CN107646845A - A kind of complex composition containing capillin and Boscalid - Google Patents
A kind of complex composition containing capillin and Boscalid Download PDFInfo
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- CN107646845A CN107646845A CN201710965558.7A CN201710965558A CN107646845A CN 107646845 A CN107646845 A CN 107646845A CN 201710965558 A CN201710965558 A CN 201710965558A CN 107646845 A CN107646845 A CN 107646845A
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- boscalid
- capillin
- complex composition
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of complex composition containing capillin and Boscalid, effective active composition is made up of capillin and Boscalid, and the weight ratio of capillin and Boscalid is 30:1~1:30.The disease excellent such as gray mold, sclerotiniose on built composition for preventing and controlling crops of the present invention, lasting period length, to Crop securify.There is significant synergistic function after capillin and Boscalid compounding, Pesticide use amount can be reduced, use cost is reduced, mitigate the pollution to environment, delay the drug-fast generation of pathogen, increase the Pesticide use life-span.
Description
Technical field
The present invention relates to pesticide complex composition and its application field, specifically with capillin and Boscalid
For the binary complex of effective active composition compounding, the preventing and treating of disease on crops is mainly used in.
Background technology
Capillin (capillin), is the active component separated in Artemisia capillaris essential oil, Artemisia capillaris belong to composite family,
There is growth sagebruss, all parts of the country.Capillin has stronger bactericidal action.
Boscalid (boscalid) is aniline fungicides, has the mechanism of action for suppressing the breathing of cause of disease thalline, interference
The division and growth of cell, there is protection and therapeutic action.Preventing and treating available for the disease such as gray mold, sclerotiniose on crops.
The long-time continuous use of agricultural chemicals single variety, resistance risk and dosage increase risk are easily produced, and then increased
Cost and carrying capacity of environment, and the compounded combination with notable synergistic function is gone out by the compound screening of different pesticide species
Thing, Pesticide use amount can not only be reduced, use cost is reduced, reduces resistance risk, moreover it is possible to reduces potential environmental risk, increases
The Pesticide use life-span.
The present inventor is during further investigation capillin and Boscalid compounded formula, surprisingly
Capillin and Boscalid are compounded, to the multiple diseases on crops in the range of certain compound proportion, especially
It is to have significant synergistic function, after further study, complete the present invention gray mold, sclerotiniose.
The content of the invention
It is an object of the invention to provide a kind of component is reasonable, obvious synergy, bactericidal effect is outstanding, the lasting period
Long, drug cost is low, can delay the drug-fast generation of pathogen, and to the pesticide complex composition of Crop securify.
Another object of the present invention is to provide a kind of complex composition preparation agent containing capillin and Boscalid
Type.
It is still another object of the present invention to provide above-mentioned complex composition on preventing and treating crops the disease such as gray mold, sclerotiniose
Harmful purposes.
Technical scheme：To achieve the above object, present invention offer one kind contains capillin and Boscalid
Complex composition, effective active composition is made up of capillin and Boscalid, the weight of capillin and Boscalid
Amount is than being 30:1~1:30, preferred weight ratio 20:1~1:20, most preferably weight ratio is 4:1.
In complex composition of the present invention, the gross weight percentage composition of capillin and Boscalid is 0.1%~85%,
It is preferred that the gross weight percentage composition of capillin and Boscalid is 1%~70%.
Complex composition of the present invention can be prepared into any application forms used in suitable agricultural production, and relatively good should
There are suspending agent, water dispersible granules, ultra low volume liquids etc. with formulation.
In various application forms prepared by complex composition of the present invention, in addition to effective active composition, in addition in agricultural chemicals
Allow to use and the various auxiliary elements of acceptable.
Auxiliary element in suspending agent includes but is not limited to：The optional freely double naphthalenesulfonate formaldehyde condensation compounds of dispersant, gather
Carboxylate, lignosulfonates, alkyl naphthalene formaldehyde condensate sulfonates, alkylphenol-polyethenoxy base ether phosphate, alkyl phenol gather
Oxyethylene group ether sulfonate, phenethyl phenol polyoxyethylene groups ether phosphate, alkyl polyoxyethylene ether sulfonate, polyoxyethylene polyoxy
One or more of mixing in propenyl ether block copolymer, pull open powder, alkylpolyoxyethylene phosphate；Wetting agent
Optional freely polyether-modified polysiloxane, alkylphenol-polyethenoxy base ether formaldehyde condensation products sulfate, phenethyl phenol polyoxy
Vinyl ethers phosphate, alkyl sulfate, alkylsulfonate, alkylnaphthalene sulfonate, alkyl phenol formaldehyde resin polyoxyethylene ether, three
One or more of mixing in phenethyl phenol polyoxyethylene polyoxypropylene block polymer；Thickener is optional freely Arabic
Glue, xanthans, carboxymethyl cellulose, polyvinyl alcohol, gaseous silicon oxide, Magnesiumaluminumsilicate, carboxyethyl cellulose, carboxylic propyl group fiber
One kind or several in element, PAA, polyvinylpyrrolidone, Sodium Polyacrylate, polyvinyl acetate, bentonite, white carbon
The mixing of kind；In the optional KF88 of Kathon CG freely of preservative, formaldehyde, benzoic acid, sodium benzoate, potassium sorbate, OIT
One or more of mixing；The optional silicone oil freely of defoamer, silicone compound, C10-20Saturated fat acids compound, C8-10
One or more of mixing in aliphatic alcohols, hexanol, butanol, octanol；The optional glycerine freely-ether diglycol of antifreezing agent, first
One or more of mixing in base propylidene diglycol, ethylene glycol, propane diols, glycerine, urea；Water is deionized water.
Auxiliary element in water dispersible granules includes but is not limited to：The optional sodium lignin sulfonate freely of dispersant, polycarboxylic acids
Salt, lauryl alcohol polyethylene glycol oxide base ether sodium sulfate, alkyl naphthalene formaldehyde condensate sulfonates, alkyl polyoxyethylene ether sulfonate, alkane
Base phenol polyethenoxy base ether formaldehyde condensation products, polyoxyethylene polyoxypropylene base ether block copolymers, alkylpolyoxyethylene
One or more of mixing in phosphate；The optional neopelex freely of wetting agent, pull open powder, alkylphenol formaldehyde tree
One or more of mixing in fat polyoxyethylene ether sulfate, alkylphenol-polyethenoxy base ether, Nonyl pheno base ether；
Disintegrant optional ammonium sulfate freely, sodium sulphate, polyvinylpyrrolidone, starch and its derivative, one kind in bentonite or several
The mixing of kind；The optional kaolin freely of filler, diatomite, precipitated calcium carbonate, white carbon, attapulgite, cornstarch, Hai Pao
One or more of mixing in stone, calcite, silica, pyrophyllite, xylitol, montmorillonite, clay.
Auxiliary element in ultra low volume liquids includes but is not limited to：The optional aliphatic alcohol polyethenoxy freely of surfactant
Ether, APES, alkylaryl polyoxyethylene polyoxypropylene ether again, APES phosphate, phenethyl
Phenol polyethenoxy ether phosphate, alkylaryl polyoxyethylene polyoxypropylene ether again phosphate, castor oil polyoxyethylene ether, dodecyl
One or more of mixing in benzene sulfonic acid calcium；In the optional azone freely of bleeding agent, thiophene ketone, fast penetrant T, isophorone
One or more of mixing；The optional ethylo benzene freely of solvent, trimethylbenzene, soybean oil, rapeseed oil, corn oil, loose base oil, oleic acid first
It is ester, ethyl oleate, methanol, ethanol, acetone, N,N-dimethylformamide, DMAC N,N' dimethyl acetamide, ethylene glycol, propane diols, sweet
One or more of mixing in oil, isooctanol, n-octyl alcohol.
The production technology of the various application forms of complex composition belongs to existing known technology, will not be repeated here.
Compared with prior art, the advantage of the invention is that：
1st, capillin and Boscalid compounding have significant synergistic function, are used alone than single dose obvious
Improve the prevention effect to disease on crops.
2nd, capillin and Boscalid two kinds of active components compounding, reduce Pesticide use amount, reduce use into
This, alleviates the pollution to environment.
3rd, capillin and Boscalid two kinds of active components compounding, the mechanism of action is different, action site increase,
Delay the drug-fast generation of pathogen, add the service life of agricultural chemicals.
Embodiment
Essence for a better understanding of the present invention, present disclosure is described further with reference to embodiment,
But limitation of the present invention can not be considered as, it is as described below to be only used for explaining the present invention, for without departing from spirit of the invention and principle
Modification, replacement or the improvement made, belong to the scope of protection of present invention.
Embodiment one
Following content of material is weight percentage：Capillin 20%, Boscalid 5%, phenethyl phenol polyoxy
Vinyl ethers phosphate 8%, alkylnaphthalene sulfonate 5%, xanthans 2.5%, Kathon CG KF88 0.2%, C10-20Saturated fat acids
Compound 0.5%, ethylene glycol 2.5%, deionized water complements to 100%.Above-mentioned material is mixed in proportion, through high speed shear point
Dissipate after being sanded in uniform, sand mill, you can 25% capillin Boscalid suspending agent is made.
It is used to prevent and treat grape grey mould using above-mentioned 25% capillin Boscalid suspending agent：25% Capillene
Ketone Boscalid suspending agent is by 800mg a.i./kg dosages after grape grey mould early period of origination progress first time dispenser, 7d
Second of dispenser is carried out, 14d is 87.17% to the preventive effect of grape grey mould after second of dispenser；20% capillin hangs
Floating agent carries out first time dispenser by 1000mg a.i./kg dosages in grape grey mould early stage, is applied for the second time after 7d
Medicine, 14d is 56.92% to the preventive effect of grape grey mould after second of dispenser；5% Boscalid suspending agent presses 300mg
A.i./kg dosages carry out first time dispenser in grape grey mould early stage, second of dispenser are carried out after 7d, in second of dispenser
14d is 62.17% to the preventive effect of grape grey mould afterwards.It can be seen that Synergistic after capillin and Boscalid binary built
Effect is notable, lasting period length, the preventive effect of grape grey mould is used alone significantly better than each single dose, meanwhile, during experiment
Do not find to produce poisoning to grape after using 25% capillin Boscalid suspending agent.
Embodiment two
Following content of material is weight percentage：Capillin 50%, Boscalid 5%, polyoxyethylene polyoxy
Propenyl ether block copolymer 10%, pull open powder 6%, polyvinylpyrrolidone 4%, kaolin complements to 100%.By above-mentioned thing
Material mixes in proportion, after air-flow crushing is well mixed, kneading is granulated, dries screening, you can 55% capillin is made
Boscalid water dispersible granules.
It is used to prevent and treat sclerotinia sclerotiorum using above-mentioned 55% capillin Boscalid water dispersible granules：55% oriental wormwood
Two acetylenic ketone Boscalid water dispersible granules in sclerotinia sclerotiorum early period of origination apply for the first time by 500g a.i./ha dosages
Medicine, second of dispenser is carried out after 7d, 14d is 84.34% to the preventive effect of sclerotinia sclerotiorum after second of dispenser；50% oriental wormwood two
Acetylenic ketone water dispersible granules carry out first time dispenser by 600g a.i./ha dosages in sclerotinia sclerotiorum early stage, and the is carried out after 7d
Secondary dispenser, 14d is 61.97% to the preventive effect of sclerotinia sclerotiorum after second of dispenser；5% Boscalid water dispersible granules are pressed
200g a.i./ha dosages carry out first time dispenser in sclerotinia sclerotiorum early stage, second of dispenser are carried out after 7d, second
14d is 67.69% to the preventive effect of sclerotinia sclerotiorum after secondary dispenser.It can be seen that assisted after capillin and Boscalid binary built
It is notable with synergistic effect, lasting period length, the preventive effect of sclerotinia sclerotiorum is used alone significantly better than each single dose, meanwhile, testing
During do not find use 55% capillin Boscalid water dispersible granules after to rape produce poisoning.
Embodiment three
Following content of material is weight percentage：Capillin 5%, Boscalid 5%, aliphatic alcohol polyethenoxy
Ether 12%, calcium dodecyl benzene sulfonate 10%, thiophene ketone 2%, trimethylbenzene 10%, rapeseed oil complements to 100%.Above-mentioned material is pressed
Ratio mixes, after stirring, you can 10% capillin Boscalid ultra low volume liquids are made.
It is used to prevent and treat gray mold of cucumber using above-mentioned 10% capillin Boscalid ultra low volume liquids：10% mattress
Old two acetylenic ketones Boscalid ultra low volume liquids carry out first by 300g a.i./ha dosages in gray mold of cucumber early period of origination
Secondary dispenser, second of dispenser is carried out after 7d, 14d is 78.91% to the preventive effect of gray mold of cucumber after second of dispenser；5% mattress
Old two acetylenic ketones ultra low volume liquids are by 600g a.i./ha dosages after gray mold of cucumber early stage progress first time dispenser, 7d
Second of dispenser is carried out, 14d is 51.89% to the preventive effect of gray mold of cucumber after second of dispenser；5% Boscalid super-low capacity
Measure liquor and carry out first time dispenser in gray mold of cucumber early stage by 200g a.i./ha dosages, applied for the second time after 7d
Medicine, 14d is 60.13% to the preventive effect of gray mold of cucumber after second of dispenser.It can be seen that capillin and Boscalid binary
Obvious synergy after compounding, lasting period length, the preventive effect of gray mold of cucumber is used alone significantly better than each single dose, together
When, do not find to produce medicine to cucumber after using 10% capillin Boscalid ultra low volume liquids during experiment
Evil.
Example IV capillin and Boscalid compounding are tested the Toxicity Determination of Pathogen of Botrytis cinerea on Grape bacterium
Test method：With reference to《Farm-chemical indoor determination test rule bactericide NY/T1156.9-2008》, using blade
Method.
Statistical analysis is carried out with DPS statistical analysis softwares, calculates the EC of each medicament50, and mixture is calculated according to the abundant methods of Sun Yun
Co-toxicity coefficient (CTC values), co-toxicity coefficient (CTC) >=120 shows as synergistic effect；Co-toxicity coefficient (CTC)≤80 shows as short of money
Anti- effect；80 ＜ co-toxicity coefficients (CTC) ＜ 120 show as summation action.
The capillin of table 1 and Boscalid compound the Toxicity Determination to Pathogen of Botrytis cinerea on Grape bacterium
| Medicament title and proportioning (weight ratio) | EC50(mg/L) | ATI | TTI | CTC |
| Capillin | 2.76 | 100.00 | ||
| Boscalid | 0.93 | 296.77 | ||
| Capillin：Boscalid (30:1) | 2.28 | 121.05 | 106.35 | 113.82 |
| Capillin：Boscalid (20:1) | 1.86 | 148.39 | 109.37 | 135.68 |
| Capillin：Boscalid (10:1) | 1.45 | 190.34 | 117.89 | 161.46 |
| Capillin：Boscalid (7:1) | 1.21 | 228.10 | 124.60 | 183.07 |
| Capillin：Boscalid (4:1) | 0.98 | 281.63 | 139.35 | 202.10 |
| Capillin：Boscalid (1:1) | 0.73 | 378.08 | 198.39 | 190.57 |
| Capillin：Boscalid (1:4) | 0.59 | 467.80 | 257.42 | 181.73 |
| Capillin：Boscalid (1:7) | 0.62 | 445.16 | 272.17 | 163.56 |
| Capillin：Boscalid (1:10) | 0.67 | 411.94 | 278.88 | 147.71 |
| Capillin：Boscalid (1:20) | 0.75 | 368.00 | 287.40 | 128.04 |
| Capillin：Boscalid (1:30) | 0.89 | 310.11 | 290.42 | 106.78 |
As it can be seen from table 1 capillin and Boscalid are 20:1~1:When being compounded in the range of 20 (by weight),
Co-toxicity coefficient (CTC) is all higher than 120, illustrates to show synergistic function to Pathogen of Botrytis cinerea on Grape bacterium；Capillin and
Boscalid is with 4:1 (by weight) compounding, synergistic function is the most notable, and co-toxicity coefficient (CTC) reaches maximum, is
202.10.It can be seen that capillin and Boscalid compounding have reasonability and feasibility.
The capillin of embodiment five and Boscalid compounding are tested the Toxicity Determination of sclerotinia sclerotiorum pathogen
Test method：With reference to《Farm-chemical indoor determination test rule bactericide NY/T1156.2-2006》, using plate
Method.
Statistical analysis is carried out with DPS statistical analysis softwares, calculates the EC of each medicament50, and mixture is calculated according to the abundant methods of Sun Yun
Co-toxicity coefficient (CTC values), co-toxicity coefficient (CTC) >=120 shows as synergistic effect；Co-toxicity coefficient (CTC)≤80 shows as short of money
Anti- effect；80 ＜ co-toxicity coefficients (CTC) ＜ 120 show as summation action.
The capillin of table 2 and Boscalid compound the Toxicity Determination to sclerotinia sclerotiorum pathogen
| Medicament title and proportioning (weight ratio) | EC50(mg/L) | ATI | TTI | CTC |
| Capillin | 2.37 | 100.00 | ||
| Boscalid | 1.24 | 191.13 | ||
| Capillin：Boscalid (30:1) | 2.37 | 100.00 | 102.94 | 97.14 |
| Capillin：Boscalid (20:1) | 1.75 | 135.43 | 104.34 | 129.80 |
| Capillin：Boscalid (10:1) | 1.51 | 156.95 | 108.28 | 144.95 |
| Capillin：Boscalid (7:1) | 1.24 | 191.13 | 111.39 | 171.59 |
| Capillin：Boscalid (4:1) | 1.03 | 230.10 | 118.23 | 194.62 |
| Capillin：Boscalid (1:1) | 0.87 | 272.41 | 145.57 | 187.13 |
| Capillin：Boscalid (1:4) | 0.81 | 292.59 | 172.90 | 169.22 |
| Capillin：Boscalid (1:7) | 0.89 | 266.29 | 179.74 | 148.15 |
| Capillin：Boscalid (1:10) | 0.95 | 249.47 | 182.85 | 136.43 |
| Capillin：Boscalid (1:20) | 1.01 | 234.65 | 186.79 | 125.62 |
| Capillin：Boscalid (1:30) | 1.14 | 207.89 | 188.19 | 110.47 |
From table 2 it can be seen that capillin and Boscalid are 20:1~1:When being compounded in the range of 20 (by weight),
Co-toxicity coefficient (CTC) is all higher than 120, illustrates to show synergistic function to sclerotinia sclerotiorum pathogen；Capillin and
Boscalid is with 4:1 (by weight) compounding, synergistic function is the most notable, and co-toxicity coefficient (CTC) reaches maximum, is
194.62.It can be seen that capillin and Boscalid compounding have reasonability and feasibility.
In summary, a kind of complex composition containing capillin and Boscalid of the present invention, Synergistic
Effect is notable, is used alone compared to each single dose and improves preventive effect, and it is a variety of effectively to prevent and treat gray mold on crops, sclerotiniose etc.
Disease, lasting period length, to Crop securify, is worth the popularization and application in agricultural production.
Claims (7)
- A kind of 1. complex composition containing capillin and Boscalid, it is characterised in that：Effective active composition is by oriental wormwood two The weight ratio of acetylenic ketone and Boscalid composition, capillin and Boscalid is 30:1~1:30.
- A kind of 2. complex composition containing capillin and Boscalid according to claim 1, it is characterised in that：Mattress The weight ratio of old two acetylenic ketones and Boscalid is 20:1~1:20.
- A kind of 3. complex composition containing capillin and Boscalid according to claim 1, it is characterised in that：Mattress The weight ratio of old two acetylenic ketones and Boscalid is 4:1.
- A kind of 4. complex composition containing capillin and Boscalid according to claim 1, it is characterised in that：It is multiple Gross weight percentage composition with capillin in composition and Boscalid is 0.1%~85%.
- A kind of 5. complex composition containing capillin and Boscalid according to claim 1, it is characterised in that：Institute The formulation for stating complex composition is suspending agent, water dispersible granules, ultra low volume liquids.
- A kind of 6. complex composition containing capillin and Boscalid according to claim 5, it is characterised in that institute When stating the formulation of complex composition suspending agent is made, weight percentage is：Capillin 20%, Boscalid 5%, benzene second Base phenol polyethenoxy base ether phosphate 8%, alkylnaphthalene sulfonate 5%, xanthans 2.5%, Kathon CG KF88 0.2%, C10-20Saturation Fatty acid compound 0.5%, ethylene glycol 2.5%, deionized water complements to 100%.
- 7. a kind of complex composition containing capillin and Boscalid described in claim 1 is used to prevent and treat grey on crops Mildew, the purposes of sclerotiniose.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114480032A (en) * | 2020-10-27 | 2022-05-13 | 山西焦煤运城盐化集团有限责任公司 | Formula and production of antibacterial and acarus killing concentrated washing powder |
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| JP2003265152A (en) * | 2002-03-15 | 2003-09-24 | Dainippon Ink & Chem Inc | Antibacterial agent comprising essential oil of artemisia capillaris, method of production for the same and food preservative |
| JP2004168669A (en) * | 2002-11-18 | 2004-06-17 | Sakamoto Yakuhin Kogyo Co Ltd | Putrefaction-preventing agent for field crop |
| JP2007119411A (en) * | 2005-10-28 | 2007-05-17 | Sakamoto Yakuhin Kogyo Co Ltd | Method for stabilizing capillin |
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| 颜范勇等: "新型烟酰胺类杀菌剂—啶酰菌胺", 《农药》 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114480032A (en) * | 2020-10-27 | 2022-05-13 | 山西焦煤运城盐化集团有限责任公司 | Formula and production of antibacterial and acarus killing concentrated washing powder |
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Address after: 610000 Northwest Biochemical Company, 388 Rongtai Avenue, Cross-Strait Science and Technology Industrial Development Park, Wenjiang District, Chengdu City, Sichuan Province Applicant after: Zhang Xilin Address before: 516000 Xiaojinkou 135 Huizhou Avenue, Huicheng District, Huizhou City, Guangdong Province Applicant before: Zhang Xilin |
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Application publication date: 20180202 |