater than 1.2 weight parts, then can reduce the fastness of pulvis parcel; Therefore, the amount of PEG-200 etc. is 0.8-1.2 weight part is feasible.
Similarly, when the amount of other component is in described scope, if the amount of calcium chloride etc. is less than 1 weight part, then there will be the incomplete problem of gel growth; If the amount of calcium chloride etc. is greater than 3 weight parts, then there will be the problem that finished capsule product intensity is excessive; Therefore, the amount of calcium chloride etc. is 1-3 weight part is rational.When the amount of other component is in described scope, if the amount of W-Gum etc. is less than 0.1 weight part, then there will be the problem that capsule circularity is inadequate; If the amount of W-Gum etc. is greater than 0.5 weight part, then there will be the problem that capsule size is bigger than normal; Therefore, the amount of W-Gum etc. is 0.1-0.5 weight part is appropriate.
PEG-200 (Macrogol 200), PEG-600 (Polyethylene Glycol-600) that the present invention uses, PEG-2000 (Macrogol 2000), PEG-6000 (polyethylene glycol 6000), calcium chloride, calcium carbonate or calcium lactate are product solds in the market, the PEG-200 such as sold with trade(brand)name Mitsui by Mitsui company.
W-Gum is the micro-yellowish powder of white.It is with 0.3% sulfurous acid soaking maize, then by broken, sieve, precipitate, dry, levigate etc. and the powder made.It contains a small amount of fat and protein etc., and it is product sold in the market, such as by Xing Mao corn development corporation, Ltd. of Zhucheng with the emerging trade product sold of trade(brand)name.
Dextrin is used to the technical terms weighing material cooking technique.
starchheating, acid or
amylaseeffect issue solution estranged and hydrolysis reaction, macromolecular Starch Conversion is become small molecules intermediate material, i.e. dextrin, it is product sold in the market, such as, meet U.S. product sold by Yunan County Yong Guang cyclodextrine company limited with trade(brand)name.
Vanillin food grade,1000.000000ine mesh is a kind of widely used edible spices.It is widely used in various need to increase milk breath blending food, tobacco, in daily life product, it is product sold in the market, such as by Shanghai Xinhua spices Food Co., Ltd with trade(brand)name snow bear product sold.
According to the present invention, the effect of described modified waxes layer is mainly to form aqueous solution kernel.
Described modified waxes layer is made up of 4-7 weight part beeswax, Microcrystalline Wax or paraffin, 1-10 parts of EVA, 1-2 weight account polyethylene, polypropylene, polyisoprene or polyvinyl acetate (PVA), 0-2 weight part tuno gum and 0-35 weight part gutta-percha.
In modified waxes layer of the present invention, when the amount of other component is in described scope, if the amount of beeswax etc. is less than 4 weight parts, then there will be the problem of modified waxes not easily melting; If the amount of beeswax etc. is greater than 7 weight parts, then there will be the problem of modified waxes low strength; Therefore, the amount of beeswax etc. is 4-7 weight part is feasible.
Similarly, when the amount of other component is in described scope, if the amount of EVA is less than 1 weight part, then there will be the problem of modified waxes low strength; If the amount of EVA is greater than 10 weight parts, then there will be the problem that modified waxes viscosity is higher; Therefore, the amount of EVA is 1-10 weight part is rational.When the amount of other component is in described scope, the amount as fruit polyethylene etc. is less than 1 weight part, then there will be the problem of modified waxes low strength; Amount as fruit polyethylene etc. is greater than 2 weight parts, then there will be the problem that modified waxes viscosity is higher; Therefore, the amount of polyethylene etc. is 1-2 weight part is appropriate.Tuno gum is identical with other component such as situation and beeswax of gutta-percha.
The beeswax that the present invention uses, EVA, polyethylene, tuno gum and gutta-percha etc. are all product solds in the market, the beeswax such as sold with trade(brand)name Kang Xin by Cangzhou Kang Xin beeswax Jiao Ye company limited, the tuno gum sold with trade(brand)name prosperous profit moral by Hubei Xin Runde Chemical Co., Ltd., by safe and comfortable Hanyin Hua Ye plant pharmaceutcal corporation, Ltd with the gutta-percha of the magnificent bright sale of trade(brand)name.
The invention still further relates to the described preparation method containing capsule with diuresis promoting function.The step of this preparation method is as follows:
A, preparation water-based capsule-core
0 ~ 40 weight part honey or glucose, 0 ~ 31 parts by wt NaCl, 0 ~ 30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1 ~ 2 weight part sanitas are dissolved in 59 ~ 99 parts by weight of deionized water, obtain described water-based capsule-core.
B, prepare aqueous solution kernel
4 ~ 7 weight part beeswaxs, Microcrystalline Wax or paraffin, 1 ~ 10 parts of EVA, 1 ~ 4 weight account polyethylene, polypropylene, polyisoprene, polyvinyl acetate (PVA) or styrene-butadiene rubber(SBR), 0 ~ 2 weight part tuno gum are mixed with 0 ~ 35 weight part gutta-percha, then heating and melting, obtains a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 20 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 100 ~ 150 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
The concrete steps preparing aqueous solution kernel are as follows:
According to the present invention, prepare a kind of transparent glass bucket that aqueous solution kernel needs use or the transparent glass bucket installing oil circulation device bottom it, its concrete structure is shown in accompanying drawing 1.
Use a kind of transparent glass bucket or the transparent glass bucket of oil circulation device is installed bottom it, at glass tank bottom filling silicone oil, its silicone oil height is 3/5 of transparent glass bucket height, adds liquid modified waxes on the surface at described silicone oil, and its modified waxes height is 1/8 of transparent glass bucket height;
Use conventional water dropper that water-based capsule-core is added drop-wise in liquid modified wax, form one deck modified waxes rete on the surface at water-based capsule-core, then by silicone oil, bottom glass tank, obtain aqueous solution kernel.
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 15 ~ 20 parts by weight of deionized water, 0.8 ~ 1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1 ~ 3 weight part calcium chloride, calcium carbonate or calcium lactate, then W-Gum, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh powder or sodium carbonate powder is sprayed, warm air drying again, so form pulvis integument on aqueous solution kernel; Aforesaid operations repeats, until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule.
In this step, the aqueous solution kernel method of truncating is that rolling friction truncates, and washing methods is the common rinsing of abluent for foodstuff.
The coating equipment in sugar production line that the present invention uses is such as the Chufa-type coating pan really sold with trade(brand)name gold by Taizhou Jin Cheng pharmaceutical machine company limited.
Described warm air drying uses Chufa-type coating pan to carry blast heater at temperature 50-80 DEG C, dry 10-20min under the condition of wind speed 10-40m/s.
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 82 ~ 246 parts by weight of deionized water, 10 ~ 41 weight part sodium alginates, 0 ~ 41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin, 1 ~ 3 weight part sanitas; then 3 ~ 10min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Described sanitas is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate.
The raw material used containing capsule with diuresis promoting function described in preparation describes above, does not repeat them here.
What adopt the inventive method to prepare has following feature containing capsule with diuresis promoting function:
Capsule with diuresis promoting function moderate strength, can wrap up water, soluble perfume and solid powder essence.All raw materials are food grade or medical grade, safety non-toxic.The suction quality of cigarette can be promoted well.
[beneficial effect]
The invention has the beneficial effects as follows: effect that can promote cigarette suction moisture feeling containing capsule with diuresis promoting function of the present invention; and cigarette feature odor type can be given; and the present invention is large containing capsule with diuresis promoting function capsule fortreating AIDS shell intensity; reach 0.5-2.2kg; not easily break; thus ensure that cigarette has stable water conservation preservation and effect, therefore, these all have very positive meaning for lifting cigarette quality.
[accompanying drawing explanation]
Fig. 1 is the dripping equipment for the preparation of aqueous solution kernel, A: interval type; B: continous way;
In figure:
1-water dropper, 2-water-based capsule-core liquid, the liquid modified wax of 3-, 4-silicone oil, 5-aqueous solution kernel, the import of 6-silicone oil, the outlet of 7-silicone oil.
Fig. 2 is equipped with the cigarette structure schematic diagram of the present invention containing capsule with diuresis promoting function;
The original-pack red plum cigarette of A-; B-is equipped with the red plum cigarette of the present invention containing capsule with diuresis promoting function in filter tip; C-in filter tip with B containing capsule with diuresis promoting function same position without the red plum cigarette of tow.
Fig. 3 is equipped with the cigarette structure schematic diagram of the present invention containing capsule with diuresis promoting function.
The original-pack red plum cigarette of A-; B-is equipped with the red plum cigarette of the present invention containing capsule with diuresis promoting function in filter tip; C-in filter tip with B containing the red plum cigarette of capsule with diuresis promoting function same position tow perforate.
[embodiment]
The present invention can be understood better by following embodiment.
Embodiment 1: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
310 parts by wt NaCl, 20 parts by weight water-soluble lemon flavours and 20 weight part potassium sorbate sanitass are dissolved in 650 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
By 80 weight part beeswaxs, 200 parts of EVA, 20 weight account polyethylenes, 70 weight part gutta-percha mixing, then heating and melting, obtains a kind of melt modification wax;
Use the equipment of accompanying drawing 1, the temperature of water-based capsule-core steps A obtained is adjusted to 10 ~ 15 DEG C, again water-based capsule-core being added drop-wise to temperature is in the melt modification wax of 120 ~ 150 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1 weight part PEG-600,3 weight part calcium chloride, then dextrin is sprayed, re-use drying plant warm air drying 2min under the condition of temperature 70 C, wind speed 15m/s, so form pulvis integument on aqueous solution kernel; Aforesaid operations repeats (0.1 weight part dextrin sprays several times), until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 2460 parts by weight of deionized water, 450 weight part sodium alginates, 60 weight part gelatin, 30 weight part potassium sorbate sanitass; then 5min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Embodiment 2: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
400 weight part honey and 10 parts by weight sodium sanitass are dissolved in 590 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
6 weight part paraffin, 1 parts of EVA, 1 weight part polyvinyl acetate (PVA), 1 weight part tuno gum are mixed with 1 weight part gutta-percha, then heating and melting, obtain a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 10 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 120 ~ 150 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1.0 weight part PEG-600,3 weight part calcium chloride, then W-Gum is sprayed, re-use drying plant warm air drying 2min under the condition of temperature 65 DEG C, wind speed 15m/s, so, aqueous solution kernel is formed pulvis integument; Aforesaid operations repeats (0.5 parts by weight Corn starch sprays several times), until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain, and described water-based glue is made up of 82 parts by weight of deionized water, 17 weight part sodium alginates and 1 parts by weight sodium sanitas, then stirs 5min; be separated; with water rinse, seasoning, obtain described containing capsule with diuresis promoting function.
Embodiment 3: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
30 weight part honey, 10 parts by weight of lemon acid are dissolved in 59 parts by weight of deionized water with 1 parts by weight sodium sanitas, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
By 7 weight part Microcrystalline Waxes, 2 parts of EVA, 1 weight part polyvinyl acetate (PVA) mixing, then heating and melting, obtains a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 10 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 110 ~ 130 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1 weight part PEG-200 and 3 weight part calcium chloride, then PEG-6000 is sprayed, re-use drying plant warm air drying 3min under the condition of temperature 70 C, wind speed 10m/s, so form pulvis integument on aqueous solution kernel; Aforesaid operations repeats (0.3 weight part PEG-6000 sprays several times), until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 246 parts by weight of deionized water, 41 weight part sodium alginates, 7 weight part gelling gums, 3 weight part guar gums and 3 weight part Sodium dehydroacetate sanitass; then 10min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Embodiment 4: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
1 weight part Sodium dehydroacetate sanitas is dissolved in 99 parts by weight of deionized water, obtains described water-based capsule-core;
B, prepare aqueous solution kernel
1 weight part beeswax, 4 weight part Microcrystalline Waxes, 2 parts of EVA, 1 weight part polyvinyl acetate (PVA) are mixed with 2 weight part tuno gums, then heating and melting, obtain a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 10 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 110 ~ 130 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1 weight part PEG-2000 and 2 weight part calcium chloride, then vanillin food grade,1000.000000ine mesh powder is sprayed, re-use drying plant warm air drying 2min under the condition of temperature 60 C, wind speed 20m/s, so, aqueous solution kernel is formed pulvis integument; Aforesaid operations repeats into (0.4 weight part vanillin food grade,1000.000000ine mesh powder sprays several times) OK, until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 246 parts by weight of deionized water, 41 weight part sodium alginates, 10 weight part agar, 3 weight part Sodium dehydroacetate sanitass; then 10min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Embodiment 5: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
30 weight part glucose, 10 weight part tobacco extracts and 1 weight part Sodium dehydroacetate sanitas are dissolved in 59 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
4 weight part Microcrystalline Waxes, 1 weight part polyvinyl acetate (PVA), 1 parts by weight of polypropylene, 2 weight part polyisoprene are mixed with 2 weight part gutta-percha, then heating and melting, obtain a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to room temperature ~ 20 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 100 ~ 120 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1 weight part PEG-200 and 3 weight part calcium lactates, then sodium carbonate powder is sprayed, re-use drying plant warm air drying 3min under the condition of temperature 75 DEG C, wind speed 10m/s, so, aqueous solution kernel is formed pulvis integument; Aforesaid operations repeats (0.2 parts by weight sodium carbonate sprays several times), until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 246 parts by weight of deionized water, 10 weight part sodium alginates, 41 weight part carrageenins, 3 weight part sodium Diacetate sanitass; then 3min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Embodiment 6: preparation is containing capsule with diuresis promoting function
The step of this preparation method is as follows:
A, preparation water-based capsule-core
30 parts by weight of lemon acid, 10 weight part tobacco extracts and 1 weight part sodium Diacetate sanitas are dissolved in 59 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
5 weight part beeswaxs, 1 weight account polyethylene, 2 weight part polyisoprene, 1 weight part polyvinyl acetate (PVA) are mixed with 1 weight part tuno gum, then heating and melting, obtain a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to room temperature ~ 20 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 100 ~ 120 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 16 parts by weight of deionized water, 1 weight part PEG-400 and 3 weight part calcium lactates, then sodium carbonate powder is sprayed, re-use drying plant warm air drying 2min under the condition of temperature 70 C, wind speed 12m/s, so, aqueous solution kernel is formed pulvis integument; Aforesaid operations repeats (0.3 parts by weight sodium carbonate part is sprayed several times), until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 246 parts by weight of deionized water, 5 weight part gelatin, 5 weight part methylcellulose gum, 41 weight part carrageenins and 3 weight part sodium Diacetate sanitass; then 3min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
Test example 1: the present invention smokes panel test on cigarette smoke moisture impact containing capsule with diuresis promoting function
Test method:
Use the red plum cigarette of Huang sold in the market as trial target.Remove 5mm filter tip silk in the longitudinal mid-way of the red plum tobacco filters of Huang to manually, for preparing at its empty cavity position placement embodiment of the present invention 1-3 contains capsule with diuresis promoting function.Control sample just removes 5mm tow.Their concrete structure is shown in accompanying drawing 2.
The method usually adopted in the art is adopted to organize 10 people's smoking groups to evaluate and test smoking effect.
Adopt the moisture content in industry ordinary method detection flue gas, the results are shown in Table 1 for it.
Table 1: containing capsule with diuresis promoting function on the impact of cigarette flue gas moisture and smoking result
The result of table 1 clearly illustrates that several effects containing capsule with diuresis promoting function with significant lifting cigarette suction moisture feeling in embodiment, and can give cigarette feature odor type, has obvious help for the quality promoting cigarette.
Test example 2: the present invention smokes panel test on cigarette smoke moisture impact containing capsule with diuresis promoting function
Test method:
Use the red plum cigarette of Huang sold in the market as trial target.To manually in the red plum tobacco bunch of Huang compound embodiment of the present invention 4-6 prepare containing capsule with diuresis promoting function.Control sample is just in its corresponding site perforate.Their concrete structure is shown in accompanying drawing 3.
The method usually adopted in the art is adopted to organize 10 people's smoking groups to evaluate and test smoking effect.
Adopt the moisture content in industry ordinary method detection flue gas, the results are shown in Table 2 for it.
Table 2: containing capsule with diuresis promoting function on the impact of cigarette flue gas moisture and smoking result
The result of table 2 clearly illustrates that several effects containing capsule with diuresis promoting function with significant lifting cigarette suction moisture feeling in embodiment, and can give cigarette feature odor type, has obvious help for the quality promoting cigarette.
Claims (10)
1., containing a capsule with diuresis promoting function, it is characterized in that it is made up of the solid gums softgel shell of water-based capsule-core with the described water-based capsule-core of parcel;
Described solid gums softgel shell is that the tactic hydrophilic film of ecto-entad, pulvis integument and modified waxes layer form;
The weight ratio of described water-based capsule-core, hydrophilic film, pulvis integument and modified waxes layer is 5.0 ~ 50.0:0.1 ~ 5.0:1.0 ~ 30.0:0.1 ~ 5.0.
2. according to claim 1 containing capsule with diuresis promoting function, it is characterized in that described water-based capsule-core is made up of 59 ~ 99 parts by weight of deionized water, 0 ~ 40 weight part honey or glucose, 0 ~ 31 parts by wt NaCl, 0 ~ 30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1 ~ 2 weight part sanitas.
3. according to claim 1 containing capsule with diuresis promoting function, it is characterized in that described hydrophilic film is made up of 10 ~ 41 weight part sodium alginates, 0 ~ 41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin and 1 ~ 3 weight part sanitas.
4. according to Claims 2 or 3 containing capsule with diuresis promoting function, it is characterized in that described sanitas is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate.
5. according to claim 1 containing capsule with diuresis promoting function, it is characterized in that described parcel bisque is made up of 0.8 ~ 1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1 ~ 3 weight part calcium chloride, calcium carbonate or calcium lactate and 0.1 ~ 0.5 parts by weight Corn starch, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh or sodium carbonate.
6. according to claim 1 containing capsule with diuresis promoting function, it is characterized in that described modified waxes layer is made up of 4 ~ 7 weight part beeswaxs, Microcrystalline Wax or paraffin, 1 ~ 10 parts of EVA, 1 ~ 4 weight account polyethylene, polypropylene, polyisoprene or polyvinyl acetate (PVA), 0 ~ 2 weight part tuno gum and 0 ~ 35 weight part gutta-percha.
7. according to claim 1 containing capsule with diuresis promoting function, it is characterized in that the intensity of described solid gums softgel shell is 0.5 to 2.2kg.
8. the preparation method containing capsule with diuresis promoting function according to claim 1, is characterized in that the step of this preparation method is as follows:
A, preparation water-based capsule-core
0 ~ 40 weight part honey or glucose, 0 ~ 31 parts by wt NaCl, 0 ~ 30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1 ~ 2 weight part sanitas are dissolved in 59 ~ 99 parts by weight of deionized water, obtain described water-based capsule-core;
B, prepare aqueous solution kernel
4 ~ 7 weight part beeswaxs, Microcrystalline Wax or paraffin, 1 ~ 10 parts of EVA, 1 ~ 4 weight account polyethylene, polypropylene, polyisoprene, polyvinyl acetate (PVA) or styrene-butadiene rubber(SBR), 0 ~ 2 weight part tuno gum are mixed with 0 ~ 35 weight part gutta-percha, then heating and melting, obtains a kind of melt modification wax;
The temperature of water-based capsule-core steps A obtained is adjusted to 5 ~ 20 DEG C, then water-based capsule-core is added drop-wise to temperature is in the melt modification wax of 100 ~ 150 DEG C, so form one deck curing hydrophobic modification cere on the surface at described water-based capsule-core, i.e. aqueous solution kernel;
C, prepare pulvis integument
The aqueous solution kernel that step B obtains is truncated and washing, the complete aqueous solution kernel of smooth surface is selected to put into coating equipment in sugar production line, spray a kind of parcel amidin be made up of 15 ~ 20 parts by weight of deionized water, 0.8 ~ 1.2 weight part PEG-200, PEG-600, PEG-2000 or PEG-6000,1 ~ 3 weight part calcium chloride, calcium carbonate or calcium lactate, then W-Gum, dextrin, PEG-6000, vanillin food grade,1000.000000ine mesh powder or sodium carbonate powder is sprayed, warm air drying again, so form pulvis integument on aqueous solution kernel; Aforesaid operations repeats, until obtain the round shaped grain capsule meeting Particle size requirements, i.e. and pelletized capsule;
D, prepare hydrophilic film
Water-based glue put into by the pelletized capsule allowing step C obtain; described water-based glue is made up of 82 ~ 246 parts by weight of deionized water, 10 ~ 41 weight part sodium alginates, 0 ~ 41 weight part gelatin, gelling gum, guar gum, methylcellulose gum, agar or carrageenin, 1 ~ 3 weight part sanitas; then 3 ~ 10min is stirred; be separated; with water rinse; seasoning, obtains described containing capsule with diuresis promoting function.
9. preparation method according to claim 7, is characterized in that described sanitas is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, Sodium dehydroacetate or calcium lactate.
10. preparation method according to claim 7, is characterized in that the step preparing aqueous solution kernel is as follows:
Use a kind of transparent glass bucket or the transparent glass bucket of oil circulation device is installed bottom it, at glass tank bottom filling silicone oil, its silicone oil height is 3/5 of transparent glass bucket height, adds liquid modified waxes on the surface at described silicone oil, and its modified waxes height is 1/8 of transparent glass bucket height;
Use conventional water dropper that water-based capsule-core is added drop-wise in liquid modified wax, form one deck modified waxes rete on the surface at water-based capsule-core, then by silicone oil, bottom glass tank, obtain aqueous solution kernel.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510063713.7A CN104726199B (en) | 2015-02-06 | 2015-02-06 | Water-bearing capsule and preparation method thereof |
| PCT/CN2015/077638 WO2016123869A1 (en) | 2015-02-06 | 2015-04-28 | Aqueous capsule and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510063713.7A CN104726199B (en) | 2015-02-06 | 2015-02-06 | Water-bearing capsule and preparation method thereof |
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| CN104726199A true CN104726199A (en) | 2015-06-24 |
| CN104726199B CN104726199B (en) | 2017-02-22 |
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| WO (1) | WO2016123869A1 (en) |
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| CN114011329B (en) * | 2021-11-29 | 2024-03-26 | 江苏大亚滤嘴材料有限公司 | Preparation method of water particles capable of increasing smoke moist feeling |
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| CN104726199B (en) | 2017-02-22 |
| WO2016123869A1 (en) | 2016-08-11 |
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Effective date of registration: 20190329 Address after: 335000 Longgang Industrial Park, Yingtan Hi-tech Industrial Development Zone, Jiangxi Province (in Yingtan CITIC Technology Co., Ltd.) Patentee after: Jiangxi Huabaoxin Technology Co., Ltd. Address before: 1180 Xingxian Road, Jiading District, Shanghai, 201821 Patentee before: Shanghai Huabao Biotechnology Co., Ltd. |