CN107711924A - One kind preventing and treating efficient medicament of Rosa roxburghii pest and disease damage and preparation method thereof - Google Patents
One kind preventing and treating efficient medicament of Rosa roxburghii pest and disease damage and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
- A01N63/10—Animals; Substances produced thereby or obtained therefrom
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
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- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
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Abstract
The invention belongs to pesticide processing technical field, more particularly to a kind of preventing and treating Rosa roxburghii pest and disease damage medicament, including following raw material：Hawthorn, leech, Semen Cuscutae, soya-bean oil, oriental wormwood；Medicament prepared by the present invention, pass through certain composition of raw materials and preparation technology, so that the medicament prepared is up to 91.5% to the fatal rate of aphid, to slug moth effective percentage up to 90%, to Aleurocanthus spiniferus effective percentage 86.0%, are up to by 82.5%, Pathogenic Bacteria Causing Brown Blotch Disease inhibiting rate and has 90.5% for carnivorism effective percentage up to 86.5% while the inhibiting rate to powdery mildew pathogenic bacteria, Sooty mould pathogenic bacteria inhibiting rate is up to 93.5%.In summary, the medicament that prepared by the present invention, wide spectrum, low toxicity, medicament efficiently, safe are belonged to.
Description
Technical field
The invention belongs to pesticide processing technical field, more particularly to a kind of efficient medicament of preventing and treating Rosa roxburghii pest and disease damage and its preparation
Method.
Background technology
Rosa roxburghii is also known as oblonga because its fruit shapes are similar to pears, and because its surface bear it is many dense
Small prickle and gain the name.Rosa roxburghii is the distinctive plant in China, may be used as medicine use, its root, stem, leaf, fruit suffer from high
Medical value.Rosa roxburghii contain abundant vitamin C (Vc), superoxide dismutase (SOD), Rosa roxburghii flavones, Polysaccharides from Rosa roxburghii and
A variety of essential amino acids.The flavone compound contained in Rosa roxburghii, there is anti-inflammatory, coronary artery dilator, influence blood pressure, protect
Shield heart blood vessel, remove free radical and the important biomolecule such as antitumor activity.
In recent years as the exploitation of new product, the demand of Rosa roxburghii increase, but wild thorn pear resource gradually decreases.Therefore,
Medicinal herb grower adds the plantation to Rosa roxburghii, easy infection powdery mildew, brown spot, Sooty mould, aphid, slug moth, black thorn powder in Rosa roxburghii plantation
Lice and carnivorism.The position of powdery mildew main harm is tender tip and tender leaf, can also endanger bud, flower and young fruit.Oriental fruit months is
Main boring pest in Rosa roxburghii insect pest, can cause fruit drop in early days, and mid-term, which can allow in fruit, black excrement class thing occurs, right
The yield and quality of Rosa roxburghii influence more serious.The position of Chinese rose Macrosiphus spp main harm is tender tip and bud, disease time master
Mid-April is concentrated on to November.Due to the backwardness of cultivation technique, existing pharmaceutical treatment effect is poor, and residual is serious so that Rosa roxburghii
Upgrowth situation is poor, and yield is relatively low, causes food-safety problem.
The content of the invention
The present invention is in order to solve the above technical problems, provide a kind of efficient medicament of preventing and treating Rosa roxburghii pest and disease damage and its preparation side
Method, realized particular by following technical scheme.
One kind preventing and treating efficient medicament of Rosa roxburghii pest and disease damage, including following mass parts raw material：Hawthorn 20-200 parts, leech 10-150
Part, Semen Cuscutae 10-100 parts, soya-bean oil 20-90 parts, oriental wormwood 20-70 parts.
Further, the described efficient medicament of preventing and treating Rosa roxburghii pest and disease damage, including following mass parts raw material：Hawthorn 130-145 parts,
Leech 100-110 parts, Semen Cuscutae 70-85 parts, soya-bean oil 20-35 parts, oriental wormwood 20-23 parts.
Further, the described efficient medicament of preventing and treating Rosa roxburghii pest and disease damage, including following preparation process：
1) hawthorn, Semen Cuscutae mixing, crush, add the clear water of 5-7 times of mixed-powder quality, 40-50KHz supersonic frequency
Lower extraction 40-50min, filtering, filtrate add isometric solution 1, stir 30-40min, filtering, add 50-55% filtrate bodies
Long-pending chloroform, layer of fetching water, obtains extract solution 1；
2) extract solution 1 adjusts pH with ammoniacal liquor, adds isometric chloroform, takes chloroform layer, adds and three chloromethanes
The isometric solution 2 of alkane layer, 30-35min is vibrated, layer of fetching water, add, dry, obtain solid 1；
3) leech crushes, and 80-90 DEG C of baking 10-15min, adds solution 3 and is mixed and made into the mixing that water content is 70-75%
Material, 24-30 DEG C of closing are fermented 2-3 days, obtain fermentation material, add the ethanol of 2-3 times of fermentation material quality, 40-45 DEG C of stirring extraction 3-
4h, filtering, filtrate are dried, and obtain solid 2, add the clear water of the 4-7 times of mass of solid 2, filtering, it is molten that filtrate adds isometric ether
Liquid, layer of fetching water, isometric n-butanol mixing vibration is added in water layer, n-butanol layer is taken, dries, obtain solid 3, add 4-8
The acetic acid solution of the mass of solid 3, filtering, filtrate are dried, and obtain medicinal extract 1；
4) solid 1, medicinal extract 1 mix, and add the solution 4 of 4-8 times of mixture quality, 60-70 DEG C of stirring 1.2-2h, filter,
Dry mixed liquid, obtain medicinal extract 2；
5) medicinal extract 2, soya-bean oil, the kaolin of 50-60 times of mass of medicinal extract 2, the pull open powder of the 0.02-0.05 times of mass of medicinal extract 2 are mixed
Close, crush, both both must.
Further, described solution 1, its mass fraction are 1.8-2.5% tartaric acid solution.
Further, it is described to adjust pH with ammoniacal liquor, it is that 9.2-10.5 is arrived into pH regulations.
Further, described solution 2, it is the sodium hydroxide solution that mass fraction is 2.4-3.2%.
Further, described solution 3 is beer, honey, rutin, water according to mass ratio 30-33:2.5-3.2:0.8-1.0:
10-13 is mixed.
Further, described acetic acid solution, its volume fraction are 5-8%.
Further, described solution 4, it is the mannitol solution that mass fraction is 4.7-6.2%.
Beneficial effect：The recipe determination and craft screening experimental analysis that medicament is carried out more than are found, implement l examples 1-3
Desinsection, fungistatic effect are more excellent, and embodiment 4-8 is because medicament stock is different or preparation method is different, so as to cause to sterilize
It is different with the active constituent content of desinsection, so as to go out to cause desinsection, fungistatic effect poor.
Medicament prepared by the present invention, 91.5% is up to the fatal rate of aphid, to slug moth effective percentage up to 90%, to black thorn powder
Lice effective percentage 86.0%, efficient to carnivorism up to 86.5% is up to 82.5% to the inhibiting rate of powdery mildew pathogenic bacteria, is brown simultaneously
Pinta pathogen inhibiting rate has 90.5%, and Sooty mould pathogenic bacteria inhibiting rate is up to 93.5%.In summary, the medicine that prepared by the present invention
Agent, belong to wide spectrum, low toxicity, medicament efficiently, safe.
Embodiment
The embodiment of the present invention is described in further detail below, but the invention is not limited in these realities
Mode is applied, any improvement or replacement on the present embodiment essence spirit, it is claimed to still fall within the claims in the present invention
Scope.
Embodiment
Embodiment 1-6 composition of raw materials is as shown in table 1.
The embodiment 1-6 composition of raw materials (g) of table 1
| Hawthorn | Leech | Semen Cuscutae | Soya-bean oil | Oriental wormwood | |
| Embodiment 1 | 130 | 100 | 70 | 20 | 20 |
| Embodiment 2 | 140 | 105 | 78 | 30 | 22 |
| Embodiment 3 | 145 | 110 | 85 | 35 | 23 |
| Embodiment 4 | 145 | - | 85 | - | 23 |
| Embodiment 5 | - | 110 | 85 | 35 | 23 |
| Embodiment 6 | 145 | 110 | - | - | 23 |
Embodiment 1-6 preparation method is as follows, for no medicinal material, is added without preparation.
Described preventing and treating Rosa roxburghii pest and disease damage medicament, including following preparation process：
The described efficient medicament of preventing and treating Rosa roxburghii pest and disease damage, including following preparation process：
1) hawthorn, Semen Cuscutae mixing, are crushed, and are added the clear water of 5 times of mixed-powder quality, are carried under 40KHz supersonic frequency
40min is taken, is filtered, filtrate adds isometric solution 1, stirs 30min, filters, and adds the chloroform of 50% filtrate volume,
Water intaking layer, obtains extract solution 1；
2) extract solution 1 adjusts pH with ammoniacal liquor, adds isometric chloroform, takes chloroform layer, adds and three chloromethanes
The isometric solution 2 of alkane layer, 30min is vibrated, layer of fetching water, add, dry, obtain solid 1；
3) leech crushes, 80 DEG C of baking 10min, adds solution 3 and is mixed and made into the compound that water content is 70%, 24 DEG C of closings
Fermentation 2 days, fermentation material is obtained, add the ethanol of 2 times of fermentation material quality, 40 DEG C of stirring extraction 3h, filter, filtrate is dried, and obtains solid
2, the clear water of 4 times of mass of solid 2, filtering are added, filtrate adds isometric diethyl ether solution, layer of fetching water, the body such as addition in water layer
Long-pending n-butanol mixing vibration, takes n-butanol layer, dries, obtain solid 3, add the acetic acid solution of the mass of 4 solid 3, filter, filter
Liquid is dried, and obtains medicinal extract 1；
4) solid 1, medicinal extract 1 mix, and add 4,60 DEG C of stirring 1.2h of solution of 4 times of mixture qualities, filtering, dry mixed
Liquid, obtain medicinal extract 2；
5) the pull open powder mixing of medicinal extract 2, soya-bean oil, the kaolin of 50 times of mass of medicinal extract 2,0.02 times of mass of medicinal extract 2, is crushed,
Both both.
Described solution 1, its mass fraction are 1.8% tartaric acid solution.
Described adjusts pH with ammoniacal liquor, is by pH regulations to 9.2.
Described solution 2, it is the sodium hydroxide solution that mass fraction is 2.4%.
Described solution 3 is beer, honey, rutin, water according to mass ratio 30:2.5:0.8:10 mix.
Described acetic acid solution, its volume fraction are 5%.
Described solution 4, it is the mannitol solution that mass fraction is 4.7%.
Embodiment 7
The formula composition of embodiment 7 is same as Example 3, and its preparation method is to mix hawthorn, leech, Semen Cuscutae, oriental wormwood,
Crush, the clear water for adding 6 times of mixture qualities decocts, and filtering, filtrate is dried, and obtains medicinal extract 1, soya-bean oil, the height of 50 times of mass of medicinal extract 2
Ridge soil, the pull open powder of 0.02 times of mass of medicinal extract 2 mix, and air-flow crushing both obtains
Embodiment 8
PH is adjusted with ammoniacal liquor described in embodiment 8, is to adjust pH to 8.5, other preparation methods are same as Example 3.
Experimental example
1st, effect assessment
1) insecticidal test
Medicament prepared by embodiment 1-8 carries out insecticidal effect test, and the object tested is aphid, slug moth, black thorn powder
Lice and carnivorism,
Killing aphids：1800 aphids are gathered respectively, are divided into 9 groups, every group is inoculated on 3 plants of rising trend identical Rosa roxburghiis, does not have
Group is covered with gauze respectively, 1-8 groups is tested with the embodiment 1-8 medicaments prepared, spray pharmacy measures preparation 0.5g, adds
Uniformly it is sprayed on Rosa roxburghii tree, sprays 3 times after the dissolving of 10ml water, is to spray once for first day respectively, sprays once within the 3rd day, the 7th day
Spray once, the 8th day statistical result.9th group is used as negative control group, sprays the clear water of same amount, and each experimental group is repeated 3 times, with
The death rate of each experimental group is counted afterwards, calculates killing rate, as a result as shown in table 2.
Slug moth is killed, kills Aleurocanthus spiniferus, kills that the experimental method of carnivorism is identical with killing aphids, counts each experimental subjects respectively
Lethal dose, fatal rate is calculated, as a result as shown in table 2.
The medicament insecticidal test result (%) of table 2
2) bacteriostatic experiment
(high seapeak, the diligent Ya Yali of nguktrum is bought to be carried the method for bibliography report, and Lee is wide, waits several bactericide pair of
Prevention effect [J] Xinjiang Agricultural Sciences of wheat powdery mildew, 2013,50 (7):1260-1264.), prepared with embodiment 1-8
Medicament carries out powdery mildew, brown spot, the suppression reality of Sooty mould pathogenic bacteria as experimental group 1-8, administration concentration 0.5g/L, medicament
Test, line blank of going forward side by side compares, and statistical result is as shown in table 3.
The medicament bacteriostatic experiment result (%) of table 3
| Powdery mildew pathogenic bacteria | Pathogenic Bacteria Causing Brown Blotch Disease inhibiting rate | Sooty mould pathogenic bacteria inhibiting rate | |
| Embodiment 1 | 82.5 | 86.6 | 90.2 |
| Embodiment 2 | 78.3 | 88.9 | 93.5 |
| Embodiment 3 | 80.6 | 90.5 | 92.7 |
| Embodiment 4 | 34.6 | 22.1 | 40.8 |
| Embodiment 5 | 37.8 | 35.7 | 30.6 |
| Embodiment 6 | 20.1 | 26.2 | 28.9 |
| Embodiment 7 | 32.3 | 20.4 | 27.7 |
| Embodiment 8 | 25.8 | 36.7 | 35.0 |
| Negative control group | 2.6 | 5.2 | 3.5 |
The recipe determination and craft screening experimental analysis that medicament is carried out more than find, implements l example 1-3 desinsections, antibacterial
Effect is more excellent, and embodiment 4-8 is because medicament stock is different or preparation method is different, so as to cause sterilization and desinsection to have
Effective component content is different, so as to go out to cause desinsection, fungistatic effect poor.
Medicament prepared by the present invention, 91.5% is up to the fatal rate of aphid, to slug moth effective percentage up to 90%, to black thorn powder
Lice effective percentage 86.0%, efficient to carnivorism up to 86.5% is up to 82.5% to the inhibiting rate of powdery mildew pathogenic bacteria, is brown simultaneously
Pinta pathogen inhibiting rate has 90.5%, and Sooty mould pathogenic bacteria inhibiting rate is up to 93.5%.In summary, the medicine that prepared by the present invention
Agent, belong to wide spectrum, low toxicity, medicament efficiently, safe.
Claims (9)
1. one kind preventing and treating efficient medicament of Rosa roxburghii pest and disease damage, it is characterised in that including following mass parts raw material：Hawthorn 20-200 parts,
Leech 10-150 parts, Semen Cuscutae 10-100 parts, soya-bean oil 20-90 parts, oriental wormwood 20-70 parts.
2. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 1, it is characterised in that described preventing and treating Rosa roxburghii pest and disease damage
Efficient medicament, including following mass parts raw material：Hawthorn 130-145 parts, leech 100-110 parts, Semen Cuscutae 70-85 parts, soya-bean oil 20-
35 parts, oriental wormwood 20-23 parts.
3. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 1, it is characterised in that described preventing and treating Rosa roxburghii pest and disease damage
Efficient medicament, including following preparation process：
1) hawthorn, Semen Cuscutae mixing, are crushed, and are added the clear water of 5-7 times of mixed-powder quality, are carried under 40-50KHz supersonic frequency
40-50min is taken, is filtered, filtrate adds isometric solution 1, stirs 30-40min, filtering, adds 50-55% filtrate volumes
Chloroform, layer of fetching water, obtains extract solution 1；
2) extract solution 1 adjusts pH with ammoniacal liquor, adds isometric chloroform, takes chloroform layer, adds and chloroform layer
Isometric solution 2,30-35min is vibrated, layer of fetching water, add, dry, obtain solid 1；
3) leech crushes, and 80-90 DEG C of baking 10-15min, adds solution 3 and is mixed and made into the compound that water content is 70-75%, 24-
30 DEG C of closings are fermented 2-3 days, obtain fermentation material, add the ethanol of 2-3 times of fermentation material quality, 40-45 DEG C of stirring extraction 3-4h, mistake
Filter, filtrate are dried, and obtain solid 2, add the clear water of the 4-7 times of mass of solid 2, filtering, and filtrate adds isometric diethyl ether solution, taken
Water layer, isometric n-butanol mixing vibration is added in water layer, n-butanol layer is taken, dries, obtain solid 3, add 4-8 solids 3
The acetic acid solution of quality, filtering, filtrate are dried, and obtain medicinal extract 1；
4) solid 1, medicinal extract 1 mix, and add the solution 4 of 4-8 times of mixture quality, 60-70 DEG C of stirring 1.2-2h, filter, dry
Mixed liquor, obtain medicinal extract 2；
5) the pull open powder mixing of medicinal extract 2, soya-bean oil, the kaolin of 50-60 times of mass of medicinal extract 2,0.02-0.05 times of mass of medicinal extract 2, powder
It is broken, both both.
4. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that described solution 1, its quality point
Number is 1.8-2.5% tartaric acid solution.
5. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that it is described to adjust pH with ammoniacal liquor,
It is that 9.2-10.5 is arrived into pH regulations.
6. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that described solution 2, be quality point
Number is 2.4-3.2% sodium hydroxide solution.
7. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that described solution 3 is beer, honeybee
Honey, rutin, water are according to mass ratio 30-33:2.5-3.2:0.8-1.0:10-13 is mixed.
8. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that described acetic acid solution, its body
Fraction is 5-8%.
9. the preventing and treating efficient medicament of Rosa roxburghii pest and disease damage as claimed in claim 3, it is characterised in that described solution 4, for quality point
Number is 4.7-6.2% mannitol solution.
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| CN102007947A (en) * | 2010-12-16 | 2011-04-13 | 天津工业大学 | Botanical farm-oriented environmental-friendly germicide and preparation method thereof |
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