CN107712267A - A kind of antibacterial aquaculture feed and preparation method thereof - Google Patents
A kind of antibacterial aquaculture feed and preparation method thereof Download PDFInfo
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- CN107712267A CN107712267A CN201710910277.1A CN201710910277A CN107712267A CN 107712267 A CN107712267 A CN 107712267A CN 201710910277 A CN201710910277 A CN 201710910277A CN 107712267 A CN107712267 A CN 107712267A
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- 238000009360 aquaculture Methods 0.000 title claims abstract description 24
- 244000144974 aquaculture Species 0.000 title claims abstract description 22
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims abstract description 16
- 238000013270 controlled release Methods 0.000 claims abstract description 15
- 150000001875 compounds Chemical class 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 10
- 235000009566 rice Nutrition 0.000 claims abstract description 10
- 229930003231 vitamin Natural products 0.000 claims abstract description 10
- 235000013343 vitamin Nutrition 0.000 claims abstract description 10
- 239000011782 vitamin Substances 0.000 claims abstract description 10
- 229940088594 vitamin Drugs 0.000 claims abstract description 10
- 150000003722 vitamin derivatives Chemical class 0.000 claims abstract description 10
- 241000194108 Bacillus licheniformis Species 0.000 claims abstract description 8
- 229920002101 Chitin Polymers 0.000 claims abstract description 8
- 229920001661 Chitosan Polymers 0.000 claims abstract description 8
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 244000046052 Phaseolus vulgaris Species 0.000 claims abstract description 8
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims abstract description 8
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims abstract description 8
- 229930006000 Sucrose Natural products 0.000 claims abstract description 8
- 229930003268 Vitamin C Natural products 0.000 claims abstract description 8
- 239000005720 sucrose Substances 0.000 claims abstract description 8
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 8
- 239000011718 vitamin C Substances 0.000 claims abstract description 8
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 7
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 7
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims abstract description 7
- 235000015099 wheat brans Nutrition 0.000 claims abstract description 7
- 240000007594 Oryza sativa Species 0.000 claims abstract 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 14
- 239000000843 powder Substances 0.000 claims description 14
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000011812 mixed powder Substances 0.000 claims description 9
- 238000000855 fermentation Methods 0.000 claims description 8
- 230000004151 fermentation Effects 0.000 claims description 8
- 239000005995 Aluminium silicate Substances 0.000 claims description 7
- 239000004113 Sepiolite Substances 0.000 claims description 7
- 235000012211 aluminium silicate Nutrition 0.000 claims description 7
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 7
- 235000010216 calcium carbonate Nutrition 0.000 claims description 7
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 claims description 7
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 7
- 239000012065 filter cake Substances 0.000 claims description 7
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 7
- 229910052901 montmorillonite Inorganic materials 0.000 claims description 7
- 229910052624 sepiolite Inorganic materials 0.000 claims description 7
- 235000019355 sepiolite Nutrition 0.000 claims description 7
- 238000000108 ultra-filtration Methods 0.000 claims description 7
- 238000001291 vacuum drying Methods 0.000 claims description 7
- 238000000746 purification Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 5
- 238000000227 grinding Methods 0.000 claims description 5
- 239000007788 liquid Substances 0.000 claims description 4
- 206010013786 Dry skin Diseases 0.000 claims description 3
- 238000000605 extraction Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- ABSPRNADVQNDOU-UHFFFAOYSA-N Menaquinone 1 Natural products C1=CC=C2C(=O)C(CC=C(C)C)=C(C)C(=O)C2=C1 ABSPRNADVQNDOU-UHFFFAOYSA-N 0.000 claims description 2
- 229930003779 Vitamin B12 Natural products 0.000 claims description 2
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 claims description 2
- SHUZOJHMOBOZST-UHFFFAOYSA-N phylloquinone Natural products CC(C)CCCCC(C)CCC(C)CCCC(=CCC1=C(C)C(=O)c2ccccc2C1=O)C SHUZOJHMOBOZST-UHFFFAOYSA-N 0.000 claims description 2
- MBWXNTAXLNYFJB-NKFFZRIASA-N phylloquinone Chemical compound C1=CC=C2C(=O)C(C/C=C(C)/CCC[C@H](C)CCC[C@H](C)CCCC(C)C)=C(C)C(=O)C2=C1 MBWXNTAXLNYFJB-NKFFZRIASA-N 0.000 claims description 2
- 235000019175 phylloquinone Nutrition 0.000 claims description 2
- 239000011772 phylloquinone Substances 0.000 claims description 2
- 229960001898 phytomenadione Drugs 0.000 claims description 2
- 235000019163 vitamin B12 Nutrition 0.000 claims description 2
- 239000011715 vitamin B12 Substances 0.000 claims description 2
- 239000002689 soil Substances 0.000 claims 2
- 239000004408 titanium dioxide Substances 0.000 claims 2
- 244000063299 Bacillus subtilis Species 0.000 claims 1
- 235000014469 Bacillus subtilis Nutrition 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 12
- 230000003115 biocidal effect Effects 0.000 abstract description 5
- 230000001954 sterilising effect Effects 0.000 abstract description 5
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 238000009472 formulation Methods 0.000 abstract description 2
- 238000000034 method Methods 0.000 abstract description 2
- 239000000203 mixture Substances 0.000 abstract description 2
- 231100000614 poison Toxicity 0.000 abstract description 2
- 230000007096 poisonous effect Effects 0.000 abstract description 2
- 241000894007 species Species 0.000 abstract description 2
- 238000012795 verification Methods 0.000 abstract description 2
- 230000002045 lasting effect Effects 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 description 7
- 241000209094 Oryza Species 0.000 description 6
- 229960000892 attapulgite Drugs 0.000 description 5
- 229910052625 palygorskite Inorganic materials 0.000 description 5
- 235000010215 titanium dioxide Nutrition 0.000 description 5
- 239000000047 product Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 238000000354 decomposition reaction Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 244000037640 animal pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 description 1
- ZLVXBBHTMQJRSX-VMGNSXQWSA-N jdtic Chemical group C1([C@]2(C)CCN(C[C@@H]2C)C[C@H](C(C)C)NC(=O)[C@@H]2NCC3=CC(O)=CC=C3C2)=CC=CC(O)=C1 ZLVXBBHTMQJRSX-VMGNSXQWSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/16—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions
- A23K10/18—Addition of microorganisms or extracts thereof, e.g. single-cell proteins, to feeding-stuff compositions of live microorganisms
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01K—ANIMAL HUSBANDRY; AVICULTURE; APICULTURE; PISCICULTURE; FISHING; REARING OR BREEDING ANIMALS, NOT OTHERWISE PROVIDED FOR; NEW BREEDS OF ANIMALS
- A01K61/00—Culture of aquatic animals
- A01K61/10—Culture of aquatic animals of fish
- A01K61/13—Prevention or treatment of fish diseases
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/10—Animal feeding-stuffs obtained by microbiological or biochemical processes
- A23K10/12—Animal feeding-stuffs obtained by microbiological or biochemical processes by fermentation of natural products, e.g. of vegetable material, animal waste material or biomass
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
- A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/163—Sugars; Polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/20—Inorganic substances, e.g. oligoelements
- A23K20/28—Silicates, e.g. perlites, zeolites or bentonites
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
- Y02A40/81—Aquaculture, e.g. of fish
- Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
- Y02P60/87—Re-use of by-products of food processing for fodder production
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Animal Husbandry (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Biotechnology (AREA)
- Molecular Biology (AREA)
- Microbiology (AREA)
- Physiology (AREA)
- Health & Medical Sciences (AREA)
- Biomedical Technology (AREA)
- Marine Sciences & Fisheries (AREA)
- Biochemistry (AREA)
- Environmental Sciences (AREA)
- Inorganic Chemistry (AREA)
- Botany (AREA)
- Mycology (AREA)
- Birds (AREA)
- Insects & Arthropods (AREA)
- Sustainable Development (AREA)
- Biodiversity & Conservation Biology (AREA)
- Fodder In General (AREA)
Abstract
The invention provides a kind of antibacterial aquaculture feed and preparation method thereof, it is prepared by the raw material of following parts by weight:10 18 parts of subtilicin, 10 20 parts of bacillus licheniformis element, 8 20 parts of lactein, 15 25 parts of dregs of beans, 10 16 parts of chitin, 5 15 parts of trehalose, 5 15 parts of chitosan, 8 16 parts of vitamin B12,6 12 parts of vitamin C, 7 14 parts of vitamin K1,5 10 parts of sucrose, 6 13 parts of nano controlled-release compound, 10 20 parts of rice bran, 10 20 parts of wheat bran.Inventive formulation is reasonable, and preparation method is simple, and by actual verification, product of the present invention is rapid-action, action time is lasting, harmless environmental protection.The aquaculture feed antibiotic and sterilizing effect is good, eliminate it is poisonous to human body and cultivation species, have the harm such as pollution to water quality and environment, operate with method is easy, suitable for extensive popularization and application.
Description
Technical field
The invention belongs to technical field of aquaculture, and in particular to a kind of antibacterial aquaculture feed and preparation method thereof.
Background technology
In order to obtain higher yield in certain water body, people have to put into substantial amounts of fertilizer into water body, with
Meet material and the requirement of control disease of aquiculture animal growth.This breeding way characterized by strong feeding weight fertilizer increases
Water body nitrogen, phosphorus, organic matter decomposition and inversion load.Again because being negligent of regulating and controlling water quality and management, microorganism decomposition link is not smooth, water body
The circulation of middle material is obstructed with energy flow, and residual bait, organic residue constantly accumulate, thus NH4+ (NH3), NO2-, H2S, etc. contain
Measure the water water standard used for aquiculture far beyond national regulation.Lake, Reservoir Eutrophication are serious, and blue-green alge wawter bloom is wantonly
It is cruel, extreme influence not only is produced to local resident's production and living, but also bring a series of ecological environment problem.It is existing to adopt
Water body cultivation is carried out with chemical fertilizer, its nutrient is single, although water body is cultivated comparatively fast, the duration is very short, water body
In nutrient run out of after, what water body again can be quickly is thin.In addition, existing Aquaculture fertilizer does not have typically
Antibiotic and sterilizing function, so while fertilizer is added, also need to add antibiosis and sterilization agent, so as to increase the work of user significantly
Measure.
The content of the invention
In order to solve technical problem existing for above prior art, it is an object of the invention to provide a kind of antibacterial aquatic products to support
Grow feed and preparation method thereof.
To achieve these goals, the present invention provides following technical scheme:
A kind of antibacterial aquaculture feed, is prepared by the raw material of following parts by weight:Subtilicin 10-18
Part, bacillus licheniformis element 10-20 parts, lactein 8-20 parts, dregs of beans 15-25 parts, chitin 10-16 parts, trehalose 5-15
Part, chitosan 5-15 parts, vitamin B12 8-16 parts, vitamin C 6-12 parts, vitamin K1 7-14 parts, sucrose 5-10 parts, receive
Rice slow release complex 6-13 parts, rice bran 10-20 parts, wheat bran 10-20 parts;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium white
Powder, attapulgite, kaolin are according to 5-10:8-15:5-16:8-18:6-14:7-15:6-15 mass ratio is mixed, and is added
In the solution of 50-100 parts by weight Methanol, 24-48h is stirred in 50-80 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber,
Dry in an oven and dry 12-24h, grinding, which is sieved, to be produced.
Preferably, a kind of antibacterial aquaculture feed of the present invention, is prepared by the raw material of following parts by weight:It is withered
Careless 15 parts of bacillocin, 15 parts of bacillus licheniformis element, 14 parts of lactein, 10 parts of dregs of beans, 13 parts of chitin, trehalose 10
Part, 10 parts of chitosan, 12 parts of vitamin B12,9 parts of vitamin C, 10 parts of vitamin K1,8 parts of sucrose, nano controlled-release compound
10 parts, 15 parts of rice bran, 15 parts of wheat bran;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium white
Powder, attapulgite, kaolin are according to 8:11:12:13:10:11:10 mass ratio is mixed, and adds 50-100 parts by weight first
In the solution of alcohol, 32h is stirred in 65 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber, dries dry 18h in an oven,
Grinding, which is sieved, to be produced.
A kind of preparation method of antibacterial aquaculture feed of the present invention, comprises the following steps:
(1) subtilicin, bacillus licheniformis element, lactein are cultivated to select strain, entered respectively
25 DEG C and 36 DEG C of row is separately cultured lawn extraction purification, and by 18 DEG C of low temperature dryings of purification into powder;
(2) remaining each raw material is sent into mixer by weight and is stirred mixing, and with biotechnology Pengization
It is ground into powder;And be sent into drier and be dried, mixed powder is obtained, the temperature of the drier is set as 100~150 DEG C,
Drying time is 20-30min;
(3) mixed-powder that the powder and step (2) obtained step (1) obtains is mixed evenly;
(4) mixed-powder after step (3) is stirred crosses 30-40 mesh sieves, is then sent through in fermentation vat and is fermented,
By the temperature control in fermentation vat at 20~30 DEG C, ferment 6~10 days, finally filtered the liquid after fermentation, dry;I.e.
Obtain antibacterial aquaculture feed of the invention.
Beneficial effect:The invention provides a kind of antibacterial aquaculture feed and preparation method thereof, inventive formulation is reasonable,
Preparation method is simple, and using products application of the present invention in water body, by actual verification, product of the present invention is rapid-action, and when acting on
Between persistently, harmless environmental protection.The Aquaculture fertilizer of the present invention has antibiotic and sterilizing function, moreover, antibiotic and sterilizing effect is good, eliminates
It is poisonous to human body and cultivation species, have the harm such as pollution to water quality and environment, operate with method is easy, can be extensive
Popularization and application.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, is allowed to load each
Component has controlled-release function, and nano-complex drugloading rate and adsorbance are larger, and fertilizer efficiency time extends more than 3 months, effectively suppresses
The increment of animal pathogen, improve the benefit of the producer.
Embodiment
The invention will now be further described with reference to specific embodiments, but embodiment is only exemplary, not to this hair
Bright scope forms any restrictions.It will be understood by those skilled in the art that without departing from the spirit and scope of the invention
The details and form of technical solution of the present invention can be modified or replaced, but these modifications and replacement each fall within the present invention's
In protection domain.
A kind of preparation method of antibacterial aquaculture feed described in following examples, comprises the following steps:
(1) subtilicin, bacillus licheniformis element, lactein are cultivated to select strain, entered respectively
25 DEG C and 36 DEG C of row is separately cultured lawn extraction purification, and by 18 DEG C of low temperature dryings of purification into powder;
(2) remaining each raw material is sent into mixer by weight and is stirred mixing, and with biotechnology Pengization
It is ground into powder;And be sent into drier and be dried, mixed powder is obtained, the temperature of the drier is set as 100~150 DEG C,
Drying time is 20-30min;
(3) mixed-powder that the powder and step (2) obtained step (1) obtains is mixed evenly;
(4) mixed-powder after step (3) is stirred crosses 30-40 mesh sieves, is then sent through in fermentation vat and is fermented,
By the temperature control in fermentation vat at 20~30 DEG C, ferment 6~10 days, finally filtered the liquid after fermentation, dry;I.e.
Obtain antibacterial aquaculture feed of the invention.
Embodiment 1
A kind of antibacterial aquaculture feed, is prepared by the raw material of following parts by weight:15 parts of subtilicin,
15 parts of clothing bacillocin, 14 parts of lactein, 10 parts of dregs of beans, 13 parts of chitin, 10 parts of trehalose, 10 parts of chitosan, dimension life
Plain 12 parts of B12,9 parts of vitamin C, 10 parts of vitamin K1,8 parts of sucrose, 10 parts of nano controlled-release compound, 15 parts of rice bran, wheat bran
15 parts;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium white
Powder, attapulgite, kaolin are according to 8:11:12:13:10:11:10 mass ratio is mixed, and adds 50-100 parts by weight first
In the solution of alcohol, 32h is stirred in 65 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber, dries dry 18h in an oven,
Grinding, which is sieved, to be produced.
Embodiment 2
A kind of antibacterial aquaculture feed, is prepared by the raw material of following parts by weight:10 parts of subtilicin,
10 parts of clothing bacillocin, 8 parts of lactein, 15 parts of dregs of beans, 10 parts of chitin, 5 parts of trehalose, 5 parts of chitosan, vitamin
8 parts of B12,6 parts of vitamin C, 7 parts of vitamin K1,5 parts of sucrose, 6 parts of nano controlled-release compound, 10 parts of rice bran, 10 parts of wheat bran;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium white
Powder, attapulgite, kaolin are according to 5:8:5:8:6:7:6 mass ratio is mixed, and is added in the solution of 50 parts by weight Methanol,
24h is stirred in 50 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber, dries dry 12h in an oven, and grinding sieving is
.
Embodiment 3
A kind of antibacterial aquaculture feed, is prepared by the raw material of following parts by weight:18 parts of subtilicin,
20 parts of clothing bacillocin, 20 parts of lactein, 25 parts of dregs of beans, 16 parts of chitin, 15 parts of trehalose, 15 parts of chitosan, dimension life
Plain 16 parts of B12,12 parts of vitamin C, 14 parts of vitamin K1,10 parts of sucrose, 13 parts of nano controlled-release compound, 20 parts of rice bran, wheat
20 parts of bran;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium white
Powder, attapulgite, kaolin are according to 10:15:16:18:14:15:15 mass ratio is mixed, and adds 100 parts by weight Methanol
Solution in, in 80 DEG C stir 48h, vacuum ultrafiltration obtain filter cake, be put into vacuum drying chamber, in an oven dry dry 24h, grind
Honed sieve produces.
Claims (3)
1. a kind of antibacterial aquaculture feed, it is characterised in that be prepared by the raw material of following parts by weight:Bacillus subtilis
Plain 10-18 parts, bacillus licheniformis element 10-20 parts, lactein 8-20 parts, dregs of beans 15-25 parts, chitin 10-16 parts, marine alga
Sugared 5-15 parts, chitosan 5-15 parts, vitamin B12 8-16 parts, vitamin C 6-12 parts, vitamin K1 7-14 parts, sucrose 5-
10 parts, nano controlled-release compound 6-13 parts, rice bran 10-20 parts, wheat bran 10-20 parts;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium dioxide, recessed
Convex rod soil, kaolin are according to 5-10:8-15:5-16:8-18:6-14:7-15:6-15 mass ratio is mixed, and adds 50-
In the solution of 100 parts by weight Methanol, 24-48h is stirred in 50-80 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber,
Dried in baking oven and dry 12-24h, grinding, which is sieved, to be produced.
2. a kind of antibacterial aquaculture feed according to claim 1, it is characterised in that by the raw material system of following parts by weight
It is standby to form:15 parts of subtilicin, 15 parts of bacillus licheniformis element, 14 parts of lactein, 10 parts of dregs of beans, chitin 13
Part, 10 parts of trehalose, 10 parts of chitosan, 12 parts of vitamin B12,9 parts of vitamin C, 10 parts of vitamin K1,8 parts of sucrose, receive
10 parts of slow release complex of rice, 15 parts of rice bran, 15 parts of wheat bran;
Described nano controlled-release compound preparation method is:(1) by calcium carbonate, sepiolite, talcum powder, montmorillonite, titanium dioxide, recessed
Convex rod soil, kaolin are according to 8:11:12:13:10:11:10 mass ratio is mixed, and adds the molten of 50-100 parts by weight Methanol
In liquid, 32h is stirred in 65 DEG C, vacuum ultrafiltration obtains filter cake, is put into vacuum drying chamber, dries dry 18h in an oven, ground
Sieve and produce.
A kind of 3. preparation method of antibacterial aquaculture feed described in claim any one of 1-2, it is characterised in that including with
Lower step:
(1) subtilicin, bacillus licheniformis element, lactein are cultivated to select strain, carries out 25 respectively
DEG C and 36 DEG C be separately cultured lawn extraction purification, and by 18 DEG C of low temperature dryings of purification into powder;
(2) remaining each raw material is sent into mixer by weight and is stirred mixing, and crushed with biotechnology Pengization
Into powder;And be sent into drier and be dried, mixed powder is obtained, the temperature of the drier is set as 100~150 DEG C, dried
Time is 20-30min;
(3) mixed-powder that the powder and step (2) obtained step (1) obtains is mixed evenly;
(4) mixed-powder after step (3) is stirred crosses 30-40 mesh sieves, is then sent through in fermentation vat and is fermented, and will send out
Temperature control in ferment pond is fermented 6~10 days at 20~30 DEG C, is finally filtered the liquid after fermentation, is dried;Produce this
The antibacterial aquaculture feed of invention.
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Cited By (2)
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CN109180332A (en) * | 2018-09-30 | 2019-01-11 | 广西走山农牧开发有限公司 | The antiviral sustained release water of one kind supports vegetable fertilizer and preparation method thereof |
CN113100189A (en) * | 2021-05-18 | 2021-07-13 | 湖北龙王恨渔具集团有限公司 | Slow-release composite bait and preparation method thereof |
-
2017
- 2017-09-29 CN CN201710910277.1A patent/CN107712267A/en active Pending
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109180332A (en) * | 2018-09-30 | 2019-01-11 | 广西走山农牧开发有限公司 | The antiviral sustained release water of one kind supports vegetable fertilizer and preparation method thereof |
CN113100189A (en) * | 2021-05-18 | 2021-07-13 | 湖北龙王恨渔具集团有限公司 | Slow-release composite bait and preparation method thereof |
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