CN107699962A - Fresh cocoon reeling method - Google Patents
Fresh cocoon reeling method Download PDFInfo
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- CN107699962A CN107699962A CN201711209309.1A CN201711209309A CN107699962A CN 107699962 A CN107699962 A CN 107699962A CN 201711209309 A CN201711209309 A CN 201711209309A CN 107699962 A CN107699962 A CN 107699962A
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- cocoon
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
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- Textile Engineering (AREA)
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Abstract
The invention discloses a kind of fresh cocoon reeling method, it is related to silk reeling technology field.This fresh cocoon reeling method is first to carry out cocoon cooking to fresh single cocoon and fresh dupion respectively to handle 1 time~2 times, containing mass fraction it is 2%~5% cocoon cooking aid in cocoon cooking liquid, the cocoon cooking aid by 20~40 parts by weight fluorocarbon surfactant, the Castor Oil Fatty Acid derivative of 20~40 parts by weight, the silk gum dissolution inhibitor of 10~20 parts by weight are formed；Then mixing filature produces.The present invention solves the problems, such as not only to have ensured that less filature fell thread in doupion silk silk reeling process but also does not reduce or formed more doupion silk feature.
Description
Technical field
The present invention relates to silk reeling technology field, especially a kind of fresh cocoon reeling method.
Background technology
The process that silk is extracted from silk cocoon is referred to as filature, on the one hand filature utilizes water usually using the mode of boiling
High temperature kills the silkworm chrysalis in cocoon, on the other hand because silk is animal origin, containing a large amount of animal colloid albumens, and by heating,
Make wherein most colloid albumen soluble in water, so as to play separation fiber, smoothly extract the purpose of silk out.At present, reeler
Skill includes several big steps, that is, collects, dry, cocoon cooking and filature.Most popular in the market is exactly doupion silk, price also compared with
Height, doupion silk are by dupion and list（It is secondary）Cocoon through what filature formed has uniform and delicate goose pimples after mixing in certain proportion
The silk product of style, these goose pimples being distributed on doupion silk are called " doupion silk feature ", the number of doupion silk feature, big
Small, distribution uniformity etc. is all the important indicator for reflecting doupion silk quality height.But doupion silk feature number and its point
Cloth has much relations with the scale shared by dupion in filature raw material, and the ratio shared by dupion is bigger, and feature is more,
And dupion is cocoond by two while spinning, during cocooing, silkworms spin silk at two be not co-ordination but each row its
It is to cause juxtaposition be present between silk.Therefore during reel silk from cocoons doupion silk, often because the ratio of dupion is excessive
The problem of generation dupion can not sequentially dissociate and cause to fall thread to lead to not normally produce too much, if reducing the ratio of dupion
Example, then the feature that the doupion silk of reel silk from cocoons has will be reduced, so as to reduce the taste of doupion silk.So doupion silk filature mistake
How to ensure that less filature falls thread but do not reduce or formed more doupion silk feature in journey is exactly that this area is urgently to be resolved hurrily
The problem of.Existing solution method is usually to start with terms of cocoon cooking, such as adds cocoon cooking aid, to promote water penetration or promote silk
Glue swelling, dissolving, degraded are even denatured, and so as to improve doupion silk feature, solve the problems, such as that dupion is unwinding poor, but all kinds of boil
Cocoon auxiliary agent has certain scope of application, more apparent to the silk cocoon action effect difference of different regions, and functionally also exists
Certain limitation.
The content of the invention
The present invention provides a kind of fresh cocoon reeling method, and it can solve both to have ensured less filature in doupion silk silk reeling process
The problem of the problem of falling thread and not reducing or formed more doupion silk feature.
In order to solve the above problems, the technical solution adopted in the present invention is：This fresh cocoon reeling method, include following step
Suddenly：
A, carry out cocoon cooking to fresh single cocoon and fresh dupion respectively to handle 1 time~2 times, it is 2% that mass fraction is contained in cocoon cooking liquid
~5% cocoon cooking aid；
B, filature is mixed；
The cocoon cooking aid is by the fluorocarbon surfactant of 20~40 parts by weight, the Castor Oil Fatty Acid derivative of 20~40 parts by weight
Thing, the silk gum dissolution inhibitor of 10~20 parts by weight are formed.
In above-mentioned technical proposal, more specifically technical scheme can also be：The fluorocarbon surfactant is perfluorinated sulfonic acid
Sodium, perfluorocarboxylic acid sodium, one or more kinds of mixtures of perfluorocarboxylic acid.
Further：The Castor Oil Fatty Acid derivative is castor oil acid imidazoline, Emulsifier EL-60, castor oil
One or more kinds of mixtures of alkanolamide.
Further：The silk gum dissolution inhibitor is glacial acetic acid, sodium bisulphite formaldehyde, the one or more of formaldehyde
Mixture.
By adopting the above-described technical solution, the present invention has the advantages that compared with prior art：
1st, the present invention first carries out cocoon cooking processing to the fresh cocoon of single cocoon and the fresh cocoon of dupion, adds cocoon cooking aid during cocoon cooking so that
The profit state of splashing of fresh silk glue is improved, and reduces the deadlocked power between strand, and silk can be incited somebody to action smoothly from cocoon layer surface
Whole intersected blocks lift to form feature, and cocoon cooking number is more, and the cooked degree of silkworm cocoon is higher, and the chance for causing to form it into feature is got over
Greatly.
2nd, one of component of this cocoon cooking aid for being added in process of cocoon of the present invention is fluorocarbon surfactant, be with
Fluorocarbon chain substitutes surfactant of the hydrocarbon chain as non-polar group in molecule.Relative to other surfaces activating agent, fluorine carbon table
Activating agent outstanding feature the most in face is：Efficiently, stably, i.e. high surface, high thermodynamic and chemical stability.
3rd, one of component of this cocoon cooking aid that the present invention adds in process of cocoon is Castor Oil Fatty Acid derivative,
It is a kind of while there is polarity and the surface active molecules of nonpolar group, can reduce the surface tension of water, guiding or increases cocoon
The penetrating power of layer water breakthrough, make inside and outside cocoon, between cocoon layer, rapid infiltrated between silk and silk, and uniformity, and then ensure cocoon cooking
When silk cocoon be heated consistent and uniform.
4th, one of component of this cocoon cooking aid that the present invention adds in process of cocoon is silk gum dissolution inhibitor, is had
Suppress silk gum to be acted on by hot water overaction dissolving, the unwinding of poor raw material can be significantly improved.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described：
Embodiment 1：
A kind of fresh cocoon reeling method, is comprised the following steps：
A, the fresh cocoon of single cocoon of 450 same day purchases, the fresh dupion of 100 same day purchases, by single cocoon and Shuan Gong are chosen
Cocoon carries out following cocoon cooking processing respectively：First carry out the vacuum infiltration that vacuum is 0.09MPaMPa, the water suction temperature of vacuum infiltration
For 45 DEG C, 4 grams of sodium metasilicate are added in vacuum infiltration bucket；It is then placed in 80 DEG C of hot water for dissolved cocoon cooking aid and soaks 30
Minute, the amount of cocoon cooking aid is the 2% of cocoon cooking liquid mass fraction；Cocoon cooking 2 times is carried out again, it is standby；
B, filature is mixed；
The cocoon cooking aid is by perfluorinated sulfonic acid sodium, castor oil acid imidazoline and glacial acetic acid with 2：4：1 ratio composition.
Embodiment 2：
A kind of fresh cocoon reeling method, is comprised the following steps：
A, the fresh cocoon of single cocoon of 400 same day purchases, the fresh dupion of 200 same day purchases, by single cocoon and Shuan Gong are chosen
Cocoon carries out following cocoon cooking processing respectively：First carry out the vacuum infiltration that vacuum is 0.09MPaMPa, the water suction temperature of vacuum infiltration
For 45 DEG C, 4 grams of sodium metasilicate are added in vacuum infiltration bucket；It is then placed in 80 DEG C of hot water for dissolved cocoon cooking aid and soaks 30
Minute, the amount of cocoon cooking aid is the 5% of cocoon cooking liquid mass fraction；Cocoon cooking 2 times is carried out again, it is standby；
B, filature is mixed；
The cocoon cooking aid is by perfluorocarboxylic acid sodium, Emulsifier EL-60 and sodium bisulphite formaldehyde 2：1：1 ratio composition.
Embodiment 3：
A kind of fresh cocoon reeling method, is comprised the following steps：
A, the fresh cocoon of single cocoon of 450 same day purchases, the fresh dupion of 150 same day purchases, by single cocoon and Shuan Gong are chosen
Cocoon carries out following cocoon cooking processing respectively：First carry out the vacuum infiltration that vacuum is 0.09MPaMPa, the water suction temperature of vacuum infiltration
For 45 DEG C, 4 grams of sodium metasilicate are added in vacuum infiltration bucket；It is then placed in 80 DEG C of hot water for dissolved cocoon cooking aid and soaks 30
Minute, the amount of cocoon cooking aid is the 5% of cocoon cooking liquid mass fraction；Cocoon cooking 2 times is carried out again, it is standby；
B, filature is mixed；
The cocoon cooking aid is by perfluorinated sulfonic acid sodium, perfluorocarboxylic acid sodium, Emulsifier EL-60 and glacial acetic acid 1：1：2:1 ratio group
Into.
Embodiment 4：
A kind of fresh cocoon reeling method, is comprised the following steps：
A, the fresh cocoon of single cocoon of 400 same day purchases, the fresh dupion of 100 same day purchases, by single cocoon and Shuan Gong are chosen
Cocoon carries out following cocoon cooking processing respectively：First carry out the vacuum infiltration that vacuum is 0.09MPaMPa, the water suction temperature of vacuum infiltration
For 45 DEG C, 4 grams of sodium metasilicate are added in vacuum infiltration bucket；It is then placed in 80 DEG C of hot water for dissolved cocoon cooking aid and soaks 30
Minute, the amount of cocoon cooking aid is the 2% of cocoon cooking liquid mass fraction；Cocoon cooking 2 times is carried out again, it is standby；
B, filature is mixed；
The cocoon cooking aid is by perfluorinated sulfonic acid sodium, perfluorocarboxylic acid sodium, castor oil acid imidazoline, Emulsifier EL-60 and glacial acetic acid
2：2：1:1:1 ratio composition.
Control group：
A kind of fresh cocoon reeling method is as follows：
The fresh cocoon of single cocoon of 450 same day purchases is chosen, the fresh dupion of 150 same day purchases, after mixing, vacuum is carried out and oozes
Thoroughly, the vacuum of vacuum infiltration is 0.09MPaMPa, and the water suction temperature of vacuum infiltration is 45 DEG C；Filature is carried out again.
The inspection for the doupion silk feature extracted out below for embodiment 1 to embodiment 4：
1. the method for inspection：The silk that reel silk from cocoons obtains on reeling machine is wound as a piece, 127mm every wide, 33 lines is arranged per 25.4mm, are counted
The number of every silk piece characteristic and record the number that this section of silk silk reeling process falls thread.What each embodiment level control group reel silk from cocoons obtained
Silk winds 3 silk pieces and examined.
2. assay such as following table：
The doupion silk Characteristic Number statistical form of table 1
The reel silk from cocoons process of table 2 falls thread number statistical form
From Tables 1 and 2, doupion silk product is made with the fresh cocoon reeling method of the present invention, falls to continue less and formed double
Palace silk feature is more.
Claims (4)
- A kind of 1. fresh cocoon reeling method, it is characterised in that comprise the following steps：A, carry out cocoon cooking to fresh single cocoon and fresh dupion respectively to handle 1 time~2 times, it is 2% that mass fraction is contained in cocoon cooking liquid ~5% cocoon cooking aid；B, filature is mixed；The cocoon cooking aid is by the fluorocarbon surfactant of 20~40 parts by weight, the Castor Oil Fatty Acid derivative of 20~40 parts by weight Thing, the silk gum dissolution inhibitor of 10~20 parts by weight are formed.
- 2. fresh cocoon reeling method according to claim 1, it is characterised in that：The fluorocarbon surfactant is perfluorinated sulfonic acid Sodium, perfluorocarboxylic acid sodium, one or more kinds of mixtures of perfluorocarboxylic acid.
- 3. the fresh cocoon reeling method according to claims 1 or 2, it is characterised in that：The Castor Oil Fatty Acid derivative For castor oil acid imidazoline, Emulsifier EL-60, castor oil alkanolamide one or more kinds of mixtures.
- 4. the fresh cocoon reeling method according to claims 1 or 2 or 3, it is characterised in that：The silk gum dissolution inhibitor For glacial acetic acid, sodium bisulphite formaldehyde, formaldehyde one or more kinds of mixtures.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711209309.1A CN107699962A (en) | 2017-11-27 | 2017-11-27 | Fresh cocoon reeling method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711209309.1A CN107699962A (en) | 2017-11-27 | 2017-11-27 | Fresh cocoon reeling method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107699962A true CN107699962A (en) | 2018-02-16 |
Family
ID=61186005
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711209309.1A Withdrawn CN107699962A (en) | 2017-11-27 | 2017-11-27 | Fresh cocoon reeling method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108411381A (en) * | 2018-05-18 | 2018-08-17 | 上海然星智能科技有限公司 | A kind of reeling machine and its manufacture craft of silk |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102586896A (en) * | 2012-01-11 | 2012-07-18 | 广西工学院 | Novel cocoon cooking aid and its application |
| CN105177730A (en) * | 2015-08-10 | 2015-12-23 | 鹿寨县贵盛茧丝工贸有限公司 | Reeling auxiliary agent |
| CN106555233A (en) * | 2016-12-07 | 2017-04-05 | 广西凯喜雅丝绸有限公司 | Silk cocoon extracts the process of silk out |
| CN106987910A (en) * | 2017-04-19 | 2017-07-28 | 潜山县龙华茧丝有限公司 | A kind of filature composite assistant |
-
2017
- 2017-11-27 CN CN201711209309.1A patent/CN107699962A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102586896A (en) * | 2012-01-11 | 2012-07-18 | 广西工学院 | Novel cocoon cooking aid and its application |
| CN105177730A (en) * | 2015-08-10 | 2015-12-23 | 鹿寨县贵盛茧丝工贸有限公司 | Reeling auxiliary agent |
| CN106555233A (en) * | 2016-12-07 | 2017-04-05 | 广西凯喜雅丝绸有限公司 | Silk cocoon extracts the process of silk out |
| CN106987910A (en) * | 2017-04-19 | 2017-07-28 | 潜山县龙华茧丝有限公司 | A kind of filature composite assistant |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108411381A (en) * | 2018-05-18 | 2018-08-17 | 上海然星智能科技有限公司 | A kind of reeling machine and its manufacture craft of silk |
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| PB01 | Publication | ||
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| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180216 |