CN107669542B - Indigo eyebrow pencil lead and preparation method and application thereof - Google Patents
Indigo eyebrow pencil lead and preparation method and application thereof Download PDFInfo
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- CN107669542B CN107669542B CN201710935953.0A CN201710935953A CN107669542B CN 107669542 B CN107669542 B CN 107669542B CN 201710935953 A CN201710935953 A CN 201710935953A CN 107669542 B CN107669542 B CN 107669542B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
Abstract
The eyebrow pencil lead comprises 1-5 parts by mass of ozokerite, 16-20 parts by mass of beeswax, 6-10 parts by mass of carnauba wax, 5-9 parts by mass of Japan wax, 1-5 parts by mass of liquid paraffin, 11-15 parts by mass of cocoa butter, 21-25 parts by mass of lanolin, 11-15 parts by mass of indigo naturalis powder and 10-14 parts by mass of iron oxide. The eyebrow pencil made of the pencil core has uniform color, rich hue, special black and fragrance, and is effective in clearing away heat and removing speckle, and is not easy to fall off when meeting water. In addition, the eyebrow pencil lead is moderate in hardness and convenient to press and form.
Description
Technical Field
The invention relates to the field of development of traditional Chinese medicine cosmetics, in particular to a natural indigo eyebrow pencil lead and a preparation method and application thereof.
Background
The existing cosmetic eyebrow pencils are various in style, the raw materials adopted for manufacturing the pencil core generally comprise oil, grease, wax and pigment, the main components are mainly paraffin wax, beeswax, ozokerite, petrolatum, carnauba wax, lanolin, cocoa butter, red bromate and carbon black pigment, the eyebrow pencils are black, tan, dark gray and the like in color, the traditional eyebrow pencils only generally have a coloring function or poor coloring capability or monotonous hue and do not have abundant changes, the traditional eyebrow pencils also do not have the effect in the aspect of medical care and health care, and the eyebrow pencils are not suitable for beauty people with allergic constitution. Indigo naturalis is used as a traditional Chinese medicine and is widely applied to treatment of skin diseases such as macula, psoriasis and the like in clinic, and the indigo naturalis is a good chromogen and is considered to have potential in being made into cosmetics. However, when only indigo powder is used as a colorant, the coloring power is not good enough, and the picture color is light cyan, uneven, and easily wiped off or dropped.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides the indigo eyebrow pencil lead and the preparation method and application thereof, and the eyebrow pencil made of the eyebrow pencil lead has the advantages of good coloring effect, rich hue, difficulty in falling off when meeting water, moderate hardness and suitability for allergic people. The specific technical scheme is as follows:
the indigo eyebrow pencil lead is characterized by comprising the following components: 1-5 parts of ozokerite, 16-20 parts of beeswax, 6-10 parts of carnauba wax, 5-9 parts of Japan wax, 1-5 parts of liquid paraffin, 11-15 parts of cocoa butter, 21-25 parts of lanolin, 11-15 parts of purified indigo naturalis powder with the particle size of less than 1000 meshes and 10-14 parts of ferric oxide.
Further, the components in the pen core are as follows: 5 parts by mass of ozokerite, 18 parts by mass of beeswax, 6 parts by mass of carnauba wax, 7 parts by mass of japan wax, 3 parts by mass of liquid paraffin, 13 parts by mass of cocoa butter, 24 parts by mass of lanolin, 12 parts by mass of indigo naturalis powder, and 12 parts by mass of iron oxide.
Furthermore, the natural indigo powder is blended with fragrance, and the content of the added essential oil is 1-2 drops per 10g of finished product.
A method of making a natural indigo eyebrow pencil lead of claim 1, comprising the steps of:
1-5 parts by mass of ozokerite, 16-20 parts by mass of beeswax, 6-10 parts by mass of carnauba wax, 5-9 parts by mass of Japan wax, 1-5 parts by mass of liquid paraffin, 11-15 parts by mass of cocoa butter and 21-25 parts by mass of lanolin are stirred in a constant-temperature water bath at 45-78 ℃ to be fully melted, then 11-15 parts by mass of indigo naturalis powder and 10-14 parts by mass of iron oxide are added to be continuously stirred to be fully melted, cooled and solidified, ground into fine powder and pressed into a pen core.
An eyebrow pencil made from the indigo eyebrow pencil lead of claim 1.
Compared with the prior art, the invention has the following beneficial effects:
the invention uses the fine-finished indigo naturalis powder, and mixes the components for forming the eyebrow pencil lead and the proportion of the components, the prepared lead keeps the effects of heat clearing, detoxifying, speckle removing and blood cooling of indigo naturalis, the color changes vividly between green and black after being coated, the color is uniform, the coloring effect is enhanced, the hue is rich, and the eyebrow pencil lead has special cyan black and fragrance and is not easy to fall off when meeting water; in addition, the eyebrow pencil lead is moderate in hardness and convenient to press and form. The invention organically combines beauty and practicability, and meets the requirement of eyebrow drawing and health care in the market.
Detailed Description
The natural indigo eyebrow pencil lead of the invention is further explained by combining the specific embodiment.
The preparation process of the natural indigo powder refers to a traditional preparation method of spiraea sinensis, and is improved by finely processing commercially available natural indigo by ultrasonic dissolution, impurity filtration, water-jet grinding, freeze-drying and other methods, adding United states Duteri brand essential oil (dotrera) to adjust fragrance and increase viscosity, and adding 1-2 drops per 10g of finished product. Finally, the grain diameter of the obtained indigo naturalis powder is less than 1000 meshes.
Example 1
Placing 5 parts by mass of ozokerite, 16 parts by mass of beeswax, 6 parts by mass of carnauba wax, 5 parts by mass of Japan wax, 1 part by mass of liquid paraffin, 11 parts by mass of cocoa butter and 22 parts by mass of lanolin in a beaker, stirring for fully melting in a constant-temperature water bath at 45 ℃, then adding 15 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 12 parts by mass of iron oxide, continuously stirring for melting for fully dissolving, cooling for solidification, cutting into slices with the thickness of 3-4 mm, grinding for 2 times by a grinder to obtain uniform fine powder, and finally putting the fine powder in a plodder for internal pressure injection to obtain the strip-shaped pen core.
Example 2
Placing 4 parts by mass of ozokerite, 18 parts by mass of beeswax, 7 parts by mass of carnauba wax, 8 parts by mass of Japan wax, 3 parts by mass of liquid paraffin, 12 parts by mass of cocoa butter and 24 parts by mass of lanolin in a beaker, stirring in a constant-temperature water bath at 70 ℃ to fully melt the ozokerite, adding 11 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 14 parts by mass of iron oxide, continuously stirring and melting to fully dissolve the ozokerite, cooling and solidifying the ozokerite, cutting the ozokerite into slices with the thickness of 3-4 mm, grinding the ezokerite for 2 times by a grinder to obtain uniform fine powder, and finally placing the fine powder in a plodder to press and inject the fine powder into a strip-shaped pen core.
Example 3
Placing 2 parts by mass of ozokerite, 15 parts by mass of beeswax, 9 parts by mass of carnauba wax, 9 parts by mass of Japan wax, 5 parts by mass of liquid paraffin, 14 parts by mass of cocoa butter and 23 parts by mass of lanolin in a beaker, stirring in a constant-temperature water bath at 78 ℃ to fully melt the ozokerite, adding 13 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 11 parts by mass of iron oxide, continuously stirring and melting to fully dissolve the ozokerite, cooling and solidifying the ozokerite, cutting the ozokerite into slices with the thickness of 3-4 mm, grinding the ezokerite for 2 times by a grinder to obtain uniform fine powder, and finally placing the fine powder in a plodder to press and inject the fine powder into a strip-shaped pen core.
Example 4
Placing 3 parts by mass of ozokerite, 19 parts by mass of beeswax, 8 parts by mass of carnauba wax, 7 parts by mass of Japan wax, 2 parts by mass of liquid paraffin, 13 parts by mass of cocoa butter and 21 parts by mass of lanolin in a beaker, stirring for fully melting in a constant-temperature water bath at 60 ℃, then adding 12 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 13 parts by mass of iron oxide, continuously stirring for melting for fully dissolving, cooling for solidification, cutting into slices with the thickness of 3-4 mm, grinding for 2 times by a grinder to obtain uniform fine powder, and finally placing the fine powder in a plodder for internal pressure injection to obtain the strip-shaped pen core.
Example 5
1 part by mass of ozokerite, 20 parts by mass of beeswax, 10 parts by mass of carnauba wax, 6 parts by mass of Japan wax, 4 parts by mass of liquid paraffin, 15 parts by mass of cocoa butter and 25 parts by mass of lanolin are placed in a beaker, stirred in a constant-temperature water bath at 60 ℃ to be fully melted, then 14 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 10 parts by mass of iron oxide are added, continuously stirred and melted to be fully dissolved, cooled and solidified, cut into slices with the thickness of 3-4 mm, ground for 2 times by a grinder to be uniform and fine powder, and finally the fine powder is placed in a plodder to be pressed into a strip-shaped pen core.
Example 6
Placing 5 parts by mass of ozokerite, 18 parts by mass of beeswax, 6 parts by mass of carnauba wax, 7 parts by mass of Japan wax, 3 parts by mass of liquid paraffin, 13 parts by mass of cocoa butter and 24 parts by mass of lanolin in a beaker, stirring for fully melting in a constant-temperature water bath at 60 ℃, then adding 12 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes and 12 parts by mass of iron oxide, continuously stirring for melting for fully dissolving, cooling for solidification, cutting into slices with the thickness of 3-4 mm, grinding for 2 times by a grinder to obtain uniform fine powder, and finally putting the fine powder in a plodder for internal pressure injection to obtain the strip-shaped pen core.
The pencil core manufactured by the six embodiments is observed and painted, is smooth and cylindrical, is dark black, has special natural indigo fragrance and is moderate in hardness. Painting on A4 paper, and adopting visual method, considering that: the pencil lead has good tinting strength, easy smearing, good ductility, and black color, and is easy to be pressed into strip-shaped pencil lead.
Comparative example 1
Placing 3 parts by mass of ozokerite, 16 parts by mass of beeswax, 6 parts by mass of carnauba wax, 5 parts by mass of Japan wax, 2.5 parts by mass of liquid paraffin, 12 parts by mass of cocoa butter and 24 parts by mass of lanolin in a beaker, stirring in a constant-temperature water bath at 60 ℃ to fully melt the ozokerite, adding 15 parts by mass of iron oxide, continuously stirring and melting to fully dissolve the ozokerite, cooling and solidifying the ozokerite, cutting the ozokerite into slices with the thickness of 3-4 mm, grinding the slices for 2 times by a grinder to form uniform fine powder, and finally placing the fine powder in a plodder to be pressed into a pen core.
Observing and painting, the pen core is dark black, has moderate hardness and special grease smell, is painted on A4 paper, and is considered to be: the pen core prepared by the proportion has strong tinting strength, can be smeared uniformly, has only black color, and can be pressed into a thinner pen core.
Comparative example 2
3 parts by mass of ozokerite, 16 parts by mass of beeswax, 6 parts by mass of carnauba wax, 5 parts by mass of japan wax, 2.5 parts by mass of liquid paraffin, 12 parts by mass of cocoa butter, and 24 parts by mass of lanolin are placed in a beaker, and stirred in a constant-temperature water bath at 60 ℃ to be sufficiently melted, and then cooled and solidified. Because of its soft texture, it cannot be pressed into a thinner refill.
When the pencil is observed and painted, the pencil core is smooth and cylindrical, colorless, has special grease smell and is soft.
Comparative example 3
Placing 3 parts by mass of ozokerite, 16 parts by mass of beeswax, 6 parts by mass of carnauba wax, 5 parts by mass of Japan wax, 2.5 parts by mass of liquid paraffin, 12 parts by mass of cocoa butter and 24 parts by mass of lanolin in a beaker, stirring in a constant-temperature water bath at 60 ℃ to fully melt the ozokerite, adding 15 parts by mass of purified and flavored indigo naturalis powder with the particle size of less than 1000 meshes, continuously stirring to melt the ozokerite to fully dissolve the ozokerite, cooling and solidifying the ozokerite, cutting the ozokerite into slices with the thickness of 3-4 mm, grinding the fine powder for 2 times by a grinder to form uniform fine powder, and finally putting the fine powder in a plodder and pressing the fine powder into a pen core.
Observing and painting, the pen core is smooth and cylindrical, is dark green, has special oil and natural indigo smell and is hard. Painting on A4 paper, and adopting visual method, considering that: the pen core has poor tinting strength, is easy to fall off when being coated, and has light cyan color. The ductility is not good, and the lead is not easy to be pressed into a pencil core.
The components and the ratios of the above examples and comparative examples are shown in table 1.
TABLE 16 contents of respective components in examples and 3 comparative examples
Visual observation and painting of the refills made of 6 examples and 3 comparative examples were carried out, the results of which are given in table 2 below:
TABLE 26 comparison of the effects of the refills made in the examples and in the 3 comparative examples
The eyebrow pencils prepared by 5 examples and 4 comparative examples were subjected to further trial investigation and evaluation test by the present invention. The implementation scheme is that 60 special volunteers are selected, the age is not limited, and spots, whelks and the like on the eyebrow ridge part of the volunteers meet the symptoms of 'excessive internal heat' in the traditional Chinese medicine. The volunteers were randomly divided into two groups, 30 female and 30 male, and evaluation tests were performed on the examples and comparative examples with a trial period of one month. The trial population is the population which is easy to fall off when meeting water or has poor coloring effect, and the test results are shown in the following table 3.
TABLE 36 questionnaire on the application effect of eyebrow pencil made of lead of example and 3 comparative examples (unit: number of people)
As can be seen from table 3: for the eyebrow dressing and water-removable population, the number of people who improved and relieved eyebrow dressing and water-removable is significantly larger in examples 1-6 than in comparative examples 1-3, and the symptoms of the user who had partially "burned" in examples 1-6 are relieved, and the scars are removed. The better waterproof effect of the eyebrow pencil of the present invention is demonstrated, and example 6 has the best remarkable improvement and alleviation effects.
For the crowd with poor coloring effect, the number of people with obvious improvement in the examples 1-6 is also obviously higher than that in the comparative examples 1-3, and the eyebrow pencil prepared in the example 6 has the best obvious improvement and relief effect, and compared with the comparative example 2, the comparison shows that the effect of obviously improving the coloring can be achieved by matching the indigo naturalis powder and the iron oxide according to a certain scientific ratio.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any changes or substitutions that can be easily conceived by those skilled in the art within the technical scope of the present invention disclosed herein should be covered within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (5)
1. The indigo eyebrow pencil lead is characterized by comprising the following components: 1-5 parts of ozokerite, 16-20 parts of beeswax, 6-10 parts of carnauba wax, 5-9 parts of Japan wax, 1-5 parts of liquid paraffin, 11-15 parts of cocoa butter, 21-25 parts of lanolin, 11-15 parts of purified indigo naturalis powder with the particle size of less than 1000 meshes and 10-14 parts of ferric oxide.
2. A natural indigo refill according to claim 1, wherein the refill specifically comprises the following components: 5 parts by mass of ozokerite, 18 parts by mass of beeswax, 6 parts by mass of carnauba wax, 7 parts by mass of japan wax, 3 parts by mass of liquid paraffin, 13 parts by mass of cocoa butter, 24 parts by mass of lanolin, 12 parts by mass of indigo naturalis powder, and 12 parts by mass of iron oxide.
3. The indigo eyebrow pencil lead core according to claim 1 or 2, wherein the indigo naturalis powder is blended with fragrance, and the content of added essential oil is 1-2 drops per 10g of finished product.
4. A method of making a natural indigo eyebrow pencil lead of claim 1, comprising the steps of:
1-5 parts by mass of ozokerite, 16-20 parts by mass of beeswax, 6-10 parts by mass of carnauba wax, 5-9 parts by mass of Japan wax, 1-5 parts by mass of liquid paraffin, 11-15 parts by mass of cocoa butter and 21-25 parts by mass of lanolin are stirred in a constant-temperature water bath at 45-78 ℃ to be fully melted, then 11-15 parts by mass of indigo naturalis powder and 10-14 parts by mass of iron oxide are added to be continuously stirred to be fully melted, cooled and solidified, ground into fine powder and pressed into a pen core;
the natural indigo powder is prepared by ultrasonically dissolving commercially available natural indigo, filtering impurities, grinding by a water-jet method, freeze-drying, adding American multitere brand essential oil to adjust fragrance and increase viscosity, and adding 1-2 drops of the natural indigo powder into each 10g of finished product.
5. An eyebrow pencil made from the indigo eyebrow pencil lead of claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710935953.0A CN107669542B (en) | 2017-10-10 | 2017-10-10 | Indigo eyebrow pencil lead and preparation method and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710935953.0A CN107669542B (en) | 2017-10-10 | 2017-10-10 | Indigo eyebrow pencil lead and preparation method and application thereof |
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| CN107669542A CN107669542A (en) | 2018-02-09 |
| CN107669542B true CN107669542B (en) | 2020-05-26 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110314123A (en) * | 2019-07-01 | 2019-10-11 | 上海欧润化妆品有限公司 | A kind of eyebrow pencil and preparation method thereof |
| CN112972307B (en) * | 2021-02-24 | 2022-12-16 | 浙江颜雪化妆品有限公司 | Waterproof sweat-proof lasting eyebrow pencil and preparation method thereof |
| CN114557923A (en) * | 2022-03-29 | 2022-05-31 | 广州笔匠化妆品有限公司 | Double-color core wood eyebrow pencils |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH10139677A (en) * | 1996-11-07 | 1998-05-26 | Yasuhiro Omori | Skin lotion |
| JP2010180175A (en) * | 2009-02-06 | 2010-08-19 | Iriya Cosmetics Co Ltd | Cosmetic for forming false eyebrow |
| CN102370603A (en) * | 2010-08-14 | 2012-03-14 | 张国防 | Tricolor eye shadow containing natural pigments |
| KR101438905B1 (en) * | 2012-09-18 | 2014-09-05 | 주식회사 엘지생활건강 | Composition for eye-makeup |
| CN105816359A (en) * | 2016-03-29 | 2016-08-03 | 高小娜 | Pencil type eyebrow pencil |
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