CN107655990B - 基于气质联用技术检测农田环境中西玛津残留量的方法 - Google Patents
基于气质联用技术检测农田环境中西玛津残留量的方法 Download PDFInfo
- Publication number
- CN107655990B CN107655990B CN201710851595.5A CN201710851595A CN107655990B CN 107655990 B CN107655990 B CN 107655990B CN 201710851595 A CN201710851595 A CN 201710851595A CN 107655990 B CN107655990 B CN 107655990B
- Authority
- CN
- China
- Prior art keywords
- sample
- simazine
- solution
- detected
- extracting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
- G01N2030/062—Preparation extracting sample from raw material
Abstract
Description
相对离子丰度/% | >50 | 20-50 | 10-20 | ≤10 |
允许的相对偏差/% | ±10 | ±15 | ±20 | ±50 |
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710851595.5A CN107655990B (zh) | 2017-09-19 | 2017-09-19 | 基于气质联用技术检测农田环境中西玛津残留量的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710851595.5A CN107655990B (zh) | 2017-09-19 | 2017-09-19 | 基于气质联用技术检测农田环境中西玛津残留量的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN107655990A CN107655990A (zh) | 2018-02-02 |
CN107655990B true CN107655990B (zh) | 2020-05-22 |
Family
ID=61129621
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710851595.5A Active CN107655990B (zh) | 2017-09-19 | 2017-09-19 | 基于气质联用技术检测农田环境中西玛津残留量的方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN107655990B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111879879B (zh) * | 2020-08-25 | 2023-09-26 | 福建省中孚检测技术有限公司 | 一种植物性食品中甲胺磷和八氯二丙醚的检测方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101718756B (zh) * | 2009-11-24 | 2012-10-24 | 湖南省烟草公司郴州市公司 | 同时测定烟田土壤中三种不同类型除草剂残留量的方法 |
-
2017
- 2017-09-19 CN CN201710851595.5A patent/CN107655990B/zh active Active
Also Published As
Publication number | Publication date |
---|---|
CN107655990A (zh) | 2018-02-02 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102735784A (zh) | 一种超高效液相色谱-串联四级杆质谱同时测定中药中100种农药残留的方法 | |
Chen et al. | Determination of arsenic species in edible mushrooms by high-performance liquid chromatography coupled to inductively coupled plasma mass spectrometry | |
CN107576741B (zh) | 一种固相萃取-气相色谱串联质谱法检测水产品中有机磷农药多组分残留的方法 | |
CN112461960B (zh) | 同时测定水质中多种杂环农药、降解物和中间体的方法 | |
Cho et al. | Effectiveness of pressurized liquid extraction and solvent extraction for the simultaneous quantification of 14 pesticide residues in green tea using GC | |
Pang et al. | High-throughput analytical techniques for multiresidue, multiclass determination of 653 pesticides and chemical pollutants in tea—part III: evaluation of the cleanup efficiency of an SPE cartridge newly developed for multiresidues in tea | |
Viana de Carvalho et al. | Two‐dimensional coordination polymer matrix for solid‐phase extraction of pesticide residues from plant Cordia salicifolia | |
Wu et al. | Development and evaluation of an automated multi-channel multiplug filtration cleanup device for pesticide residue analysis on mulberry leaves and processed tea | |
CN104713974A (zh) | 一种蔬菜中55种农药残留量测定的方法 | |
Lu et al. | Effect of pretreatment on detection of 37 pesticide residues in Chrysanthemum indicum | |
CN105548431A (zh) | 同时检测蔬菜/水果中杀线威和杀线威肟残留量的方法 | |
CN107655990B (zh) | 基于气质联用技术检测农田环境中西玛津残留量的方法 | |
Qin et al. | Multi-residue method for determination of selected neonicotinoid insecticides in traditional Chinese medicine using modified dispersive solid-phase extraction combined with ultra-performance liquid chromatography tandem mass spectrometry | |
Kadir et al. | Analysis of pesticide residues in tea using accelerated solvent extraction with in-cell cleanup and gas chromatography tandem mass spectrometry | |
Wang et al. | Determination of agrochemical residues in aquatic vegetables by solid-phase extraction combined with HPLC spectrometry analyses | |
CN204789501U (zh) | 一种用于链格孢毒素检测的多功能净化柱 | |
CN114264755B (zh) | 针对植物源性食品中砜吡草唑残留量的气相色谱-三重四极杆质谱检测方法 | |
CN110554132A (zh) | 一种柑橘中丙硫唑残留量的检测方法 | |
Komarova et al. | Determination of ametoctradin in plant residues and environmental samples by HPLC with an UV detector | |
CN105938102B (zh) | 一种化学显色法快速测定果蔬中农药残留的方法 | |
Wang et al. | A Rapid Multi-Residue Determination Method of Herbicides in Grain by GC—MS-SIM | |
CN114577951A (zh) | 一种气相色谱-三重四极杆质谱法测定植物源性产品中草枯醚和氟除草醚残留量的方法 | |
CN103558299A (zh) | 利用凝胶渗透色谱处理生物检材的拟除虫菊酯类农药检验方法 | |
CN109212108B (zh) | 一种同时测定稻米和大豆中三种痕量喹啉类除草剂的气相色谱-质谱联用法 | |
CN112924599A (zh) | 一种稻田环境中溴虫氟苯双酰胺残留的提取与检测方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB02 | Change of applicant information | ||
CB02 | Change of applicant information |
Address after: 110016, 106 Binhe Road, Shenhe District, Liaoning, Shenyang Applicant after: Shenyang Customs Technical Center Applicant after: SHENYANG AGRICULTURAL University Address before: 110016, 106 Binhe Road, Shenhe District, Liaoning, Shenyang Applicant before: INSPECTION AND QUARANTINE COMPREHENSIVE TECHNOLOGY CENTER, SHENYANG ENTRY-EXIT INSPECTION AND QUARANTINE BUREAU Applicant before: SHENYANG AGRICULTURAL University |
|
CB03 | Change of inventor or designer information | ||
CB03 | Change of inventor or designer information |
Inventor after: Xu Yihong Inventor after: Zhang Min Inventor after: Fu Hai Inventor after: Zhong Yu Inventor after: Zhao Ying Inventor before: Xu Yihong Inventor before: Fu Hai Inventor before: Zhang Min Inventor before: Zhao Ying Inventor before: Zhong Yu |
|
GR01 | Patent grant | ||
GR01 | Patent grant |