CN107699394A - A kind of tea seed washes clean rapidly dissolving tablet and its preparation method and application - Google Patents
A kind of tea seed washes clean rapidly dissolving tablet and its preparation method and application Download PDFInfo
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- CN107699394A CN107699394A CN201710929762.3A CN201710929762A CN107699394A CN 107699394 A CN107699394 A CN 107699394A CN 201710929762 A CN201710929762 A CN 201710929762A CN 107699394 A CN107699394 A CN 107699394A
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- China
- Prior art keywords
- parts
- tea seed
- rapidly dissolving
- dissolving tablet
- clean rapidly
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Links
- 241001122767 Theaceae Species 0.000 title claims abstract description 42
- 238000002360 preparation method Methods 0.000 title abstract description 18
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims abstract description 25
- 229930182490 saponin Natural products 0.000 claims abstract description 25
- 150000007949 saponins Chemical class 0.000 claims abstract description 25
- 235000020357 syrup Nutrition 0.000 claims abstract description 20
- 239000006188 syrup Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- TZBAVQKIEKDGFH-UHFFFAOYSA-N n-[2-(diethylamino)ethyl]-1-benzothiophene-2-carboxamide;hydrochloride Chemical compound [Cl-].C1=CC=C2SC(C(=O)NCC[NH+](CC)CC)=CC2=C1 TZBAVQKIEKDGFH-UHFFFAOYSA-N 0.000 claims abstract description 19
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 18
- 229930195725 Mannitol Natural products 0.000 claims abstract description 18
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 18
- 235000010355 mannitol Nutrition 0.000 claims abstract description 18
- 239000000594 mannitol Substances 0.000 claims abstract description 18
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 17
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical compound OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 12
- 239000011248 coating agent Substances 0.000 claims abstract description 9
- 238000000576 coating method Methods 0.000 claims abstract description 9
- 150000007524 organic acids Chemical class 0.000 claims abstract description 9
- 235000012055 fruits and vegetables Nutrition 0.000 claims abstract description 8
- 239000003905 agrochemical Substances 0.000 claims abstract description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 36
- 238000005406 washing Methods 0.000 claims description 15
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 6
- 239000011975 tartaric acid Substances 0.000 claims description 6
- 235000002906 tartaric acid Nutrition 0.000 claims description 6
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- LCPVQAHEFVXVKT-UHFFFAOYSA-N 2-(2,4-difluorophenoxy)pyridin-3-amine Chemical compound NC1=CC=CN=C1OC1=CC=C(F)C=C1F LCPVQAHEFVXVKT-UHFFFAOYSA-N 0.000 claims 1
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Substances [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims 1
- 238000009835 boiling Methods 0.000 abstract description 2
- 238000007873 sieving Methods 0.000 abstract 1
- 239000000575 pesticide Substances 0.000 description 15
- 239000007788 liquid Substances 0.000 description 9
- RZYKUPXRYIOEME-UHFFFAOYSA-N CCCCCCCCCCCC[S] Chemical compound CCCCCCCCCCCC[S] RZYKUPXRYIOEME-UHFFFAOYSA-N 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 6
- 229910052708 sodium Inorganic materials 0.000 description 6
- 239000011734 sodium Substances 0.000 description 6
- 239000003599 detergent Substances 0.000 description 5
- 235000013311 vegetables Nutrition 0.000 description 5
- 235000010149 Brassica rapa subsp chinensis Nutrition 0.000 description 4
- 235000000536 Brassica rapa subsp pekinensis Nutrition 0.000 description 4
- 241000499436 Brassica rapa subsp. pekinensis Species 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 240000007124 Brassica oleracea Species 0.000 description 3
- 235000003899 Brassica oleracea var acephala Nutrition 0.000 description 3
- 235000011301 Brassica oleracea var capitata Nutrition 0.000 description 3
- 235000001169 Brassica oleracea var oleracea Nutrition 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 3
- 239000002253 acid Substances 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 239000008399 tap water Substances 0.000 description 3
- 235000020679 tap water Nutrition 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
- 239000005946 Cypermethrin Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 description 2
- 229960005424 cypermethrin Drugs 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000004128 high performance liquid chromatography Methods 0.000 description 2
- 238000009533 lab test Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 229960000583 acetic acid Drugs 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000008504 concentrate Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000004851 dishwashing Methods 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000021393 food security Nutrition 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000003845 household chemical Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003094 microcapsule Substances 0.000 description 1
- 239000004570 mortar (masonry) Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/04—Detergent materials or soaps characterised by their shape or physical properties combined with or containing other objects
- C11D17/041—Compositions releasably affixed on a substrate or incorporated into a dispensing means
- C11D17/042—Water soluble or water disintegrable containers or substrates containing cleaning compositions or additives for cleaning compositions
- C11D17/045—Multi-compartment
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3707—Polyethers, e.g. polyalkyleneoxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C11D2111/14—
Abstract
The invention discloses a kind of tea seed to wash clean rapidly dissolving tablet and its preparation method and application, and the tea seed is washed clean rapidly dissolving tablet each component and is calculated by weight as：10 30 parts of Tea Saponin, 15 parts of anhydrous sodium sulfate, 2 10 parts of lauryl sodium sulfate, 5 20 parts of organic acid, 1 15 parts of sodium acid carbonate, 1 10 parts of mannitol, Macrogol 4000 are 1 10 parts, 5 20 parts of syrup.The step of its preparation method is：A. syrup and Macrogol 4000 are mixed and heated by proportioning, boiling coating is carried out to Tea Saponin and organic acid, room temperature is cooled to and sieves；B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, grinding sieving；C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.It dissolves in 25 DEG C of water is less than 5min, and the dissolving water is used to remove fruit and vegetable surfaces agricultural chemicals.
Description
Technical field
The invention belongs to household chemicals field, and in particular to a kind of tea seed washes clean rapidly dissolving tablet and its preparation method and application.
Background technology
One of exceeded subject matter faced as China's food security of residues of pesticides.Because most of fruit and vegetable is
Eat when fresh, and amount is big, thus harm of their remains of pesticide to human body is bigger.Residues of banned pesticides in vegetable and fruit
Removal substantially have washing, peeling and culinary art three kinds, the fruit and vegetable for being unable to peeling or culinary art, washing is unique selection.
Home sale is few dedicated for cleaning the product of vegetable and fruit residues of banned pesticides at present, and many is washed with common tableware
Agent replacement is washed, and dish washing detergent is chemical products mostly, it is in the majority with neopelex etc., and peace be present in these products
Full property is not high, long-term use of unfavorable to health.More or less remain in after washing in vegetable and fruit, turn into secondary dirt
Dye source.
Contain natural surfactant Tea Saponin in tea seed, available for washing vegetable and fruit.Chinese patent
CN102296007A, CN103232902A disclose one kind using tea seed cake or tea seed powder as fruits and vegetables cleaning powder made of raw material, but tea
The dregs of rice and tea seed powder are not soluble in water, work slow；Although Chinese patent CN103725439A, using Tea Saponin as raw material, its easy moisture absorption is not
Poor performance that is stable, directly using or be used cooperatively with other surfaces activating agent.And fast dissolving solid preparation is made in Tea Saponin
Report is had no for fruits and vegetables cleaning.
The content of the invention
(1) technical problems to be solved
In view of the shortcomings of the prior art, the technical problem to be solved in the present invention is to provide a kind of tea seed to wash clean rapidly dissolving tablet, this
Invention additionally provides the preparation method that the tea seed washes clean rapidly dissolving tablet, and the tea seed washes the application of clean rapidly dissolving tablet.
(2) technical scheme
In order to solve the above-mentioned technical problem, the invention provides such a tea seed to wash clean rapidly dissolving tablet, and wherein each component is pressed
Parts by weight are calculated as：Tea Saponin 10-30 parts, anhydrous sodium sulfate 1-5 parts, lauryl sodium sulfate 2-10 parts, organic acid 5-20 parts,
Sodium acid carbonate 1-15 parts, mannitol 1-10 parts, Macrogol 4000 are 1-10 parts, syrup 5-20 parts.
Preferably, organic acid is any one in tartaric acid, citric acid or citric acid.
Present invention also offers the preparation method that a kind of above-mentioned tea seed washes clean rapidly dissolving tablet, comprise the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 50~80 DEG C, Tea Saponin and organic acid are carried out
Boiling coating, is cooled to room temperature, crosses 60~200 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 60~
200 mesh sieves；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Present invention also offers the application that a kind of above-mentioned tea seed washes clean rapidly dissolving tablet, and it dissolves in 25 DEG C of water is less than
5min, the dissolving water are used to remove fruit and vegetable surfaces agricultural chemicals.
The principle of the present invention：Syrup and Macrogol 4000 form film layer, are coated on Tea Saponin and organic acid surface, are formed
Micro-capsule.It is tabletted again with alkaline builder compatibility, isolate soda acid, will not direct interaction, so as to ensure that tea soap
The stabilization of element and preparation.When in use, because aqueous acid medium alkali interacts, fater disintegration, synergist and Tea Saponin are common
Have an effect, improve clean result.
(3) beneficial effect
The present invention is had the following advantages relative to prior art and effect：
1. the present invention use Tea Saponin microencapsulation and soda acid separation method, make Tea Saponin when in use just with alkaline builder
Reaction, so as to improve product bin stability, ensure that product quality；
2. product of the present invention is solid tablet, easily storage transport, due to the effect of soda acid, fater disintegration, washing during use
Effect is good, thus easy to use, easy to spread；
3. preparation technology of the present invention is simple, it is easy to industrialized production.
Embodiment
, below will be right to be easy to understand the technical means, the inventive features, the objects and the advantages of the present invention
Technical scheme in the embodiment of the present invention carries out clear, complete description, so that the present invention is expanded on further, it is clear that described
Embodiment is only the part of the embodiment of the present invention, rather than whole embodiments.
Embodiment 1
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 30g, anhydrous sodium sulfate 5g, dodecyl sulphur
Sour sodium 2g, tartaric acid 10g, sodium acid carbonate 10g, mannitol 2g, Macrogol 4000 5g, syrup 10g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 50 DEG C, Tea Saponin and tartaric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 60 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 60 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 2
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 10g, anhydrous sodium sulfate 1g, dodecyl sulphur
Sour sodium 2g, citric acid 5g, sodium acid carbonate 1g, mannitol 1g, Macrogol 4000 1g, syrup 5g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 60 DEG C, Tea Saponin and citric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 80 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 80 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 3
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 20g, anhydrous sodium sulfate 3g, dodecyl sulphur
Sour sodium 6g, citric acid 6g, sodium acid carbonate 5g, mannitol 4g, Macrogol 4000 3g, syrup 6g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 80 DEG C, Tea Saponin and citric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 100 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 100 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 4
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 25g, anhydrous sodium sulfate 4g, dodecyl sulphur
Sour sodium 10g, tartaric acid 20g, sodium acid carbonate 15g, mannitol 10g, Macrogol 4000 10g, syrup 20g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 70 DEG C, Tea Saponin and tartaric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 200 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 200 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 5
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 15g, anhydrous sodium sulfate 2g, dodecyl sulphur
Sour sodium 7g, citric acid 15g, sodium acid carbonate 10g, mannitol 8g, Macrogol 4000 8g, syrup 15g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 55 DEG C, Tea Saponin and citric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 80 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 80 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 6
A kind of tea seed washes clean rapidly dissolving tablet, and wherein each component quality is：Tea Saponin 20g, anhydrous sodium sulfate 4g, dodecyl sulphur
Sour sodium 5g, citric acid 5g, sodium acid carbonate 8g, mannitol 7g, Macrogol 4000 5g, syrup 6g.
Its preparation method comprises the following steps：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 70 DEG C, Tea Saponin and citric acid are seethed with excitement
Coating, room temperature is cooled to, crosses 150 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 150 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
Embodiment 7
Tea seed made from embodiment 1~6 washes the weight differential and dissolubility test of clean rapidly dissolving tablet.
Experimental method：
Tea seed made from Example 1~6 washes each 20 of clean rapidly dissolving tablet, weighs, and calculates tablet weight variation.Separately 1 is taken respectively
It is placed in 6 beakers for filling 200mL water, 25 ± 1 DEG C of water temperature, records the time of tablet dissolved.
Experimental result：Tea seed made from embodiment 1~6 wash clean rapidly dissolving tablet average weight be respectively 1.365g, 1.384g,
1.422g, 1.395g, 1.434g, 1.397g, tablet weight variation are less than 5%.It is placed in water, immediately it is observed that bubble produces,
When gas stops overflowing, tablet dissolved and it is dispersed in water, the particle of no aggregation is left.Dissolution time be respectively 4.4min,
3.5min、4.1min、4.8min、3.9min、4.0min.Show that tea seed made from embodiment 1~6 washes clean rapidly dissolving tablet dissolution time
Respectively less than 5min, solubility property are good.
Embodiment 8
Tea seed made from embodiment 1~6 washes the clean result experiment of clean rapidly dissolving tablet
Method：Surface is chosen completely without vegetables sample of the Chinese cabbage substantially damaged as this experiment.
The preparation of pollution by pesticides liquid：0.25g effective cypermethrins emulsion is weighed in 50mL95% ethanol, is stirred,
It is standby with running water quantitative to 1000mL.With pollution by pesticides liquid active ingredient (effective cypermethrin) concentration value be
250mg/kg。
The preparation of pollution by pesticides fruits and vegetables sample：Selected Chinese cabbage is immersed in pollution by pesticides liquid after 30min and taken out, gets rid of table
Face residual droplets, 12h is placed in room temperature shady place.By the cabbages leaves prepared be divided into 9 groups (including do not wash group 1 group, a water washing
Group 1 group, 1 group of liquid detergent washing group, tea seed wash clean 6 groups of rapidly dissolving tablet washing group), it is every group 2 parts, every part of 10g, standby.
Water washing：200mL running water is taken in beaker, while is put into the cabbages leaves after a pollution by pesticides, is placed in super
4min is cleaned in sound wave washer.200mL tap water rinses are used again, in triplicate.Carry out parallel laboratory test simultaneously.
Liquid detergent washs：Take liquid detergent 0.4g to be placed in beaker, with running water quantitative to 200mL, that is, be made into 0.2% and wash
Clean smart solution, stirs.The cabbages leaves being put into after a pollution by pesticides, are placed in ultrasonic cleaner and clean 4min.Again
With 200mL tap water rinses, in triplicate.Carry out parallel laboratory test simultaneously.
Tea seed washes clean rapidly dissolving tablet washing：Tea seed made from Example 1~6 washes each 1 of clean rapidly dissolving tablet, is respectively placed in 6
It is each to add 200mL water in 250mL beakers, 25 ± 1 DEG C of water temperature, after its disintegration completely, the Chinese cabbage that is put into after a pollution by pesticides
Sample, it is placed in ultrasonic cleaner and cleans 4min.200mL tap water rinses are used afterwards, in triplicate.Carry out parallel reality simultaneously
Test.
Pesticide concentration determines：The Chinese cabbage sample prepared is cut into small pieces with scissors, after sample is smashed to pieces with mortar.It will smash
Sample after broken is placed in beaker, is added 100mL95% ethanol, is stirred with glass bar, ultrasonic extraction 3min, pour out extraction
Liquid repeats extraction 2 times, combining extraction liquid by the above process in beaker.The extract prepared is put in 70 DEG C of water-baths and rotated
To about 8mL, concentrate is transferred in 50mL volumetric flasks, with 95% ethanol constant volume, contained with Syrups by HPLC cypermethrin
Amount.HPLC conditions：Mobile phase：Methanol：Water：Glacial acetic acid=80:20:0.1, flow velocity：0.2mL/min, chromatographic column：YMC-Pack
ODS (C18) post, 4.6 × 100mm, column temperature：30 DEG C, wavelength：276nm, sample size：20μL.
As a result：Compared with not washing group, water washing group pesticides removal rate 19.8%, liquid detergent washing group pesticides removal rate
31.6%, tea seed wash clean rapidly dissolving tablet washing group pesticides removal rate for 85.4%, 89.5%, 93.4%, 87.6%, 89.7%,
95.2%, it is optimal to show that tea seed washes clean rapidly dissolving tablet clean result.
The technical characteristics and general principle and associated advantages of the present invention are the foregoing described, for those skilled in the art
For, it is clear that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and it is in the design without departing substantially from the present invention or substantially special
In the case of sign, the present invention can be realized in other specific forms.Therefore, all should be by embodiment no matter from the point of view of which point
To regard exemplary as, and be nonrestrictive, the scope of the present invention is limited by appended claims rather than described above,
It is intended that all changes fallen in the implication and scope of the equivalency of claim are included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (4)
1. a kind of tea seed washes clean rapidly dissolving tablet, it is characterised in that wherein each component is calculated by weight as：Tea Saponin 10-30 parts, nothing
Aqueous sodium persulfate 1-5 parts, lauryl sodium sulfate 2-10 parts, organic acid 5-20 parts, sodium acid carbonate 1-15 parts, mannitol 1-10 parts,
Macrogol 4000 is 1-10 parts, syrup 5-20 parts.
2. a kind of tea seed according to claim 1 washes clean rapidly dissolving tablet, it is characterised in that organic acid is tartaric acid, citric acid
Or any one in citric acid.
A kind of 3. method for preparing tea seed as claimed in claim 1 or 2 and washing clean rapidly dissolving tablet, it is characterised in that including following step
Suddenly：
A. syrup and Macrogol 4000 are mixed by proportioning, is heated to 50~80 DEG C, Tea Saponin and organic acid are seethed with excitement
Coating, room temperature is cooled to, crosses 60~200 mesh sieves；
B. anhydrous sodium sulfate, lauryl sodium sulfate, sodium acid carbonate and mannitol are mixed by proportioning, ground 60~200 mesh
Sieve；
C. by step A and step B powder mixed pressuring plate, produce tea seed and wash clean rapidly dissolving tablet.
4. a kind of tea seed according to claim 1 or 2 washes tea seed prepared by clean rapidly dissolving tablet and/claim 3 methods described
Wash the application of clean rapidly dissolving tablet, it is characterised in that tea seed, which is washed clean rapidly dissolving tablet and dissolved in 25 DEG C of water, is less than 5min, and the dissolving water is used
In removing fruit and vegetable surfaces agricultural chemicals.
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| CN111040886A (en) * | 2019-12-31 | 2020-04-21 | 赣南医学院 | Tea saponin dispersible tablet and preparation method and application thereof |
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