CN107604347A - A kind of architectural shape surface conditioning agent and its preparation technology - Google Patents
A kind of architectural shape surface conditioning agent and its preparation technology Download PDFInfo
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- CN107604347A CN107604347A CN201710902121.9A CN201710902121A CN107604347A CN 107604347 A CN107604347 A CN 107604347A CN 201710902121 A CN201710902121 A CN 201710902121A CN 107604347 A CN107604347 A CN 107604347A
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Abstract
The invention discloses a kind of architectural shape surface conditioning agent and its preparation technology, surface conditioning agent component includes 10 20 parts of phytic acid, 10 26 parts of sodium fluoborate, 8 12 parts of DBSA, 4 12 parts of fluotitanic acid, 5 10 parts of fluorine zirconic acid, 4 12 parts of butanedioic acid, 26 parts of nano silicon, 28 parts of nano titanium oxide, 4 10 parts of chitosan, 14 parts of corrosion inhibiter in parts by weight, preparation technology of the present invention is simple, obtained surface conditioning agent can effectively be passivated architectural shape surface, oxidative phenomena is prevented, while oxide-film can also be formed on architectural shape surface.
Description
Technical field
The present invention relates to surface conditioning agent preparing technical field, specially a kind of architectural shape surface conditioning agent and its preparation
Technique.
Background technology
Iron and steel parts will do antirust treatment, it is common practice to paint, and in order to increase coating and steel plate before painting
Bonding strength, the surface treatment before will painting to iron and steel parts, make to be formed outside iron and steel parts a kind of similar
Honeycomb-like tissue, increase adhesion strength.But easily corrode Surface of profile in existing surface conditioning agent, using effect is poor.
The content of the invention
It is an object of the invention to provide a kind of architectural shape surface conditioning agent and its preparation technology, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical scheme：A kind of architectural shape surface conditioning agent, surface treatment
Agent component includes phytic acid 10-20 parts, sodium fluoborate 10-26 parts, DBSA 8-12 parts, fluotitanic acid 4- in parts by weight
12 parts, fluorine zirconic acid 5-10 parts, butanedioic acid 4-12 parts, nano silicon 2-6 parts, nano titanium oxide 2-8 parts, chitosan 4-
10 parts, corrosion inhibiter 1-4 parts.
Preferably, the preferable composition proportion of surface conditioning agent component includes 15 parts of phytic acid, 18 parts of sodium fluoborate, dodecyl
10 parts of benzene sulfonic acid, 8 parts of fluotitanic acid, 8 parts of fluorine zirconic acid, 8 parts of butanedioic acid, 4 parts of nano silicon, 5 parts of nano titanium oxide, shell
7 parts of glycan, 2 parts of corrosion inhibiter.
Preferably, its preparation technology comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation technology of the present invention is simple, obtained surface conditioning agent
Architectural shape surface can be effectively passivated, prevents oxidative phenomena, while oxide-film can also be formed on architectural shape surface；
Wherein, nano silicon, the nano titanium oxide added in the present invention, it can be ensured that the film of formation has wear-resisting, corrosion resistant
Effect；Chitosan, the corrosion inhibiter of addition, effectively can prevent Surface of profile from oxidative phenomena occur, in addition, what the present invention used
Preparation technology is simple to operate, it can be ensured that each component material is sufficiently mixed, while uses heating water bath, can prevent having in material
Imitate ingredients from lossing.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belong to the model that the present invention protects
Enclose.
The present invention provides following technical scheme：A kind of architectural shape surface conditioning agent, surface conditioning agent component is by weight
Number includes phytic acid 10-20 parts, sodium fluoborate 10-26 parts, DBSA 8-12 parts, fluotitanic acid 4-12 parts, fluorine zirconic acid 5-
10 parts, butanedioic acid 4-12 parts, nano silicon 2-6 parts, nano titanium oxide 2-8 parts, chitosan 4-10 parts, corrosion inhibiter 1-4
Part.
Embodiment one：
Surface conditioning agent component includes 10 parts of phytic acid, 10 parts of sodium fluoborate, 8 parts of DBSA, fluorine titanium in parts by weight
4 parts of acid, 5 parts of fluorine zirconic acid, 4 parts of butanedioic acid, 2 parts of nano silicon, 2 parts of nano titanium oxide, 4 parts of chitosan, corrosion inhibiter 1
Part.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Embodiment two：
Surface conditioning agent component includes 20 parts of phytic acid, 26 parts of sodium fluoborate, 12 parts of DBSA, fluorine titanium in parts by weight
12 parts of acid, 10 parts of fluorine zirconic acid, 12 parts of butanedioic acid, 6 parts of nano silicon, 8 parts of nano titanium oxide, 10 parts of chitosan, inhibition
4 parts of agent.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Embodiment three：
Surface conditioning agent component includes 12 parts of phytic acid, 13 parts of sodium fluoborate, 9 parts of DBSA, fluorine titanium in parts by weight
5 parts of acid, 6 parts of fluorine zirconic acid, 5 parts of butanedioic acid, 3 parts of nano silicon, 3 parts of nano titanium oxide, 5 parts of chitosan, corrosion inhibiter 1
Part.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Example IV：
Surface conditioning agent component includes 18 parts of phytic acid, 24 parts of sodium fluoborate, 11 parts of DBSA, fluorine titanium in parts by weight
11 parts of acid, 9 parts of fluorine zirconic acid, 11 parts of butanedioic acid, 5 parts of nano silicon, 7 parts of nano titanium oxide, 9 parts of chitosan, corrosion inhibiter
3 parts.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Embodiment five：
Surface conditioning agent component includes 14 parts of phytic acid, 15 parts of sodium fluoborate, 9 parts of DBSA, fluorine titanium in parts by weight
5 parts of acid, 9 parts of fluorine zirconic acid, 10 parts of butanedioic acid, 5 parts of nano silicon, 7 parts of nano titanium oxide, 8 parts of chitosan, corrosion inhibiter 3
Part.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Embodiment six：
Surface conditioning agent component includes 15 parts of phytic acid, 18 parts of sodium fluoborate, 10 parts of DBSA, fluorine titanium in parts by weight
8 parts of acid, 8 parts of fluorine zirconic acid, 8 parts of butanedioic acid, 4 parts of nano silicon, 5 parts of nano titanium oxide, 7 parts of chitosan, corrosion inhibiter 2
Part.
The preparation technology of the present embodiment comprises the following steps：
A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank
Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；
B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is
40 DEG C, time 25min, obtain mixture B；
C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing
Rate is 80 revs/min, mixing time 10min, obtains mixture C；
Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Preparation technology of the present invention is simple, and obtained surface conditioning agent can effectively be passivated architectural shape surface, prevent out
Existing oxidative phenomena, while oxide-film can also be formed on architectural shape surface；Wherein, the present invention in add nano silicon,
Nano titanium oxide, it can be ensured that the film of formation has the effect of wear-resisting, corrosion resistant；Chitosan, the corrosion inhibiter of addition, can be effective
Prevent Surface of profile from oxidative phenomena occur, in addition, the preparation technology that uses of the present invention is simple to operate, it can be ensured that each component material
Material is sufficiently mixed, while uses heating water bath, can prevent that active ingredient is lost in material.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
- A kind of 1. architectural shape surface conditioning agent, it is characterised in that：Surface conditioning agent component includes phytic acid 10-20 in parts by weight Part, sodium fluoborate 10-26 parts, DBSA 8-12 parts, fluotitanic acid 4-12 parts, fluorine zirconic acid 5-10 parts, butanedioic acid 4-12 Part, nano silicon 2-6 parts, nano titanium oxide 2-8 parts, chitosan 4-10 parts, corrosion inhibiter 1-4 parts.
- A kind of 2. architectural shape surface conditioning agent according to claim 1, it is characterised in that：Surface conditioning agent component is preferred Composition proportion include 15 parts of phytic acid, 18 parts of sodium fluoborate, 10 parts of DBSA, 8 parts of fluotitanic acid, 8 parts of fluorine zirconic acid, 8 parts of butanedioic acid, 4 parts of nano silicon, 5 parts of nano titanium oxide, 7 parts of chitosan, 2 parts of corrosion inhibiter.
- 3. realize a kind of preparation technology of architectural shape surface conditioning agent described in claim 1, it is characterised in that：It prepares work Skill comprises the following steps：A, added after mixing phytic acid, sodium fluoborate, DBSA, fluotitanic acid, fluorine zirconic acid, butanedioic acid in stirred tank Even stirring, stir speed (S.S.) are 2000 revs/min, mixing time 15min, obtain mixture A；B, chitosan, corrosion inhibiter are added in mixture A, heating water bath in water-bath is added after mixing, water bath heating temperature is 40 DEG C, time 25min, obtain mixture B；C, nano silicon, nano titanium oxide are added in mixture B, stirring at low speed, stirring are fast at normal temperatures after mixing Rate is 80 revs/min, mixing time 10min, obtains mixture C；Mixture C is placed to 4h at normal temperatures, that is, obtain surface conditioning agent D,.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710902121.9A CN107604347A (en) | 2017-09-29 | 2017-09-29 | A kind of architectural shape surface conditioning agent and its preparation technology |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710902121.9A CN107604347A (en) | 2017-09-29 | 2017-09-29 | A kind of architectural shape surface conditioning agent and its preparation technology |
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Citations (8)
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|---|---|---|---|---|
| JPS5468733A (en) * | 1977-11-11 | 1979-06-02 | Nippon Packaging Kk | Surface treatment of tin plated steel plate and can |
| US4339310A (en) * | 1980-11-25 | 1982-07-13 | Hooker Chemicals & Plastics Corp. | Method of surface treatment of tin plated cans and tin plated steel sheets |
| GB2097429A (en) * | 1981-03-26 | 1982-11-03 | Nippon Paint Co Ltd | Process and composition for treating phosphated metal surfaces |
| CN101250699A (en) * | 2008-03-27 | 2008-08-27 | 武汉科技大学 | Chromium-free passivation liquid for galvanized sheet and manufacture method thereof |
| CN104342685A (en) * | 2013-07-23 | 2015-02-11 | 无锡市石塘湾工业园区开发建设有限公司 | Preparation method of chromium-free passivating solution for zinc-coated steel parts |
| CN105088207A (en) * | 2015-08-24 | 2015-11-25 | 当涂县华艺金属制品有限公司 | Architectural aluminum profile chromate-free passivation treating fluid and preparation method thereof |
| CN105755454A (en) * | 2016-03-03 | 2016-07-13 | 福建省闽发铝业股份有限公司 | Chromate-free passivation surface treatment agent applied before aluminum profile coating |
| CN106835106A (en) * | 2016-12-30 | 2017-06-13 | 张庆 | A kind of good shitosan Inorganic whisker passivating film of film forming |
-
2017
- 2017-09-29 CN CN201710902121.9A patent/CN107604347A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5468733A (en) * | 1977-11-11 | 1979-06-02 | Nippon Packaging Kk | Surface treatment of tin plated steel plate and can |
| US4339310A (en) * | 1980-11-25 | 1982-07-13 | Hooker Chemicals & Plastics Corp. | Method of surface treatment of tin plated cans and tin plated steel sheets |
| GB2097429A (en) * | 1981-03-26 | 1982-11-03 | Nippon Paint Co Ltd | Process and composition for treating phosphated metal surfaces |
| CN101250699A (en) * | 2008-03-27 | 2008-08-27 | 武汉科技大学 | Chromium-free passivation liquid for galvanized sheet and manufacture method thereof |
| CN104342685A (en) * | 2013-07-23 | 2015-02-11 | 无锡市石塘湾工业园区开发建设有限公司 | Preparation method of chromium-free passivating solution for zinc-coated steel parts |
| CN105088207A (en) * | 2015-08-24 | 2015-11-25 | 当涂县华艺金属制品有限公司 | Architectural aluminum profile chromate-free passivation treating fluid and preparation method thereof |
| CN105755454A (en) * | 2016-03-03 | 2016-07-13 | 福建省闽发铝业股份有限公司 | Chromate-free passivation surface treatment agent applied before aluminum profile coating |
| CN106835106A (en) * | 2016-12-30 | 2017-06-13 | 张庆 | A kind of good shitosan Inorganic whisker passivating film of film forming |
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Application publication date: 20180119 |