CN104726199B - Water-bearing capsule and preparation method thereof - Google Patents
Water-bearing capsule and preparation method thereof Download PDFInfo
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- CN104726199B CN104726199B CN201510063713.7A CN201510063713A CN104726199B CN 104726199 B CN104726199 B CN 104726199B CN 201510063713 A CN201510063713 A CN 201510063713A CN 104726199 B CN104726199 B CN 104726199B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Dispersion Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Materials Engineering (AREA)
- Medicinal Preparation (AREA)
- Confectionery (AREA)
Abstract
The invention relates to a water-bearing capsule and a preparation method thereof. The water-bearing capsule consists of a water-based capsule core and a solid capsule shell wrapping the water-based capsule core, wherein the solid capsule shell consists of a hydrophobic membrane layer, a powder wrapping layer and a modified wax layer from outside in sequentially, and the strength of the solid capsule shell reaches 0.5-2.2kg. The water-bearing capsule can significantly reduce multiple harmful ingredients in smoke, reduces harms of a cigarette, and has the efficacy of improving a cigarette smoking moist feeling; the characteristic odor type can be endowed to the cigarette; in addition, the solid capsule shell of the water-bearing capsule is great in strength and difficult to break, so that stable water holding and quality guaranteeing effects of the cigarette are ensured; and the above benefits have very positive significance in improving the cigarette quality.
Description
【Technical field】
The invention belongs to technical field of cigarette processing, more particularly it relates to a kind of contain capsule with diuresis promoting function, further relate to described
Preparation method containing capsule with diuresis promoting function.
【Background technology】
At present, domestic cigarette market occurs in that quick-fried pearl, the fashion trend of capsule cigarette.By adding in cigarette filter
Capsule, squeezes broken capsule before suction, discharges essence, to lift the mouthfeel of suction.But all of capsule cigarette is without exception all on the market
It is to wrap up oiliness essence using hydrophilic gel softgel shell layer, moisture content of flue gas adopting is no affected.And the raising of flue gas moisture, Ke Yirou
With flue gas cigarette perfume, reduction excitant hence it is evident that improving the suction quality of cigarette, improve suction moisture feeling.In addition, existing flavouring essence for tobacco is fragrant
Material mostly is water-soluble substances, can only be dissolved in water it is impossible to be dissolved in oil-based solvent, the perfume (or spice) that therefore capsule smoked sheet capsule can use on the market
Smart species and scope are greatly reduced, and available essence is extremely limited.Meanwhile, water is a kind of good solvent, can dissolve
Many harmful components in flue gas, reduce the harm of cigarette.
Therefore develop a kind of brand-new capsule with diuresis promoting function, to make up the deficiency of existing oiliness soft capsule.In Hubei, cigarette industry is limited
The CN 201410059720.5 of responsible company's application discloses a kind of three layers of capsule with diuresis promoting function.It uses sodium alginate complex compound to wrap up water
Property essence, then wrapped up with wax.But comparatively, process equipment is complicated, and the wax insufficient strength of outer layer, broken, can cause simultaneously
The volatilization of moisture in capsule with diuresis promoting function.Their another application CN 201410059949.9 discloses four layers of capsule with diuresis promoting function and its preparation
Method.Reduce the rupture of wax coat by increasing the diaphragm that sodium alginate is raw material, thus increased production cost.Thus
It can be seen that, they do not solve capsule circularity and wax coat strength problem, and they do not possess the function of parcel essence powder.
【Content of the invention】
[technical problem to be solved]
It is an object of the invention to provide a kind of contain capsule with diuresis promoting function.
It is a further object to provide the described preparation method containing capsule with diuresis promoting function.
[technical scheme]
The present invention is achieved through the following technical solutions.
The present invention relates to a kind of contain capsule with diuresis promoting function.
Described is made up of with the solid gum softgel shell wrapping up described aqueous capsule-core aqueous capsule-core containing capsule with diuresis promoting function；
Described solid gum softgel shell is the tactic hydrophilic film of ecto-entad, pulvis integument and modified wax layer group
Become；
The weight of described aqueous capsule-core, hydrophilic film, pulvis integument and modified wax layer is than for 5.0～50.0：0.1
～5.0：1.0～30.0：0.1～5.0.
According to a preferred embodiment of the present invention, described aqueous capsule-core be by 59～99 parts by weight of deionized water, 0
～40 weight portion honey or glucose, 0～31 parts by wt NaCl, 0～30 parts by weight of lemon acid, water-soluble lemon essence or cigarette
Careless medicinal extract and 1～2 weight portion preservative composition.
According to another preferred embodiment of the present invention, described hydrophilic film is by 10～41 weight portion marine algas
Sour sodium, 0～41 weight portion gelatin, gellan gum, guar gum, methylcellulose, agar or carragheen and 1～3 weight portion preservative
Constitute.
According to another preferred embodiment of the present invention, described preservative is selected from potassium sorbate, sodium Diacetate, benzene first
Sour sodium, dehydroactic acid sodium or calcium lactate.
According to another preferred embodiment of the present invention, described parcel bisque is by 0.8～1.2 weight portion PEG-
200th, PEG-600, PEG-2000 or PEG-6000,1～3 weight portion calcium chloride, calcium carbonate or calcium lactate and 0.1～0.5 weight
Part cornstarch, dextrin, PEG-6000, vanillic aldehyde or sodium carbonate composition.
According to another preferred embodiment of the present invention, described modified wax layer is by 4～7 weight portion beeswaxs, crystallite
Wax or paraffin, 1～10 parts of EVA, 1～4 weight account polyethylene, polypropylene, polyisoprene or polyvinyl acetate, 0～2
Weight portion tunny gum and 0～35 weight portion gutta-percha composition.
According to another preferred embodiment of the present invention, the intensity of described solid gum softgel shell is 0.5～2.2kg.
The invention still further relates to the described preparation method containing capsule with diuresis promoting function.The step of this preparation method is as follows：
A, prepare aqueous capsule-core
Will be sour, water-soluble to 0～40 weight portion honey or glucose, 0～31 parts by wt NaCl, 0～30 parts by weight of lemon
Lemon extract or tobacco extract and 1～2 weight portion preservative are dissolved in 59～99 parts by weight of deionized water, obtain described aqueous
Capsule-core；
B, prepare aqueous solution kernel
By 4～7 weight portion beeswaxs, microwax or paraffin, 1～10 parts of EVA, 1～4 weight account polyethylene, polypropylene,
Polyisoprene, polyvinyl acetate or butadiene-styrene rubber, 0～2 weight portion tunny gum are mixed with 0～35 weight portion gutta-percha,
Then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～20 DEG C, more aqueous capsule-core is added drop-wise to temperature for 100
In～150 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is, water-soluble
Liquid kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of by 15～20 parts by weight of deionized water, 0.8～1.2 weight portion PEG-200, PEG-600,
PEG-2000 or PEG-6000, the parcel amidin of 1～3 weight portion calcium chloride, calcium carbonate or calcium lactate composition, then spray
Cornstarch, dextrin, PEG-6000, vanillic aldehyde powder or carbonic acid sodium powder, then heated-air drying, then form powder on aqueous solution kernel
Agent integument；Aforesaid operations repeat, until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
The pelletized capsule that step C obtains is allowed to put in aqueous glue, described aqueous glue is by 82～246 weight portions
Deionized water, 10～41 weight portion sodium alginates, 0～41 weight portion gelatin, gellan gum, guar gum, methylcellulose, agar
Or carragheen, 1～3 weight portion preservative composition, then stir 3～10min, separate, with water rinsing, spontaneously dry, obtain
Described containing capsule with diuresis promoting function.
According to another preferred embodiment of the present invention, described preservative is selected from potassium sorbate, sodium Diacetate, benzene first
Sour sodium, dehydroactic acid sodium or calcium lactate..
According to another preferred embodiment of the present invention, the step preparing aqueous solution kernel is as follows：
The clear glass bucket of oil circulation device is installed, in glass bottom of the barrel using a kind of clear glass bucket or in its bottom
Filling silicone oil, its silicone oil height is the 3/5 of clear glass bucket height, adds liquid modified waxes, it changes on described silicone oil surface
Property wax height is the 1/8 of clear glass bucket height；
Using conventional water dropper, aqueous capsule-core is added drop-wise in liquid modified wax, one layer of modification is formed on aqueous capsule-core surface
Cere layer, then passes through silicone oil, obtains aqueous solution kernel in glass bottom of the barrel.
The present invention is described in more detail below.
The present invention relates to a kind of contain capsule with diuresis promoting function.
Described is made up of with the solid gum softgel shell wrapping up described aqueous capsule-core aqueous capsule-core containing capsule with diuresis promoting function；
Described solid gum softgel shell is the tactic hydrophilic film of ecto-entad, pulvis integument and modified wax layer group
Become.
The weight of described aqueous capsule-core, hydrophilic film, pulvis integument and modified wax layer is than for 5.0～50.0：0.1
～5.0：1.0～30.0：0.1～5.0.
According to the present invention, if the amount of aqueous capsule-core is less than 5.0, and when the weight of other layer is more constant than holding, then can go out
Existing capsule is difficult the situation pinched brokenly；If the amount of aqueous capsule-core is more than 50.0, occurs that capsule size is bigger than normal, be unfavorable for filter stick
Compound problem；Therefore, the amount of aqueous capsule-core is 5.0～50.0 to be appropriate.
Similarly, if the amount of hydrophilic film is less than 0.1, and when the weight of other layer is more constant than holding, then occur
Capsule intensity is inadequate, the flaky problem of pulvis integument；If the amount of hydrophilic film is more than 5.0, occur capsule not
The situation easily pinched brokenly；Therefore, the amount of hydrophilic film is rational for 0.1～5.0.
If the amount of pulvis integument is less than 1.0, and when the weight of other layer is more constant than holding, then capsule circularity occurs
Not, it is unfavorable for the problem that filter stick is combined；If the amount of pulvis integument is more than 30.0, occur that capsule size is bigger than normal, no
The problem being combined beneficial to filter stick；Therefore, the amount of pulvis integument is rational for 1.0～30.0.
If the amount of modified wax layer is less than 0.1, and when the weight of other layer is more constant than holding, then aqueous solution kernel occurs
Broken, it is difficult the problem of subsequent treatment；If the amount of modified wax layer is more than 5.0, truncating of aqueous solution kernel can be unfavorable for
Operation；Therefore, the amount of modified wax layer is 0.1～5.0 to be feasible.
In the present invention, according to Industry methods, using instrumental test, the intensity of described solid gum softgel shell is 0.5～
2.2kg.
According to the present invention, the effect of described aqueous capsule-core essentially consists in and provides moisture, fragrance for cigarette, improves smoker
Suction mouthfeel.Described aqueous capsule-core is by 59-99 parts by weight of deionized water, 0-40 weight portion honey or glucose, 0-31
Parts by wt NaCl, the acid of 0-30 parts by weight of lemon, water-soluble lemon essence or tobacco extract and 1-2 weight portion preservative composition.
Wherein, honey, glucose, sodium chloride and citric acid are all widely known products, the water solubility that the present invention uses
Lemon extract and tobacco extract are also all the products extensively sold in the market, and the such as taste essence and flavoring agent by Hangzhou taste is limited
The water-soluble lemon essence that company is sold with the taste essence of trade name taste；By Guangzhou daily use chemicals Chemical Co., Ltd. with trade name cloud and mist
The tobacco extract that medicinal extract is sold.
Described preservative is the important component in cigarette products, and cigarette quality is had a significant impact, and the present invention makes
Preservative is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, dehydroactic acid sodium or calcium lactate, and they are all existing markets
The upper product extensively sold.
According to the present invention, the effect of described hydrophilic film essentially consists in fixing pulvis integument, lifts capsule intensity.
Described hydrophilic film be by 10-41 weight portion sodium alginate, 0-41 weight portion gelatin, gellan gum, guar gum,
Methylcellulose, agar or carragheen and 1-3 weight portion preservative are constituted.
In the hydrophilic film of the present invention, when the amount of other components is in described scope, if the amount of sodium alginate
Less than 10 weight portions, then occur that pelletized capsule surface gel growth is excessively slow, the inadequate problem of gel strength；If alginic acid
The amount of sodium is more than 41 weight portions, then occur that gel growth is too fast, capsule breaking strength problem bigger than normal；Therefore, sodium alginate
Amount be feasible for 10-41 weight portion.Similarly, when the amount of other components is in described scope, if the amount of gelatin etc.
More than 41 weight portions, then occur that gelatin viscosity is bigger than normal, be difficult dispersed with stirring, finished capsule product intensity problem bigger than normal；Therefore, bright
The amount of glue etc. is feasible for 0-41 weight portion.
The sodium alginate of present invention use and gelatin etc. are the products sold in the market, such as by Qingdao bright moon marine alga
The sodium alginate that Group Co., Ltd is sold with trade name bright moon；The knot sold with trade name Fu Feng by Fu Feng Group Co., Ltd
Cold glue.The step for the preservative that uses identical with previously described, will not be described here.
According to the present invention, the effect of described pulvis integument essentially consists in the circularity of lifting capsule, gives parcel powdery
The function of essence.
Described parcel bisque is by 0.8-1.2 weight portion PEG-200, PEG-600, PEG-2000 or PEG-6000,1-3
Weight portion calcium chloride, calcium carbonate or calcium lactate and 0.1-0.5 parts by weight Corn starch, dextrin, PEG-6000, vanillic aldehyde or carbonic acid
Sodium composition.
In the parcel bisque of the present invention, when the amount of other components is in described scope, if the amount of PEG-200 etc. is little
In 0.8 weight portion, then occur that aqueous solution core surface hydrophobicity is too strong, the problem that pulvis is difficult to wrap up；If PEG-200 etc.
Amount be more than 1.2 weight portions, then can reduce pulvis parcel fastness；Therefore, the amount of PEG-200 etc. for 0.8-1.2 weight portion is
Feasible.
Similarly, when the amount of other components is in described scope, if the amount of calcium chloride etc. is less than 1 weight portion, can
The incomplete problem of gel growth occurs；If the amount of calcium chloride etc. is more than 3 weight portions, finished capsule product intensity mistake occurs
Big problem；Therefore, the amount of calcium chloride etc. is rational for 1-3 weight portion.When the amount of other components is in described scope, such as
The amount of fruit cornstarch etc. is less than 0.1 weight portion, then capsule circularity inadequate problem occurs；If the amount of cornstarch etc. is big
In 0.5 weight portion, then capsule size bigger than normal problem occurs；Therefore, the amount of cornstarch etc. is proper for 0.1-0.5 weight portion
When.
The PEG-200 (polyethylene glycol 200) of present invention use, PEG-600 (Macrogol 600), PEG-2000 (poly- second two
Alcohol 2000), PEG-6000 (Macrogol 6000), calcium chloride, calcium carbonate or calcium lactate be all the product sold in the market,
The PEG-200 for example being sold with trade name three well by Mitsui company.
Cornstarch is the white flaxen powder of micro-strip.It is with 0.3% sulfurous acid soaking maize, then by broken,
Sieve, precipitate, dry, levigate etc. the and powder made.It contains fat and protein etc. on a small quantity, and it is to sell in the market
Product, the product for example sold with the emerging trade of trade name by Xing Mao corn development corporation, Ltd. of Zhucheng.
Dextrin is used to weigh the technical terms of material cooking technique.StarchHeating, acid orAmylaseIn the presence of send out
Solution estranged and hydrolysis, the Starch Conversion of macromolecular are become small molecule intermediate material, i.e. dextrin, it is to sell in the market
The product sold, for example, met the product of U.S. sale by Yunan County Yong Guang cyclodextrine Co., Ltd with trade name.
Vanillic aldehyde is a kind of widely used edible spices.It is widely used in the various blending needing increase milk breath
In food, tobacco, daily life product, it is the product sold in the market, such as by the limited public affairs of Shanghai Xinhua spices food
The product that department is sold with trade name snow bear.
According to the present invention, the effect of described modified wax layer essentially consists in formation aqueous solution kernel.
Described modified wax layer is by 4-7 weight portion beeswax, microwax or paraffin, 1-10 parts of EVA, 1-2 weight portion
Polyethylene, polypropylene, polyisoprene or polyvinyl acetate, 0-2 weight portion tunny gum and 0-35 weight portion gutta-percha group
Become.
In the modified wax layer of the present invention, when the amount of other components is in described scope, if the amount of beeswax etc. is less than 4
Weight portion, then occur the problem that modified waxes are difficult to melt；If the amount of beeswax etc. is more than 7 weight portions, modified waxes occur
The problem of low strength；Therefore, the amount of beeswax etc. is feasible for 4-7 weight portion.
Similarly, when the amount of other components is in described scope, if the amount of EVA is less than 1 weight portion, occurs and change
The problem of property wax low strength；If the amount of EVA is more than 10 weight portions, modified waxes viscosity higher problem occurs；Therefore,
The amount of EVA is rational for 1-10 weight portion.When the amount of other components is in described scope, the amount of such as fruit polyethylene etc. is less than
1 weight portion, then occur the problem of modified waxes low strength；Amount as fruit polyethylene etc. is more than 2 weight portions, then modification occurs
The higher problem of wax viscosity；Therefore, the amount of polyethylene etc. is appropriate for 1-2 weight portion.Tunny gum and the situation of gutta-percha
Identical with other components such as beeswaxs.
Beeswax, EVA, polyethylene, tunny gum and gutta-percha that the present invention uses etc. are all the products sold in the market
Product, the beeswax for example sold with trade name Kang Xin by Cangzhou Kang Xin beeswax Jiao Ye Co., Ltd, limited by Xin Run Dehua, Hubei work
Tunny gum that company is sold with trade name prosperous profit moral, by safe and comfortable Hanyin Hua Ye plant pharmaceutcal corporation, Ltd with the bright pin of trade name China
The gutta-percha sold.
The invention still further relates to the described preparation method containing capsule with diuresis promoting function.The step of this preparation method is as follows：
A, prepare aqueous capsule-core
Will be sour, water-soluble to 0～40 weight portion honey or glucose, 0～31 parts by wt NaCl, 0～30 parts by weight of lemon
Lemon extract or tobacco extract and 1～2 weight portion preservative are dissolved in 59～99 parts by weight of deionized water, obtain described aqueous
Capsule-core.
B, prepare aqueous solution kernel
By 4～7 weight portion beeswaxs, microwax or paraffin, 1～10 parts of EVA, 1～4 weight account polyethylene, polypropylene,
Polyisoprene, polyvinyl acetate or butadiene-styrene rubber, 0～2 weight portion tunny gum are mixed with 0～35 weight portion gutta-percha,
Then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～20 DEG C, more aqueous capsule-core is added drop-wise to temperature for 100
In～150 DEG C of melt modification wax, one layer of curing hydrophobic modification cere, i.e. water are then formed on described aqueous capsule-core surface
Solution kernel；
Prepare comprising the following steps that of aqueous solution kernel：
According to the present invention, prepare a kind of clear glass bucket of aqueous solution kernel needs use or follow in its bottom installation silicone oil
The clear glass bucket of loop device, its concrete structure is shown in accompanying drawing 1.
The clear glass bucket of oil circulation device is installed, in glass bottom of the barrel using a kind of clear glass bucket or in its bottom
Filling silicone oil, its silicone oil height is the 3/5 of clear glass bucket height, adds liquid modified waxes, it changes on described silicone oil surface
Property wax height is the 1/8 of clear glass bucket height；
Using conventional water dropper, aqueous capsule-core is added drop-wise in liquid modified wax, one layer of modification is formed on aqueous capsule-core surface
Cere layer, then passes through silicone oil, obtains aqueous solution kernel in glass bottom of the barrel.
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of by 15～20 parts by weight of deionized water, 0.8～1.2 weight portion PEG-200, PEG-600,
PEG-2000 or PEG-6000, the parcel amidin of 1～3 weight portion calcium chloride, calcium carbonate or calcium lactate composition, then spray
Cornstarch, dextrin, PEG-6000, vanillic aldehyde powder or carbonic acid sodium powder, then heated-air drying, then form powder on aqueous solution kernel
Agent integument；Aforesaid operations repeat, until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule.
In this step, the aqueous solution kernel method of truncating is that rolling friction truncates, and washing methods is that abluent for foodstuff is general
Logical rinsing.
The coating equipment in sugar production line that the present invention uses e.g. really is sold with trade name gold by Taizhou Jin Cheng pharmaceutical machine Co., Ltd
Chufa-type coating pan.
Described heated-air drying is to carry blast heater in temperature 50-80 DEG C, wind speed 10-40m/ using Chufa-type coating pan
10-20min is dried under conditions of s.
D, prepare hydrophilic film
The pelletized capsule that step C obtains is allowed to put in aqueous glue, described aqueous glue is by 82～246 weight
Part deionized water, 10～41 weight portion sodium alginates, 0～41 weight portion gelatin, gellan gum, guar gum, methylcellulose, agar
Or carragheen, 1～3 weight portion preservative composition, then stir 3～10min, separate, with water rinsing, spontaneously dry, obtain
Described containing capsule with diuresis promoting function.
Described preservative is selected from potassium sorbate, sodium Diacetate, Sodium Benzoate, dehydroactic acid sodium or calcium lactate.
The described raw material being used containing capsule with diuresis promoting function of preparation, previously mentioned, will not be described here.
Containing capsule with diuresis promoting function, there are following features using what the inventive method prepared：
Capsule with diuresis promoting function moderate strength, can wrap up water, soluble perfume and solid powder essence.All raw materials are food
Level or medical grade, safety non-toxic.The suction quality of cigarette can be lifted well.
[beneficial effect]
The invention has the beneficial effects as follows：The present invention can lift, containing capsule with diuresis promoting function, effect that cigarette aspirates moisture feeling, and can assign
Give cigarette feature odor type, and present invention capsule fortreating AIDS containing capsule with diuresis promoting function shell intensity is big, reaches 0.5-2.2kg, is not easily broken, thus
Ensure that cigarette has stable water conservation preservation and effect, therefore, these all have very positive meaning for lifting cigarette quality.
【Brief description】
Fig. 1 is the dripping equipment for preparing aqueous solution kernel, A：Clearance-type；B：Continous way；
In figure：
1- water dropper, 2- aqueous capsule-core liquid, the liquid modified wax of 3-, 4- silicone oil, 5- aqueous solution kernel, 6- silicone oil import, 7- silicon
Oil export.
Fig. 2 is equipped with the cigarette structure schematic diagram that the present invention contains capsule with diuresis promoting function；
The original-pack red plum cigarette of A-；B- contains the red plum cigarette of capsule with diuresis promoting function in filter tip equipped with the present invention；C- in filter tip with the containing of B
The red plum cigarette of capsule with diuresis promoting function same position no tow.
Fig. 3 is equipped with the cigarette structure schematic diagram that the present invention contains capsule with diuresis promoting function.
The original-pack red plum cigarette of A-；B- contains the red plum cigarette of capsule with diuresis promoting function in filter tip equipped with the present invention；C- in filter tip with the containing of B
The red plum cigarette of capsule with diuresis promoting function same position tow perforate.
【Specific embodiment】
Will be better understood that the present invention by following embodiments.
Embodiment 1：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
310 parts by wt NaCl, 20 parts by weight water-soluble lemon extracts and 20 weight portion potassium sorbate preservatives are dissolved in
In 650 parts by weight of deionized water, obtain described aqueous capsule-core；
B, prepare aqueous solution kernel
By 80 weight portion beeswaxs, 200 parts of EVA, 20 weight account polyethylenes, 70 weight portion gutta-percha mixing, Ran Houjia
Heat fusing, obtains a kind of melt modification wax；
Using the equipment of accompanying drawing 1, the temperature adjustment to 10～15 DEG C of the aqueous capsule-core that step A is obtained, then aqueous capsule
Core is added drop-wise in the melt modification wax that temperature is 120～150 DEG C, then forms one layer of solidification on described aqueous capsule-core surface and dredges
Water modification cere, i.e. aqueous solution kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of bag being made up of 16 parts by weight of deionized water, 1 weight portion PEG-600,3 weight portion calcium chloride
Wrap up in amidin, then spray dextrin, reuse drying equipment heated-air drying under conditions of temperature 70 C, wind speed 15m/s
2min, then forms pulvis integument on aqueous solution kernel；Aforesaid operations repeat that (0.1 weight portion dextrin, sprays several times
Spread), until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
The pelletized capsule that step C obtains is allowed to put in aqueous glue, described aqueous glue is to be gone by 2460 weight portions
Ionized water, 450 weight portion sodium alginates, 60 weight portion gelatin, 30 weight portion potassium sorbate preservatives form, and then stir
5min, separates, and with water rinsing, spontaneously dries, obtain described containing capsule with diuresis promoting function.
Embodiment 2：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
400 weight portion honey and 10 parts by weight sodium preservatives are dissolved in 590 parts by weight of deionized water, obtain institute
The aqueous capsule-core stated；
B, prepare aqueous solution kernel
By 6 weight portion paraffin, 1 parts of EVA, 1 weight portion polyvinyl acetate, 1 weight portion tunny gum and 1 weight portion
Gutta-percha mixes, and then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～10 DEG C, more aqueous capsule-core is added drop-wise to temperature for 120
In～150 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is, water-soluble
Liquid kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, sprinkling is a kind of to be made up of 16 parts by weight of deionized water, 1.0 weight portion PEG-600,3 weight portion calcium chloride
Parcel amidin, then sprays cornstarch, reuses drying equipment hot blast under conditions of 65 DEG C of temperature, wind speed 15m/s
2min is dried, pulvis integument is then formed on aqueous solution kernel；Aforesaid operations repeat (0.5 parts by weight Corn shallow lake
Powder, sprays several times), until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 82 weight portions go from
Sub- water, 17 weight portion sodium alginates and 1 parts by weight sodium preservative composition, then stir 5min, separate, floated with water
Wash, spontaneously dry, obtain described containing capsule with diuresis promoting function.
Embodiment 3：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
By 30 weight portion honey, 10 parts by weight of lemon acid with 1 parts by weight sodium preservative be dissolved in 59 weight portions go from
In sub- water, obtain described aqueous capsule-core；
B, prepare aqueous solution kernel
By 7 weight portion microwaxes, 2 parts of EVA, 1 weight portion polyvinyl acetate mixing, then heating melting, obtains
A kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～10 DEG C, more aqueous capsule-core is added drop-wise to temperature for 110
In～130 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is, water-soluble
Liquid kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of bag being made up of with 3 weight portion calcium chloride 16 parts by weight of deionized water, 1 weight portion PEG-200
Wrap up in amidin, then spray PEG-6000, reuse drying equipment hot air drying under conditions of temperature 70 C, wind speed 10m/s
Dry 3min, then forms pulvis integument on aqueous solution kernel；Aforesaid operations repeat (0.3 weight portion PEG-6000, point
Repeatedly spray), until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 246 weight portions go from
Sub- water, 41 weight portion sodium alginates, 7 weight portion gellan gums, 3 weight portion guar gums and 3 weight portion dehydroactic acid sodium preservative groups
Become, then stir 10min, separate, with water rinsing, spontaneously dry, obtain described containing capsule with diuresis promoting function.
Embodiment 4：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
1 weight portion dehydroactic acid sodium preservative is dissolved in 99 parts by weight of deionized water, obtains described aqueous capsule-core；
B, prepare aqueous solution kernel
By 1 weight portion beeswax, 4 weight portion microwaxes, 2 parts of EVA, 1 weight portion polyvinyl acetate and 2 weight portions sugar
Gum glue mixes, and then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～10 DEG C, more aqueous capsule-core is added drop-wise to temperature for 110
In～130 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is, water-soluble
Liquid kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, sprinkling is a kind of to be made up of 16 parts by weight of deionized water, 1 weight portion PEG-2000 and 2 weight portion calcium chloride
Parcel amidin, then sprays vanillic aldehyde powder, reuses drying equipment hot blast under conditions of temperature 60 C, wind speed 20m/s
2min is dried, pulvis integument is then formed on aqueous solution kernel；Aforesaid operations repeat into (0.4 weight portion vanillic aldehyde powder,
Spray several times) OK, until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 246 weight portions go from
Sub- water, 41 weight portion sodium alginates, 10 weight portion agar, 3 weight portion dehydroactic acid sodium preservatives form, and then stir
10min, separates, and with water rinsing, spontaneously dries, obtain described containing capsule with diuresis promoting function.
Embodiment 5：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
30 weight portion glucose, 10 weight portion tobacco extracts and 1 weight portion dehydroactic acid sodium preservative are dissolved in 59 weight
In part deionized water, obtain described aqueous capsule-core；
B, prepare aqueous solution kernel
By 4 weight portion microwaxes, 1 weight portion polyvinyl acetate, 1 parts by weight of polypropylene, 2 weight portion polyisoprene with
2 weight portion gutta-percha mixing, then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained is to room temperature～20 DEG C, more aqueous capsule-core is added drop-wise to temperature is
In 100～120 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is,
Aqueous solution kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of bag being made up of with 3 weight portion calcium lactates 16 parts by weight of deionized water, 1 weight portion PEG-200
Wrap up in amidin, then spray carbonic acid sodium powder, reuse drying equipment hot air drying under conditions of 75 DEG C of temperature, wind speed 10m/s
Dry 3min, pulvis integument is then formed on aqueous solution kernel；Aforesaid operations repeat (0.2 parts by weight sodium carbonate, point
Repeatedly spray), until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 246 weight portions go from
Sub- water, 10 weight portion sodium alginates, 41 weight portion carragheens, 3 weight portion sodium Diacetate preservatives form, and then stir
3min, separates, and with water rinsing, spontaneously dries, obtain described containing capsule with diuresis promoting function.
Embodiment 6：Preparation contains capsule with diuresis promoting function
The step of this preparation method is as follows：
A, prepare aqueous capsule-core
30 parts by weight of lemon acid, 10 weight portion tobacco extracts and 1 weight portion sodium Diacetate preservative are dissolved in 59 weight portions
In deionized water, obtain described aqueous capsule-core；
B, prepare aqueous solution kernel
By 5 weight portion beeswaxs, 1 weight account polyethylene, 2 weight portion polyisoprene, 1 weight portion polyvinyl acetate and 1
Weight portion tunny gum mixes, and then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained is to room temperature～20 DEG C, more aqueous capsule-core is added drop-wise to temperature is
In 100～120 DEG C of melt modification wax, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is,
Aqueous solution kernel；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete is put
Enter in coating equipment in sugar production line, spray a kind of bag being made up of with 3 weight portion calcium lactates 16 parts by weight of deionized water, 1 weight portion PEG-400
Wrap up in amidin, then spray carbonic acid sodium powder, reuse drying equipment hot air drying under conditions of temperature 70 C, wind speed 12m/s
Dry 2min, pulvis integument is then formed on aqueous solution kernel；Aforesaid operations repeat (0.3 parts by weight sodium carbonate part,
Spray several times), until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 246 weight portions go from
Sub- water, 5 weight portion gelatin, 5 weight portion methylcellulose, 41 weight portion carragheens and 3 weight portion sodium Diacetate preservatives composition
, then stir 3min, separate, with water rinsing, spontaneously dry, obtain described containing capsule with diuresis promoting function.
Test example 1：The present invention contains capsule with diuresis promoting function and cigarette smoke moisture impact is smoked panel test
Test method：
The Huang in the market sold red plum cigarette is used as trial target.Manually in yellow red plum tobacco filters longitudinally
Centre position removes 5mm filter tip silk, in the placement embodiment of the present invention 1-3 preparation of its empty cavity position containing capsule with diuresis promoting function.Control sample
Simply remove 5mm tow.Their concrete structure is shown in accompanying drawing 2.
Inhale group using method tissue 10 moral standing generally adopting in the art product suction effect is evaluated and tested.
Moisture in flue gas is detected using industry conventional method, the results are shown in Table 1 for it.
Table 1：Inhale result containing the impact to cigarette flue gas moisture for the capsule with diuresis promoting function and product
The result of table 1 clearly illustrate in embodiment several have containing capsule with diuresis promoting function be obviously improved cigarette and aspirate moisture feeling
Effect, and cigarette feature odor type can be given, the quality for lifting cigarette has obvious help.
Test example 2：The present invention contains capsule with diuresis promoting function and cigarette smoke moisture impact is smoked panel test
Test method：
The Huang in the market sold red plum cigarette is used as trial target.Compound in yellow red plum tobacco bunch manually
The embodiment of the present invention 4-6 preparation containing capsule with diuresis promoting function.Control sample is in its corresponding site perforate.Their concrete structure is shown in attached
Fig. 3.
Inhale group using method tissue 10 moral standing generally adopting in the art product suction effect is evaluated and tested.
Moisture in flue gas is detected using industry conventional method, the results are shown in Table 2 for it.
Table 2：Inhale result containing the impact to cigarette flue gas moisture for the capsule with diuresis promoting function and product
The result of table 2 clearly illustrate in embodiment several have containing capsule with diuresis promoting function be obviously improved cigarette and aspirate moisture feeling
Effect, and cigarette feature odor type can be given, the quality for lifting cigarette has obvious help.
Claims (6)
1. a kind of containing capsule with diuresis promoting function it is characterised in that it by aqueous capsule-core and wrap up described aqueous capsule-core solid gum softgel shell form；
Described solid gum softgel shell is the tactic hydrophilic film of ecto-entad, pulvis integument and modified wax layer composition
's；Described parcel bisque is by 0.8～1.2 weight portion PEG-200, PEG-600, PEG-2000 or PEG-6000,1～3 weight
Amount part calcium chloride, calcium carbonate or calcium lactate and 0.1～0.5 parts by weight Corn starch, dextrin, PEG-6000, vanillic aldehyde or carbonic acid
Sodium composition；
The weight of described aqueous capsule-core, hydrophilic film, pulvis integument and modified wax layer is than for 5.0～50.0：0.1～
5.0：1.0～30.0：0.1～5.0；
Described aqueous capsule-core is by 59～99 parts by weight of deionized water, 0～40 weight portion honey or glucose, 0～31 weight
Part sodium chloride, 0～30 parts by weight of lemon acid, water-soluble lemon essence or tobacco extract and 1～2 weight portion preservative composition；
Described hydrophilic film is by 10～41 weight portion sodium alginates, 0～41 weight portion gelatin, gellan gum, guar gum, first
Base cellulose, agar or carragheen and 1～3 weight portion preservative are constituted；
Described modified wax layer be by 4～7 weight portion beeswaxs, microwax or paraffin, 1～10 parts by weight of ethylene-vinylacetate,
1～4 weight account polyethylene, polypropylene, polyisoprene or polyvinyl acetate, 0～2 weight portion tunny gum and 0～35 weight
Amount part gutta-percha composition.
2. according to claim 1 containing capsule with diuresis promoting function it is characterised in that described preservative be selected from potassium sorbate, diacetic acid
Sodium, Sodium Benzoate, dehydroactic acid sodium or calcium lactate.
3. according to claim 1 containing capsule with diuresis promoting function it is characterised in that the intensity of described solid gum softgel shell be 0.5 to 2.2kg.
4. the preparation method containing capsule with diuresis promoting function according to claim 1 is it is characterised in that the step of this preparation method is as follows：
A, prepare aqueous capsule-core
By 0～40 weight portion honey or glucose, 0～31 parts by wt NaCl, 0～30 parts by weight of lemon acid, water-soluble lemon
Essence or tobacco extract and 1～2 weight portion preservative are dissolved in 59～99 parts by weight of deionized water, obtain described aqueous capsule
Core；
B, prepare aqueous solution kernel
By 4～7 weight portion beeswaxs, microwax or paraffin, 1～10 parts by weight of ethylene-vinylacetate, the poly- second of 1～4 weight portion
Alkene, polypropylene, polyisoprene, polyvinyl acetate or butadiene-styrene rubber, 0～2 weight portion tunny gum and 0～35 weight portion Du
Secondary glue mixing, then heating melting, obtains a kind of melt modification wax；
The temperature adjustment of the aqueous capsule-core that step A is obtained to 5～20 DEG C, more aqueous capsule-core is added drop-wise to temperature for 100～150
DEG C melt modification wax in, one layer of curing hydrophobic modification cere is then formed on described aqueous capsule-core surface, that is, in the aqueous solution
Core；
C, prepare pulvis integument
The aqueous solution kernel that step B is obtained is truncated and is washed, and the aqueous solution kernel selecting smooth surface complete puts into bag
In clothing equipment, spray one kind by 15～20 parts by weight of deionized water, 0.8～1.2 weight portion PEG-200, PEG-600, PEG-
The parcel amidin of 2000 or PEG-6000,1～3 weight portion calcium chloride, calcium carbonate or calcium lactate composition, then sprays corn
Starch, dextrin, PEG-6000, vanillic aldehyde powder or carbonic acid sodium powder, then heated-air drying, then form pulvis bag on aqueous solution kernel
Covering layer；Aforesaid operations repeat, until obtaining the round shaped grain capsule meeting Particle size requirements, i.e. pelletized capsule；
D, prepare hydrophilic film
Allow the pelletized capsule that step C obtains put in aqueous glue, described aqueous glue be by 82～246 weight portions go from
Sub- water, 10～41 weight portion sodium alginates, 0～41 weight portion gelatin, gellan gum, guar gum, methylcellulose, agar or OK a karaoke club
Glue, 1～3 weight portion preservative composition, then stir 3～10min, separate, with water rinsing, spontaneously dry, and obtain described
Containing capsule with diuresis promoting function.
5. preparation method according to claim 4 is it is characterised in that described preservative is selected from potassium sorbate, diacetic acid
Sodium, Sodium Benzoate, dehydroactic acid sodium or calcium lactate.
6. preparation method according to claim 4 is it is characterised in that the step preparing aqueous solution kernel is as follows：
The clear glass bucket of oil circulation device is installed, in glass tank bottom filling using a kind of clear glass bucket or in its bottom
Silicone oil, its silicone oil height is the 3/5 of clear glass bucket height, adds liquid modified waxes, its modified waxes on described silicone oil surface
Height is the 1/8 of clear glass bucket height；
Using conventional water dropper, aqueous capsule-core is added drop-wise in liquid modified wax, one layer of modified cere is formed on aqueous capsule-core surface
Layer, then passes through silicone oil, obtains aqueous solution kernel in glass bottom of the barrel.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510063713.7A CN104726199B (en) | 2015-02-06 | 2015-02-06 | Water-bearing capsule and preparation method thereof |
| PCT/CN2015/077638 WO2016123869A1 (en) | 2015-02-06 | 2015-04-28 | Aqueous capsule and preparation method therefor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510063713.7A CN104726199B (en) | 2015-02-06 | 2015-02-06 | Water-bearing capsule and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN104726199A CN104726199A (en) | 2015-06-24 |
| CN104726199B true CN104726199B (en) | 2017-02-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510063713.7A Active CN104726199B (en) | 2015-02-06 | 2015-02-06 | Water-bearing capsule and preparation method thereof |
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| Country | Link |
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| CN (1) | CN104726199B (en) |
| WO (1) | WO2016123869A1 (en) |
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| CN113367383A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Water blasting bead |
| CN113367379A (en) * | 2020-03-09 | 2021-09-10 | 深圳波顿香料有限公司 | Tobacco product |
| CN112021652B (en) * | 2020-10-16 | 2022-04-19 | 河南中烟工业有限责任公司 | Core-shell structure blasting bead for cigarettes and preparation method thereof |
| CN112385880A (en) * | 2020-11-25 | 2021-02-23 | 武汉纺织大学 | Temperature-adjusting cigarette filter tip and preparation method thereof |
| CN112931932B (en) * | 2021-02-07 | 2022-08-30 | 福建中烟工业有限责任公司 | Cooling sphere and preparation method thereof |
| CN113331473B (en) * | 2021-06-10 | 2023-10-13 | 五邑大学 | Water-soluble essence-coated cigarette explosion bead and preparation method thereof |
| CN114011329B (en) * | 2021-11-29 | 2024-03-26 | 江苏大亚滤嘴材料有限公司 | Preparation method of water particles capable of increasing smoke moist feeling |
| CN115486557A (en) * | 2022-10-21 | 2022-12-20 | 广西中烟工业有限责任公司 | Water-soluble spice micro-blasting bead and preparation method thereof |
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Effective date of registration: 20190329 Address after: 335000 Longgang Industrial Park, Yingtan Hi-tech Industrial Development Zone, Jiangxi Province (in Yingtan CITIC Technology Co., Ltd.) Patentee after: Jiangxi Huabaoxin Technology Co., Ltd. Address before: 1180 Xingxian Road, Jiading District, Shanghai, 201821 Patentee before: Shanghai Huabao Biotechnology Co., Ltd. |