CN107691476A - A kind of sterilization processing agent of wheat seed - Google Patents
A kind of sterilization processing agent of wheat seed Download PDFInfo
- Publication number
- CN107691476A CN107691476A CN201710833843.3A CN201710833843A CN107691476A CN 107691476 A CN107691476 A CN 107691476A CN 201710833843 A CN201710833843 A CN 201710833843A CN 107691476 A CN107691476 A CN 107691476A
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- Prior art keywords
- parts
- enzyme
- processing agent
- sterilization processing
- intermixture
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N61/00—Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
- A01N31/16—Oxygen or sulfur directly attached to an aromatic ring system with two or more oxygen or sulfur atoms directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
- A01N33/18—Nitro compounds
- A01N33/20—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group
- A01N33/22—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group having at least one oxygen or sulfur atom and at least one nitro group directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/40—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides
- A01N47/46—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having a double or triple bond to nitrogen, e.g. cyanates, cyanamides containing —N=C=S groups
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of sterilization processing agent of wheat seed, it is prepared by the raw material of following parts by weight:10 20 parts of non-ionic polyacrylamide, 12 parts of isothiocyano methyl formate, 5 15 parts of organic-silicon-modified starch aqueous emulsion, 6 14 parts of graft modification soybean protein, 1.5 6.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 15 parts of eugenol, 5 10 parts of bacterium enzyme intermixture, 5 10 parts of carbon enzyme, 7 15 parts of Sodium p-nitrophenoxide, 10 20 parts of Ethyl formate.The bacterium enzyme intermixture is by wax printing fabric, bacillus licheniformis, the compound detoxication enzymes of β in mass ratio 5:2:3 mixing gained.The present invention have the advantages that efficient, low toxicity, low-residual, quick-acting are good, the lasting period is long, it is environmentally friendly, be not likely to produce the resistance to the action of a drug, and the germination rate of seed can be improved.
Description
Technical field
The present invention relates to agriculture field, and in particular to a kind of sterilization processing agent of wheat seed.
Background technology
Wheat is most important cereal raise crop, and the cereal crops that China is important in the world.Head blight, white powder
Disease, banded sclerotial blight, rust and leaf blight are to threaten the important fungal disease of Wheat Production, have a strong impact on the yield and product of wheat
Matter.
It is still the important measures of effective prevention and control wheat fungal disease using chemical bactericide at present, but with service life
Growth and dosage increase, fungal disease germ already to based on carbendazim etc. benzimidazole germicide produce
The raw resistance to the action of a drug, and fastness frequency is continuously increased, resistant range expands year by year, often results in the preventing and treating failure of wheat fungal disease, makes
Aggravate into plant disease epidemic.The administration of a large amount of chemical bactericides causes the destruction of farmland ecosystem, while brings controlling object
The problems such as resistance to the action of a drug, chemical pesticide residual.With the food-safe increasingly attention of the public, global protection environment increasingly gradually
High cry, develop and utilize has favorable compatibility with environment, and the seed disinfectant harmless to the mankind also becomes scientific research people
The research emphasis and focus of member.
The content of the invention
To solve the above problems, the invention provides a kind of sterilization processing agent of wheat seed, have efficient, less toxic, low
Residual, quick-acting is good, the lasting period is long, it is environmentally friendly, be not likely to produce the advantages that resistance to the action of a drug, and the sprouting of seed can be improved
Rate.
To achieve the above object, the technical scheme taken of the present invention is:
A kind of sterilization processing agent of wheat seed, is prepared by the raw material of following parts by weight:
Non-ionic polyacrylamide 10-20 parts, isothiocyano methyl formate 1-2 parts, organic-silicon-modified starch aqueous emulsion 5-
15 parts, graft modification soybean protein 6-14 parts, toVerticilliumdahliaActivitie Activitie S of Relative albumen 1.5-6.5 parts, eugenol 1-5 parts, bacterium enzyme intermixture
5-10 parts, carbon enzyme 5-10 parts, Sodium p-nitrophenoxide 7-15 parts, Ethyl formate 10-20 parts.
Wherein, the bacterium enzyme intermixture is by wax printing fabric, bacillus licheniformis, β-compound detoxication enzyme in mass ratio 5:
2:3 mixing gained.
Preferably, it is prepared by the raw material of following parts by weight:
10 parts of non-ionic polyacrylamide, 1 part of isothiocyano methyl formate, 5 parts of organic-silicon-modified starch aqueous emulsion, grafting
6 parts of modified soy-bean protein, 1.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 1 part of eugenol, 5 parts of bacterium enzyme intermixture, 5 parts of carbon enzyme, to nitro
7 parts of sodium phenate, 10 parts of Ethyl formate.
Preferably, it is prepared by the raw material of following parts by weight:
20 parts of non-ionic polyacrylamide, 2 parts of isothiocyano methyl formate, 15 parts of organic-silicon-modified starch aqueous emulsion, connect
It is 14 parts of modified soy-bean protein of branch, 6.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 5 parts of eugenol, 10 parts of bacterium enzyme intermixture, 10 parts of carbon enzyme, right
15 parts of p-nitrophenol sodium, 20 parts of Ethyl formate.
Preferably, it is prepared by the raw material of following parts by weight:
15 parts of non-ionic polyacrylamide, 1.5 parts of isothiocyano methyl formate, 10 parts of organic-silicon-modified starch aqueous emulsion,
10 parts of graft modification soybean protein, 4 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 3 parts of eugenol, 7.5 parts of bacterium enzyme intermixture, 7.5 parts of carbon enzyme,
11 parts of Sodium p-nitrophenoxide, 15 parts of Ethyl formate.
Wherein, the organic-silicon-modified starch aqueous emulsion is as obtained by prepared by following steps:
S1, the starch aqueous emulsion that mass fraction is 30-40% is prepared, stir lower addition starch water quality of the emulsion 1.5%
Mass concentration is 1% copper-bath, is that 6% sodium hydrate aqueous solution adjusts pH value to 9.5 with mass fraction, rear slowly to add
The concentration for entering starch emulsion quality 1.5-2.5% is 9.3-15.3mgL-1Micro-/ nano bubble Ozone Water, the reaction of 50 DEG C of constant temperature
3h, after be 3% using mass fraction hydrochloric acid neutralize to pH value as 6.0-6.5, add starch emulsion 1.5%, mass fraction is
10% sodium sulfite aqueous solution terminating reaction, it is last it is scrubbed, dry, crush to obtain oxidized starch;
S2, the oxidized starch of gained is scattered in the water that quality is its 400%-500%, it is 3% to add mass fraction
Hydrochloric acid solution, its pH value is adjusted to 5, after system temperature is risen into 50 DEG C, be added dropwise quality be oxidized starch quality 15-
30% vinyl three ('beta '-methoxy ethyoxyl) silane, and being stirred with 160-200rmp speed, 50 DEG C of isothermal reactions 2 hours
Afterwards, room temperature is cooled to, adds oxidized starch quality 1%-3% PAMA, 100-150rmp is stirred at room temperature
30min is mixed, produces organic-silicon-modified starch aqueous emulsion.
Wherein, the graft modification soybean protein is the soybean protein being modified with glycidyl methacrylate graft,
Its grafting degree is between 38%-54%.
The invention has the advantages that:
Used by the collaborations of the active ingredients such as isothiocyano methyl formate, toVerticilliumdahliaActivitie Activitie S of Relative albumen, eugenol, from more
Individual aspect inhibits the growth of germ, and the resistance risk that can reduce pathogen to chemical agent is horizontal, is advantageous to pathogen
The holding of susceptibility, while germ can be delayed the resistance to the action of a drug occur to single dose in formula, while bactericidal effect is notable, can effectively prevent and treat
Wheat scab, wheat powdery mildew, wheat rust, wheat sharp eyespot and wheat leaf blight, reduce disease to production estimation
Caused by cause harm, improve the yield and quality of agricultural product.By microbial degradation and biological adsorption, it can significantly mitigate toxin
Injury to crop and animal.The addition of carbon enzyme, it on the one hand can increase the carbon in soil, promoting root growth strong sprout, the opposing party
Face, it has minimum molecular organic acids, can penetrate into crop root rapidly with reference to nutrition, improves nutrient utilization, while can be with
Activating soil, suppress disease, equilibrium ph lifts crop quality, and there is Sodium p-nitrophenoxide stronger permeability and physiology to live
Property, easily enter cytoplasm with nutrient interaction, and the Rational flow of plasm and nutrient can be promoted, promote plant while absorb more
Kind nutrition, releases the antagonism between fertilizer;Non-ionic polyacrylamide, graft modification soybean protein, machine Si modification form sediment
Powder aqueous emulsion assembles symphysis into netted structure during reaction, can be very good to be wrapped on seed.
Embodiment
In order that objects and advantages of the present invention are more clearly understood, the present invention is carried out with reference to embodiments further
Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair
It is bright.
In following examples, used organic-silicon-modified starch aqueous emulsion is as obtained by prepared by following steps:
S1, the starch aqueous emulsion that mass fraction is 30-40% is prepared, stir lower addition starch water quality of the emulsion 1.5%
Mass concentration is 1% copper-bath, is that 6% sodium hydrate aqueous solution adjusts pH value to 9.5 with mass fraction, rear slowly to add
The concentration for entering starch emulsion quality 1.5-2.5% is 9.3-15.3mgL-1Micro-/ nano bubble Ozone Water, the reaction of 50 DEG C of constant temperature
3h, after be 3% using mass fraction hydrochloric acid neutralize to pH value as 6.0-6.5, add starch emulsion 1.5%, mass fraction is
10% sodium sulfite aqueous solution terminating reaction, it is last it is scrubbed, dry, crush to obtain oxidized starch;
S2, the oxidized starch of gained is scattered in the water that quality is its 400%-500%, it is 3% to add mass fraction
Hydrochloric acid solution, its pH value is adjusted to 5, after system temperature is risen into 50 DEG C, be added dropwise quality be oxidized starch quality 15-
30% vinyl three ('beta '-methoxy ethyoxyl) silane, and being stirred with 160-200rmp speed, 50 DEG C of isothermal reactions 2 hours
Afterwards, room temperature is cooled to, adds oxidized starch quality 1%-3% PAMA, 100-150rmp is stirred at room temperature
30min is mixed, produces organic-silicon-modified starch aqueous emulsion.
The graft modification soybean protein is the soybean protein being modified with glycidyl methacrylate graft, and it is grafted
Degree is between 38%-54%.
Remaining material is commercially available.
Embodiment 1
A kind of sterilization processing agent of wheat seed, is prepared by the raw material of following parts by weight:
10 parts of non-ionic polyacrylamide, 1 part of isothiocyano methyl formate, 5 parts of organic-silicon-modified starch aqueous emulsion, grafting
6 parts of modified soy-bean protein, 1.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 1 part of eugenol, 5 parts of bacterium enzyme intermixture, 5 parts of carbon enzyme, to nitro
7 parts of sodium phenate, 10 parts of Ethyl formate;The bacterium enzyme intermixture is by wax printing fabric, bacillus licheniformis, β-compound detoxication enzyme
In mass ratio 5:2:3 mixing gained.
Embodiment 2
A kind of sterilization processing agent of wheat seed, is prepared by the raw material of following parts by weight:
20 parts of non-ionic polyacrylamide, 2 parts of isothiocyano methyl formate, 15 parts of organic-silicon-modified starch aqueous emulsion, connect
It is 14 parts of modified soy-bean protein of branch, 6.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 5 parts of eugenol, 10 parts of bacterium enzyme intermixture, 10 parts of carbon enzyme, right
15 parts of p-nitrophenol sodium, 20 parts of Ethyl formate, the bacterium enzyme intermixture is by wax printing fabric, bacillus licheniformis, β-compound
Detoxication enzyme in mass ratio 5:2:3 mixing gained.
Embodiment 3
A kind of sterilization processing agent of wheat seed, is prepared by the raw material of following parts by weight:
15 parts of non-ionic polyacrylamide, 1.5 parts of isothiocyano methyl formate, 10 parts of organic-silicon-modified starch aqueous emulsion,
10 parts of graft modification soybean protein, 4 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 3 parts of eugenol, 7.5 parts of bacterium enzyme intermixture, 7.5 parts of carbon enzyme,
11 parts of Sodium p-nitrophenoxide, 15 parts of Ethyl formate, the bacterium enzyme intermixture is by wax printing fabric, bacillus licheniformis, β-multiple
Close detoxication enzyme in mass ratio 5:2:3 mixing gained.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (7)
1. the sterilization processing agent of a kind of wheat seed, it is characterised in that be prepared by the raw material of following parts by weight:
Non-ionic polyacrylamide 10-20 parts, isothiocyano methyl formate 1-2 parts, organic-silicon-modified starch aqueous emulsion 5-15 parts,
Graft modification soybean protein 6-14 parts, toVerticilliumdahliaActivitie Activitie S of Relative albumen 1.5-6.5 parts, eugenol 1-5 parts, bacterium enzyme intermixture 5-10
Part, carbon enzyme 5-10 parts, Sodium p-nitrophenoxide 7-15 parts, Ethyl formate 10-20 parts.
2. the sterilization processing agent of a kind of wheat seed as claimed in claim 1, it is characterised in that the bacterium enzyme intermixture is by wax
Shape bacillus, bacillus licheniformis, β-compound detoxication enzyme in mass ratio 5:2:3 mixing gained.
3. the sterilization processing agent of a kind of wheat seed as claimed in claim 1, it is characterised in that by the raw material of following parts by weight
It is prepared:
10 parts of non-ionic polyacrylamide, 1 part of isothiocyano methyl formate, 5 parts of organic-silicon-modified starch aqueous emulsion, graft modification
6 parts of soybean protein, 1.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 1 part of eugenol, 5 parts of bacterium enzyme intermixture, 5 parts of carbon enzyme, p-nitrophenol
7 parts of sodium, 10 parts of Ethyl formate.
4. the sterilization processing agent of a kind of wheat seed as claimed in claim 1, it is characterised in that by the raw material of following parts by weight
It is prepared:
20 parts of non-ionic polyacrylamide, 2 parts of isothiocyano methyl formate, 15 parts of organic-silicon-modified starch aqueous emulsion, grafting change
14 parts of soybean protein of property, 6.5 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 5 parts of eugenol, 10 parts of bacterium enzyme intermixture, 10 parts of carbon enzyme, to nitro
15 parts of sodium phenate, 20 parts of Ethyl formate.
5. the sterilization processing agent of a kind of wheat seed as claimed in claim 1, it is characterised in that by the raw material of following parts by weight
It is prepared:
15 parts of non-ionic polyacrylamide, 1.5 parts of isothiocyano methyl formate, 10 parts of organic-silicon-modified starch aqueous emulsion, grafting
10 parts of modified soy-bean protein, 4 parts of toVerticilliumdahliaActivitie Activitie S of Relative albumen, 3 parts of eugenol, 7.5 parts of bacterium enzyme intermixture, 7.5 parts of carbon enzyme, to nitre
11 parts of base sodium phenate, 15 parts of Ethyl formate.
A kind of 6. sterilization processing agent of wheat seed as claimed in claim 1, it is characterised in that the organic-silicon-modified starch
Aqueous emulsion is as obtained by prepared by following steps:
S1, the starch aqueous emulsion that mass fraction is 30-40% is prepared, stir the lower quality for adding starch water quality of the emulsion 1.5%
Concentration is 1% copper-bath, is that 6% sodium hydrate aqueous solution adjusts pH value to 9.5 with mass fraction, after be slowly added to form sediment
Powder quality of the emulsion 1.5-2.5% concentration is 9.3-15.3mgL-1Micro-/ nano bubble Ozone Water, 50 DEG C of constant temperature reaction 3h,
The hydrochloric acid for being afterwards 3% using mass fraction is neutralized to pH value as 6.0-6.5, adds starch emulsion 1.5%, mass fraction 10%
Sodium sulfite aqueous solution terminating reaction, it is last it is scrubbed, dry, crush to obtain oxidized starch;
S2, the oxidized starch of gained is scattered in the water that quality is its 400%-500%, adds the salt that mass fraction is 3%
Acid solution, its pH value is adjusted to 5, after system temperature is risen into 50 DEG C, the 15-30% that quality is oxidized starch quality is added dropwise
Vinyl three ('beta '-methoxy ethyoxyl) silane, and stirred with 160-200rmp speed, after 50 DEG C of isothermal reactions 2 hours,
Room temperature is cooled to, adds oxidized starch quality 1%-3% PAMA, 100-150rmp is stirred at room temperature
30min, produce organic-silicon-modified starch aqueous emulsion.
A kind of 7. sterilization processing agent of wheat seed as claimed in claim 1, it is characterised in that the graft modification soybean egg
White is the soybean protein being modified with glycidyl methacrylate graft, and its grafting degree is between 38%-54%.
Priority Applications (1)
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CN201710833843.3A CN107691476A (en) | 2017-09-15 | 2017-09-15 | A kind of sterilization processing agent of wheat seed |
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CN201710833843.3A CN107691476A (en) | 2017-09-15 | 2017-09-15 | A kind of sterilization processing agent of wheat seed |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108782608A (en) * | 2018-07-20 | 2018-11-13 | 海南省农业科学院植物保护研究所 | A kind of composition pesticide for preventing root-knot nematode |
CN111202089A (en) * | 2020-01-19 | 2020-05-29 | 浙江省农业科学院 | Disinfectant for bean sprout production and application thereof |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1158217A (en) * | 1996-11-19 | 1997-09-03 | 刘文治 | High effect microorganism seed growth accelerating agent |
CN105440972A (en) * | 2015-07-31 | 2016-03-30 | 湖南工业大学 | Nano-compound biomass waterborne adhesive |
CN105994359A (en) * | 2016-05-19 | 2016-10-12 | 王星竹 | Wheat seed sterilization treatment agent |
CN106508970A (en) * | 2016-11-08 | 2017-03-22 | 山西省农业科学院果树研究所 | Compound sterilizing composition and application thereof |
CN106922737A (en) * | 2017-03-19 | 2017-07-07 | 佳木斯大学 | A kind of microbial pesticide improved the ecological environment |
-
2017
- 2017-09-15 CN CN201710833843.3A patent/CN107691476A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1158217A (en) * | 1996-11-19 | 1997-09-03 | 刘文治 | High effect microorganism seed growth accelerating agent |
CN105440972A (en) * | 2015-07-31 | 2016-03-30 | 湖南工业大学 | Nano-compound biomass waterborne adhesive |
CN105994359A (en) * | 2016-05-19 | 2016-10-12 | 王星竹 | Wheat seed sterilization treatment agent |
CN106508970A (en) * | 2016-11-08 | 2017-03-22 | 山西省农业科学院果树研究所 | Compound sterilizing composition and application thereof |
CN106922737A (en) * | 2017-03-19 | 2017-07-07 | 佳木斯大学 | A kind of microbial pesticide improved the ecological environment |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108782608A (en) * | 2018-07-20 | 2018-11-13 | 海南省农业科学院植物保护研究所 | A kind of composition pesticide for preventing root-knot nematode |
CN111202089A (en) * | 2020-01-19 | 2020-05-29 | 浙江省农业科学院 | Disinfectant for bean sprout production and application thereof |
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Application publication date: 20180216 |